CN101485622A - Shampoo containing extract of Moringa oleifera and preparation method thereof - Google Patents

Shampoo containing extract of Moringa oleifera and preparation method thereof Download PDF

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Publication number
CN101485622A
CN101485622A CNA2009101199897A CN200910119989A CN101485622A CN 101485622 A CN101485622 A CN 101485622A CN A2009101199897 A CNA2009101199897 A CN A2009101199897A CN 200910119989 A CN200910119989 A CN 200910119989A CN 101485622 A CN101485622 A CN 101485622A
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CN
China
Prior art keywords
moringa
shampoo
extract
leaf
oleifera
Prior art date
Application number
CNA2009101199897A
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Chinese (zh)
Inventor
张嘉恒
刘婷婷
Original Assignee
张嘉恒
刘婷婷
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 张嘉恒, 刘婷婷 filed Critical 张嘉恒
Priority to CNA2009101199897A priority Critical patent/CN101485622A/en
Publication of CN101485622A publication Critical patent/CN101485622A/en

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Abstract

The invention discloses a shampoo containing moringa plant extract, and a preparation method thereof. The shampoo comprises a surfactant, a foam increasing agent, tackifier, conditioner, additives, preservative, pigment, essence and deionized water, and is characterized in that the shampoo also contains active composition of moringa kernels and extract of moringa leaves, and the extract of the moringa kernels and the moringa leaves accounts for 0.05 to 15.0 percent of the weight of the shampoo. The shampoo contains characteristic low-molecular water-soluble proteins of moringa seeds, and the proteins have extremely good flocculation characteristics and can obviously reduce the turbidity of water and remove over 99 percent of bacteria. The average oil content of the moringa kernels is 40 percent, and the moringa-oil fatty acid is similar to olive oil in species composition, not easy to oxidize and great in washing and foaming effects. In addition, the shampoo which is also rich in quercetin flavone and other flavonoid substances can achieve the effects of resisting oxidation, preventing radiation, sterilizing, relieving itch, dispelling dandruff, resisting inflammation, resisting allergy, preventing skin cancer, strengthening immunity and the like. The shampoo has the advantages of convenient use, mildness, plentiful foam, direct contact with scalp and pleasant dandruff removal, can improve scalp environment, and is a multifunctional shampoo integrating the functions of cleaning, protecting hair and invigorating skin.

Description

A kind of shampoo that contains extract of Moringa oleifera and preparation method thereof

Technical field

The present invention relates to a kind of shampoo that contains plant extract.

Background technology

Shampoo is requisite article of everyday use in the life, and along with improving constantly of living standard, people are more and more higher to the requirement of shampoo.It not only needs to have good cleaning performance, also requires to have the function of nursing conditioning, and to the human body safety non-toxic.Under the trend of back to nature, naturalization of product, nutrient laden, avirulence are favored by popular day by day.Therefore containing natural components faces wilderness demand in interior meticulous prescription and technology.

Summary of the invention

The object of the present invention is to provide a kind of shampoo that contains extract of Moringa oleifera, product has antioxidation, radioprotective, sterilization, antipruritic, anti-dandruff, antiinflammatory, antiallergic, and effects such as prevention skin carcinoma, enhancing immunity, this product is easy to use, gentle, foam enriches, straight contact skin, pleasant anti-dandruff, and can improve the scalp environment, be collection cleaning, defend the doctrine and skin and complexion improving in the multifunctional hair cleaning water of one.

For achieving the above object, the technical solution used in the present invention is: a kind of shampoo that contains extract of Moringa oleifera and preparation method thereof, it comprises surfactant, suds booster, viscosifier, conditioner, additive, antiseptic, pigment, essence, deionized water, it is characterized by: also contain Moringa kernel active component and leaf of Moringa extract in the described shampoo, it is 0.05-15.0% that described Moringa kind Renhe leaf of Moringa extract accounts for the shampoo percentage by weight.

Preferably, described Moringa (Moringa Oleifera) belongs to Moringaceae, Moringa, be the perennial woody plant, the extracting method of its kernel active ingredient is: the Moringa seed after shelling, to pulverize to 0.5mm (100 order) granule gets Moringa kernel powder, and the extracting method of leaf of Moringa extract is: get leaf of Moringa powder g, put in the reflux, extract, device, add a certain proportion of alcohol reflux, extracting solution merges, with rotary evaporator concentrating under reduced pressure (temperature is 60-70 ℃); Concentrated solution is with petroleum ether extraction 2~3 times, defat, decolouring, lower floor's solution is put in the volumetric flask, the ethanol distilling under reduced pressure that adds corresponding concentration be concentrated to brown when thick cooling stand-by.

Preferably, described surfactant is selected from one or more combination of ammonium lauryl sulfate, Sodium Alcohol Ether Sulphate or fat alcohol polyethylene ether ammonium sulfate.

Preferably, described suds booster and viscosifier are selected from one or more combination of coconut monoethanolamide, cocoanut oil diethan olamide, Oleum Cocois acyl group CAB or sodium chloride.

Preferably, described conditioner is selected from one or more combinations of cation guar gum, polyquaternium-7.

Preferably, described additive is selected from one or more combinations of emulsified silicone oil, glycerol, Oleum Camelliae.

Preferably, described antiseptic is one or more combinations of methyl hydroxybenzoate, isothiazolone magnesium sulfate.

Moringa kernel active ingredient is low macromolecule water-solubility albumen, and these albumen have big absorption affinity to the solid suspended particle in the water body, and can remove the antibacterial more than 99%.And the average oil content of Moringa kernel is 40%, and the kind of fatty acid is formed extremely similar to olive oil, and is difficult for oxidation, has potent washing and makes the bubble effect.Leaf of Moringa then is rich in multiple flavonoid substance, has strong free radical scavenging activity and the effect of antiinflammatory bacteriostatic.Also contain materials such as β-sitoesterol, 2-nitrile glycosides in addition in the leaf of Moringa extract, have the effect that brings high blood pressure down with cholesterol and antitumor and cancer.

The present invention extracts the active ingredient of Moringa kind Renhe leaf of Moringa and is applied in the shampoo, reach high-efficient and lasting ground antioxidation, radioprotective, sterilization, antipruritic, anti-dandruff, antiinflammatory, antiallergic, and effects such as prevention skin carcinoma, enhancing immunity, and, make product antioxidation, radioprotective, sterilization, antipruritic, anti-dandruff, antiinflammatory, antiallergic, and effects such as prevention skin carcinoma, enhancing immunity in conjunction with other surfactants.

In order to achieve the above object, the present invention selects Sodium Alcohol Ether Sulphate (AES), ammonium lauryl sulfate (K12A), fatty polyvinylether ammonium sulfate (AESA) for use; With coconut monoethanolamide (CMEA); cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) and sodium chloride are as suds booster and viscosifier; play foam enhancing; the effect of steady bubble and tackify; with cation guar gum (C-14-S); polyquaternium-7 (M550) is a conditioner; additive is selected emulsified silicone oil for use; glycerol and Oleum Camelliae; antiseptic is selected methyl hydroxybenzoate and isothiazolone magnesium sulfate for use; product clean result after these compositions are composite is good; foam is abundant fine and smooth; and has an ability of bacteria growing inhibiting; can keep hair quality soft and smooth, not damage hair quality.

The batch process production method is adopted in the production procedure that contains the shampoo of extract of Moringa oleifera of the present invention.In reactor, be warming up to 75 ℃ earlier with surfactant ammonium lauryl sulfate (K12A); Sodium Alcohol Ether Sulphate (AES) or fat alcohol polyethylene ether ammonium sulfate (AESA) dissolving; be cooled to 60 ℃ of Moringa kernel that add after pulverizing after adding chelating agen; water disperses the back to add cation guar gum; add coconut monoethanolamide (CMEA) again; cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) and sodium chloride; as suds booster and viscosifier and other conditioners and add emulsified silicone oil; be cooled to about 40 ℃ and add glycerol; Oleum Camelliae; the leaf of Moringa extract; essence; antiseptic etc. stir.

The shampoo sample that contains extract of Moringa oleifera of the present invention meets national body lotion industry standard through check, and its every index meets the sanitary quality standard and the security requirement of national regulation fully.

The specific embodiment

Embodiment 1

1, get one of Moringa kernel, the back pulverizing of shelling is stand-by for 0.5mm (100 order) granule gets Moringa kernel powder.

2, get leaf of Moringa powder 5g, put in the reflux, extract, device, add a certain proportion of alcohol reflux, extracting solution merges, with rotary evaporator concentrating under reduced pressure (temperature is 60-70 ℃). concentrated solution petroleum ether extraction 2~3 times, defat, decolouring, lower floor's solution is put in the 100ml volumetric flask, the ethanol distilling under reduced pressure that adds corresponding concentration be concentrated to brown when thick cooling stand-by.

3, raw material is disposed than row by following

AES (polyoxyethylene lauryl ether sodium sulfate) 10.0%

Ammonium lauryl sulfate (K12A) 5.0%

6501 (coconut oil diethanol amides) 6.0%

Coconut monoethanolamide (CMEA) 2.0%

CAB (dodecanamide propyl betanin) 2.0%

Emulsified silicone oil 2.0%

Glycerol 0.8%

Oleum Camelliae 0.4%

Methyl hydroxybenzoate 0.2%

EDTA-2Na 0.2%

Hydroxyl guar gum 0.2%

NaCl 0.6%

Essence is an amount of

The leaf of Moringa extract, Moringa kernel powder 5%

Deionized water adds to 100%

4; in reactor, be warming up to 75 ℃ earlier with surfactant ammonium lauryl sulfate (K12A); Sodium Alcohol Ether Sulphate (AES) dissolving; be cooled to 60 ℃ of Moringa kernel that add after pulverizing after adding chelating agen EDTA-2Na; water disperses the back to add cation guar gum; add coconut monoethanolamide (CMEA) again; cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) and sodium chloride; emulsified silicone oil is as suds booster and viscosifier and other conditioners; be cooled to about 40 ℃ and add glycerol; Oleum Camelliae; the leaf of Moringa extract; essence; antiseptic etc. stir.

Embodiment 2

1, get one of Moringa kernel, the back pulverizing of shelling is stand-by for 0.5mm (100 order) granule gets Moringa kernel powder.

2, get leaf of Moringa powder 10g, put in the reflux, extract, device, add a certain proportion of alcohol reflux, extracting solution merges, with rotary evaporator concentrating under reduced pressure (temperature is 60-70 ℃). concentrated solution petroleum ether extraction 2~3 times, defat, decolouring, lower floor's solution is put in the 100ml volumetric flask, the ethanol distilling under reduced pressure that adds corresponding concentration be concentrated to brown when thick cooling stand-by.

3, raw material is disposed than row by following

AES (polyoxyethylene lauryl ether sodium sulfate) 5.0%

Ammonium lauryl sulfate (K12A) 8.0%

6501 (coconut oil diethanol amides) 2.0%

Coconut monoethanolamide (CMEA) 3.0%

CAB (dodecanamide propyl betanin) 2.0%

Emulsified silicone oil 2.0%

Glycerol 1.0%

Oleum Camelliae 0.5%

Methyl hydroxybenzoate 0.2%

EDTA chelating agen 0.2%

Hydroxyl guar gum 0.2%

NaCl 0.6%

Essence is an amount of

The leaf of Moringa extract, Moringa kernel powder 8%

Deionized water adds to 100%

4; in reactor, be warming up to 75 ℃ earlier with surfactant ammonium lauryl sulfate (K12A); Sodium Alcohol Ether Sulphate (AES) dissolving; be cooled to 60 ℃ of Moringa kernel that add after pulverizing after adding chelating agen EDTA-2Na; water disperses the back to add cation guar gum; add coconut monoethanolamide (CMEA) again; cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) and sodium chloride; emulsified silicone oil is as suds booster and viscosifier and other conditioners; be cooled to about 40 ℃ and add glycerol; Oleum Camelliae; the leaf of Moringa extract; essence; antiseptic etc. stir.

Embodiment 3

1, get one of Moringa kernel, the back pulverizing of shelling is stand-by for 0.5mm (100 order) granule gets Moringa kernel powder.

2, get leaf of Moringa powder 20g, put in the reflux, extract, device, add a certain proportion of alcohol reflux, extracting solution merges, with rotary evaporator concentrating under reduced pressure (temperature is 60-70 ℃). concentrated solution petroleum ether extraction 2~3 times, defat, decolouring, lower floor's solution is put in the 100ml volumetric flask, the ethanol distilling under reduced pressure that adds corresponding concentration be concentrated to brown when thick cooling stand-by.

3, raw material is disposed than row by following

AES (polyoxyethylene lauryl ether sodium sulfate) 5.0%

Ammonium lauryl sulfate (K12A) 3.0%

Fat polyvinylether ammonium sulfate (AESA) 3.0%

6501 (coconut oil diethanol amides) 2.0%

Coconut monoethanolamide (CMEA) 3.0%

CAB (dodecanamide propyl betanin) 2.0%

Emulsified silicone oil 2.0%

Glycerol 1.0%

Oleum Camelliae 1.0%

Methyl hydroxybenzoate 0.2%

EDTA chelating agen 0.2%

Hydroxyl guar gum 0.2%

NaCl 0.6%

Essence is an amount of

The leaf of Moringa extract, Moringa kernel powder 15%

Deionized water adds to 100%

4; in reactor, be warming up to 75 ℃ earlier with surfactant ammonium lauryl sulfate (K12A); Sodium Alcohol Ether Sulphate (AES) and fat alcohol polyethylene ether ammonium sulfate (AESA) dissolving; be cooled to 60 ℃ of Moringa kernel that add after pulverizing after adding chelating agen EDTA-2Na; water disperses the back to add cation guar gum; add coconut monoethanolamide (CMEA) again; cocoanut oil diethan olamide (6501) and Oleum Cocois acyl group CAB (CAB) and sodium chloride; emulsified silicone oil is as suds booster and viscosifier and other conditioners; be cooled to about 40 ℃ and add glycerol; Oleum Camelliae; the leaf of Moringa extract; essence; antiseptic etc. stir.

Claims (7)

1, a kind of shampoo that contains extract of Moringa oleifera and preparation method thereof, it comprises surfactant, suds booster, viscosifier, conditioner, additive, antiseptic, pigment, essence, deionized water, it is characterized in that: also contain Moringa kernel active component and leaf of Moringa extract in the described shampoo, it is 0.05-15.0% that described Moringa kind Renhe leaf of Moringa extract accounts for the shampoo percentage by weight.
2, shampoo that contains extract of Moringa oleifera as claimed in claim 1 and preparation method thereof, it is characterized in that: described Moringa (Moringa Oleifera) belongs to Moringaceae, Moringa, be the perennial woody plant, the extracting method of its kernel active ingredient is: the Moringa seed after shelling, pulverize and get Moringa kernel powder for 0.5mm (100 order) granule, the extracting method of leaf of Moringa extract is: get the leaf of Moringa powder, put in the reflux, extract, device, add a certain proportion of alcohol reflux, extracting solution merges, with rotary evaporator concentrating under reduced pressure (temperature is 60-70 ℃); Concentrated solution is with petroleum ether extraction 2~3 times, defat, decolouring, lower floor's solution is put in the volumetric flask, the ethanol distilling under reduced pressure that adds corresponding concentration be concentrated to brown when thick cooling stand-by.
3, shampoo that contains extract of Moringa oleifera as claimed in claim 1 or 2 and preparation method thereof is characterized in that: described surfactant is selected from one or more combination of ammonium lauryl sulfate, Sodium Alcohol Ether Sulphate or fat alcohol polyethylene ether ammonium sulfate.
4, shampoo that contains extract of Moringa oleifera as claimed in claim 1 or 2 and preparation method thereof is characterized in that: described suds booster and viscosifier are selected from one or more combination of coconut monoethanolamide, cocoanut oil diethan olamide, Oleum Cocois acyl group CAB or sodium chloride.
5, shampoo that contains extract of Moringa oleifera as claimed in claim 1 or 2 and preparation method thereof is characterized in that: described conditioner is selected from one or more combinations of cation guar gum, polyquaternium-7.
6, shampoo that contains extract of Moringa oleifera as claimed in claim 1 or 2 and preparation method thereof is characterized in that: described additive is selected from one or more combinations of emulsified silicone oil, glycerol, Oleum Camelliae.
7, shampoo that contains extract of Moringa oleifera as claimed in claim 1 or 2 and preparation method thereof is characterized in that: described antiseptic is one or more combinations of methyl hydroxybenzoate, isothiazolone magnesium sulfate.
CNA2009101199897A 2009-03-03 2009-03-03 Shampoo containing extract of Moringa oleifera and preparation method thereof CN101485622A (en)

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102784074A (en) * 2012-07-19 2012-11-21 东华大学 Functional hair washing shampoo and its preparation method
CN103223000A (en) * 2012-01-31 2013-07-31 株式会社爱茉莉太平洋 Skin external composition containing drumstick tree seed extract
CN103330664A (en) * 2013-06-08 2013-10-02 南方医科大学 Application of traditional Chinese medicine extract with dandruff removing function to hair cosmetics
CN103652930A (en) * 2013-12-31 2014-03-26 广州天来宝生物科技有限公司 Moringa calcium total nutrient and preparation method thereof
CN103919703A (en) * 2014-04-25 2014-07-16 韩雁如 Liquid shampoo containing lemon-onion extraction solution
CN104224862A (en) * 2013-06-07 2014-12-24 韩国原子力研究院 Composition containing moringa oleifera leave water soluble extract as effective component and used for treating or preventing cancer and preparation method for moringa oleifera leave extract
CN104606087A (en) * 2014-12-24 2015-05-13 卢颖 Nourishing shampoo containing traditional Chinese medicine extract and preparation method thereof
CN104622753A (en) * 2015-02-10 2015-05-20 广东雅倩化妆品有限公司 Natural hair-care shampoo and preparation method and application thereof
CN104739707A (en) * 2013-12-31 2015-07-01 大连美乐生物技术开发有限公司 Traditional Chinese medicine liquid shampoo and preparation method thereof
CN104745316A (en) * 2015-02-10 2015-07-01 广东雅倩化妆品有限公司 Natural fruit and vegetable cleaning agent as well as preparation method and application of natural fruit and vegetable cleaning agent
CN105250175A (en) * 2015-10-29 2016-01-20 广州赛莱拉生物基因工程有限公司 Natural body wash containing argy wormwood leaf extract and preparation method thereof
CN105395593A (en) * 2015-12-09 2016-03-16 广州赛莱拉生物基因工程有限公司 Itching relieving ointment containing folium artemisiae argyi extract and preparation method thereof
CN105560124A (en) * 2016-01-26 2016-05-11 廖丽萍 Chinese medicine liquid shampoo containing moringa extract and preparation method thereof
CN105796431A (en) * 2016-04-29 2016-07-27 安徽恋尚你食品有限公司 Moringa oleifera skin moisturizer
WO2017185227A1 (en) * 2016-04-26 2017-11-02 L'oreal Composition for treating keratin fibers
CN107519067A (en) * 2016-06-22 2017-12-29 广州市优品化妆品科技有限公司 Moringa tree shampoo and preparation method

Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103223000B (en) * 2012-01-31 2018-06-01 株式会社爱茉莉太平洋 The Dermatologic preparation composition of Moringa seed extract
CN103223000A (en) * 2012-01-31 2013-07-31 株式会社爱茉莉太平洋 Skin external composition containing drumstick tree seed extract
CN102784074A (en) * 2012-07-19 2012-11-21 东华大学 Functional hair washing shampoo and its preparation method
CN104224862B (en) * 2013-06-07 2018-05-25 韩国原子力研究院 Water-soluble extractive containing leaf of Moringa is used to treat or prevent the composition of cancer and the preparation method of moringa oleifera leaf extractive for active ingredient
CN104224862A (en) * 2013-06-07 2014-12-24 韩国原子力研究院 Composition containing moringa oleifera leave water soluble extract as effective component and used for treating or preventing cancer and preparation method for moringa oleifera leave extract
CN103330664A (en) * 2013-06-08 2013-10-02 南方医科大学 Application of traditional Chinese medicine extract with dandruff removing function to hair cosmetics
CN104739707A (en) * 2013-12-31 2015-07-01 大连美乐生物技术开发有限公司 Traditional Chinese medicine liquid shampoo and preparation method thereof
CN103652930A (en) * 2013-12-31 2014-03-26 广州天来宝生物科技有限公司 Moringa calcium total nutrient and preparation method thereof
CN103652930B (en) * 2013-12-31 2015-07-08 广州天来宝生物科技有限公司 Moringa calcium total nutrient and preparation method thereof
CN103919703A (en) * 2014-04-25 2014-07-16 韩雁如 Liquid shampoo containing lemon-onion extraction solution
CN104606087A (en) * 2014-12-24 2015-05-13 卢颖 Nourishing shampoo containing traditional Chinese medicine extract and preparation method thereof
CN104745316A (en) * 2015-02-10 2015-07-01 广东雅倩化妆品有限公司 Natural fruit and vegetable cleaning agent as well as preparation method and application of natural fruit and vegetable cleaning agent
CN104622753A (en) * 2015-02-10 2015-05-20 广东雅倩化妆品有限公司 Natural hair-care shampoo and preparation method and application thereof
CN104622753B (en) * 2015-02-10 2017-08-25 广东雅倩化妆品有限公司 One kind naturally washes conditioner and its preparation method and application
CN105250175A (en) * 2015-10-29 2016-01-20 广州赛莱拉生物基因工程有限公司 Natural body wash containing argy wormwood leaf extract and preparation method thereof
CN105250175B (en) * 2015-10-29 2018-03-13 广州赛莱拉生物基因工程有限公司 A kind of Value of natural bath & shower dew containing Folium Artemisiae Argyi extract and preparation method thereof
CN105395593A (en) * 2015-12-09 2016-03-16 广州赛莱拉生物基因工程有限公司 Itching relieving ointment containing folium artemisiae argyi extract and preparation method thereof
CN105560124A (en) * 2016-01-26 2016-05-11 廖丽萍 Chinese medicine liquid shampoo containing moringa extract and preparation method thereof
WO2017185227A1 (en) * 2016-04-26 2017-11-02 L'oreal Composition for treating keratin fibers
CN105796431A (en) * 2016-04-29 2016-07-27 安徽恋尚你食品有限公司 Moringa oleifera skin moisturizer
CN107519067A (en) * 2016-06-22 2017-12-29 广州市优品化妆品科技有限公司 Moringa tree shampoo and preparation method

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Open date: 20090722