CN106880551B - Body lotion for tightening, moistening and smoothing skin and preparation method thereof - Google Patents

Body lotion for tightening, moistening and smoothing skin and preparation method thereof Download PDF

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CN106880551B
CN106880551B CN201710122093.9A CN201710122093A CN106880551B CN 106880551 B CN106880551 B CN 106880551B CN 201710122093 A CN201710122093 A CN 201710122093A CN 106880551 B CN106880551 B CN 106880551B
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CN106880551A (en
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孙淑萍
李红星
杨梅
彭欢
董婷玉
谢东
吴成华
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Guangzhou Meisi Biotechnology Co ltd
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Wannan Medical College
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A61K8/988Honey; Royal jelly, Propolis
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Abstract

The invention discloses body lotion for tightening, moistening and smoothing skin and a preparation method thereof, wherein the body lotion contains the following substances: organic strawberry seed oil, sea buckthorn oil, evening primrose oil, macadamia nut oil, jasmine flower extracting solution, lemon extracting solution, rosemary extracting solution, roselle extracting solution, honey, natural APG liquid crystal type emulsifier, AC-402 compound type emulsifier, sodium carboxymethylcellulose, an ice crystal forming agent AVC, sodium alginate, seaweed extract, Liponic EG-1, ethylparaben, 1, 2-propylene glycol, distilled water and essence. Compared with the prior art, the body lotion provided by the invention is fine, uniform, light and moist, fragrant in smell and rapid to absorb, can deeply nourish the skin, adjust the moisture degree of the skin, thoroughly change the state of the skin and enable the skin to be full, moist and elastic.

Description

Body lotion for tightening, moistening and smoothing skin and preparation method thereof
Technical Field
The invention relates to the field of skin care products, and particularly relates to body lotion for tightening, moistening and smoothing skin and a preparation method thereof.
Background
The skin is a protective layer of our body and can help us to resist the damage of harmful substances in the environment. Harmful substances in the air such as ultraviolet rays, floating dust, bacteria, fungi and the like, and grease, sweat and the like secreted by the skin influence the normal function of the skin, even cause serious skin problems such as infection and the like, cause physiological and psychological burden and influence daily life. In addition, the rhythm of the modern social life is tense, people pay more attention to the facial skin problem and neglect the skin care of other parts of the body.
The body lotion, as the name implies, is a skin care lotion for the body, and has the effects of moisturizing the whole body, whitening and moistening. Particularly in dry winter, dry air can compete for moisture in skin, nutrient structures in the skin can also change, and the skin needs deep moisturizing body lotion to adjust the moisture degree of the skin and strengthen a natural skin moisturizing layer. At the moment, the body lotion can deeply moisten the horny layer of the skin while nourishing the skin, continuously supplement water and nutrients required by the skin, thoroughly change the state of the skin and enable the skin to be full, watery and elastic.
Object of the Invention
The invention aims to provide body lotion for tightening, moistening and smoothing skin, which contains various vegetable oils and plant extract components, can deeply moisten the horny layer of the skin and continuously supplement water and nutrients required by the skin.
The invention also provides a preparation method of the body lotion for tightening, moistening and smoothing skin.
The invention provides body lotion for firming, moistening and smoothing skin, which consists of the following raw materials in parts by weight:
Figure BDA0001237348720000011
Figure BDA0001237348720000021
the jasmine flower extracting solution is prepared by the following method:
weighing a proper amount of dried jasmine flowers, soaking for 1-2h, heating and decocting at 80-100 ℃ for 3 times, adding 20-30 times of water for 1 time, extracting for 1.5-2.5h, adding 10-20 times of water for 2 times, extracting for 1-1.5h, adding 5-10 times of water for 3 times, extracting for 0.5-1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 3-12 times mL/g of the weight of the dried jasmine flowers, and filtering with two layers of gauze for later use.
The volume of the filtrate is concentrated to 3-12 times mL/g of the weight of the dried jasmine flowers, namely the volume of the filtrate obtained after extracting and concentrating every 1g of dried jasmine flowers is 3-12 mL.
The lemon extract is prepared by the following method:
weighing an appropriate amount of dry lemon slice coarse powder, adding water, soaking for 0.5-0.75h, heating, decocting and extracting for 3 times, adding 10-15 times of water for 1 time, extracting for 0.5-2h, adding 8-12 times of water for 2 times, extracting for 0.5-1.5h, adding 8-10 times of water for 3 times, extracting for 0.5-1.5h, filtering each time, combining filtrates, concentrating the volume of the filtrate to 4-8 times mL/g of the weight of the dry lemon slice coarse powder, and filtering to obtain lemon extract.
The rosemary extract is prepared by the following method:
weighing an appropriate amount of rosemary, soaking in 80% ethanol solution for 0.25-0.75h, reflux extracting for 3 times, adding 25-30 times of 80% ethanol solution for 1 time to 1 time, extracting for 1-2.5h, adding 20-25 times of 80% ethanol solution for 2 times, extracting for 1-1.5h, adding 10-15 times of 80% ethanol solution for 3 times, extracting for 1-1.5h, filtering with four layers of gauze each time, mixing filtrates, concentrating the filtrate to 1-3 times mL/g of rosemary weight, and filtering to obtain rosemary extract for later use.
The roselle extract is prepared by the following method:
weighing a proper amount of dry roselle coarse powder, soaking for 1.5-2h, heating and decocting at 90-100 ℃ for 3 times, adding 20-25 times of water for 1 time, extracting for 1.5-2.5h, adding 15-20 times of water for 2 times, extracting for 1-1.5h, adding 8-12 times of water for 3 times, extracting for 0.5-1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 4-10 mL/g of dry roselle coarse powder, filtering with double layers of gauze to obtain roselle extract for later use.
The essence is selected from one or more of rose essence, cucumber essence, lily essence, sweet osmanthus essence, lemon essence or lavender essence.
The invention provides a preparation method of body lotion for tightening, moistening and smoothing skin, which comprises the following steps:
a) weighing 0.2-1.5g of sodium carboxymethylcellulose, dissolving in 10-80mL of distilled water, standing for 12-24 h, and obtaining a uniform and transparent sodium carboxymethylcellulose solution for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
b) weighing 0.1-1.0g of sodium alginate, adding 10-30mL of distilled water, stirring, transferring to water of 60-80 deg.C, stirring for 3-8min, taking out, standing at normal temperature for 2-5 hr to obtain uniform sodium alginate solution with moderate viscosity;
c) weighing 0.01-0.2g of ice crystal forming agent AVC, dissolving in 5-30mL of distilled water, stirring, transferring to water of 60-80 ℃, continuously stirring for 5-10min, taking out, standing for 2-6 h at normal temperature to obtain uniform and transparent solution of ice crystal forming agent AVC for later use;
d) respectively weighing 0.1-1.5g of organic strawberry seed oil, 0.1-1.5g of sea buckthorn oil, 0.1-1.5g of evening primrose oil, 0.1-1.5g of macadamia nut oil, 0.5-4.0g of natural APG liquid crystal type emulsifier and 0.5-4.0g of AC-402 composite emulsifier, mixing, placing in a constant-temperature water bath kettle at 75-90 ℃, heating while stirring to uniformly mix to obtain an oil phase for later use;
e) measuring 5-20mL of distilled water, and heating in a constant-temperature water bath kettle at 75-90 ℃ to obtain a water phase for later use;
f) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed, and emulsifying for 15-30min to obtain O/W emulsion matrix;
g) weighing 0.1-0.5g of ethylparaben, adding 1-3mL of 1, 2-propylene glycol, and stirring for dissolving to obtain a preservative solution;
h) weighing 1-20mL of jasmine extract, 1-15mL of lemon extract, 1-20mL of rosemary extract, 1-15mL of roselle extract and 1-10mL of honey, then weighing 1.0-3.0g of saralaxyl and 0.5-2.0g of Liponic EG-1, mixing, stirring for dissolving, and uniformly mixing to obtain a mixed solution;
i) adding the prepared sodium carboxymethylcellulose solution, sodium alginate solution, ice crystal forming agent AVC solution, mixed solution, antiseptic solution, and 0.05-0.4mL essence into O/W type emulsion matrix, stirring, and mixing to obtain body lotion for tightening and moistening skin.
The components in the invention are as follows:
macadamia nut oil is mild in nature, does not irritate the skin, contains a large amount of natural vegetable oil of palmitoleic acid, has a fatty acid composition similar to that of human sebum, contains nutrients necessary for forming a grease protective layer on the skin, has a high dispersion coefficient and permeability on the skin, protects cell membranes, moistens and moisturizes the skin, can soften and revitalize aged or dry skin, has a high permeation speed on the skin, and can leave a smooth and non-greasy feeling on the skin.
The evening primrose oil has good stability, small viscosity change and good skin affinity, is a good emollient and softener, is easily absorbed by skin capillaries, can promote blood circulation, prevent epidermal cell keratinization, keep skin smooth and delay skin aging. Unsaturated fatty acid molecules in evening primrose oil provide sufficient toughness to the skin structure and prevent loss of skin moisture.
The oleum Hippophae contains fructus Hippophae flavone, carotene, carotenoid, phospholipid compounds, vitamin E, and mineral selenium, has strong antioxidation effect, and can rapidly promote microcirculation, repair skin cells, and improve skin metabolism. The oleum Hippophae is rich in vitamin C, and can effectively inhibit abnormal pigment deposition on skin, thereby reducing melanin formation and whitening skin.
The organic strawberry seed oil is high-grade natural vegetable oil, is an excellent natural soothing emollient, has excellent skin-friendly property, and can effectively enhance the smoothness and tenderness of skin, help to reduce the water loss of skin and increase the elasticity. The strawberry seed oil contains abundant skin-moistening nutrient components and has soft skin-friendly property, can be mixed with other light oil (such as sweet almond oil) and applied to common body nourishing oil or lotion, and has good effect.
Hibiscus sabdariffa contains abundant proteins, organic acids, vitamin C, various amino acids, natural pigments and various minerals such as calcium, iron, zinc and selenium, and has effects of replenishing blood, invigorating qi, promoting metabolism, scavenging free radicals, caring skin, eliminating macula, and caring skin. The natural fruit acid component contained in the skin care product can dissolve cutin and shrink pores, so that the skin becomes more delicate.
The lemon is rich in vitamin B1Vitamin B2Vitamin C, limonene, bitter essence and citric acidThe skin care product has the effects of relieving fatigue, improving the working capacity of muscles, activating epidermal cells of skin, preventing and eliminating skin pigmentation, whitening skin, softening the horny layer of the skin, whitening and brightening the skin, has strong antioxidant effect, delays senility and promotes the metabolism of the skin, and is a natural good product for beautifying.
The rosemary extract can strongly astringe and compact the skin, increase the skin elasticity, relieve itching, has the function of preventing wrinkles, can condition greasy skin, enables the skin to be fresh and cool, promotes blood circulation, stimulates hair regeneration, and relieves hyperemia, edema and swelling of the skin. The rosemary has obvious effects on oxidation resistance and bacteriostasis, can effectively inhibit the oxidation of various lipoids, delays skin aging and promotes the generation of collagen. It is helpful for cleaning hair follicle and deep skin, and making skin more delicate and transparent. Rosemary is one of common components of antioxidant products, has unique antioxidant effect, promotes skin to have vitality and elasticity, purifies pores, and removes acnes. It can be used for moistening dry skin with lack of water, aging, pachylosis, and wrinkle, and can also be used for treating dark eye and pouch due to frequent overtime work and long-term computer exposure.
The jasmine flower extract can keep moisture and elasticity of skin, promote cell regeneration, has the effects of diminishing inflammation and calming, has the conditioning effect on dry, water-deficient, oily and sensitive skin, eczema and inflammation, can fade striae gravidarum and scars, increase skin elasticity, has remarkable effect of delaying skin aging, can effectively relieve skin fatigue and pressure, simultaneously resists photoaging, sensitivity, redness and ultrastrong antioxidant effect, discharges skin turbidity, removes somberness and sinks, can effectively activate skin, provides comprehensive moistening and moisturizing effects, can shape plastic, moisten, compact and tender healthy skin, remarkably improves skin elasticity and shows perfect balance of skin. The flos Jasmini sambac has effects of inhibiting various bacteria, killing bacteria, relieving inflammation, promoting cell regeneration, and balancing sebum secretion. The jasmine flower can keep moisture, but cannot block pores, and has pleasant and comfortable fragrance.
The honey is sweet in taste and neutral in nature, is rich in various elements such as vitamins, fructose, glucose, potassium, sodium, iron, malic acid, amylase, oxidase and the like, can stimulate blood circulation of skin, moisten skin, improve nutritional status, resist wrinkle, keep moisture, prevent sunburn, protect skin, remove dead skin, improve metabolism level, enhance antibacterial power and vitality of skin, can effectively reduce melanin deposition, promote cell growth, delay aging, enhance elasticity and toughness of skin, prevent lip chapping, eliminate scars, remove acnes and make skin whiter, tender and smooth.
The saralin mainly contains polysaccharide components in sargassum, has high water solubility, is rich in anions, and has effects of promoting skin metabolism, stimulating fibroblast to produce more colloid, elastin, mucopolysaccharide, etc., promoting epidermal cell growth, promoting metabolism, and preventing skin aging. It has wide application, smooth skin feeling, and soft and smooth skin feeling after washing. It has effects of keeping moisture and removing wrinkle, especially in facial mask and eye gel, and can immediately tighten skin. It has effects in promoting epidermal cell growth, promoting metabolism, and preventing skin aging. In addition, the texture and viscosity of the finished product can be increased.
Liponic EG-1 has a smooth and fine tactile sensation as a moisturizer and a lubricant. It can be used as skin conditioner, and has good compatibility with cationic, nonionic and anionic surfactants. In addition to being highly effective as a humectant, Liponic EG-1 is also a good dispersion vehicle, viscosity modifier, plasticizer, foam modifier and excellent lubricant.
The macadamia nut oil can increase the lubrication degree and the nourishing degree, so that the skin is soft and active; the evening primrose oil can prevent epidermal cell from keratinization and keep skin smooth; the oleum Hippophae can repair skin cells and improve skin metabolism; the organic strawberry seed oil can effectively enhance the smoothness and tenderness of skin and help to reduce the water loss of the skin; hibiscus sabdariffa contains components with remarkable antioxidant function, and has skin caring effect; lemon can prevent and eliminate skin pigmentation; the rosemary can effectively astringe and compact the skin; the jasmine flower can keep the moisture and elasticity of the skin; the honey can stimulate blood circulation of skin, and improve skin elasticity and toughness. In a word, the components supplement each other to achieve the effects of firming, moistening and smoothing the skin. The emulsion prepared by the invention is semitransparent creamy yellow, has proper viscosity, is fine, smooth and even, is light and moist, is bright and fair, has good spreading property, is quickly absorbed, and has fragrant smell.
Compared with the prior art, the body lotion prepared by the invention can deeply moisten similar body lotions, regulate the moisture degree of skin and strengthen a natural skin moisturizing layer. Meanwhile, the skin care product can deeply moisten the horny layer of the skin, continuously supplement water and nutrients required by the skin, thoroughly change the state of the skin and enable the skin to be full, watery and elastic.
Detailed Description
The present invention will be further described with reference to the following examples.
According to the rules of pharmacopoeia, in the preparation process, the coarse powder can completely pass through a No. two sieve, but is mixed with powder which can pass through a No. four sieve by no more than 40%; the concentration of the ethanol is volume concentration; all extractions were carried out under slightly boiling conditions.
Example 1
A body lotion for tightening, moistening and smoothing skin is composed of the following raw materials in proportion:
Figure BDA0001237348720000081
1.1 preparation of jasmine flower extract:
weighing a proper amount of dried jasmine flowers, soaking for 1h, heating and decocting at 80 ℃ for 3 times, adding 20 times of water for 1 time, extracting for 1.5h, adding 10 times of water for 2 times, extracting for 1h, adding 5 times of water for 3 times, extracting for 0.5h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 5 times mL/g of the weight of the dried jasmine flowers, and filtering with two layers of gauze for later use.
1.2 preparing rosemary extract:
weighing an appropriate amount of rosemary, soaking in 80% ethanol solution for 0.25h, performing reflux extraction for 3 times, adding 25 times of 80% ethanol solution for 1 time, extracting for 1h, adding 20 times of 80% ethanol solution for 2 times, extracting for 1h, adding 10 times of 80% ethanol solution for 3 times, extracting for 1h, filtering with four layers of gauze each time, combining filtrates, concentrating the filtrate to 2 times mL/g of the weight of the rosemary, and filtering to obtain rosemary extract for later use.
1.3 preparation of Hibiscus sabdariffa extract:
weighing a proper amount of dry roselle coarse powder, soaking for 1.5h, heating and decocting at 90 ℃ for 3 times, adding 20 times of water for 1 time, extracting for 1.5h, adding 15 times of water for 2 times, extracting for 1h, adding 8 times of water for 3 times, extracting for 0.5h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 4 mL/g of the weight of roselle, and filtering with double layers of gauze to obtain roselle extract for later use.
1.4 preparation of lemon extract:
weighing an appropriate amount of dry lemon slice coarse powder, adding water, soaking for 0.5h, heating, decocting and extracting for 3 times, adding 10 times of water for 1 time, extracting for 0.5h, adding 8 times of water for 2 times, extracting for 0.5h, adding 8 times of water for 3 times, extracting for 0.5h, filtering each time, combining the filtrates, concentrating the volume of the filtrate to 4 times mL/g of the weight of the dry lemon slices, and filtering to obtain the lemon slice.
1.5A preparation method of body lotion for tightening, moistening and smoothing skin comprises the following steps:
a) weighing 0.5g of sodium carboxymethylcellulose, dissolving in 20mL of distilled water, standing for 12h, and obtaining a uniform and transparent sodium carboxymethylcellulose solution for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
b) weighing 0.5g of sodium alginate, adding 15mL of distilled water, stirring with a clean glass rod, transferring to water with the temperature of 60 ℃, continuously stirring for 3min, taking out, standing for 2h at normal temperature to obtain a uniform sodium alginate solution with moderate viscosity for later use;
c) weighing 0.1g of ice crystal forming agent AVC, dissolving in 10mL of distilled water, stirring with a clean glass rod, transferring to water of 60 ℃, continuously stirring for 5min, taking out, standing for 2h at normal temperature to obtain a uniform and transparent solution of ice crystal forming agent AVC for later use;
d) respectively weighing 0.5g of organic strawberry seed oil, 0.5g of sea buckthorn oil, 0.5g of evening primrose oil, 0.5g of macadamia nut oil, 1g of natural APG liquid crystal type emulsifier and 1g of AC-402 compound type emulsifier, placing the mixture in a clean beaker 1, placing the beaker in a 75 ℃ constant temperature water bath kettle, heating and stirring the beaker to uniformly mix the mixture to obtain an oil phase for later use;
e) measuring 10mL of distilled water, and heating in a constant-temperature water bath kettle at 75 ℃ to be used as a water phase for later use;
f) slowly adding the water phase into the oil phase along the wall of the beaker when the oil phase and the water phase reach the same temperature, heating and uniformly stirring along the same direction, and emulsifying after 15min to obtain O/W type emulsion matrix;
g) weighing 0.1g of ethylparaben, adding 1mL of 1, 2-propylene glycol, and stirring to dissolve to obtain a preservative solution;
h) measuring 5mL of jasmine extract, 5mL of lemon extract, 5mL of rosemary extract, 5mL of roselle extract and 5mL of honey; weighing 1.0g of saralalin and 0.5g of Liponicic EG-1, mixing, stirring for dissolving, and uniformly mixing to obtain a solution 1;
i) adding the prepared sodium carboxymethylcellulose solution, the sodium alginate solution, the ice crystal forming agent AVC solution, the solution 1, the preservative solution and 0.05mL of rose essence into the emulsion matrix, and stirring and mixing uniformly to obtain the body lotion for firming, moistening and smoothing skin.
Example 2
A body lotion for tightening, moistening and smoothing skin is composed of the following raw materials in proportion:
Figure BDA0001237348720000101
Figure BDA0001237348720000111
2.1 preparation of jasmine flower extract:
weighing a proper amount of dried jasmine flowers, soaking for 1.5h, heating and decocting at 90 ℃ for 3 times, adding 25 times of water for 1 time, extracting for 2h, adding 15 times of water for 2 times, extracting for 1.5h, adding 8 times of water for 3 times, extracting for 1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 10 times mL/g of the weight of the dried jasmine flowers, and filtering with two layers of gauze for later use.
2.2 preparing rosemary extract:
weighing an appropriate amount of rosemary, soaking in 80% ethanol solution for 0.5h, performing reflux extraction for 3 times, adding 30 times of 80% ethanol solution for 1 time, extracting for 2h, adding 25 times of 80% ethanol solution for 2 times, extracting for 1.5h, adding 12 times of 80% ethanol solution for 3 times, extracting for 1h, filtering with four layers of gauze for each time, combining filtrates, concentrating the filtrate to 2 times mL/g of the weight of the rosemary, and filtering to obtain rosemary extract for later use.
2.3 preparation of Hibiscus sabdariffa extract:
weighing a proper amount of dry roselle coarse powder, soaking for 2h, heating and decocting at 95 ℃ for 3 times, adding 22 times of water for 1 time, extracting for 2h, adding 18 times of water for 2 times, extracting for 1.5h, adding 10 times of water for 3 times, extracting for 1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 8 mL/g of the weight of the dry roselle coarse powder, and filtering with double layers of gauze to obtain a roselle extract for later use.
2.4 preparation of lemon extract:
weighing a proper amount of dry lemon slice coarse powder, adding water, soaking for 0.5h, heating, decocting and extracting for 3 times, adding 12 times of water for the 1 st time, extracting for 1h, adding 10 times of water for the 2 nd time, extracting for 1h, adding 8 times of water for the 3 rd time, extracting for 1h, filtering each time, combining the filtrates, concentrating the volume of the filtrate to 6 times mL/g of the weight of the dry lemon slice coarse powder, and filtering to obtain the lemon slice coarse powder.
2.5A preparation method of the body lotion for tightening, moistening and smoothing skin comprises the following steps:
a) weighing 1g of sodium carboxymethylcellulose, dissolving the sodium carboxymethylcellulose in 60mL of distilled water, standing for 24h, and obtaining a uniform and transparent sodium carboxymethylcellulose solution for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
b) weighing 0.5g of sodium alginate, adding 20mL of distilled water, stirring with a clean glass rod, transferring to 75 ℃ water, continuously stirring for 6min, taking out, standing for 4h at normal temperature to obtain a uniform sodium alginate solution with moderate viscosity for later use;
c) weighing 0.15g of ice crystal forming agent AVC, dissolving in 20mL of distilled water, stirring with a clean glass rod, transferring to 75 ℃ water, continuously stirring for 8min, taking out, standing for 5h at normal temperature to obtain a uniform and transparent ice crystal forming agent AVC solution for later use;
d) respectively weighing 1.0g of organic strawberry seed oil, 1.0g of sea buckthorn oil, 1.0g of evening primrose oil, 1.0g of macadamia nut oil, 2.0g of natural APG liquid crystal type emulsifier and 2.0g of AC-402 compound type emulsifier, placing the mixture in a clean beaker 1, placing the beaker in a constant-temperature water bath kettle at 75 ℃, heating and stirring the beaker to uniformly mix the mixture to obtain an oil phase for later use;
e) measuring 20mL of distilled water, and heating in a constant-temperature water bath kettle at 75 ℃ to be used as a water phase for later use;
f) slowly adding the water phase into the oil phase along the wall of the beaker when the oil phase and the water phase reach the same temperature, heating and stirring uniformly along the same side, and completing emulsification after 20min to obtain an O/W type emulsion matrix;
g) weighing 0.2g of ethylparaben, adding 2mL of 1, 2-propylene glycol, and stirring to dissolve to obtain a preservative solution;
h) weighing 10mL of jasmine extract, 10mL of lemon extract, 10mL of rosemary extract, 10mL of roselle extract and 8mL of honey; weighing 2.0g of saralalin and 1.0g of Liponicic EG-1, mixing, stirring for dissolving, and uniformly mixing to obtain a solution 1;
i) adding sodium carboxymethylcellulose solution, sodium alginate solution, ice crystal forming agent AVC solution, solution 1, antiseptic solution, and 0.2ml Bulbus Lilii essence into emulsion matrix, stirring, and mixing to obtain body lotion for tightening and moistening skin.
Example 3
A body lotion for tightening, moistening and smoothing skin is composed of the following raw materials in proportion:
Figure BDA0001237348720000131
Figure BDA0001237348720000141
3.1 preparation of jasmine flower extract:
weighing a proper amount of dried jasmine flowers, soaking for 2h, heating and decocting at 100 ℃ for 3 times, adding 30 times of water for 1 time, extracting for 2.5h, adding 20 times of water for 2 times, extracting for 1.5h, adding 10 times of water for 3 times, extracting for 1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 12 times mL/g of the weight of the dried jasmine flowers, and filtering with two layers of gauze for later use.
3.2 preparing rosemary extract:
weighing an appropriate amount of rosemary, soaking in 80% ethanol solution for 0.75h, performing reflux extraction for 3 times, adding 30 times of 80% ethanol solution for 1 time, extracting for 2.5h, adding 25 times of 80% ethanol solution for 2 times, extracting for 1.5h, adding 15 times of 80% ethanol solution for 3 times, extracting for 1.5h, filtering with four layers of gauze each time, combining filtrates, concentrating the filtrate to 3 mL/g of rosemary weight, and filtering to obtain rosemary alcohol extract for later use.
3.3 preparation of Hibiscus sabdariffa extract:
weighing a proper amount of dry roselle coarse powder, soaking for 2h, heating and decocting at 100 ℃ for 3 times, adding 25 times of water for 1 time, extracting for 2.5h, adding 20 times of water for 2 times, extracting for 1.5h, adding 12 times of water for 3 times, extracting for 1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 10 mL/g of the weight of the dry roselle coarse powder, and filtering with two layers of gauze to obtain a roselle extract for later use.
3.4 preparation of lemon extract:
weighing a proper amount of dry lemon slice coarse powder, adding water, soaking for 0.75h, heating, decocting and extracting for 3 times, adding 15 times of water for the 1 st time, extracting for 2h, adding 12 times of water for the 2 nd time, extracting for 1.5h, adding 10 times of water for the 3 rd time, extracting for 1.5h, filtering each time, combining the filtrates, concentrating the volume of the filtrate to 8 times mL/g of the weight of the dry lemon slice coarse powder, and filtering to obtain the lemon slice coarse powder.
3.5A preparation method of the body lotion for tightening, moistening and smoothing skin comprises the following steps:
a) weighing 1.5g of sodium carboxymethylcellulose, dissolving in 80mL of distilled water, standing for 24h, and obtaining a uniform and transparent sodium carboxymethylcellulose solution for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
b) weighing 1.0g of sodium alginate, adding 30mL of distilled water, stirring with a clean glass rod, transferring to 80 ℃ water, continuously stirring for 8min, taking out, standing for 5h at normal temperature to obtain a uniform sodium alginate solution with moderate viscosity for later use;
c) weighing 0.2g of ice crystal forming agent AVC, dissolving in 30mL of distilled water, stirring with a clean glass rod, transferring to 80 ℃ water, continuously stirring for 10min, taking out, standing for 6 h at normal temperature to obtain a uniform and transparent ice crystal forming agent AVC solution for later use;
d) respectively weighing 1.5g of organic strawberry seed oil, 1.5g of sea buckthorn oil, 1.5g of evening primrose oil, 1.5g of macadamia nut oil, 4.0g of natural APG liquid crystal type emulsifier and 4.0g of AC-402 compound type emulsifier, placing the mixture in a clean beaker 1, placing the beaker in a constant-temperature water bath kettle at 80 ℃, heating while stirring to uniformly mix the mixture to obtain an oil phase for later use;
e) measuring 20mL of distilled water, and heating in a 90 ℃ constant-temperature water bath kettle to be used as a water phase for later use;
f) slowly adding the water phase into the oil phase along the wall of the beaker when the oil phase and the water phase reach the same temperature, heating and stirring uniformly along the same side, and completing emulsification after 30min to obtain an O/W type emulsion matrix;
g) weighing 0.5g of ethylparaben, adding 3mL of 1, 2-propylene glycol, and stirring to dissolve to obtain a preservative solution;
h) weighing 20mL of jasmine extract, 15mL of lemon extract, 20mL of rosemary extract, 15mL of roselle extract and 10mL of honey; weighing 3.0g of saralalin and 2.0g of Liponicic EG-1, mixing, stirring for dissolving, and uniformly mixing to obtain a solution 1;
i) adding sodium carboxymethylcellulose solution, sodium alginate solution, ice crystal forming agent AVC solution, solution 1, antiseptic solution, and flos Osmanthi Fragrantis essence 0.3ml into emulsion matrix, stirring, and mixing to obtain body lotion for tightening and moistening skin.
Example 4
The physical and chemical indexes of the examples 1,2 and 3 are as follows:
4.1 Properties
The invention is semitransparent creamy yellow, has proper viscosity, is fine, smooth and even, is light and moist, is bright and fair, has good spreading performance, is quickly absorbed and has fragrant smell.
4.2pH check
Taking the product, and measuring with pH meter to obtain pH value of 6-7.
4.3 Cold-Heat test
The body milk is packaged in a transparent cosmetic bottle and refrigerated in a refrigerator at 4 ℃ for one month for observation without layering phenomenon. The emulsion is placed in a constant temperature box at 55 ℃ for 24 hours, and the phenomena of layering, emulsification and odor change of the emulsion are avoided.
4.4 centrifugal test
The body milk is packaged in a test tube with a plug and centrifuged at 3000r/min for 20min, and no layering phenomenon occurs.
4.5 Room temperature standing experiment
The body milk prepared in the examples 1,2 and 3 was placed in an emulsion bottle and left standing at room temperature for 6 months, and no demixing phenomenon, no change in feeling after use and no change in odor were observed.
4.6 irritation test and allergy test
The back of the white mouse was cut to remove hairs, and body lotions prepared according to examples 1,2, and 3 were applied to the cut-out parts, respectively, to compare with the non-coated parts, resulting in no irritation or allergic reaction.
A proper amount of the body lotion prepared in examples 1,2 and 3 was applied to the hands of volunteers (15-70 years old, 100 persons), and no redness, rash or blister appeared after 30 minutes.
4.7 comprehensive Effect examination of body milk
The efficacy of the body milks produced in examples 1,2 and 3 was evaluated by the following trial feeling. A civil investigation and grading method is adopted, 120 volunteers in the age range of 15-70 years are selected as trial objects, the trial objects are divided into three groups at will, the body milk prepared in the embodiment 1, the embodiment 2 and the embodiment 3 is respectively smeared on all parts of the body, and the using time is two months. The using effects of the ingredients are divided into 5 points: the fifth is the highest score, which shows good and very satisfactory; 4, the division is better; 3 is acceptable; when the amount is less than 3 points, the results are not acceptable. The average score of each item is as follows. The results are shown in Table 1
Table 1 comprehensive effect investigation
Figure BDA0001237348720000171
Figure BDA0001237348720000181
In conclusion, the prepared body lotion is fine, uniform, light and moist, has fragrant smell and quick absorption, and can deeply nourish the skin and regulate the moisture degree of the skin.

Claims (2)

1. The body lotion for tightening and moistening the smooth skin is characterized by comprising the following raw materials in parts by weight:
organic strawberry seed oil 0.1-1.5g
Sea buckthorn oil 0.1-1.5g
Evening primrose oil 0.1-1.5g
Macadamia nut oil 0.1-1.5g
0.5-4.0g of natural APG liquid crystal type emulsifier
0.5-4.0g of AC-402 compound emulsifier
0.01-0.2g of ice crystal forming agent AVC
Sodium carboxymethylcellulose 0.2-1.5g
Sodium alginate 0.1-1.0g
1-20mL of jasmine flower extract
1-15mL of lemon extract
Rosemary extract 1-20mL
Hibiscus sabdariffa extract 1-15mL
1-10mL of honey
Liponic EG-1 0.5-2.0g
0.05-0.4mL of essence
1.0-3.0g saralin
30-160mL of distilled water
1-3mL of 1, 2-propanediol
0.1-0.5g of ethylparaben;
the jasmine flower extracting solution is prepared by the following method:
weighing a proper amount of dried jasmine flowers, soaking for 1-2h, heating and decocting at 80-100 ℃ for 3 times, adding 20-30 times of water for 1 time, extracting for 1.5-2.5h, adding 10-20 times of water for 2 times, extracting for 1-1.5h, adding 5-10 times of water for 3 times, extracting for 0.5-1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 3-12 times mL/g of the weight of the dried jasmine flowers, and filtering with two layers of gauze for later use;
the rosemary extract is prepared by the following method:
weighing an appropriate amount of rosemary, soaking in 80% ethanol solution for 0.25-0.75h, performing reflux extraction for 3 times, adding 25-30 times of 80% ethanol solution for 1 time to 2.5h, adding 20-25 times of 80% ethanol solution for 2 times, extracting for 1-1.5h, adding 10-15 times of 80% ethanol solution for 3 times, extracting for 1-1.5h, filtering with four layers of gauze each time, mixing filtrates, concentrating the filtrate to 1-3 times mL/g of the weight of the rosemary, and filtering to obtain rosemary extract for later use;
the lemon extract is prepared by the following method:
weighing an appropriate amount of dry lemon slice coarse powder, adding water, soaking for 0.5-0.75h, heating, decocting and extracting for 3 times, adding 10-15 times of water for 1 time, extracting for 0.5-2h, adding 8-12 times of water for 2 times, extracting for 0.5-1.5h, adding 8-10 times of water for 3 times, extracting for 0.5-1.5h, filtering each time, combining filtrates, concentrating the volume of the filtrate to 4-8 times mL/g of the weight of the dry lemon slice coarse powder, and filtering to obtain a lemon extract;
the roselle extract is prepared by the following method:
weighing a proper amount of dry roselle coarse powder, soaking for 1.5-2h, heating and decocting at 90-100 ℃ for 3 times, adding 20-25 times of water for 1 time, extracting for 1.5-2.5h, adding 15-20 times of water for 2 times, extracting for 1-1.5h, adding 8-12 times of water for 3 times, extracting for 0.5-1h, filtering with three layers of gauze each time, combining filtrates, concentrating the volume of the filtrate to 4-10 times mL/g of the weight of the dry roselle coarse powder, filtering with double layers of gauze to obtain roselle extract for later use;
the preparation method of the body lotion for tightening, moistening and smoothing skin comprises the following steps:
a) weighing 0.2-1.5g of sodium carboxymethylcellulose, dissolving in 10-80mL of distilled water, standing for 12-24 h, and obtaining a uniform and transparent sodium carboxymethylcellulose solution for later use after the sodium carboxymethylcellulose is naturally swelled and dissolved;
b) weighing 0.1-1.0g of sodium alginate, adding 10-30mL of distilled water, stirring, transferring to water of 60-80 deg.C, stirring for 3-8min, taking out, standing at normal temperature for 2-5 hr to obtain uniform sodium alginate solution with moderate viscosity;
c) weighing 0.01-0.2g of ice crystal forming agent AVC, dissolving in 5-30mL of distilled water, stirring, transferring to water of 60-80 ℃, continuously stirring for 5-10min, taking out, standing for 2-6 h at normal temperature to obtain uniform and transparent solution of ice crystal forming agent AVC for later use;
d) respectively weighing 0.1-1.5g of organic strawberry seed oil, 0.1-1.5g of sea buckthorn oil, 0.1-1.5g of evening primrose oil, 0.1-1.5g of macadamia nut oil, 0.5-4.0g of natural APG liquid crystal type emulsifier and 0.5-4.0g of AC-402 composite emulsifier, mixing, placing in a constant-temperature water bath kettle at 75-90 ℃, heating while stirring to uniformly mix to obtain an oil phase for later use;
e) measuring 5-20mL of distilled water, and heating in a constant-temperature water bath kettle at 75-90 ℃ to obtain a water phase for later use;
f) slowly adding the water phase into the oil phase along the wall of the container when the oil phase and the water phase reach the same temperature, heating and stirring at the same direction at constant speed, and emulsifying for 15-30min to obtain O/W emulsion matrix;
g) weighing 0.1-0.5g of ethylparaben, adding 1-3mL of 1, 2-propylene glycol, and stirring for dissolving to obtain a preservative solution;
h) weighing 1-20mL of jasmine extract, 1-15mL of lemon extract, 1-20mL of rosemary extract, 1-15mL of roselle extract and 1-10mL of honey, then weighing 1.0-3.0g of saralaxyl and 0.5-2.0g of Liponic EG-1, mixing, stirring for dissolving, and uniformly mixing to obtain a mixed solution;
i) adding the prepared sodium carboxymethylcellulose solution, sodium alginate solution, ice crystal forming agent AVC solution, mixed solution, antiseptic solution, and 0.05-0.4mL essence into O/W type emulsion matrix, stirring, and mixing to obtain body lotion for tightening and moistening skin.
2. The firming and moisturizing and skin-smoothing body lotion according to claim 1, wherein the essence is selected from one or more of rose essence, cucumber essence, lily essence, osmanthus essence, lemon essence or lavender essence.
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