CN102093486B - Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same - Google Patents

Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same Download PDF

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Publication number
CN102093486B
CN102093486B CN201110000268A CN201110000268A CN102093486B CN 102093486 B CN102093486 B CN 102093486B CN 201110000268 A CN201110000268 A CN 201110000268A CN 201110000268 A CN201110000268 A CN 201110000268A CN 102093486 B CN102093486 B CN 102093486B
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China
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water
ganoderan
ganoderma lucidum
extracting solution
oil phase
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CN201110000268A
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Chinese (zh)
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CN102093486A (en
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宋斌
曾宏彬
李泰辉
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广东省微生物研究所
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Abstract

The invention relates to decolorized ganoderma lucidum polysaccharide extract and a method for preparing hand cream by using the same. The decolorized ganoderma lucidum polysaccharide extract is characterized by being prepared by the following steps: performing refluxing extraction in hot water on ganoderma lucidum fruiting body, precipitating in ethanol, performing suction filtration, drying the precipitate, grinding the precipitate to obtain ganoderma lucidum powder, adding deionized water, uniformly mixing to prepare solution, adding active carbon according to a principle that the mass of the active carbon is 1 to 3 percent based on the total mass of the solution, uniformly mixing by ultrasonic waves, centrifuging at a rotation speed of 4,000 to 10,000r.min<-1>, and collecting supernate to obtain the colorless transparent ganoderma lucidum extract; preparing a water phase by using the extract, propylene glycol, triethanolamine and propylparaben, preparing an oil phase by using mineral oil, lanolin and cetanol, heating the oil phase and water phase respectively till the solutes dissolve, adding the oil phase into the water phase, emulsifying, standing and cooling to prepare the hand cream. When the method is used, the decolorizing rate of the ganoderma lucidum reaches 99.6 percent, the retention rate of the ganoderma lucidum reaches 66.7 percent, and the hand cream prepared by the ganoderma lucidum is pure white, fine and lubricant, has obvious moisturizing effect and gives off natural fragrance of ftillgi.

Description

A kind of ganoderan extracting solution of decolouring and be used to prepare the method for hand lotion

Technical field

The present invention relates to a kind of ganoderan extracting solution, relate in particular to a kind of ganoderan extracting solution that utilizes gac and UW decolouring to obtain; Also relate to the method for preparing hand lotion with this ganoderan extracting solution in addition.

Background technology

Modern society, people not only are in the environment of various electromagnetic radiation for a long time, and usually will contact all kinds of chemical lotions (cleaning agent, soap lye, washing powder etc.), cause skin lack of water or resistance of oxidation to descend and become lack flexibility, dry, coarse.Existing skin care handguard product is many to be main with the chemical ingredients that contains heavy metal; Though can make skin moisturizing, whiten; But life-time service can cause thinning of skin; Accumulation can cause more serious skin problem, and develops natural, effective nourishes rough skin, and the skin care handguard product anti-oxidant, the anti-light aging ability that increases skin will have vast market prospect.

Glossy ganoderma is wide biological activity that find so far, an existing Chinese medicine treasure without any side effects again.The beautification function of glossy ganoderma is mainly derived from the synergy that organic germanium in the Ganoderma sporophore, macromolecule polysaccharide body, abundant trace element and other bio-active substance are verified and delayed senility and play.Ganoderan can significantly improve the SOD activity, effectively removes the radical that body produces, thereby stops the damage of radical pair body, prevents the peroxo-of body, protection cell tissue, delaying cell aging.Ganoderan can significantly promote cell nuclear dna synthesis capability, and can increase the division algebraically of cell.So the antisenility function of ganoderan is very powerful, and ganoderan can keep and regulate moisture of skin; Recover skin elasticity; Suppress melanic formation and deposition in the skin, improve oxyproline and SOD content and be dose-dependently, the aging that these effects can both delaying skin.Blackspot, freckle, the comedo that people face produces is owing to some impuritys generation depositions in the blood of human body are caused; And pachylosis produces wrinkle, and being that cell metabolism is not vigorous causes.Through absorbing organic germanium, polysaccharide isoreactivity material, can reach clean blood decontamination, impel cell regeneration, eliminate speckle, comedo, delay skin aging retains youthful vitality, and reaches the purpose of beauty treatment.

But the ganoderan that generally obtains through water extraction and alcohol precipitation method all can have the sorrel of glossy ganoderma itself, directly adds to make then in the newborn frost that product contains darker sorrel to, and appearance color is poor, and quality is more coarse.The decoloring method of polysaccharide extraction liquid generally adopts active carbon adsorption, hydrogen peroxide oxidation method and macroreticular resin absorbing method at present; Wherein activated carbon method bleaching time length and polysaccharide loss rate are big; Hydrogen peroxide oxidation method can damage polysaccharide structures, influences its biological activity.Macroporous resin is stronger to the pigment adsorptive power, and its percent of decolourization can reach more than 85%, and the polysaccharide retention rate can reach more than 85%, but technology is complicated, and cost is higher.

Summary of the invention

The objective of the invention is to overcome above-described problem, develop a kind of ganoderan extracting solution that can be used for skin care item.Another purpose is to develop the method for preparing hand lotion with this ganoderan extracting solution.

The decoloring method that we combine with UW through gac; Obtain a kind of percent of decolourization and be 99.6% ganoderan extracting solution; And the retention rate of ganoderan wherein is 66.7%, also prepares hand lotion with this ganoderan extracting solution in addition, thereby has realized the object of the invention.

The ganoderan extracting solution of a kind of decolouring of the present invention is characterized in that preparing through following step:

(1) with after the Ganoderma sporophore section, adds zero(ppm) water, through 75~99 ℃ of hot water refluxing extraction; Adding ethanol makes the ethanol final concentration be 60%~90%, 4~25 ℃ and staticly settles suction filtration in extracting solution; The deposition oven dry obtains ganoderan powder russet after the pulverizing;

(2) in the ratio of the mass ratio 1~2.5: 500 of ganoderan powder and deionized water, the ganoderan powder that step (1) is obtained adds deionized water, and mixing is processed solution; Add gac, make quality of activated carbon account for 1%~3% of solution total mass, regulate pH 2.5~4.5; Ultrasonic mixing 20~60s; Keeping envrionment temperature is 20~40 ℃, leaves standstill 20~100min, with rotating speed 4000~10000rmin -1Centrifugal 10~30min gets supernatant, obtains water white ganoderan extracting solution.

The consumption of the described adding zero(ppm) water of step (1) can be 10~50 times of Ganoderma sporophore quality, described backflow preferably 1~3 time, and the described time of staticly settling is preferably 10~24h, preferably 40~60 ℃ of described bake out temperatures.

The preparation method of a kind of ganoderan extracting solution of the present invention and optimal conditions thereof are with above-mentioned.

The preparation method of hand lotion of the present invention, its characteristic comprises the steps:

(1) the water white ganoderan extracting solution that above-mentioned steps (2) is obtained, Ucar 35, trolamine and propylben are made into water; And with MO, yolk and Tego Alkanol 16 are mixed with oil phase, and the consumption of above-mentioned each component is in 100 parts of ganoderan extracting solution mass fractions; Ucar 35 is 25~30 parts, 0.1~0.3 part of trolamine, 0.05~0.2 part of propylben; 4~8 parts in MO, 1~3 part in yolk, 2~4 parts of Tego Alkanol 16s;

(2) described oil phase of step (1) and water are heated to dissolving respectively, keep 50~85 ℃ of temperature, the maintenance mixing speed is 320~720rmin -1, oil phase is slowly added among the water, emulsification 5~35min leaves standstill and is cooled to room temperature, obtains hand lotion.

The present invention adopts a kind of simple, effective decoloring method, can make the ganoderan percent of decolourization reach 99.6%, and the ganoderan retention rate reaches 66.7%; The hand lotion product color of processing is pure white, and quality is fine and smooth, lubricious, and pH 6.0~7.0; Humidity-holding effect is obvious, has the natural aromatic flavor of fungus.

Embodiment

Following examples are to further specify of the present invention, are not limitations of the present invention.

Embodiment 1:

After getting 10g Ganoderma sporophore section, add 100mL zero(ppm) water, 75 ℃ of hot water refluxing extraction 1 time add ethanol and make the ethanol final concentration be 60%, 4 ℃ to staticly settle 10h in extracting solution, suction filtration, deposition is through 40 ℃ of oven dry, after the pulverizing the ganoderan powder.

Take by weighing 1g ganoderan powder and be dissolved in the 500mL water mixing and process solution, add the 5.01g gac, regulate pH to 2.5, ultrasonic mixing 20s leaves standstill 20min, 4000rmin in 20 ℃ of conditions -1Centrifugal 10min gets supernatant, obtains water white ganoderan extracting solution.The mensuration of ganoderma polyoses content adopts the phenol sulfuric acid process, and the mensuration of ganoderan percent of decolourization adopts the OD before and after the working sample decolouring 490nm, obtain the ganoderan percent of decolourization at last and be 99.6% with ganoderan retention rate 66.7%.

Embodiment 2:

After getting 10g Ganoderma sporophore section, add 500mL zero(ppm) water, 99 ℃ of hot water refluxing extraction 3 times add ethanol and make the ethanol final concentration be 90%, 25 ℃ to staticly settle 24h in extracting solution, suction filtration, deposition is through 60 ℃ of oven dry, after the pulverizing the ganoderan powder.

Take by weighing 2.5g ganoderan powder and be dissolved in the 500mL water mixing and process solution, add the 15.075g gac, regulate pH to 4.5, ultrasonic mixing 60s leaves standstill 100min, 10000rmin in 40 ℃ of conditions -1Centrifugal 30min gets supernatant, obtains water white ganoderan extracting solution, percent of decolourization be 99.5% with polysaccharide retention rate 66.6%.

Embodiment 3:

With the ganoderan extracting solution 100g of embodiment 1 decolouring, Ucar 35 25g, trolamine 0.1g and propylben 0.05g are made into water, and again with MO 4g, yolk 1g and Tego Alkanol 16 2g are mixed with oil phase.Oil phase and water are heated to dissolving respectively, keep 50 ℃ of temperature, the maintenance rotating speed is 320rmin -1, oil phase is slowly added among the water, emulsification 5min leaves standstill and is cooled to room temperature, obtains hand lotion.

Embodiment 4:

With the ganoderan extracting solution 100g of decolouring, Ucar 35 30g, trolamine 0.3g and propylben 0.2g are made into water, again with MO 8g, yolk 3g, Tego Alkanol 16 4g is mixed with oil phase.Oil phase and water are heated to dissolving respectively, keep 85 ℃ of temperature, the maintenance rotating speed is 720rmin -1, oil phase is slowly added among the water, emulsification 35min leaves standstill and is cooled to room temperature, obtains hand lotion.

Claims (3)

1. the ganoderan extracting solution of a decolouring is characterized in that preparing through following step:
(1) with after the Ganoderma sporophore section, adds zero(ppm) water, through 75~99 ℃ of hot water refluxing extraction; Adding ethanol makes the ethanol final concentration be 60%~90%, 4~25 ℃ and staticly settles suction filtration in extracting solution; The deposition oven dry obtains ganoderan powder russet after the pulverizing;
(2) in the ratio of the mass ratio 1~2.5: 500 of ganoderan powder and deionized water, the ganoderan powder that step (1) is obtained adds deionized water, and mixing is processed solution; Add gac, make quality of activated carbon account for 1%~3% of solution total mass, regulate pH 2.5~4.5; Ultrasonic mixing 20~60s; Keeping envrionment temperature is 20~40 ℃, leaves standstill 20~100min, with rotating speed 4000~10000rmin -1Centrifugal 10~30min gets supernatant, obtains water white ganoderan extracting solution.
2. the ganoderan extracting solution of a kind of decolouring according to claim 1; The consumption that it is characterized in that the described adding zero(ppm) water of step (1) is 10~50 times of Ganoderma sporophore quality; Described backflow is 1~3 time; The described time of staticly settling is 10~24h, and described bake out temperature is 40~60 ℃.
3. the preparation method of a hand lotion, its characteristic comprises the steps:
(1) with the ganoderan extracting solution of the described decolouring of claim 1, Ucar 35, trolamine and propylben are made into water; And with MO, yolk and Tego Alkanol 16 are mixed with oil phase, and the consumption of above-mentioned each component is in 100 parts of ganoderan extracting solution mass fractions; Ucar 35 is 25~30 parts, 0.1~0.3 part of trolamine, 0.05~0.2 part of propylben; 4~8 parts in MO, 1~3 part in yolk, 2~4 parts of Tego Alkanol 16s;
(2) described oil phase of step (1) and water are heated to dissolving respectively, keep 50~85 ℃ of temperature, the maintenance mixing speed is 320~720rmin -1, oil phase is slowly added among the water, emulsification 5~35min leaves standstill and is cooled to room temperature, obtains hand lotion.
CN201110000268A 2011-01-04 2011-01-04 Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same CN102093486B (en)

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CN102871934A (en) * 2012-10-30 2013-01-16 葛新 Anti-cracking oil with mineral elements
CN103601813A (en) * 2013-12-06 2014-02-26 武汉苏妃玛索科技有限公司 Extraction method for ganoderma lucidum polysaccharide
CN104387495A (en) * 2014-12-14 2015-03-04 桂林宏旺菌业股份有限公司 Preparation method of ganoderma lucidum polysaccharide
CN105985885A (en) * 2015-01-28 2016-10-05 青岛乐泊饮品有限公司 Preparation method of health-caring functional liquor
CN105943441A (en) * 2016-06-01 2016-09-21 合肥丰瑞隆生物科技有限公司 Lucid ganoderma paste mask and preparation method thereof
CN105997654A (en) * 2016-06-21 2016-10-12 安徽诚亚生物科技有限公司 Traditional Chinese medicine mask powder with skin whitening effect
CN107569432A (en) * 2017-08-29 2018-01-12 皖南医学院 A kind of draft nourishes hand lotion of the white moisturizing of releiving of profit and preparation method thereof

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CN101282708A (en) * 2005-10-05 2008-10-08 江崎格力高株式会社 External preparation for skin containing a phosphorlated saccharide
CN101434660A (en) * 2008-08-01 2009-05-20 湖北省农业科学院农产品加工与核农技术研究所 Method for extracting Ganoderma lucidum polysaccharide by ultrasonic wave-microwave combination
CN101693745A (en) * 2009-09-01 2010-04-14 广东神农烟科技术有限公司 Lucid ganoderma polysaccharide and extraction method thereof as well as cigarette containing lucid ganoderma polysaccharide and preparation method thereof
CN101724088A (en) * 2009-11-24 2010-06-09 浙江工业大学 Method for removing proteins and pigments in ganoderma lucidum crude polysaccharide

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BRPI0711970A2 (en) * 2006-06-01 2012-01-10 Sakura Properties Llc fucoidan compositions and methods

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Publication number Priority date Publication date Assignee Title
CN101282708A (en) * 2005-10-05 2008-10-08 江崎格力高株式会社 External preparation for skin containing a phosphorlated saccharide
CN101434660A (en) * 2008-08-01 2009-05-20 湖北省农业科学院农产品加工与核农技术研究所 Method for extracting Ganoderma lucidum polysaccharide by ultrasonic wave-microwave combination
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CN101724088A (en) * 2009-11-24 2010-06-09 浙江工业大学 Method for removing proteins and pigments in ganoderma lucidum crude polysaccharide

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Address after: 510070 No. 100 martyrs Middle Road, Guangdong, Guangzhou

Patentee after: Guangdong Institute of Microbiology (Guangdong province microbiological analysis and testing center)

Address before: 510070 No. 100 martyrs Middle Road, Guangdong, Guangzhou

Patentee before: Guangdong Institute of Microbiology