CN108578253A - A kind of moisturizing cream and preparation method thereof with good liquid crystal structure - Google Patents
A kind of moisturizing cream and preparation method thereof with good liquid crystal structure Download PDFInfo
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- CN108578253A CN108578253A CN201810261628.5A CN201810261628A CN108578253A CN 108578253 A CN108578253 A CN 108578253A CN 201810261628 A CN201810261628 A CN 201810261628A CN 108578253 A CN108578253 A CN 108578253A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0295—Liquid crystals
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The present invention provides a kind of moisturizing cream with good liquid crystal structure, and by weight percentage, the moisturizing cream includes mainly following components：Alkyl-glucoside 0.5 5%, higher aliphatic 1 8%, polyglycerol ester 0.5 3%, grease 10 40%, macromolecule thickener 0.1 5%, moisturizer 0.1 10%, surplus is water.The present invention is reasonably combined by alkyl glycosides and polyglycerol ester, higher aliphatic, adjusts interface Packing parameter, can form the complete layered liquid crystal structure of more homogeneous and bright, and is formed by liquid crystal structure stabilization.The moisturizing cream of the present invention not only has excellent moisture-keeping functions, but also can be substantially reduced percutaneous water loss rate, has excellent effect on keeping moisture of skin.
Description
Technical field
The invention belongs to cosmetic fields, and in particular to a kind of moisturizing cream and its preparation side with good liquid crystal structure
Method.
Background technology
Liquid crystal type skin care item are the novel skin care item being concerned in recent years.Because layered liquid crystal has oil/liquid crystal/water
Structure, it is closely similar with the structure of human skin barrier, can be lotion when it is stable in the presence of in oil-in-water type facial treatment milk
The effects that providing efficient moisture-retention and slow-release, it is played to can help to specialized function product and medicine adornment skin care item
The nursing skin makeup of bigger acts on.
Liquid crystal emulsifier mainly has six major class, is phospholipid, glucose glycoside, sucrose ester, phosphoric acid ester, olive respectively
Esters and stearoyl class etc..As the glucose glycoside emulsifier of one of liquid crystal emulsifier, due to its plant origin and excellent
Skin sense and skin compatibility, compare paid close attention to by people in recent years.But when it is used alone as emulsifier, emulsifying capacity compared with
Low, the liquid crystal structure of generation is larger by recipe-imposed, and the factor for influencing Formation of liquid crystals is more.Therefore, arbitrarily raw material is selected to carry out
There are layered liquid crystals to form a series of problems, such as probability is small, shape is imperfect, quantity is few for the preparation of product, to sorting limitation compared with
Greatly.Currently, many products using glucose glycoside liquid crystal emulsifier on the market, rarer to observe with relatively good liquid crystal
Structure.
Therefore, a kind of using glucose glycoside liquid crystal emulsifier there is an urgent need for developing, and the moisturizing cream with good liquid crystal structure
Frost.
Invention content
The technical problem to be solved by the present invention is to deficiencies existing for the above-mentioned prior art, provide a kind of with good
The moisturizing cream and the preparation method and application thereof of good liquid crystal structure, which not only has good liquid crystal structure, but also has
There are excellent moisture-keeping functions, stability good.
To achieve the goals above, the present invention uses technical solution below：
A kind of moisturizing cream with good liquid crystal structure, by weight percentage, the moisturizing cream mainly include with
Lower component：Alkyl-glucoside 0.5-5%, higher aliphatic 1-8%, polyglycerol ester 0.5-3%, grease 10-40%, macromolecule
Thickener 0.1-5%, moisturizer 0.1-10%, surplus are water.
Preferably, a kind of moisturizing cream with good liquid crystal structure, by weight percentage, the moisturizing cream is main
Including following components：Alkyl-glucoside 0.5-3%, higher aliphatic 2-6%, polyglycerol ester 0.5-2%, grease 10-30%,
Macromolecule thickener 0.1-2%, moisturizer 3-10%, surplus are water.
Preferably, the alkyl-glucoside is C12-C22 glucosides.
Particularly preferred, the alkyl glycosides is C14-C20 alkyl glycosides.
Most preferably, the alkyl glycosides is C16-C18 alkyl glycosides.
Preferably, in the higher aliphatic selection cetostearyl alcohol, behenyl alcohols, stearyl alcohol, cetanol, cetostearyl alcohol
One or more kinds of mixing.
Particularly preferred, the higher aliphatic is cetostearyl alcohol.
Preferably, the polyglycerol ester is -2 stearate of polyglycereol.
Preferably, the moisturizing grease is selected from one or both of vegetable fat, Synthetic Oil, animal fat and silicone oil
The above mixing.
Particularly preferred, the moisturizing grease is saualane, jojoba oil, dimethyl silicone polymer and isononyl isononanoate
Mixture.
Preferably, it is total to be selected from hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate for the water soluble polymer thickener
One or both of polymers (EMT-10), polyacrylate cross-linked polymer -6, Sodium Polyacrylate, polyacrylic polymer
The above mixing.
Particularly preferred, the water soluble polymer thickener is hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate
Copolymer.
Preferably, the moisturizer is selected from glycerine, 1,3-PD, 1,3-BDO, Sodium Hyaluronate, polysaccharide moisturizing
One or more of agent mixes.
Particularly preferred, the moisturizer is the mixture of glycerine, 1,3-BDO and Sodium Hyaluronate.
Preferably, a kind of moisturizing cream with good liquid crystal structure, by weight percentage, the moisturizing cream is also wrapped
Containing following components：Auxiliary agent 0.1-5%, the auxiliary agent are that one or more of pigment, preservative, essence, chelating agent are mixed
Close object.
The present invention also provides the preparation methods of above-mentioned moisturizing cream, and this approach includes the following steps：
S1：Water intaking, moisturizer and water soluble polymer thickener, mixing are warming up to 80 DEG C, and insulated and stirred 20 minutes is made
Obtain water phase；
S2：Alkyl-glucoside, higher aliphatic, polyglycerol ester and moisturizing grease are taken, is mixed, is warming up to 80 DEG C, heat preservation
Oil phase is made until being completely dissolved in stirring 15 minutes；
S3：The oil phase is added to the aqueous phase, and under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes is cooling, is cooled to 45 DEG C,
Auxiliary material is added, after stirring 30 minutes, inspection discharges after qualified.
Beneficial effects of the present invention：
1, the moisturizing cream provided by the invention with good liquid crystal structure, by alkyl glycosides and polyglycerol ester, advanced
Fatty alcohol is reasonably combined, adjusts interface Packing parameter, can form the complete layered liquid crystal structure of more homogeneous and bright, and formed
Liquid crystal structure stablize.
2, moisturizing cream of the invention has good liquid crystal structure, contains combination in the layered liquid crystal that skin surface is formed
Water can provide skin more moisture, have excellent moisture-keeping functions；On the other hand, being formed in skin has water retaining function
Liquid crystal film, percutaneous water loss rate can be substantially reduced, keep moisture of skin on have excellent effect.
Description of the drawings
Fig. 1 is the liquid crystal structure figure of the moisturizing cream A prepared by the embodiment of the present invention 1；
Fig. 2 is the liquid crystal structure figure of the moisturizing cream B prepared by the embodiment of the present invention 2；
Fig. 3 is the liquid crystal structure figure of the moisturizing cream C prepared by the embodiment of the present invention 3；
Fig. 4 is the liquid crystal structure figure of the moisturizing cream D prepared by comparative example 1 of the present invention；
Fig. 5 is the liquid crystal structure figure of the moisturizing cream E prepared by comparative example 2 of the present invention；
Fig. 6 is the liquid crystal structure figure of the moisturizing cream F prepared by comparative example 3 of the present invention；
Fig. 7 is the liquid crystal structure after 2 moisturizing cream B of the embodiment of the present invention is placed 3 months under the conditions of temperature is -18 DEG C
Figure；
Fig. 8 is the liquid crystal structure figure after 2 moisturizing cream B of the embodiment of the present invention is placed 3 months under normal temperature condition；
Fig. 9 is the liquid crystal structure figure after 2 moisturizing cream B of the embodiment of the present invention is placed 3 months under the conditions of temperature is 40 DEG C；
Figure 10 is the liquid crystal structure after 3 moisturizing cream F of comparative example of the present invention is placed 3 months under the conditions of temperature is -18 DEG C
Figure；
Figure 11 is the liquid crystal structure figure after 3 moisturizing cream F of comparative example of the present invention is placed 3 months under normal temperature condition；
Figure 12 is the liquid crystal structure after 3 moisturizing cream F of comparative example of the present invention is placed 3 months under the conditions of temperature is 40 DEG C
Figure.
Specific implementation mode
Technical scheme of the present invention is described further with reference to embodiment and comparative example and effete test embodiment：
Various reagents used in following embodiment are commercial goods, are that can buy to obtain by commercial sources.
Embodiment 1-3
The moisturizing cream A-C with good liquid crystal structure of embodiment 1-3 is prepared according to table 1.
Table 1 has the moisturizing cream A-C of good liquid crystal structure
The preparation method of the above-mentioned moisturizing cream A-C with good liquid crystal structure includes the following steps：
S1：Water intaking, moisturizer and water soluble polymer thickener, mixing are warming up to 80 DEG C, and insulated and stirred 20 minutes is made
Obtain water phase；
S2：Alkyl-glucoside, higher aliphatic, polyglycerol ester and moisturizing grease are taken, is mixed, is warming up to 80 DEG C, heat preservation
Oil phase is made until being completely dissolved in stirring 15 minutes；
S3：The oil phase is added to the aqueous phase, and under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes is cooling, is cooled to 45 DEG C,
Auxiliary material is added, after stirring 30 minutes, inspection discharges after qualified.
Comparative example 1-3
The moisturizing cream D-F of comparative example 1-3 is prepared according to table 2.
2 moisturizing cream D-F of table
The preparation method of above-mentioned moisturizing cream D-F includes the following steps：
S1：Water intaking, moisturizer and water soluble polymer thickener, mixing are warming up to 80 DEG C, and insulated and stirred 20 minutes is made
Obtain water phase；
S2：Alkyl-glucoside, higher aliphatic, polyglycerol ester and moisturizing grease are taken, is mixed, is warming up to 80 DEG C, heat preservation
Oil phase is made until being completely dissolved in stirring 15 minutes；
S3：The oil phase is added to the aqueous phase, and under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes is cooling, is cooled to 45 DEG C,
Auxiliary material is added, after stirring 30 minutes, inspection discharges after qualified.
Comparative example 4-6
Comparative example 4-6 is that corresponding embodiment 1-3 destroys the moisturizing cream G-I after liquid crystal structure.
Using the formula of embodiment 1-3, the moisturizing cream G- after destroying liquid crystal structure is prepared by following preparation method
I：
S1：Water intaking, moisturizer and water soluble polymer thickener, mixing are warming up to 80 DEG C, and insulated and stirred 20 minutes is made
Obtain water phase；
S2：Alkyl-glucoside, higher aliphatic, polyglycerol ester and moisturizing grease are taken, is mixed, is warming up to 80 DEG C, heat preservation
Oil phase is made until being completely dissolved in stirring 15 minutes；
S3：The oil phase is added to the aqueous phase, and under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes is cooling, is cooled to 45 DEG C,
Auxiliary material is added, after stirring 30 minutes；
S4：High speed homogenization again, under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes.
Step S3, in cooling, the liquid crystal structure of moisturizing creams has been formed, and high speed homogenization can destroy the liquid of formation again
Crystal structure makes it not have liquid crystal structure.
Comparative example 7-9
With the commercially available of the 7-9 as a comparison case of 3 moisturizing creams in before past 5 years domestic market sales 10 moisturizing cream
Moisturizing cream J-L.
Effect example 1
Liquid crystal structure is evaluated
Experimental method：It is prepared by the moisturizing cream A-C with good liquid crystal structure, comparative example 1-3 prepared by Example 1-3
Moisturizing cream D-F be placed on glass slide, flattened with coverslip, then observed under the microscope.First under microscopical light field
Observation, after emulsion particle capable of can be clearly seen, then observes mesomorphic state in the state of 400 times of polarised lights.Liquid crystal structure figure
See Fig. 1-6.
From Fig. 1-6 as can be seen that the moisturizing cream A-C with good liquid crystal structure prepared by embodiment 1-3 all has greatly
The bright uniformly complete liquid crystal structure of amount, lotion appearance are fine and smooth；And moisturizing cream D-F prepared by comparative example 1-3 is not observed
To the liquid crystal structure of apparent big quantity.Illustrate that the moisturizing cream with good liquid crystal structure of the present invention is forming liquid crystal structure
Aspect has the effect of excellent.
Effect example 2
Liquid crystal structure long term stability tests
Due to the moisturizing cream B with good liquid crystal structure prepared by embodiment 2 liquid crystal structure in embodiment most
Good, the effect liquid crystal relative contrast example 1,2 of the moisturizing cream F prepared by comparative example 3 will be got well, therefore selection example 2 is with good
The moisturizing cream B of the good liquid crystal structure and moisturizing cream F of comparative example 3 does the evaluation of liquid crystal structure long-time stability.
Experimental method：Prepared by moisturizing cream B with good liquid crystal structure and comparative example 3 prepared by Example 2
Moisturizing cream F respectively under conditions of -18 DEG C, room temperature, 45 DEG C, place 3 months, take sample to be placed on glass slide, with lid glass
Piece flattens, and then observes under the microscope.First observed under microscopical light field, after emulsion particle capable of can be clearly seen, then
Mesomorphic state is observed in the state of 400 times of polarised lights.Liquid crystal structure figure is shown in Fig. 7-12.
From Fig. 7-12 as can be seen that the moisturizing cream B with good liquid crystal structure prepared by embodiment 2-18 DEG C, it is normal
Temperature, after placing 3 months under the conditions of 45 DEG C, liquid crystal quantity does not significantly reduce, and all has a large amount of bright uniformly complete liquid crystal knots
Structure, lotion appearance are fine and smooth.After moisturizing cream F prepared by comparative example 3 is placed 3 months under the conditions of -18 DEG C, 45 DEG C, liquid crystal knot
Structure quantity significantly reduces.Illustrate that the formed liquid crystal structure stability of the moisturizing cream with good liquid crystal structure of the present invention is excellent
It is different.
Effect example 3
Moistening effect is tested
Test sample：The moisturizing cream A-C with good liquid crystal structure, comparative example 4-6 prepared by embodiment 1-3 are destroyed
The commercially available moisturizing cream J-L of moisturizing cream G-I, comparative example 7-9 after liquid crystal structure.
Test equipment：Dual MPA580 skinanalysis apparatus
Test position：Human body Medial upper arm
Test method：30 people of volunteer of skin health, no skin disease and allergies is randomly selected, and chooses volunteer's
Medial upper arm area proper area is test section.Allow volunteer in room temperature (25 ± 2) DEG C, relative humidity (50 ± 2) % rings before test
It quiets down in border, tested region is cleaned by cleaning products, then naturally dry 15min after uniformly being wiped with alcohol.It will be tested
Region division is 9 pieces (respectively taking 3cm × 3cm), and every piece takes 5 points to measure, and is averaged as tested area data result.
It first measures the skin Corneometer value (moisturizing numerical value) before non-spread product and obtains blank value.After carry out product
It smears, by tested material with 1.25 μ L/cm2Smearing density be applied to each tested region, gently pat to absorb after, surveyed with skin
Examination instrument measures the skin Corneometer value (moisturizing numerical value) using rear 1h, 3h and 6h respectively, passes through its guarantor of data evaluation
Wet effect.Test result is shown in Table 3.
3 moistening effect test result of table
| Sample | Blank | Use rear 1h | Use rear 3h | Use rear 6h |
| Embodiment 1 | 23.3 | 48.4 | 45.1 | 42.7 |
| Embodiment 2 | 23.1 | 47.3 | 44.8 | 41.4 |
| Embodiment 3 | 22.2 | 48.1 | 44.5 | 41.8 |
| Comparative example 4 | 22.0 | 43.1 | 39.4 | 35.4 |
| Comparative example 5 | 22.8 | 42.9 | 39.8 | 35.8 |
| Comparative example 6 | 23.1 | 42.4 | 38.7 | 35.2 |
| Comparative example 7 | 23.7 | 40.7 | 37.7 | 34.5 |
| Comparative example 8 | 21.8 | 43.6 | 39.4 | 35.9 |
| Comparative example 9 | 22.5 | 38.6 | 35.1 | 32.7 |
From table 3 it can be seen that recipient site, which has smeared embodiment 1-3, has the moisturizing cream A-C 1h of good liquid crystal structure
Moisturizing cream of the moisture of skin obviously higher than comparative example 4-9 afterwards.After using 3h and 6h, embodiment 1-3 has been smeared with good
The moisture of skin of the moisturizing cream A-C of good liquid crystal structure is significantly higher than the moisturizing cream of comparative example 4-9.Offer of the present invention is provided
The layered liquid crystal for having the moisturizing cream of good liquid crystal structure that can be formed in skin surface contain in conjunction with water, provided to skin more
Moisture, possess superior moistening effect.
Effect example 4
Percutaneous water loss degree test
Test sample：The moisturizing cream A-C with good liquid crystal structure, comparative example 4-6 prepared by embodiment 1-3 are destroyed
The commercially available moisturizing cream J-L of moisturizing cream G-I, comparative example 7-9 after liquid crystal structure.
Test equipment：Dual MPA580 skinanalysis apparatus
Test position：Human body Medial upper arm
Test method：Skin health, several people of volunteer of no skin disease and allergies are randomly selected, and choose volunteer
Medial upper arm area proper area be test section.Allow volunteer in room temperature (25 ± 2) DEG C, relative humidity (50 ± 2) % before test
It quiets down in environment, tested region is cleaned by cleaning products, then naturally dry 15min after uniformly being wiped with alcohol.It will be by
It is 4 pieces (respectively taking 3cm × 3cm) to try region division, first measures (the percutaneous moisture streams of the Tewameter value before non-spread product
Mistake degree) obtain blank value.Product smearing is carried out afterwards, tested material is applied to the smearing density of 1.25 μ L/cm2 each tested
Region, is gently patted to after absorbing, and measures the skin Tewameter using rear 1h, 3h and 6h respectively with skinanalysis apparatus
Value (percutaneous water loss degree), its percutaneous water loss situation by data evaluation.Test result is shown in Table 4.
4 percutaneous water loss degree test result of table
From table 4, it can be seen that being compared with comparative example 4-9 moisturizing creams are used, recipient site, which has smeared embodiment 1-3, to be had
It is reduced obviously through skin water loss degree after the moisturizing cream A-C 1h of good liquid crystal structure；3h and 6h is being used, although through the severe edema due to hypofunction of the spleen
Shunting mistake degree increases, but percutaneous water loss degree is remained less than using comparative example 4-9 moisturizing creams.Therefore, illustrate this hair
The moisturizing cream with good liquid crystal structure of bright offer can form the liquid crystal film with water retaining function in skin, hence it is evident that reduce warp
Skin water loss rate has excellent effect on keeping moisture of skin.
The above described is only a preferred embodiment of the present invention, limitation in any form not is done to the present invention, therefore
All contents without departing from technical solution of the present invention, it is made to the above embodiment according to the technical essence of the invention any simply to repair
Change, equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (10)
1. a kind of moisturizing cream with good liquid crystal structure, which is characterized in that by weight percentage, the moisturizing cream master
It to include following components：Alkyl-glucoside 0.5-5%, higher aliphatic 1-8%, polyglycerol ester 0.5-3%, moisturizing grease
10-35%, water soluble polymer thickener 0.1-5%, moisturizer 0.1-10%, auxiliary material 0.1-3%, surplus is water.
2. moisturizing cream according to claim 1, which is characterized in that by weight percentage, the moisturizing cream is main
Including following components：Alkyl-glucoside 0.5-3%, higher aliphatic 2-6%, polyglycerol ester 0.5-2%, moisturizing grease 10-
30%, macromolecule thickener 0.1-2%, moisturizer 3-10%, auxiliary material 0.1-2%, surplus are water.
3. moisturizing cream according to claim 1 or 2, it is characterised in that：The alkyl-glucoside is C12-C22 grapes
Glucosides.
4. moisturizing cream according to claim 3, it is characterised in that：The alkyl glycosides is C14-C20 alkyl glycosides.
5. moisturizing cream according to claim 1 or 2, it is characterised in that：The higher aliphatic selection cetostearyl alcohol,
One or more of behenyl alcohol, stearyl alcohol, cetanol, cetostearyl alcohol mix；The polyglycerol ester is polyglycereol -2
Stearate.
6. moisturizing cream according to claim 1 or 2, it is characterised in that：The moisturizing grease is selected from vegetable fat, synthesis
One or more of grease, animal fat and silicone oil mix.
7. moisturizing cream according to claim 1 or 2, it is characterised in that：The water soluble polymer thickener is selected from third
Olefin(e) acid hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers, polyacrylate cross-linked polymer -6, Sodium Polyacrylate, poly- third
One or more of alkene acids polymers mix.
8. moisturizing cream according to claim 1 or 2, it is characterised in that：The moisturizer is selected from glycerine, 1,3- the third two
One or more of alcohol, 1,3-BDO, Sodium Hyaluronate, polysaccharide moisturizer mix.
9. moisturizing cream according to claim 1 or 2, which is characterized in that by weight percentage, the moisturizing cream is also
Including following components：Auxiliary agent 0.1-5%, the auxiliary agent are one or more of pigment, preservative, essence, chelating agent
Mixture.
10. the preparation method of moisturizing cream as claimed in claim 1 or 2, which is characterized in that include the following steps：
S1：Water intaking, moisturizer and water soluble polymer thickener, mixing are warming up to 80 DEG C, and water is made in insulated and stirred 20 minutes
Phase；
S2：Alkyl-glucoside, higher aliphatic, polyglycerol ester and moisturizing grease are taken, mixes, is warming up to 80 DEG C, insulated and stirred
15 minutes, until being completely dissolved, oil phase is made；
S3：The oil phase is added to the aqueous phase, and under the conditions of rotating speed is 3000r/min, homogeneous 10 minutes is cooling, is cooled to 45 DEG C, is added
Auxiliary material, after stirring 30 minutes, inspection discharges after qualified.
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| CN109276484A (en) * | 2018-11-20 | 2019-01-29 | 浙江大学华南工业技术研究院 | A kind of mineral clay mask with layer structure |
| CN109288763A (en) * | 2018-12-05 | 2019-02-01 | 广州睿森生物科技有限公司 | A kind of multi-functional face cleaning cream and preparation method thereof |
| CN109646327A (en) * | 2019-01-07 | 2019-04-19 | 广州葆妍生物科技有限公司 | A kind of moisturiser and preparation method thereof with liquid crystal structure |
| CN110974742A (en) * | 2019-12-04 | 2020-04-10 | 威莱(广州)日用品有限公司 | Moisturizing and repairing hand cream with liquid crystal structure and preparation method thereof |
| CN111297699A (en) * | 2020-01-14 | 2020-06-19 | 名臣健康用品股份有限公司 | Moisturizing body lotion with good liquid crystal structure and preparation method thereof |
| CN111529464A (en) * | 2020-05-20 | 2020-08-14 | 广东创美抗衰老研究有限公司 | Moisturizing cream suitable for diabetic patients |
| CN113244116A (en) * | 2021-04-27 | 2021-08-13 | 广州立白企业集团有限公司 | Structured compositions and uses thereof |
| CN114712271A (en) * | 2022-03-30 | 2022-07-08 | 广州优肌源化妆品有限公司 | Liquid crystal type oil-in-water matte composition, cream and preparation method thereof |
| CN115778835A (en) * | 2022-12-29 | 2023-03-14 | 羽楠(广州)化妆品有限公司 | Polyglycerol ester moisturizer and preparation method thereof |
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Application publication date: 20180928 |