CN110251417A - Essence cream and preparation method thereof before oil-control reparation adornment - Google Patents
Essence cream and preparation method thereof before oil-control reparation adornment Download PDFInfo
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- CN110251417A CN110251417A CN201910630174.9A CN201910630174A CN110251417A CN 110251417 A CN110251417 A CN 110251417A CN 201910630174 A CN201910630174 A CN 201910630174A CN 110251417 A CN110251417 A CN 110251417A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P29/00—Non-central analgesic, antipyretic or antiinflammatory agents, e.g. antirheumatic agents; Non-steroidal antiinflammatory drugs [NSAID]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
Abstract
The present invention relates to essence creams before a kind of oil-control reparation adornment and preparation method thereof, belong to cosmetic field.Essence cream includes following components before the adornment: emulsifier: 1-5 parts by weight, preferably 2-4.5 parts by weight；Emollient: 3-15 parts by weight, preferably 5-14 parts by weight；Moisturizing component: 5-15 parts by weight, preferably 7-12 parts by weight；Oil-control ingredient: 1.0-5.0 parts by weight, preferably 1.5-4.5 parts by weight；Ceramide: 1.0-5.0 parts by weight, preferably 2.0-4.5 parts by weight.Essence cream can effectively adsorb the grease of skin secretion, not adsorb the moisture of skin itself, maintain the water and oil balance of skin surface, persistently fix for the oil-control reparation of sensitive skin before adornment is repaired in oil-control of the invention.Essence cream can repair the barrier function of skin before oil-control reparation adornment, prevent skin from playing scurf and drying, subsequent makeup can seem docile, persistently.
Description
Technical field
The present invention relates to essence creams before a kind of oil-control reparation adornment and preparation method thereof, belong to cosmetic field.
Background technique
With atmosphere pollution, the damages such as light radiation it is more prevalent, the environment that skin is exposed is more and more severe, and skin is asked
Topic continuously emerges, and the number that Chinese women is perplexed by skin problem rises year by year.The female consumer use bottom of sensitive skin
When adornment product, it may appear that dry decortication, rise bits, general red, itch, it is intractable, not lasting the problems such as.With to makeups habit and meaning
Know upgrading, women increasingly focuses on skin care health problem while makeup.According to Ying Minte data analyze, adornment foremilk category due to
It is using time saving, quick, using the more docile lasting advantage of rear adornment sense, over the past two years with twice of speed rapid growth, more
Liked to get over by the majority of consumers.
Adornment foremilk common in the art, can substantially divide several types.Such as: isolated form adornment foremilk, humidity-preserving type adornment
Foremilk, pore covering type adornment foremilk etc..Wherein, isolated form adornment foremilk is mainly used for making up skin color unevenness, obscure disadvantage, office
Portion is easy that face is made to seem white using skin capable of being made to be modified, unnatural.Humidity-preserving type adornment foremilk relatively moistens, can be with
It prevents skin from the problem of drying, furfur occur, but has many oil contents, skin is difficult to absorb, but also can cause the bad of skin
Reaction.Pore covering type adornment foremilk, is added a large amount of elastomer silicones, can play the role of stealthy pore, but can make skin
It is very dry, it is easy to produce and rubs mud phenomenon with the hands.
Citation [1] provides a kind of cosmetic composition, specifically for liquid cosmetic composition form, in physiology
Include in medium: (i) is at least one to have > 1.6 refraction index and with 1 micron to 20 microns, preferably 1 micron to 15 microns
Granularity piece type filler, (ii) at least one silicone elastomer, preferably non-emulsified silicone elastomer, and (iii) at least one has
The filler of oil absorption capacity more than or equal to 1 ml/g.The composition is preferably used as being intended to reduce skin defect, especially
The visibility of pore, and the skin care or color make-up bottoming liquid that keep pore covering effect lasting or adornment foremilk.The cosmetic composition makes
With a large amount of elastomer silicone, stealthy pore can be played the role of, but skin can be made very dry, it is existing to be easy to produce stranding mud
As.
It includes following component that citation [2], which provides a kind of skin care compositions and its application, the skin care compositions: remaining
Sweet sub- berry extract, phllostachys pubescens leaf ext and seaweed extract.It is found through experiments that, emblic berry extract, Moso Bamboo Leaves extract
Object and seaweed extract compounding, can generate synergistic function at anti-oxidant aspect, have the skin care compositions stronger
Free radical scavenging ability.But oil-control effect is poor, but cannot repair impaired skin, can not block extraneous other injuries.
Citation [1] CN104379216A
Citation [2] CN109350577A
Summary of the invention
Problems to be solved by the invention
In view of the technical problems existing in the prior art, essence is newborn before repairing adornment present invention firstly provides a kind of oil-control.
The mistake many greases of sauce of the essence cream property of can choose absorption skin secretion, has strong adsorption capacity to grease, to be formed good before the adornment
Good oil-control effect.Essence cream is used before adornment before adornment of the invention, bottom adornment product can be helped more preferably to hold adornment, while having moisturizing
With the effect for repairing skin barrier.
Further, the present invention also provides a kind of preparation methods of essence cream before adornment, and preparation method is simple for this, former
Material is easily obtained.
The solution to the problem
The present invention provides essence cream before a kind of adornment comprising following components:
Emulsifier: 1-5 parts by weight, preferably 2-4.5 parts by weight；
Emollient: 3-15 parts by weight, preferably 5-14 parts by weight；
Moisturizing component: 5-15 parts by weight, preferably 7-12 parts by weight；
Oil-control ingredient: 1.0-5.0 parts by weight, preferably 1.5-4.5 parts by weight；
Ceramide: 1.0-5.0 parts by weight, preferably 2.0-4.5 parts by weight.
Essence cream before adornment according to the present invention, wherein the emulsifier includes primary emulsion and assistant for emulsifying agent, wherein
The primary emulsion include C20-22 alkyl phosphate (and) C20-22 fatty alcohol；
The assistant for emulsifying agent include cetostearyl alcohol (and) cocoyl glucoside.
Essence cream before adornment according to the present invention, wherein the additional amount of the primary emulsion is 0.5-3.0 parts by weight, described
The additional amount of assistant for emulsifying agent is 0.5-2.0 parts by weight.
Before adornment according to the present invention essence cream, wherein the emollient include carbonic acid dioctyl ester, cetanol ethylhexyl,
Isononyl isononanoate, octyl dodecanol, dimethicone and polydimethyl siloxanes/polydimethy siloxanes cross-linked polymer
One or more of combination.
Essence cream before adornment according to the present invention, wherein the moisturizing component includes glycerol, butanediol, Sodium Hyaluronate, swallow
The group of one or more of wheat glucan, glycerin polyether -26, Xylitol-based glucoside/anhydro xylitol/xylitol
It closes.
Essence cream before adornment according to the present invention, wherein the oil-control ingredient includes functional composite granule, the functionality
Composite granule includes hydroxyapatite and zinc oxide；Preferably, the mass ratio of the hydroxyapatite and the zinc oxide is
0.25~25:1.
Essence cream before adornment according to the present invention, wherein the preparation method of the functionality composite granule includes using silane
The step of coating hydroxyapatite and zinc oxide.
Essence cream before adornment according to the present invention, wherein the ceramide includes Cer EOS, Cer NP, nerve
The combination of one or more of amide 6-II.
Before adornment according to the present invention essence cream, wherein before the adornment essence cream further include thickener, pH adjusting agent, essence,
The combination of one or more of preservative.
The present invention also provides a kind of preparation methods of essence cream before adornment according to the present invention, wherein including will be described
Before adornment the step of each component mixing of essence cream.
The effect of invention
Essence cream can effectively adsorb skin secretion for the oil-control reparation of sensitive skin before adornment is repaired in oil-control of the invention
Grease, do not adsorb the moisture of skin itself, maintain the water and oil balance of skin surface, persistently fix.Essence before adornment is repaired in oil-control
Cream can repair the barrier function of skin, prevent skin from playing scurf and drying, and subsequent makeup can seem docile, persistently.
Further, preparation method is simple for essence cream before adornment of the invention, and raw material is easily obtained, and is suitble to high-volume
Production.
Specific embodiment
It will be detailed below various exemplary embodiments, feature and aspect of the invention.Dedicated word " example herein
Property " mean " being used as example, embodiment or illustrative ".Here as any embodiment illustrated by " exemplary " should not necessarily be construed as
Preferred or advantageous over other embodiments.
In addition, in order to better illustrate the present invention, numerous details is given in specific embodiment below.
It will be appreciated by those skilled in the art that without certain details, the present invention equally be can be implemented.In other example,
Method well known to those skilled in the art, means, equipment and step are not described in detail, in order to highlight master of the invention
Purport.
Such as without Special Statement, unit used in the present invention is SI units, and the number occurred in the present invention
Value, numberical range should all be interpreted as containing the inevitable Systematic Errors of institute in industrial production.
" water " described herein can be deionized water, distilled water, distilled water, ion exchange water, reverse osmosis water, pure water etc..
<first embodiment>
First embodiment of the invention provides essence cream before a kind of adornment comprising following components:
Emulsifier: 1-5 parts by weight, preferably 2-4.5 parts by weight；
Emollient: 3-15 parts by weight, preferably 5-14 parts by weight；
Moisturizing component: 5-15 parts by weight, preferably 7-12 parts by weight；
Oil-control ingredient: 1.0-5.0 parts by weight, preferably 1.5-4.5 parts by weight；
Ceramide: 1.0-5.0 parts by weight, preferably 2.0-4.5 parts by weight.
Essence cream not only has high-intensitive fatty acid selectivity adsorption capacity before adornment of the present invention, can effectively control
The secretion of liquefaction rouge keeps the water and oil balance of skin, and can also significantly improve bottom adornment product holds adornment, while having anti-inflammatory anti-
Acne effect.
The reduction of problem skin barrier function, skin are easy to experience extraneous stimulation, and sensitive skin is intercellular lipid
Balance, which is destroyed, causes amount of moisture to lose, and shows as easily peeling, easily general red, dry, the symptoms such as itch.And it is smart before adornment of the invention
Magnificent cream can provide the effect of excellent reparation skin barrier function.
In addition, essence cream also has good performance of keeping humidity before adornment of the invention, strengthen skin barrier, long-acting moisturizing reaches
To good moistening effect.Specifically:
Emulsifier
It is preferable to use the emulsifiers of plant origin for emulsifier of the invention.Specifically, the emulsifier of the invention includes
Primary emulsion and assistant for emulsifying agent, wherein the primary emulsion include C20-22 alkyl phosphate (and) C20-22 fatty alcohol；It is described
Assistant for emulsifying agent include cetostearyl alcohol (and) cocoyl glucoside.
Wherein, C20-22 alkyl phosphate (and) C20-22 fatty alcohol is a kind of multi-functional anion emulsifier, be ideal
Skin care emulsifier, apply the velvet-like skin sense that can make skin that there is dumb light in front of adornment of the invention essence cream, relax
Suitable softness skin, while there is good water repelling property, frivolous and ventilative waterproofing membrane can be formed on the skin.In addition, C20-
22 alkyl phosphates (and) C20-22 fatty alcohol has brilliant dispersibility to pigment.
Cetostearyl alcohol (and) emulsifying capacity of cocoyl glucoside is strong, soft moistens.Emulsifiable multiple types are high
Content (such as: oil up to 50%) mutually and in -25 DEG C or less holdings is stablized.In addition, cetostearyl alcohol (and) cocoyl glucose
The compatibility of glycosides and other ingredients of essence cream before adornment of the invention is good.
Present invention preferably uses C20-22 alkyl phosphate (and) C20-22 fatty alcohol and cetostearyl alcohol (and) cocounut oil
The combination of base glucoside, C20-22 alkyl phosphate (and) C20-22 fatty alcohol and cetostearyl alcohol (and) cocoyl glucoside
It is all based on the emulsifier of liquid crystal structure, the two is used in compounding mutually can form elastic network structure and exist with corresponding oil with water phase
Formation stratiform liquid crystal structure in continuous phase, performance is mild and can bring the effect of long-acting moisturizing.
In invention, the content of the emulsifier is 1-5 parts by weight, preferably 2-4.5 parts by weight, and the content of emulsifier is 1-
When 5 parts by weight, product has preferable stability is soft simultaneously to moisten.Specifically, the content of the emulsifier can be
1.5 parts by weight, 2.5 parts by weight, 3 parts by weight, 3.5 parts by weight, 4 parts by weight etc..
Preferably, in the present invention, the additional amount of the primary emulsion is 0.5-2.5 parts by weight, such as: 0.8 parts by weight,
1.0 parts by weight, 1.2 parts by weight, 1.5 parts by weight, 1.8 parts by weight, 2 parts by weight, 2.2 parts by weight etc.；The assistant for emulsifying agent adds
Entering amount is 0.5-2.0 parts by weight；Such as: 0.8 parts by weight, 1.0 parts by weight, 1.2 parts by weight, 1.5 parts by weight, 1.8 parts by weight etc..
Emollient
The emollient of the invention may include carbonic acid dioctyl ester, cetanol ethylhexyl, isononyl isononanoate, octyl
One or both of lauryl alcohol, dimethicone and polydimethyl siloxanes/polydimethy siloxanes cross-linked polymer with
On combination.Preferably, the emollient includes carbonic acid dioctyl ester, cetanol ethylhexyl, octyl dodecanol and poly- diformazan
The combination of one or more of radical siloxane/Dimethicone Crosspolymer.
By the present invention in that skin can be made to form protective film, and smooth non-greasy, there are silk wipings with emollient
Sense can moisten soft skin.Emollient of the invention has the function of moisturizing, moistens, protection, and its spreadability is strong, is easy to
Emulsification, skin sense are soft.In addition, emollient of the invention also has, preferable foundation cream is dispersed, other groups with essence cream before adornment
Dividing has good compatibility.
In the present invention, the additional amount of emollient can be 3-15 parts by weight, preferably 5-14 parts by weight.When adding for emollient
When entering amount less than 3 parts by weight, so that the moisturizing effect of essence cream is unobvious before adornment of the invention, when the additional amount of emollient is greater than
When 15 parts by weight, skin sense is partially greasy, not enough clearly.Specifically, the content of the emollient can be 4 parts by weight, 6 parts by weight, 8
Parts by weight, 10 parts by weight, 12 parts by weight etc..
Moisturizing component
The moisturizing component of the invention includes glycerol, butanediol, Sodium Hyaluronate, oat beta-glucan, glycerin polyether-
26, the combination of one or more of Xylitol-based glucoside/anhydro xylitol/xylitol.
Moisturizing component of the invention can lock moisture in skin, and repair cytoplasm.So that skin epidermis
And cuticula has hygroscopicity, and has regulatory function to skin acid value, skin-friendly is splendid, so that it is flat so that skin is reached water oil
Weighing apparatus.
In the present invention, the additional amount of the moisturizing component is 5-15 parts by weight, preferably 7-12 parts by weight.When moisturizing component
Additional amount less than 5 parts by weight when, it is difficult to play preferable moistening effect, when moisturizing component additional amount be greater than 15 parts by weight
When, skin sense is thick and heavy, and using effect is bad.Specifically, the content of the moisturizing component can be 6 parts by weight, 8 parts by weight, 10 weights
Measure part, 11 parts by weight, 13 parts by weight etc..
Oil-control ingredient
It is preferable to use functional composite granules for oil-control ingredient of the invention.The functionality composite granule includes hydroxy-apatite
Stone and zinc oxide, it is preferable that the zinc oxide is nanoscale zinc oxide.Functional composite granule of the invention is to fatty acid oil
Rouge has the function of high-intensitive selective absorption, can effectively control the secretion of grease, keep the water and oil balance of skin, so as to
To significantly improve the features such as holding adornment and colour stability of bottom adornment product.
In the present invention, the structure of functional composite granule is laminated structure, enhances adhesive force on the skin, is not easy
It falls off, adornment and patch skin are held in enhancing.The grease of the adsorbable skin surface of hydroxyapatite in functional composite granule, especially
It is not adsorb the moisture of skin for the mistake many greases of sauce of summer secretion, easily solves the problems, such as the grease of summer secretion；And it aoxidizes
Zinc can not only play the role of the effect of oil-control, also have and play certain bactericidal antiphlogistic to sensitive skin, prevent skin
There is the symptom of itch and shouting pain.
Further, the preparation method of functional composite granule of the invention includes using silane cladding hydroxyapatite and oxygen
The step of changing zinc.
Specifically, functional composite granule of the invention preparation method the following steps are included:
Step 1) takes hydroxyapatite and zinc oxide and mixes；Preferably, the hydroxyapatite and the zinc oxide
Mass ratio is 0.25~25:1, preferably 0.3~20:1, more preferable 0.3~15:1；Further preferably 0.5~10:1, more into one
Walk preferably 0.6~8:1.
Step 2) takes silane to be sprayed in the obtained mixture of step 1)；Preferably, the hydroxyapatite with it is described
The mass ratio of silane are as follows: 1~50:1,2~45:1,3~40:1,4~35:1,5~30:1,6~25:1,7~20:1 etc..
Preferably, before being mixed hydroxyapatite and zinc oxide, include the steps that dry；The drying when
Between can be 2 hours or more, preferably 4 hours or more, such as 3 hours, 5 hours, 6 hours, 7 hours, 8 hours, 9 hours, 10 is small
When, 11 hours, 12 hours etc.；The temperature of the drying is 80-120 DEG C, preferably 100-120 DEG C.
Preferably, after step 2), further include the steps that dispersion；The time of the dispersion is 5-20 minutes, preferably 8-
15 minutes.
In addition, the present invention is not particularly limited silane, any feasible silane in this field can be, such as: three ethoxies
Base octyl silane etc..
Further, in the present invention, the additional amount of oil-control ingredient can be 1.0-5.0 parts by weight, preferably 1.5-4.5 weight
Part, when the additional amount of oil-control ingredient is 1.0-5.0 parts by weight, it will not only increase burden to skin, but also have good oil-control effect.
Specifically, the content of the oil-control ingredient can be 2 parts by weight, 2.5 parts by weight, 3 parts by weight, 3.5 parts by weight, 4 parts by weight etc..
Ceramide
Since long-time contacts color make-up product, the habit such as makeup removing, can allow the barrier function of skin to be destroyed regularly,
Skin is led to problems such as drying, furfur, itch, erythema, shouting pain occur.Contain 50% neural acyl in healthy skin barrier lipids
Amine plays the role of resisting stimulant, prevents water loss；The impaired major reason of skin barrier is the deficiency of ceramide.
Ceramide is added in essence cream before adornment of the invention, there is excellent compatibility with other components, so as to repair skin
The barrier function of skin prevents skin from playing scurf and drying, and subsequent makeup can seem docile, persistently.
Specifically, ceramide of the invention may include Cer EOS, Cer NP, one in Cer AP-II
Kind or two or more combinations.Wherein, by the infiltration between lipid, percutaneous absorption is played by Cer EOS and Cer AP-II
Consolidate and supplement the ceramide lacked in vivo；Then maintenance is damaged skin barrier to Cer NP from the root, forms protective film,
Extraneous injury is blocked, the effect of maintenance skin barrier function is played.
In the present invention, the additional amount of ceramide is 1.0-5.0 parts by weight, preferably 2.0-4.5 parts by weight.When neural acyl
When the additional amount of amine is 1.0-5.0 parts by weight, the effect for repairing skin barrier can be effectively achieved.Specifically, the neural acyl
The content of amine can be 1.5 parts by weight, 2.5 parts by weight, 3 parts by weight, 3.5 parts by weight, 4 parts by weight etc..
In addition, present invention preferably uses the combination of Cer EOS, Cer NP, Cer AP-II, wherein neural acyl
Amine 1, Cer NP, Cer AP-II mass ratio be 0.1~10:0.1~10:1, preferably 0.5~8:0.5~8:1；More
It is preferred that 0.6~5:0.6~5:1；More preferable 0.8~4:0.8~4:1；Further preferred 1~3:1~3:1.
Other ingredients
Essence cream further includes one or both of thickener, pH adjusting agent, essence, preservative before the adornment of the invention
Above combination.
Thickener can be used in improving the viscosity of oil-control water-setting cream or form gel, keeps the stability of water-setting cream, changes
The physical behavior of kind water-setting cream.Water-setting cream is assigned to stick lubricant nature and have emulsification, stabilization concurrently or it is made to be in the effect of suspended state.This hair
In bright, thickener for example can be carbomer, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, acryloyl
The combination of one or more of dimethyltaurine ammonium/VP copolymer etc..
PH adjusting agent is the substance to maintain or adjust water-setting lactic acid basicity.PH adjusting agent can change and maintain water-setting
The pH value of cream makes the pH of essence cream before adornment close to human skin pH value.Preferably, the pH adjusting agent is arginine, nothing
Color is tasteless, mild pro-skin, provides safeguard for the mildness of oil-control water-setting cream.In addition, arginine is the beneficial ammonia of a kind of pair of human body
Base acid not only can also adjust essence cream pH value before adornment in alkalinity with skin care.
<second embodiment>
Second embodiment of the present invention provides the preparation method of essence cream before the adornment of first embodiment a kind of, including
The step of each component of essence cream before the adornment is mixed.
Specifically, the present invention provides a kind of preparation method of essence cream before the specific adornment comprising following steps:
1) it by part moisturizing component, thickener and part preservative, is added in water phase pot, is heated to 75-80 DEG C, stir molten
Solution completely, keeps the temperature 5-20min, obtains water phase；
2) oil-control ingredient and part emollient are placed in oily phase pot first homogeneous 5-20min, are uniformly mixed, exquisiteness is without particle
It is spare after shape；Then oily phase pot is added after mixing evenly in remaining emollient, is warming up to 70-85 DEG C, keeps the temperature 5-15min, obtain
To oily phase；
3) it takes pH adjusting agent soluble in water, obtains being pre-dissolved object；
4) water phase is placed in emulsion pot, part is added and is pre-dissolved object, stirs evenly, oily phase is pumped into, in 70-85 DEG C of temperature
High speed homogenization 5-10min under lower insulated and stirred continues stirring cooling, and 50 DEG C of additions are remaining to be pre-dissolved object and ceramide, residue
Moisturizing component, essence, after remaining preservative, stir evenly, control cooling rate, slowly cool down, continue 20-40min,
25-45 DEG C of stopping stirring, vacuum defoaming, preparation are completed.
Embodiment
Embodiment of the present invention is described in detail below in conjunction with embodiment, but those skilled in the art will
Understand, the following example is merely to illustrate the present invention, and should not be taken as limiting the scope of the invention.It is not specified in embodiment specific
Condition person carries out according to conventional conditions or manufacturer's recommended conditions.Reagents or instruments used without specified manufacturer is
It can be with conventional products that are commercially available.
Embodiment 1-6
According to the parts by weight of each component of embodiment 1-6 in the following table 1,3,5, and implementation is prepared by the following method
Essence cream before the adornment of example 1-6.
(1) A phase (part moisturizing component, thickener, methyl hydroxybenzoate) is added in water phase pot, is heated to 75-80 DEG C, stirring
Dissolution completely, keeps the temperature 10min, obtains water phase.
(2) G phase (oil-control ingredient and part emollient) is placed in oily phase pot first homogeneous 10min, be uniformly mixed, fine and smooth nothing
It is spare after graininess；Then oily phase pot is added after mixing evenly in B phase (remaining emollient), is warming up to 75 DEG C, heat preservation
10min obtains oily phase.
(3) it after taking D phase (arginine and water) to mix, obtains being pre-dissolved object；
(4) A phase is pumped into emulsion pot, addition is pre-dissolved the 1/2 of object gross mass, stirs evenly, and is pumped into oily phase, heat preservation 75
DEG C, lower high speed homogenization 5-10min is stirred, stirring cooling, 50 DEG C of addition residue D phases and E phase (ceramide, remaining guarantor are continued
Wet component, essence, Phenoxyethanol), it stirs evenly, controls cooling rate, slowly cool down, continue 30min, 35 DEG C of stoppings are stirred,
Vacuum defoaming, preparation are completed.
Comparative example 1-2
According to the parts by weight of each component of comparative example 1-2 in the following table 1,5, and according to method identical with embodiment 1-6
Essence is newborn before the adornment of comparative example 1-2 is prepared.
In embodiment and comparative example, the preparation method of functional composite granule the following steps are included:
(1) the dry hydroxyapatite of preparation, zinc oxide.
It is hydroxyapatite, zinc oxide is 4 hours dry in 105 DEG C in drier respectively, wherein hydroxyapatite adds
Entering amount is 60g；The additional amount of zinc oxide is 38g.
(2) hydroxyapatite and zinc oxide form compound.
The hydroxyapatite and zinc oxide that prepare in step (1) are put into the container of belt stirrer, in container together
It is mixed by high-speed stirred, the complex solid powder of hydroxyapatite and zinc oxide composition is thus made.
(3) solid powder is coated using triethoxy octyl silane
Triethoxy octyl silane 5g is sprayed on the complex solid powder of step 2) acquisition, is mixed and divided later
It dissipates 10 minutes, obtains functional composite granule.
Table 1
10 qualified volunteers of selection are screened by volunteer to take one's test as subject.The instrument used is Germany
CK company skin oil and fat moisture content pH value SSC3 tester, grease are tested using universally acknowledged SEBUMETER method, it is
Based on photometer principle, after a kind of special delustring adhesive tape of 0.1mm thickness absorbs grease on human skin, a kind of half just will become
Transparent adhesive tape, its light transmission capacity will change, and the grease of absorption is more, and light transmission capacity will be bigger, can thus survey
Measure the content of skin oil and fat.After testing raw value, subject cleans face using benchmark mildy wash, tests after drying initial
Value uses test sample later, tests the skin oil and fat content of 3 hours, 6 hours, and concrete outcome is as shown in table 2 below.
Table 2
As can be seen from Table 2, the skin oil and fat of sample application area and blank district 3h, 6h after sample use,
1 value added of embodiment is smaller than blank district and comparative example 1, there is significant difference, illustrates that the oil-control ability of embodiment 1 compares
By force, it can be effectively controlled skin and secrete a large amount of grease.
Table 3
Selection 10 or more qualified volunteers are screened by volunteer to take one's test as subject.It uses within 4 days respectively
After embodiment 2-4 and the sample of comparative example 1, identical foundation emulsion is coated, is kept under same humidity temperature, it is small at 6 daily
Shi Hou observes it respectively and holds adornment effect, and scores it.Wherein, 10 points of, concrete outcome such as the following table 4 best for integrity degree
It is shown.
Table 4
| Volunteer | Embodiment 2 | Comparative example 1 | Embodiment 3 | Embodiment 4 |
| 1 | 9 | 6.8 | 7.8 | 8.5 |
| 2 | 9 | 6.9 | 8.0 | 9.0 |
| 3 | 9 | 6.5 | 8.1 | 8.6 |
| 4 | 9 | 6.7 | 7.9 | 8.7 |
| 5 | 9 | 7.0 | 7.8 | 8.5 |
| 6 | 9 | 7.2 | 7.5 | 8.0 |
| 7 | 10 | 6 | 7.8 | 8.2 |
| 8 | 9 | 7.3 | 7.6 | 8.6 |
| 9 | 9 | 7.2 | 7.9 | 8.2 |
| 10 | 9 | 7.6 | 7.9 | 8.1 |
As can be seen from Table 4, the present invention using after essence cream before the adornment of embodiment 2 to hold adornment effect more preferable.And embodiment 3
It is slightly lower with the functional composite granule content of embodiment 4, it holds adornment effect and is slightly worse than embodiment 2.And comparative example 1 is due to without active
Energy property composite granule, it is worst to hold adornment effect.
Table 5
Selection 10 or more qualified volunteers are screened by volunteer to take one's test as subject.Subject uses base
Quasi- mildy wash cleaning face, using moisture of skin tester, tests initial value after drying, use test sample later, and test 6 is small
When, the skin epidermis moisture at each position is tested with moisture of skin tester, wherein numerical value is higher, indicates that its performance of keeping humidity is better.
Skin moisture content the results are shown in Table shown in 6.
Table 6
As shown in 6 tables, data are shown after tested, and the moisture content value of 10 female volunteers is using embodiment 4-6's
Before adornment after essence cream, hence it is evident that higher than 2 moisture content of comparative example, it was demonstrated that essence cream has good moisturizing before the adornment of embodiment 4-6
Degree.
Since the content of the ceramide of embodiment 4 is higher, moisture content is higher than embodiment 5 and embodiment 6.
The above embodiment of the present invention be only to clearly illustrate example of the present invention, and not be to the present invention
Embodiment restriction.For those of ordinary skill in the art, it can also make on the basis of the above description
Other various forms of variations or variation.There is no necessity and possibility to exhaust all the enbodiments.It is all of the invention
Made any modifications, equivalent replacements, and improvements etc., should be included in the protection of the claims in the present invention within spirit and principle
Within the scope of.
Claims (10)
1. essence cream before a kind of adornment, which is characterized in that including following components:
Emulsifier: 1-5 parts by weight, preferably 2-4.5 parts by weight；
Emollient: 3-15 parts by weight, preferably 5-14 parts by weight；
Moisturizing component: 5-15 parts by weight, preferably 7-12 parts by weight；
Oil-control ingredient: 1.0-5.0 parts by weight, preferably 1.5-4.5 parts by weight；
Ceramide: 1.0-5.0 parts by weight, preferably 2.0-4.5 parts by weight.
2. essence cream before adornment according to claim 1, which is characterized in that the emulsifier includes primary emulsion and assistant for emulsifying agent,
Wherein,
The primary emulsion include C20-22 alkyl phosphate (and) C20-22 fatty alcohol；
The assistant for emulsifying agent include cetostearyl alcohol (and) cocoyl glucoside.
3. essence cream before adornment according to claim 2, which is characterized in that the additional amount of the primary emulsion is 0.5-3.0
Parts by weight, the additional amount of the assistant for emulsifying agent are 0.5-2.0 parts by weight.
4. essence cream before adornment according to claim 1-3, which is characterized in that the emollient includes that carbonic acid two is pungent
Ester, cetanol ethylhexyl, isononyl isononanoate, octyl dodecanol, dimethicone and dimethyl silicone polymer/poly- diformazan
The combination of one or more of radical siloxane cross-linked polymer.
5. before adornment according to claim 1-4 essence cream, which is characterized in that the moisturizing component include glycerol,
Butanediol, Sodium Hyaluronate, oat beta-glucan, glycerin polyether -26, in Xylitol-based glucoside/anhydro xylitol/xylitol
A combination of one or more.
6. essence cream before adornment according to claim 1-5, which is characterized in that the oil-control ingredient includes functionality
Composite granule, the functionality composite granule includes hydroxyapatite and zinc oxide；Preferably, the hydroxyapatite with it is described
The mass ratio of zinc oxide is 0.25~25:1.
7. essence cream before adornment according to claim 1-6, which is characterized in that the system of the functionality composite granule
Preparation Method is included the steps that using silane cladding hydroxyapatite and zinc oxide.
8. essence cream before adornment according to claim 1-7, which is characterized in that the ceramide includes neural acyl
The combination of one or more of amine 1, Cer NP, Cer AP-II.
9. essence cream before adornment according to claim 1-8, which is characterized in that essence cream further includes increasing before the adornment
Thick dose, the combination of pH adjusting agent, essence, one or more of preservative.
10. the preparation method of essence cream before a kind of -9 described in any item adornments according to claim 1, which is characterized in that including inciting somebody to action
Before the adornment the step of each component mixing of essence cream.
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| CN116407483A (en) * | 2023-06-06 | 2023-07-11 | 广东时尚女孩生物科技有限公司 | Formula and preparation method of oil-control moisturizing facial cleanser |
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