CN114306204A - Pure natural spirulina polypeptide mask and preparation method thereof - Google Patents
Pure natural spirulina polypeptide mask and preparation method thereof Download PDFInfo
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- CN114306204A CN114306204A CN202210004514.9A CN202210004514A CN114306204A CN 114306204 A CN114306204 A CN 114306204A CN 202210004514 A CN202210004514 A CN 202210004514A CN 114306204 A CN114306204 A CN 114306204A
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Abstract
A pure natural spirulina polypeptide mask comprises the following components in percentage by mass: 10-30% of spirulina polypeptide liquid, 5-25% of polyvinyl alcohol, 5-25% of glycerol, 2-5% of 1, 2-propylene glycol, 2-5% of coconut oil, 0.1-0.3% of xanthan gum and 0.1-0.3% of jasmine tea essence, wherein when the concentration of the spirulina facial mask essence is 0.4-1g/L, the DPPH free radical scavenging rate is 57.52-66.36%, and when the concentration of the spirulina facial mask essence is 1.5-3g/L, the tyrosinase inhibition rate is 46.5-60.3%.
Description
Technical Field
The invention relates to the technical field of mask preparation, in particular to a pure natural spirulina polypeptide mask and a preparation method thereof.
Background
The skin is a protective organ of human body and can prevent bacterial invasion and water loss. If the skin is damaged, the skin becomes dry and sensitive, the immunity is reduced, black spots and wrinkles easily grow, so that the skin moisture is locked, the integrity of the skin barrier is maintained, and the good state of the skin is maintained.
The mask is widely used as a carrier of facial beauty care products, can help facial skin temporarily isolate outside air and pollution, dilate pores of the skin, promote secretion and metabolism of sweat glands, increase oxygen content of the skin, permeate moisture in the mask into horny layers of the skin epidermis, soften the skin and increase elasticity.
The existing mask products on the market are various in types and different in quality, but most of the existing mask products contain chemical components, although the curative effect is quick in a short period, the toxic and side effects are obvious, even some masks contain hormone components, the irritation to the skin is large after the mask products are used, and the harm such as red and swollen facial skin, desquamation and the like is often caused. Therefore, a plurality of natural non-irritant facial masks appear in the market, and some facial masks have the effects of whitening and beautifying by directly extracting active ingredients in natural plants, such as pearl, angelica dahurica and other Chinese herbal medicine extracts. And the other part of the skin-care product has certain antioxidant effect by extracting active substances, such as polysaccharide, polypeptide, phenolic compounds and the like, in the active substances.
The polypeptide can improve the regeneration capability of skin tissues, so that the polypeptide can quickly penetrate into the epidermis and be absorbed by the dermis layer to play a role in deep repair. The skin care product can quickly supplement nutrients, directly activate and nourish skin cells, effectively promote skin metabolism, improve skin texture, and has the effects of repairing wrinkles, whitening and moisturizing. The natural bioactive peptide is a natural resource treasure house for screening medicines, has the characteristics of high efficiency, low toxicity, no pollution and the like, and has wide application prospects in the industries of food and cosmetics.
The spirulina is used as a natural and reliable antioxidant source, the protein content can reach 60% -70% of the dry weight, and the pure natural spirulina polypeptide mask prepared according to a certain proportion and a certain process flow can achieve the effects of resisting oxidation and preventing aging of skin, can obviously improve the luster and the elasticity of the skin, can be directly formed into a film, is very easy to clean, and avoids the pollution of a mask carrier to the environment. Has effects in improving skin elasticity, moistening skin, removing wrinkle, and removing speckle; can promote skin metabolism and reduce scar; meanwhile, the skin care liquid has good permeability, can play a role in nourishing and caring the surface and deep layers of the skin, is very safe to use, and has no stimulation and sensitization on the skin.
At present, the research on the spirulina polypeptide facial mask is less, (such as CN201810093899.4, CN201510295166.5, CN201310244911.4, CN201310249597.9, CN99117822.X, CN96107835.9 and the like) and most of the spirulina polypeptide facial mask is not subjected to enzymolysis treatment, so that effective components cannot penetrate deeply into the skin surface layer to supplement nutrients rapidly and are not easy to absorb. The method is characterized in that a spirulina industrial garden is built in inner Mongolia Eyokeqi from 2009 to the present, the spirulina industrial garden becomes one of the largest spirulina culture bases in China, annual spirulina powder is 5000 tons, and currently, annual spirulina series products are 4000 tons, but related deep processing products are few and the additional value is low, so that the spirulina polypeptide facial mask can be added into a facial mask, deep processing products can be obtained, the additional value is improved, an industrial chain is extended, and meanwhile, the developed pure natural spirulina polypeptide facial mask can also improve the skin problem.
Based on the above situation, the invention develops a pure natural spirulina polypeptide mask and a preparation method thereof.
Disclosure of Invention
In order to solve the technical problems in the background art, the invention provides a pure natural spirulina polypeptide facial mask essence which comprises the following components in percentage by mass: 10-30% of spirulina polypeptide liquid, 5-25% of polyvinyl alcohol, 5-25% of glycerol, 2-5% of 1, 2-propylene glycol, 2-5% of coconut oil, 0.1-0.3% of xanthan gum, 0.1-0.3% of jasmine tea essence and water for supplementing to 100%.
In one embodiment, the preparation method of the spirulina polypeptide liquid comprises the following steps: and (2) breaking the walls of the spirulina by adopting a method combining repeated freezing and melting and colloid grinding for wall breaking, performing enzymolysis on the spirulina liquid subjected to wall breaking treatment, selecting neutral protease, adding 0.1-0.3% of enzyme based on the weight of a substrate, performing centrifugation for 20-30min after 1-3 hours of enzymolysis, and obtaining the spirulina polypeptide liquid with the content of 10-30%.
In one embodiment, a preparation method of pure natural spirulina polypeptide facial mask essence is disclosed, which comprises the following steps:
(a) preparing deionized water in a beaker;
(b) accurately adding polyvinyl alcohol, coconut oil and 1, 2-propylene glycol, heating while stirring, and blending to be uniform;
(c) putting deionized water in a beaker into a water bath kettle to heat to 80 ℃;
(d) adding xanthan gum, stirring thoroughly until completely dissolved, then cooling to 40 deg.C, adding glycerol, and stirring to obtain component A;
(e) adding the spirulina polypeptide liquid after enzymolysis into the other beaker to obtain a component B;
(f) mixing the component A and the component B, mixing the materials in the beaker, dispersing uniformly, adding jasmine tea essence, standing at room temperature, and emulsifying for 8 min.
In a specific embodiment, the patch type facial mask is made of pure cotton fiber facial mask paper 270mm × 203mm, and is packaged into facial mask bags, each of which is filled with 8-10g of spirulina facial mask essence according to claim 1, and the facial mask bags are sealed after filling.
In one embodiment, the use of a mask for the preparation of a cosmetic for preventing skin aging; and/or, the application of the facial mask in preparing the cosmetic for whitening skin, when the concentration of the spirulina facial mask essence is 0.4-1g/L, the DPPH free radical clearance rate is 57.52-66.36%, and when the concentration of the spirulina facial mask essence is 1.5-3g/L, the tyrosinase inhibition rate is 46.5-60.3%.
The mask has the following technical effects:
(1) anti-aging: has antioxidant effect and free radical scavenging activity in vitro and in vivo, and the DPPH free radical scavenging rate of the essence of spirulina facial mask can reach 57.52-66.36%. Can effectively delay skin aging. Can promote the formation of collagen, make the skin more white and rich in elasticity, so that the human body can continuously supplement the special anti-aging effect.
(2) Whitening: the tyrosinase inhibition rate of the spirulina facial mask essence is 46.5-60.3%. The pure natural spirulina facial mask prepared by the experiment can inhibit the activity of tyrosinase and prevent the generation of melanin so as to achieve the whitening effect.
(3) And (3) moisturizing: the invention has higher moisture retention, the water loss rate is between 3.42 +/-0.12 percent, the invention is easy to absorb, fine and glossy, improves the metabolism of the skin and delays the skin aging.
(4) Pure natural: the pure natural facial mask has stable property and good temperature stability, does not contain substances such as ethanol, preservatives and the like, has pH of 6.3-6.6, meets the standard, has no irritation and allergy phenomena, and is a pure natural facial mask which is green, environment-friendly and safe.
Drawings
FIG. 1 shows a spirulina powder
FIG. 2 shows the essence and bloom of spirulina
FIG. 3 mask result display diagram
FIG. 4 facial mask processing flow
Detailed Description
Example 1
The specific implementation steps are as follows:
a pure natural spirulina polypeptide mask is composed of the following raw materials in parts by weight:
1. 10g of spirulina polypeptide liquid, 5g of polyvinyl alcohol, 5g of glycerol, 3g of 1, 2-propylene glycol, 3g of coconut oil, 0.2g of xanthan gum and 0.2g of jasmine tea essence, and water is added to make up to 100 g.
2. 100ml of deionized water was prepared in a beaker.
3. 5g of polyvinyl alcohol, 3g of coconut oil and 3g of 1, 2-propylene glycol were added thereto, and the mixture was stirred while heating, and the mixture was stirred until uniform.
4. Deionized water in a beaker was placed in a water bath and heated to 80 ℃.
5. Then 0.2g of xanthan gum is added, the mixture is fully stirred until the xanthan gum is completely dissolved, then the temperature is reduced to 40 ℃, 5g of glycerol is added, and the mixture is uniformly stirred, wherein the component A is the component A.
6. Adding the enzymolyzed spirulina polypeptide liquid into the other beaker to obtain the component B.
And 7, fully and uniformly mixing the component A and the component B, mixing and dispersing the materials in the beaker until the materials are uniform, and standing and emulsifying for 8min at room temperature.
8. Selecting pure cotton fiber facial mask paper 270mm × 203mm, filling into facial mask bags, filling 8g of spirulina facial mask essence into each facial mask bag, and sealing after filling.
9. When the addition amount of the spirulina polypeptide liquid is 10g, the DPPH free radical clearance rate is 38.17 percent, and the tyrosinase inhibition rate is 37.78 percent.
Example 2
The specific implementation steps are as follows:
a pure natural spirulina polypeptide mask is composed of the following raw materials in parts by weight:
1. the spirulina polypeptide liquid is added with 20g of polyvinyl alcohol 15g, glycerin 15g, 1, 2-propylene glycol 3g, coconut oil 3g, xanthan gum 0.2g and jasmine tea essence 0.2g, and water is added to make up to 100 g.
2. 100ml of deionized water was prepared in a beaker.
3. 15g of polyvinyl alcohol, 3g of coconut oil and 3g of 1, 2-propylene glycol were added thereto, and the mixture was stirred while heating, and the mixture was stirred until uniform.
4. Deionized water in a beaker was placed in a water bath and heated to 80 ℃.
5. Then 0.2g of xanthan gum is added, the mixture is fully stirred until the xanthan gum is completely dissolved, then the temperature is reduced to 40 ℃, 15g of glycerol is added, and the mixture is uniformly stirred, wherein the component A is the component A.
6. Adding the enzymolyzed spirulina polypeptide liquid into the other beaker to obtain the component B.
And 7, fully and uniformly mixing the component A and the component B, mixing and dispersing the materials in the beaker until the materials are uniform, and standing and emulsifying for 8min at room temperature.
8. Selecting pure cotton fiber facial mask paper 270mm × 203mm, filling into facial mask bags, filling 9g of spirulina facial mask essence into each facial mask bag, and sealing after filling.
9. When the addition amount of the spirulina polypeptide liquid is 20g, the DPPH free radical clearance rate is 53.16%, and the tyrosinase inhibition rate is 62.11%.
Example 3
The specific implementation steps are as follows:
a pure natural spirulina polypeptide mask is composed of the following raw materials in parts by weight:
1. the spirulina polypeptide liquid is added with 30g of polyvinyl alcohol 25g, glycerol 25g, 1, 2-propylene glycol 3g, coconut oil 3g, xanthan gum 0.2g and jasmine tea essence 0.2g, and water is added to make up to 100 g.
2. 100ml of deionized water was prepared in a beaker.
3. 25g of polyvinyl alcohol, 3g of coconut oil and 3g of 1, 2-propylene glycol were added thereto, and the mixture was stirred while heating, and the mixture was stirred until uniform.
4. Deionized water in a beaker was placed in a water bath and heated to 80 ℃.
5. Then 0.2g of xanthan gum is added, the mixture is fully stirred until the xanthan gum is completely dissolved, then the temperature is reduced to 40 ℃, 25g of glycerol is added, and the mixture is uniformly stirred, wherein the component A is the component A.
6. Adding the enzymolyzed spirulina polypeptide liquid into the other beaker to obtain the component B.
And 7, fully and uniformly mixing the component A and the component B, mixing and dispersing the materials in the beaker until the materials are uniform, and standing and emulsifying for 8min at room temperature.
8. Selecting pure cotton fiber facial mask paper 270mm × 203mm, filling into facial mask bags, filling 10g of spirulina facial mask essence into each facial mask bag, and sealing after filling.
9. When the addition amount of the spirulina polypeptide liquid is 30g, the DPPH free radical clearance rate is 57.11%, and the tyrosinase inhibition rate is 64.21%.
Claims (6)
1. The pure natural spirulina polypeptide facial mask essence is characterized by comprising the following components in percentage by mass: 10-30% of spirulina polypeptide liquid, 5-25% of polyvinyl alcohol, 5-25% of glycerol, 2-5% of 1, 2-propylene glycol, 2-5% of coconut oil, 0.1-0.3% of xanthan gum, 0.1-0.3% of jasmine tea essence and water for supplementing to 100%.
2. The mask essence of claim 1, wherein the spirulina polypeptide liquid is prepared by a method comprising the following steps: and (2) breaking the walls of the spirulina by adopting a method combining repeated freezing and melting and colloid grinding for wall breaking, performing enzymolysis on the spirulina liquid subjected to wall breaking treatment, selecting neutral protease, adding 0.1-0.3% of enzyme based on the weight of a substrate, performing centrifugation for 20-30min after 1-3 hours of enzymolysis, and obtaining the spirulina polypeptide liquid with the content of 10-30%.
3. The method for preparing the pure natural spirulina polypeptide facial mask essence of claim 1, which is characterized by comprising the following steps:
(a) preparing deionized water in a beaker;
(b) accurately adding polyvinyl alcohol, coconut oil and 1, 2-propylene glycol, heating while stirring, and blending to be uniform;
(c) putting deionized water in a beaker into a water bath kettle to heat to 80 ℃;
(d) adding xanthan gum, stirring thoroughly until completely dissolved, then cooling to 40 deg.C, adding glycerol, and stirring to obtain component A;
(e) adding the spirulina polypeptide liquid after enzymolysis into the other beaker to obtain a component B;
(f) mixing the component A and the component B, mixing the materials in the beaker, dispersing uniformly, adding jasmine tea essence, standing at room temperature, and emulsifying for 8 min.
4. A pure natural spirulina polypeptide facial mask is characterized in that a patch type facial mask is made of pure cotton fiber facial mask paper 270mm x 203mm, the pure cotton fiber facial mask paper is placed into facial mask bags, 8-10g of the spirulina facial mask essence liquid of claim 1 is filled into each piece of facial mask, and sealing is carried out after filling.
5. Use of the mask pack of claim 4 for the preparation of a cosmetic for preventing skin aging; and/or, the application of the facial mask in preparing a skin whitening cosmetic.
6. The use of a facial mask according to claim 5 for the preparation of a cosmetic for preventing skin aging, wherein the DPPH radical scavenging rate is 57.52 to 66.36% when the concentration of spirulina facial mask essence is 0.4 to 1g/L, and the tyrosinase inhibition rate is 46.5 to 60.3% when the concentration of spirulina facial mask essence is 1.5 to 3 g/L.
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| CN202210004514.9A CN114306204A (en) | 2022-01-04 | 2022-01-04 | Pure natural spirulina polypeptide mask and preparation method thereof |
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| CN202210004514.9A CN114306204A (en) | 2022-01-04 | 2022-01-04 | Pure natural spirulina polypeptide mask and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116919847A (en) * | 2023-08-30 | 2023-10-24 | 广州沙艾生物科技有限公司 | Cosmetic rich in cell active factors and application thereof |
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2022
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116919847A (en) * | 2023-08-30 | 2023-10-24 | 广州沙艾生物科技有限公司 | Cosmetic rich in cell active factors and application thereof |
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