CN105985885A - Preparation method of health-caring functional liquor - Google Patents
Preparation method of health-caring functional liquor Download PDFInfo
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- CN105985885A CN105985885A CN201510041729.8A CN201510041729A CN105985885A CN 105985885 A CN105985885 A CN 105985885A CN 201510041729 A CN201510041729 A CN 201510041729A CN 105985885 A CN105985885 A CN 105985885A
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Abstract
The invention discloses a preparation method of health-caring functional liquor which is prepared from ganoderma sinensis and base liquor as raw materials. The weight ratio of the ganoderma sinensis to the base liquor is 10-20:100. The functional liquor is 42.01-43.68% in content of polysaccharide, is 0.040-0.049 mg/g in content of sinensoic acid and is 0.510-0.553% in the content of total flavones. Compared with the prior art, the ganoderma sinensis is subjected to secondary extraction, wherein the active components in the ganoderma sinensis are all dissolved in the base liquor, thereby increasing the utilization rate of the ganoderma sinensis. The secondary extraction removes the impurities in the ganoderma sinensis. The health-caring functional liquor prepared from the ganoderma sinensis can be drunk and store for long period, and solves the problem that the liquor cannot be stored for a long period, is easy to deteriorate and causes waste, or causes damage on body when people drink the liquor after deterioration.
Description
Technical field
The invention belongs to new functional liquor production technical field, be specifically related to the preparation method of a kind of heath-function Chinese liquor.
Background technology
China white wine has the succession culture of thousand of years, and the quality of Chinese liquor is also the process that development change always improves.Along with
The development of society, the consumption idea of people also there occurs the biggest change, and people's " raw sense stage " has been entered in the consumption of people, i.e. exists
While meeting material life demand, pursue the needs of cultural life, be the most no longer the demand of " full abdomen ", but " scientifically
Eat ", the high-quality pursuit of " eating health ", health has become the needs that people are the most basic.So the development of Chinese liquor, also must
Must keep up with the trend of the times, Tong Bu with social development, develop the Chinese liquor of " high-quality, health, the nutrition " that adapts to consumer demand.
In order to meet above-mentioned consumer demand, occurring in that part of functions Chinese liquor the most on the market, it is mainly with edible wine
Essence, solid state process produce Chinese liquor be wine base, be added thereto to some ingredients, science processes, thus, functional in vain
Wine had both had liquor style and liquor, had again the characteristic of nutrition wine；But, the new functional liquor prepared after adding ingredient,
Due to limited to extract drugs technology, in medicine, the residue of residual has had a strong impact on the nutritive value of new functional liquor.
Summary of the invention
The present invention proposes the preparation method of a kind of heath-function Chinese liquor, wherein adds Ganoderma, spirit in new functional liquor wine base
Sesame is extracted meticulously through twice, and the new functional liquor prepared is colourless, without flavour of a drug and be of high nutritive value.
Its technical solution includes:
One of task of the present invention is to provide a kind of new functional liquor, and it prepares with Ganoderma and base liquor for raw material, institute
The weight ratio stating Ganoderma and described base liquor is 10～20:100, and in described new functional liquor, polyoses content is 43.68, Ganoderma acid
Content is 0.049mg/g, and the content of total flavones is 0.553.
The two of the task of the present invention are to provide the preparation method of above-mentioned functions Chinese liquor, and it comprises the following steps:
A, Ganoderma is carried out pretreatment,
Weigh Ganoderma according to said ratio, cleaned, grind to obtain Ganoderma powder, described Ganoderma powder is joined in single port flask,
In described single port flask, add the ethanol extraction 3h of 20mL 95, after cold filtration, collect filtrate one and residue one；
B, second extraction,
To the residue obtained a kind of ethanol extraction 3h adding 20ml95 of step a, cold filtration, collect filtrate two and residue two；
C, acquisition extracting solution, merge filtrate one and filtrate two, be positioned in Rotary Evaporators, and decompression distills out ethanol, must carry
Take liquid；
D, activation extraction liquid, put in activator by step c gained extracting solution, is closed by activator, at temperature 95-380 DEG C
Heat 1-2 hour；
E, after step d activation extraction liquid cools down, be added thereto to a certain amount of base liquor, stirring a period of time makes its mix homogeneously,
New functional liquor is i.e. obtained after filtration.
Above-mentioned Ganoderma is the wild Ganoderma in Yunnan Province, and Ganoderma nature and flavor are sweet flat, and wherein mainly contain special angle sterol, organic acid, ammonia
The ergosterols such as base glucose, polysaccharide, resin, mannitol and polysaccharide polyol, contain alkaloid, propyl ester, coumarin, water again
Soluble proteins and multiple enzyme.
In step e, mixing time is 15 days, makes base liquor and extracting solution be sufficiently mixed.
The Advantageous Effects that the present invention is brought:
The present invention proposes the preparation method of a kind of heath-function Chinese liquor, its choosing at raw material, and it is to add in base liquor
Ganoderma, and Ganoderma chooses the wild Ganoderma in Yunnan Province, it is ensured that product no pollution；In preparation method, to Ganoderma second extraction
Process, obtain extracting solution, then this extracting solution is put into and activator carries out activation processing, in the temperature set at this, can make
Extracting liquid decoloration, after the extracting solution after second extraction mixes 15 days with base liquor the most at last, obtains heath-function Chinese liquor.Compare existing
Having technology, by Ganoderma by after second extraction, the effective ingredient in Ganoderma is all dissolved in base liquor, improves the utilization of Ganoderma
Rate, and second extraction eliminates the impurity in Ganoderma.
The present invention, the new functional liquor prepared by Ganoderma, can with long-term drink and storage, it is to avoid by other method system
Work can not long term storage perishable cause waste, or rotten after also drink the harm problem that health is caused.
Accompanying drawing explanation
Below in conjunction with the accompanying drawings the present invention is done the clearest, complete explanation:
Fig. 1 is the process chart of the present invention a kind of heath-function Chinese liquor.
Detailed description of the invention
The invention discloses the preparation method of a kind of heath-function Chinese liquor, in order to make advantages of the present invention, technical scheme more clear
Chu, clearly, does the present invention below in conjunction with specific embodiment and the most clearly and detailedly illustrates.
The present invention, a kind of new functional liquor, it is using aromatic Chinese spirit as base liquor, adds after then Ganoderma carries out pretreatment
Preparing in this base liquor, aromatic Chinese spirit can be selected for commercially available any one, and Ganoderma chooses the purple of the wild growth in Yunnan Province
Sesame, Yunnan Province is little due to environmental pollution, and its nature and flavor of the Ganoderma of wild growth are sweet flat, wherein mainly contain special angle sterol, have
The ergosterols such as machine acid, glucosamine, polysaccharide, resin, mannitol and polysaccharide polyol, contain alkaloid, propyl ester, perfume (or spice) again
Bean essence, water soluble protein and multiple enzyme.
Embodiment 1:
Shown in Fig. 1, the preparation method of above-mentioned functions Chinese liquor, it specifically includes following steps:
Step 1, it is that 10:100 weighs according to the weight ratio of Ganoderma Yu base liquor, Ganoderma is carried out, grinds to obtain Ganoderma powder,
Process of lapping is ground to particle diameter as far as possible and is less than 2 microns, and the Ganoderma powder after grinding joins in the single port flask of 1000mL,
In this single port flask, add the ethanol extraction 3h of 20mL 95, after cold filtration, collect filtrate one and residue one；
Step 2, collect above-mentioned residue one, it is carried out second extraction, is added thereto to the ethanol extraction of 20mL 95 equally
3h, after cold filtration, collects filtrate two and residue two；
Step 3, collection filtrate one and filtrate two, merge filtrate one and filtrate two, be positioned in Rotary Evaporators, and decompression is steamed
Distillate ethanol, obtain extracting solution；
Step 4, extracting solution slightly color now, in order to not affect the color and luster of new functional liquor, take off said extracted liquid
Color processes, and is positioned in activator by step 3 gained extracting solution, is closed by activator, heats 1-2 hour at temperature 95 DEG C；
Step 5, until above-mentioned activation extraction liquid cool down after, be added thereto to the load weighted base liquor of step 1, stir 15 days so that it is
Mix homogeneously, i.e. obtains new functional liquor after filtration.
The partial properties index of the new functional liquor that the present embodiment prepares carries out detection and analyzes, the following mensuration for flavones content
Method:
The extraction of flavone and assay:
Measure the selection of wavelength, take sample liquid i.e. above-mentioned functions Chinese liquor 1.0mL, add the sodium nitrite of 0.3mL 5,4.0mL 4
Sodium hydroxide solution and the aluminum nitrate of 0.3mL 10%, in the basic conditions, flavone and aluminum nitrate carry out complex reaction, raw
Becoming red complex, after colour developing, with reagent for blank reference, measure A in the range of 420-700nm, complex is in 510nm
There is maximum absorption band at place, selects this wavelength during mensuration；
According to the drafting of ordinary curve, weigh and be dried the rutin 2.9mg to constant weight, after being placed in 25ml volumetric flask, add mass fraction
Being the 2.9mg of 80, add the ethanol constant volume that mass fraction is 80 after being placed in 25ml volumetric flask, obtaining concentration is
The standard solution of 0.116mg/ml, measures A and calculates general flavone content, and finally recording general flavone content is 0.510, many
Sugar content is 42.01, and Ganoderma acid content is 0.040mg/g.
Embodiment 2:
Difference from Example 1 is, in step 4, is closed by activator, heats 1-2 hour at temperature is 120 DEG C；
The new functional liquor that the present embodiment prepares, finally recording general flavone content is 0.524, and polyoses content is 42.36, purple
Sesame acid content is 0.042mg/g.
Embodiment 3:
Difference from Example 1 is, in step 4, is closed by activator, heats 1-2 hour at temperature is 180 DEG C；
The new functional liquor that the present embodiment prepares, finally recording general flavone content is 0.553, and polyoses content is 43.68, purple
Sesame acid content is 0.049mg/g.
Embodiment 4:
Difference from Example 1 is, in step 4, is closed by activator, heats 1-2 hour at temperature is 380 DEG C；
The new functional liquor that the present embodiment prepares, finally recording general flavone content is 0.539, and polyoses content is 43.31, purple
Sesame acid content is 0.044mg/g.
Comparative example 1:
Step 1, it is that 10:100 weighs according to the weight ratio of Ganoderma Yu base liquor, Ganoderma is carried out, grinds to obtain Ganoderma powder,
Process of lapping is ground to particle diameter as far as possible and is less than 2 microns, and the Ganoderma powder after grinding joins in the single port flask of 1000mL,
In this single port flask, add the ethanol extraction 3h of 20mL 95, after cold filtration, collect filtrate one and residue one；
Step 2, collect above-mentioned residue one, it is carried out second extraction, is added thereto to the ethanol extraction of 20mL 95 equally
3h, after cold filtration, collects filtrate two and residue two；
Step 3, collection filtrate one and filtrate two, merge filtrate one and filtrate two, be positioned in Rotary Evaporators, and decompression is steamed
Distillate ethanol, obtain extracting solution；
Step 4, until said extracted liquid cool down after, be added thereto to the load weighted base liquor of step 1, stir 15 days so that it is mix
Uniformly, new functional liquor is i.e. obtained after filtration.
The new functional liquor color and luster that this comparative example prepares is light brown, and recording general flavone content in new functional liquor is 0.43,
Polyoses content is 38.61, and ganoderic acid content is 0.035mg/g.
Comparative example 2:
Step 1, it is that 10:100 weighs according to the weight ratio of Ganoderma Yu base liquor, Ganoderma is carried out, grinds to obtain Ganoderma powder,
Process of lapping is ground to particle diameter as far as possible and is less than 2 microns, and the Ganoderma powder after grinding joins in the single port flask of 1000mL,
In this single port flask, add the ethanol extraction 3h of 20mL 95, after cold filtration, collect filtrate one and residue one；
Step 2, collect above-mentioned residue one, it is carried out second extraction, is added thereto to the ethanol extraction of 20mL 95 equally
3h, after cold filtration, collects filtrate two and residue two；
Step 3, collection filtrate one and filtrate two, merge filtrate one and filtrate two, be positioned in Rotary Evaporators, and decompression is steamed
Distillate ethanol, obtain extracting solution；
Step 4, until said extracted liquid cool down after, be added thereto to the load weighted base liquor of step 1, stir 15 days so that it is mix
Uniformly, new functional liquor is i.e. obtained after filtration.
The new functional liquor that the present embodiment prepares is light brown, and recording general flavone content in new functional liquor is 0.51, polysaccharide
Content is 40.68, and Ganoderma acid content is 0.043mg/g.
By above-described embodiment 1,2,3,4 and comparative example 1, comparative example 2, in the selection of raw material, Ganoderma is prepared into
To new functional liquor be better than the new functional liquor that Ganoderma prepares, extracting solution is activated, be possible not only to reduce colourity,
In the new functional liquor finally prepared, the content of polysaccharide, the content of total flavones are superior to the conventional step not having activation.
Claims (4)
1. a new functional liquor, it is characterised in that: it prepares with Ganoderma and base liquor for raw material, described Ganoderma and institute
The weight ratio stating base liquor is 10～20:100, and in described new functional liquor, polyoses content is 42.01-43.68, Ganoderma acid content
For 0.040-0.049mg/g, the content of total flavones is 0.510-0.553.
The preparation method of new functional liquor the most according to claim 1, it is characterised in that comprise the following steps:
A, Ganoderma is carried out pretreatment,
Weigh Ganoderma according to said ratio, cleaned, grind to obtain Ganoderma powder, described Ganoderma powder is joined in single port flask,
In described single port flask, add the ethanol extraction 3h of 20mL 95, after cold filtration, collect filtrate one and residue one；
B, second extraction,
To the residue obtained a kind of ethanol extraction 3h adding 20ml95 of step a, cold filtration, collect filtrate two and residue two；
C, acquisition extracting solution, merge filtrate one and filtrate two, be positioned in Rotary Evaporators, and decompression distills out ethanol, must carry
Take liquid；
D, activation extraction liquid, put in activator by step c gained extracting solution, is closed by activator, at temperature 95-380 DEG C
Heat 1-2 hour；
E, after step d activation extraction liquid cools down, be added thereto to a certain amount of base liquor, stirring a period of time makes its mix homogeneously,
New functional liquor is i.e. obtained after filtration.
The preparation method of new functional liquor the most according to claim 2, it is characterised in that: described Ganoderma is that Yunnan Province is wild
Ganoderma.
The preparation method of new functional liquor the most according to claim 2, it is characterised in that: in step e, mixing time is
15 days.
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| CN201510041729.8A CN105985885A (en) | 2015-01-28 | 2015-01-28 | Preparation method of health-caring functional liquor |
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| CN201510041729.8A CN105985885A (en) | 2015-01-28 | 2015-01-28 | Preparation method of health-caring functional liquor |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1246527A (en) * | 1998-09-03 | 2000-03-08 | 孙自强 | Process for brewing glossy ganoderma spirits |
| CN1762392A (en) * | 2005-10-14 | 2006-04-26 | 中国药科大学 | Coriolus versicolor zymolyte, its preparation method and use for adjuvant as alcoholic drink |
| CN101856383A (en) * | 2010-06-09 | 2010-10-13 | 广东神农烟科技术有限公司 | Liver-protecting white spirit and preparation method thereof |
| CN101974399A (en) * | 2010-11-24 | 2011-02-16 | 曹光荣 | Functional white wine and preparation method thereof |
| CN102093486A (en) * | 2011-01-04 | 2011-06-15 | 广东省微生物研究所 | Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same |
| CN104099223A (en) * | 2014-07-24 | 2014-10-15 | 四川理工学院 | Ganoderma lucidum medicinal liquor preparation process |
-
2015
- 2015-01-28 CN CN201510041729.8A patent/CN105985885A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1246527A (en) * | 1998-09-03 | 2000-03-08 | 孙自强 | Process for brewing glossy ganoderma spirits |
| CN1762392A (en) * | 2005-10-14 | 2006-04-26 | 中国药科大学 | Coriolus versicolor zymolyte, its preparation method and use for adjuvant as alcoholic drink |
| CN101856383A (en) * | 2010-06-09 | 2010-10-13 | 广东神农烟科技术有限公司 | Liver-protecting white spirit and preparation method thereof |
| CN101974399A (en) * | 2010-11-24 | 2011-02-16 | 曹光荣 | Functional white wine and preparation method thereof |
| CN102093486A (en) * | 2011-01-04 | 2011-06-15 | 广东省微生物研究所 | Decolorized ganoderma lucidum polysaccharide extract and method for preparing hand cream by using same |
| CN104099223A (en) * | 2014-07-24 | 2014-10-15 | 四川理工学院 | Ganoderma lucidum medicinal liquor preparation process |
Non-Patent Citations (1)
| Title |
|---|
| 陈士瑜 等编著: "《蕈菌医方集成》", 31 January 2000, 上海科学技术文献出版社出版发行 * |
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