CN102093486B - Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same - Google Patents
Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same Download PDFInfo
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- CN102093486B CN102093486B CN201110000268A CN201110000268A CN102093486B CN 102093486 B CN102093486 B CN 102093486B CN 201110000268 A CN201110000268 A CN 201110000268A CN 201110000268 A CN201110000268 A CN 201110000268A CN 102093486 B CN102093486 B CN 102093486B
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- 239000005017 polysaccharide Substances 0.000 title abstract description 9
- 240000008397 Ganoderma lucidum Species 0.000 title abstract 9
- 235000001637 Ganoderma lucidum Nutrition 0.000 title abstract 9
- 239000008269 hand cream Substances 0.000 title abstract 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 39
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000002156 mixing Methods 0.000 claims abstract description 12
- 239000000843 powder Substances 0.000 claims abstract description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 9
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 9
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 6
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- 238000010992 reflux Methods 0.000 claims abstract description 5
- 238000000967 suction filtration Methods 0.000 claims abstract description 5
- 239000006210 lotion Substances 0.000 claims description 12
- 241000222336 Ganoderma Species 0.000 claims description 11
- 230000008021 deposition Effects 0.000 claims description 6
- 210000002969 egg yolk Anatomy 0.000 claims description 6
- 229960004418 trolamine Drugs 0.000 claims description 6
- 238000004945 emulsification Methods 0.000 claims description 4
- 238000012423 maintenance Methods 0.000 claims description 4
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 239000006228 supernatant Substances 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 3
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- 229910052799 carbon Inorganic materials 0.000 abstract description 3
- 230000003020 moisturizing effect Effects 0.000 abstract description 2
- 239000003921 oil Substances 0.000 abstract 3
- 239000002244 precipitate Substances 0.000 abstract 2
- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 abstract 2
- 239000004166 Lanolin Substances 0.000 abstract 1
- 229960000541 cetyl alcohol Drugs 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 230000001804 emulsifying effect Effects 0.000 abstract 1
- 239000003205 fragrance Substances 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 abstract 1
- 229940039717 lanolin Drugs 0.000 abstract 1
- 235000019388 lanolin Nutrition 0.000 abstract 1
- 239000000314 lubricant Substances 0.000 abstract 1
- 239000002480 mineral oil Substances 0.000 abstract 1
- 235000010446 mineral oil Nutrition 0.000 abstract 1
- 229940042472 mineral oil Drugs 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 235000010232 propyl p-hydroxybenzoate Nutrition 0.000 abstract 1
- 239000004405 propyl p-hydroxybenzoate Substances 0.000 abstract 1
- 229960003415 propylparaben Drugs 0.000 abstract 1
- 238000004042 decolorization Methods 0.000 description 6
- 238000000151 deposition Methods 0.000 description 5
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 description 2
- 235000005291 Rumex acetosa Nutrition 0.000 description 2
- 240000007001 Rumex acetosella Species 0.000 description 2
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- 210000004369 blood Anatomy 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910052732 germanium Inorganic materials 0.000 description 2
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 235000003513 sheep sorrel Nutrition 0.000 description 2
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- 230000006820 DNA synthesis Effects 0.000 description 1
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- 206010027146 Melanoderma Diseases 0.000 description 1
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- OQUKIQWCVTZJAF-UHFFFAOYSA-N phenol;sulfuric acid Chemical compound OS(O)(=O)=O.OC1=CC=CC=C1 OQUKIQWCVTZJAF-UHFFFAOYSA-N 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
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Abstract
The invention relates to decolorized ganoderma lucidum polysaccharide extract and a method for preparing hand cream by using the same. The decolorized ganoderma lucidum polysaccharide extract is characterized by being prepared by the following steps: performing refluxing extraction in hot water on ganoderma lucidum fruiting body, precipitating in ethanol, performing suction filtration, drying the precipitate, grinding the precipitate to obtain ganoderma lucidum powder, adding deionized water, uniformly mixing to prepare solution, adding active carbon according to a principle that the mass of the active carbon is 1 to 3 percent based on the total mass of the solution, uniformly mixing by ultrasonic waves, centrifuging at a rotation speed of 4,000 to 10,000r.min<-1>, and collecting supernate to obtain the colorless transparent ganoderma lucidum extract; preparing a water phase by using the extract, propylene glycol, triethanolamine and propylparaben, preparing an oil phase by using mineral oil, lanolin and cetanol, heating the oil phase and water phase respectively till the solutes dissolve, adding the oil phase into the water phase, emulsifying, standing and cooling to prepare the hand cream. When the method is used, the decolorizing rate of the ganoderma lucidum reaches 99.6 percent, the retention rate of the ganoderma lucidum reaches 66.7 percent, and the hand cream prepared by the ganoderma lucidum is pure white, fine and lubricant, has obvious moisturizing effect and gives off natural fragrance of ftillgi.
Description
Technical field
The present invention relates to a kind of ganoderan extracting solution, relate in particular to a kind of ganoderan extracting solution that utilizes gac and UW decolouring to obtain; Also relate to the method for preparing hand lotion with this ganoderan extracting solution in addition.
Background technology
Modern society, people not only are in the environment of various electromagnetic radiation for a long time, and usually will contact all kinds of chemical lotions (cleaning agent, soap lye, washing powder etc.), cause skin lack of water or resistance of oxidation to descend and become lack flexibility, dry, coarse.Existing skin care handguard product is many to be main with the chemical ingredients that contains heavy metal; Though can make skin moisturizing, whiten; But life-time service can cause thinning of skin; Accumulation can cause more serious skin problem, and develops natural, effective nourishes rough skin, and the skin care handguard product anti-oxidant, the anti-light aging ability that increases skin will have vast market prospect.
Glossy ganoderma is wide biological activity that find so far, an existing Chinese medicine treasure without any side effects again.The beautification function of glossy ganoderma is mainly derived from the synergy that organic germanium in the Ganoderma sporophore, macromolecule polysaccharide body, abundant trace element and other bio-active substance are verified and delayed senility and play.Ganoderan can significantly improve the SOD activity, effectively removes the radical that body produces, thereby stops the damage of radical pair body, prevents the peroxo-of body, protection cell tissue, delaying cell aging.Ganoderan can significantly promote cell nuclear dna synthesis capability, and can increase the division algebraically of cell.So the antisenility function of ganoderan is very powerful, and ganoderan can keep and regulate moisture of skin; Recover skin elasticity; Suppress melanic formation and deposition in the skin, improve oxyproline and SOD content and be dose-dependently, the aging that these effects can both delaying skin.Blackspot, freckle, the comedo that people face produces is owing to some impuritys generation depositions in the blood of human body are caused; And pachylosis produces wrinkle, and being that cell metabolism is not vigorous causes.Through absorbing organic germanium, polysaccharide isoreactivity material, can reach clean blood decontamination, impel cell regeneration, eliminate speckle, comedo, delay skin aging retains youthful vitality, and reaches the purpose of beauty treatment.
But the ganoderan that generally obtains through water extraction and alcohol precipitation method all can have the sorrel of glossy ganoderma itself, directly adds to make then in the newborn frost that product contains darker sorrel to, and appearance color is poor, and quality is more coarse.The decoloring method of polysaccharide extraction liquid generally adopts active carbon adsorption, hydrogen peroxide oxidation method and macroreticular resin absorbing method at present; Wherein activated carbon method bleaching time length and polysaccharide loss rate are big; Hydrogen peroxide oxidation method can damage polysaccharide structures, influences its biological activity.Macroporous resin is stronger to the pigment adsorptive power, and its percent of decolourization can reach more than 85%, and the polysaccharide retention rate can reach more than 85%, but technology is complicated, and cost is higher.
Summary of the invention
The objective of the invention is to overcome above-described problem, develop a kind of ganoderan extracting solution that can be used for skin care item.Another purpose is to develop the method for preparing hand lotion with this ganoderan extracting solution.
The decoloring method that we combine with UW through gac; Obtain a kind of percent of decolourization and be 99.6% ganoderan extracting solution; And the retention rate of ganoderan wherein is 66.7%, also prepares hand lotion with this ganoderan extracting solution in addition, thereby has realized the object of the invention.
The ganoderan extracting solution of a kind of decolouring of the present invention is characterized in that preparing through following step:
(1) with after the Ganoderma sporophore section, adds zero(ppm) water, through 75～99 ℃ of hot water refluxing extraction; Adding ethanol makes the ethanol final concentration be 60%～90%, 4～25 ℃ and staticly settles suction filtration in extracting solution; The deposition oven dry obtains ganoderan powder russet after the pulverizing;
(2) in the ratio of the mass ratio 1～2.5: 500 of ganoderan powder and deionized water, the ganoderan powder that step (1) is obtained adds deionized water, and mixing is processed solution; Add gac, make quality of activated carbon account for 1%～3% of solution total mass, regulate pH 2.5～4.5; Ultrasonic mixing 20～60s; Keeping envrionment temperature is 20～40 ℃, leaves standstill 20～100min, with rotating speed 4000～10000rmin
-1Centrifugal 10～30min gets supernatant, obtains water white ganoderan extracting solution.
The consumption of the described adding zero(ppm) water of step (1) can be 10～50 times of Ganoderma sporophore quality, described backflow preferably 1～3 time, and the described time of staticly settling is preferably 10～24h, preferably 40～60 ℃ of described bake out temperatures.
The preparation method of a kind of ganoderan extracting solution of the present invention and optimal conditions thereof are with above-mentioned.
The preparation method of hand lotion of the present invention, its characteristic comprises the steps:
(1) the water white ganoderan extracting solution that above-mentioned steps (2) is obtained, Ucar 35, trolamine and propylben are made into water; And with MO, yolk and Tego Alkanol 16 are mixed with oil phase, and the consumption of above-mentioned each component is in 100 parts of ganoderan extracting solution mass fractions; Ucar 35 is 25～30 parts, 0.1～0.3 part of trolamine, 0.05～0.2 part of propylben; 4～8 parts in MO, 1～3 part in yolk, 2～4 parts of Tego Alkanol 16s;
(2) described oil phase of step (1) and water are heated to dissolving respectively, keep 50～85 ℃ of temperature, the maintenance mixing speed is 320～720rmin
-1, oil phase is slowly added among the water, emulsification 5～35min leaves standstill and is cooled to room temperature, obtains hand lotion.
The present invention adopts a kind of simple, effective decoloring method, can make the ganoderan percent of decolourization reach 99.6%, and the ganoderan retention rate reaches 66.7%; The hand lotion product color of processing is pure white, and quality is fine and smooth, lubricious, and pH 6.0～7.0; Humidity-holding effect is obvious, has the natural aromatic flavor of fungus.
Embodiment
Following examples are to further specify of the present invention, are not limitations of the present invention.
Embodiment 1:
After getting 10g Ganoderma sporophore section, add 100mL zero(ppm) water, 75 ℃ of hot water refluxing extraction 1 time add ethanol and make the ethanol final concentration be 60%, 4 ℃ to staticly settle 10h in extracting solution, suction filtration, deposition is through 40 ℃ of oven dry, after the pulverizing the ganoderan powder.
Take by weighing 1g ganoderan powder and be dissolved in the 500mL water mixing and process solution, add the 5.01g gac, regulate pH to 2.5, ultrasonic mixing 20s leaves standstill 20min, 4000rmin in 20 ℃ of conditions
-1Centrifugal 10min gets supernatant, obtains water white ganoderan extracting solution.The mensuration of ganoderma polyoses content adopts the phenol sulfuric acid process, and the mensuration of ganoderan percent of decolourization adopts the OD before and after the working sample decolouring
490nm, obtain the ganoderan percent of decolourization at last and be 99.6% with ganoderan retention rate 66.7%.
Embodiment 2:
After getting 10g Ganoderma sporophore section, add 500mL zero(ppm) water, 99 ℃ of hot water refluxing extraction 3 times add ethanol and make the ethanol final concentration be 90%, 25 ℃ to staticly settle 24h in extracting solution, suction filtration, deposition is through 60 ℃ of oven dry, after the pulverizing the ganoderan powder.
Take by weighing 2.5g ganoderan powder and be dissolved in the 500mL water mixing and process solution, add the 15.075g gac, regulate pH to 4.5, ultrasonic mixing 60s leaves standstill 100min, 10000rmin in 40 ℃ of conditions
-1Centrifugal 30min gets supernatant, obtains water white ganoderan extracting solution, percent of decolourization be 99.5% with polysaccharide retention rate 66.6%.
Embodiment 3:
With the ganoderan extracting solution 100g of embodiment 1 decolouring, Ucar 35 25g, trolamine 0.1g and propylben 0.05g are made into water, and again with MO 4g, yolk 1g and Tego Alkanol 16 2g are mixed with oil phase.Oil phase and water are heated to dissolving respectively, keep 50 ℃ of temperature, the maintenance rotating speed is 320rmin
-1, oil phase is slowly added among the water, emulsification 5min leaves standstill and is cooled to room temperature, obtains hand lotion.
Embodiment 4:
With the ganoderan extracting solution 100g of decolouring, Ucar 35 30g, trolamine 0.3g and propylben 0.2g are made into water, again with MO 8g, yolk 3g, Tego Alkanol 16 4g is mixed with oil phase.Oil phase and water are heated to dissolving respectively, keep 85 ℃ of temperature, the maintenance rotating speed is 720rmin
-1, oil phase is slowly added among the water, emulsification 35min leaves standstill and is cooled to room temperature, obtains hand lotion.
Claims (3)
1. the ganoderan extracting solution of a decolouring is characterized in that preparing through following step:
(1) with after the Ganoderma sporophore section, adds zero(ppm) water, through 75～99 ℃ of hot water refluxing extraction; Adding ethanol makes the ethanol final concentration be 60%～90%, 4～25 ℃ and staticly settles suction filtration in extracting solution; The deposition oven dry obtains ganoderan powder russet after the pulverizing;
(2) in the ratio of the mass ratio 1～2.5: 500 of ganoderan powder and deionized water, the ganoderan powder that step (1) is obtained adds deionized water, and mixing is processed solution; Add gac, make quality of activated carbon account for 1%～3% of solution total mass, regulate pH 2.5～4.5; Ultrasonic mixing 20～60s; Keeping envrionment temperature is 20～40 ℃, leaves standstill 20～100min, with rotating speed 4000～10000rmin
-1Centrifugal 10～30min gets supernatant, obtains water white ganoderan extracting solution.
2. the ganoderan extracting solution of a kind of decolouring according to claim 1; The consumption that it is characterized in that the described adding zero(ppm) water of step (1) is 10～50 times of Ganoderma sporophore quality; Described backflow is 1～3 time; The described time of staticly settling is 10～24h, and described bake out temperature is 40～60 ℃.
3. the preparation method of a hand lotion, its characteristic comprises the steps:
(1) with the ganoderan extracting solution of the described decolouring of claim 1, Ucar 35, trolamine and propylben are made into water; And with MO, yolk and Tego Alkanol 16 are mixed with oil phase, and the consumption of above-mentioned each component is in 100 parts of ganoderan extracting solution mass fractions; Ucar 35 is 25～30 parts, 0.1～0.3 part of trolamine, 0.05～0.2 part of propylben; 4～8 parts in MO, 1～3 part in yolk, 2～4 parts of Tego Alkanol 16s;
(2) described oil phase of step (1) and water are heated to dissolving respectively, keep 50～85 ℃ of temperature, the maintenance mixing speed is 320～720rmin
-1, oil phase is slowly added among the water, emulsification 5～35min leaves standstill and is cooled to room temperature, obtains hand lotion.
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| CN102871934A (en) * | 2012-10-30 | 2013-01-16 | 葛新 | Anti-cracking oil with mineral elements |
| CN103601813A (en) * | 2013-12-06 | 2014-02-26 | 武汉苏妃玛索科技有限公司 | Extraction method for ganoderma lucidum polysaccharide |
| CN104387495A (en) * | 2014-12-14 | 2015-03-04 | 桂林宏旺菌业股份有限公司 | Preparation method of ganoderma lucidum polysaccharide |
| CN105985885A (en) * | 2015-01-28 | 2016-10-05 | 青岛乐泊饮品有限公司 | Preparation method of health-caring functional liquor |
| CN105943441A (en) * | 2016-06-01 | 2016-09-21 | 合肥丰瑞隆生物科技有限公司 | Lucid ganoderma paste mask and preparation method thereof |
| CN105997654A (en) * | 2016-06-21 | 2016-10-12 | 安徽诚亚生物科技有限公司 | Traditional Chinese medicine mask powder with skin whitening effect |
| CN107569432B (en) * | 2017-08-29 | 2020-05-19 | 皖南医学院 | Herbal hand cream capable of nourishing, whitening, relieving and replenishing water and preparation method thereof |
| CN113768141B (en) * | 2021-09-18 | 2022-10-18 | 广东粤微食用菌技术有限公司 | Anti-oxidation repairing ganoderma lucidum extract and preparation method thereof |
| CN115381759A (en) * | 2022-10-14 | 2022-11-25 | 佛山天韵化妆品科技有限公司 | Dendrobium nobile-containing moisturizing composition and preparation method thereof |
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| AU2007267823A1 (en) * | 2006-06-01 | 2007-12-06 | Sakura Properties, Llc | Fucoidan compositions and methods |
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