CN103222943A - Preparation method for instantaneous penetration skin regeneration water composition containing pansy flower extract, guava extract and hydrolyzed pearl - Google Patents
Preparation method for instantaneous penetration skin regeneration water composition containing pansy flower extract, guava extract and hydrolyzed pearl Download PDFInfo
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- CN103222943A CN103222943A CN2013101564312A CN201310156431A CN103222943A CN 103222943 A CN103222943 A CN 103222943A CN 2013101564312 A CN2013101564312 A CN 2013101564312A CN 201310156431 A CN201310156431 A CN 201310156431A CN 103222943 A CN103222943 A CN 103222943A
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Abstract
The present invention relates to a preparation method for an instantaneous penetration skin regeneration water composition containing a pansy flower extract, a guava extract and hydrolyzed pearl. The preparation comprises: 1) carrying out sterilization on deionized water, cooling to a temperature of 70 DEG C, adding carbomer and sodium hyaluronate, and uniformly stirring; 2) when a temperature achieves about 45 DEG C, adding a phase 2, completely and uniformly stirring, and discharging the material, wherein the phase 2 comprises, by weight, 15% of glycerol, 8% of a witch hazel extract, 1% of 1,2-hexanediol/caprylyl glycol, 1% of dipotassium glycyrrhizinate, 1% of triethanolamine, 0.4% of a solubilizer, 0.2% of an essence, 0.4% of a preservative, 2% of a pansy flower extract, 2% of a guava extract, and 2% of hydrolyzed pearl; and 3) sequentially carrying out storage, half finished product inspection, filling, finished product inspection, and warehousing. With the composition, moisturizing can be performed on skin at night, deep penetration channels of skin can be opened, amino acids can be supplied, skin regeneration can be strengthened, and skin breathing is smooth.
Description
Present patent application is an application for a patent for invention (application number: the 201110289426.X applying date: 11-09-27, innovation and creation
Title: a kind of wink saturating granulation promoting water composition and preparation method thereof) divide an application.
Technical field
The invention belongs to a kind of wink saturating granulation promoting water composition and preparation method thereof of moisturizing immediately.
Background technology
Because modern people's rhythm of life is fast, and is subjected to various environmental effects, skin often is in exsiccosis, dry, intensely dark pool.
Chinese invention patent application (application number: 200910010837.3 applyings date: 2009-03-24) disclose a kind of skincare humectant.It is made of according to the following number of weight ratio following component: the skin protection base material: natural dimethylamino proline acid: glycerol: Mel: shea butter: vitamin E=80-120: 5-12: 1-3: 10-20: 1-3: 2-4.This invention contains shea butter, glycerol, Mel isoreactivity and nourishes the composition of preserving moisture, and can help rapidly to moisten dry skin, makes the skin exquisiteness soft and smooth.
Chinese invention patent application (application number: 200710150410.4 applyings date: 2007-11-26) disclose a kind of cosmetic humectant that contains xylitol, it is made up of following materials based on weight: 2-10 part wetting agent, 0.1-2 part oils and fats, emulsifying agent 5-15 part, 60～80 parts in water.The cosmetic humectant of this invention can more deeply be diffused into the skin depths, combines with deep water, keeps skin moistened.
Summary of the invention
Often be in exsiccosis in order to solve people's skin, the problem in dry, intensely dark pool an object of the present invention is to provide saturating granulation promoting water composition of a kind of wink, and said composition has instant moisturizing, makes skin full, is full of elasticity, tender white glossy characteristics.Another one purpose of the present invention provides the preparation method of saturating granulation promoting water composition of a kind of above-mentioned wink.
In order to realize above-mentioned first purpose, the present invention has adopted following technical scheme:
A kind of wink saturating granulation promoting water composition, described granulation promoting water composition comprises following component by mass percentage:
(a) 0.01% to 20% wetting agent;
(b) 0.01% to 10% thickening polymer;
(c) 0.01% to 10% antiinflammatory;
(d) 0.01% to 10% skin conditioning agent;
(e) 10% to 90% deionized water.
As preferably, described granulation promoting water composition comprises following component by mass percentage:
(a) 1% to 20% wetting agent;
(b) 0.01% to 8% thickening polymer;
(c) 0.01% to 10% antiinflammatory;
(d) 0.01% to 10% skin conditioning agent;
(e) 10% to 90% deionized water.
As preferred again, described granulation promoting water composition comprises following component by mass percentage:
(a) 2% to 20% wetting agent;
(b) 0.01% to 6% thickening polymer;
(c) 0.01% to 10% antiinflammatory;
(d) 0.01% to 10% skin conditioning agent;
(e) 10% to 90% deionized water.
As preferably, above-mentioned wetting agent is selected propylene glycol, sorbitol, butanediol, 1 for use, in 2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol and the Polyethylene Glycol one or more, what be preferred for this compositions is glycerol or 1,2-hexanediol/caprylyl glycol.
As preferably, above-mentioned thickening polymer is selected one or more in carboxylic acid polyalcohol, cross-linked polyacrylate polymer, the synthetic high molecular polymer of cellulose ethers, the natural high molecular polymer for use; Preferably acrylic crosslinking polymer is more preferably the material by CTFA called after carbomer.
As preferably, above-mentioned antiinflammatory is a glycyrrhizic acid dipotassium.
As preferably, above-mentioned skin conditioning agent is selected from one or more in hydrolyzed pearl, hyaluronate sodium, Radix Hamamelidis Mollis extract, America Ramulus Sambuci Williamsii extract, Herba Violae Hortensis flower extract and the Fructus psidii guajavae immaturus extract.
As preferably, above-mentioned compositions has also comprised antiseptic and essence.
The present composition also can comprise various other compositions.The function of the concrete composition of compositions of the present invention and effect will be described in more detail below.
Wetting agent
About by weight wetting agent of 0.01% to 20% among the present invention is a polyhydric alcohol, compositions described herein preferably comprises by the weight of described compositions about 1% to 20%, the wetting agent of 2%-20% more preferably, example comprises propylene glycol, sorbitol, butanediol, 1,2-hexanediol, caprylyl glycol, dipropylene glycol, glycerol, diglycerol, pentanediol, Polyethylene Glycol, and their mixture, what be preferred for this compositions is glycerol, 1,2-hexanediol/caprylyl glycol.
Thickening agent
In some embodiments, compositions of the present invention can also comprise one or more thickening agents, and described compositions comprises by the weight of described compositions about 0.01% to 10%, preferably is about 0.01% to 8%, more preferably from about 0.01% to 6% thickening agent.
The non-limiting kind of thickening agent comprises and is selected from following material: carboxylic acid polyalcohol (as Carbopol980), cross-linked polyacrylate polymer, synthetic high molecular polymer (as cellulose ethers), natural high molecular polymer (as natural gum), acrylic crosslinking polymer is preferably more preferably pressed the material of CTFA called after carbomer.
Antiinflammatory
Present composition antiinflammatory is a glycyrrhizic acid dipotassium, molecular formula: C
42H
60K
2O
16Radix Glycyrrhizae just has detoxifcation, antiinflammatory anti-allergic effects as medicine since ancient times.Its curative effect is widely known by the people.Effective ingredient further investigation to Radix Glycyrrhizae extract shows: glycyrrhizic acid and potassium salt thereof have the effect of good anti-allergic effects, Detoxication and similar adrenal gland's sebum hormone, even life-time service also has no side effect.Glycyrrhizic acid dipotassium such as is used for cosmetics and has antiinflammatory, antiallergic, preserve moisture at effect.
Skin conditioning agent
The various skin conditioner that the present composition added is Radix Hamamelidis Mollis extract, America Ramulus Sambuci Williamsii extract, Herba Violae Hortensis flower extract, Fructus psidii guajavae immaturus extract.
The content of the Radix Hamamelidis Mollis extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Radix Hamamelidis Mollis extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The Radix Hamamelidis Mollis extract that the present composition adds, main component includes tannin, gallic acid, catechin, procyanidin, flavonoid element (kaempferol, Quercetin), quintessence oil (carvacrol, eugenol, hexenol), choline and Saponin etc., well astringent and antioxidant are also very effective when being used for treating comedo.
The content of the America Ramulus Sambuci Williamsii extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the America Ramulus Sambuci Williamsii extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The America Ramulus Sambuci Williamsii extract that the present composition adds contains the Ramulus Sambuci Williamsii anthocyanin, anthocyanidin glycoside, morroniside etc.Have superpower moisturizing effect, and can make the eye skin in time absorb nutritional labeling; Promote the cutaneous circulation flow velocity simultaneously, reduce the eye edema, very effective to dispeling the eye black eye, allow two pupils look eagle-eyed.
The content of the Herba Violae Hortensis flower extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Herba Violae Hortensis flower extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The Herba Violae Hortensis flower extract of the present composition is rich in globulariacitrin, Saponin and vitamin C, tocopherol etc.The conditioning skin has antibacterial action, the pox that significantly disappears effect to the equilibrated health status of water oil comprehensively.
The content of the Fructus psidii guajavae immaturus extract that the present composition adds is preferably about 0.01% to 8% by the weight of described compositions, more preferably from about 0.01% to 6%, the active quantities of the Fructus psidii guajavae immaturus extract of the present composition is preferred about 0.001% to 8% by the weight of described compositions, and more preferably from about 0.001% to 6%.
The Fructus psidii guajavae immaturus extract of the present composition, be rich in trace element such as vitamin C, protein, fat, vitamin A, category-B vitamin, calcium, phosphorus, ferrum, can be effectively in and free radical, enhance metabolism, help skin to discharge " toxin ", bring into play the whitening skin and preserving moisture effect immediately.
The hydrolyzed pearl of the present composition, its content is by the weight of the present composition about 0.01% to 10%, preferably be about 0.01% to 8%, be more preferably 0.01% to 6%, its active matter content is by the weight of the present composition about 0.001% to 10%, preferred about 0.001% to 8%, more preferably from about 0.001% to 6%.
The hydrolyzed pearl of the present composition is that the enzymolysis process by Margarita powder obtains, and contains a large amount of calcium ions and pearl protein, has the elimination oxygen-derived free radicals, anti-aging effects, and light speckle makes the beautiful gloss of skin.
The hyaluronate sodium of the present composition is the glutinous sugar of a kind of bionical thing, and molecular weight is greater than 1,000,000, and the hyaluronic acid sodium content of the present composition is about 0.01% to 10% by the invention composition weight meter, and is preferred about 0.01% to 5%, is more preferably 0.01% to 3%.
Contain 10% to 20% moisture in the normal human skin horny layer, it prevents skin aging, prevents that the various stimulations of external environment from all having significant role skin care.With advancing age or the variation of environment, moisture can drop to below 10%, and skin can be dry, produces wrinkle.The hyaluronate sodium of the present composition can be alleviated this problem, and its theoretical water retention value reaches 1000ml/g, is the key component of water conservation in the human body skin, and not only moistening effect is good, and do not have greasy feeling and stop up pore etc. shortcoming.Can also eliminate oxygen-derived free radicals, repair the skin that shines the back damage.
As preferred again, described granulation promoting water composition is made of following component by mass percentage:
| Deionized water | 50%～80% |
| Carbomer | 0.2%～１.５% |
| Hyaluronate sodium | 0.2%～1.5% |
| Glycerol | ８％～２0％ |
| The Radix Hamamelidis Mollis extract | 2%～15% |
| 1,2-hexanediol/caprylyl glycol | 0.5%～1.5% |
| Glycyrrhizic acid dipotassium | 0.5%～3.0% |
| Triethanolamine | 0.2%～1.5% |
| Solubilizing agent | 0%～1.0% |
| Essence | 0%～0.8% |
| Antiseptic | 0%～1.0% |
| Hydrolyzed pearl | 0%～5.0% |
| The America Ramulus Sambuci Williamsii extract | 0%～5.0% |
| The Herba Violae Hortensis flower extract | 0%～5.0% |
| Guava extract | 0%～5.0% |
It is not 0 that above-mentioned hydrolyzed pearl, America Ramulus Sambuci Williamsii extract, Herba Violae Hortensis flower extract and Fructus psidii guajavae immaturus extract have a kind of composition at least.
In order to realize second above-mentioned purpose, the present invention has adopted following technical scheme:
A kind of preparation method for preparing saturating granulation promoting water composition of above-mentioned wink, this method comprises the steps:
1) deionized water after the sterilization, adds thickening polymer and skin conditioning agent when being cooled to 65～75 ℃, stir;
2) to about 40～50 ℃, add other components, stir discharging;
3) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
The present invention is owing to adopted above-mentioned technical scheme, and product can be to the instant moisturizing of skin after use, and the effective ingredient Titanium Dioxide in the plant extract promotes the glossy degree of skin.
The specific embodiment
Preparation process of the present invention is the state that each composition is mixed to the comparison homogeneous, and step is:
1. deionized water after the sterilization, adds carbomer and hyaluronate sodium when being cooled to 70 ℃, stirs.
2. to about 45 ℃, add other components, stir discharging.
3. storage → the inspection of semifinished product → fill → product inspection → warehouse-in.
Specific embodiment:
Mutually 1 put into container and mix, stirring and dissolving is complete; 2 adding phases 1 stir discharging mutually.
Method of testing:
In order to test saturating, cosmetic result of wink of the present invention, carried out investigation experiment on probation:
1, respondent: each department ordinary consumer 50 people, the trial state feedback form of Shou Huiing is 45 parts at last;
2, control time: December in 2008 on February 10th, 1 2009 on the 10th;
3, use product: No. 1 product is the product according to formulation of the present invention; No. 2 products are the rival factory similar products;
4, method of testing: after the tester face cleaning, about respectively No. 1 product and No. 2 products being coated on two cheek, observe and experience result of use;
5, the test form is as follows:
The use of No. 1 product of table 1 (60 days) feedback conclusive table
No. 2 products of table 2 use (60 days) feedback conclusive table
Saturating effect contrast of the wink of No. 1 product of table 3 and No. 2 products statistical table
The cosmetic result contrast statistical table of No. 1 product of table 4 and No. 2 products
The statistical table of table 5 tester recommended products model
| Proposed model | No. 1 | No. 2 |
| The recommendation number | ３９ | ６ |
| Percentage ratio | 86.67% | 13.33% |
6, feedback conclusion:
The tester represents that all the wink of No. 1 product, saturating moisturizing effect was quite outstanding, and skin moment is softening level and smooth; Slightly sticking sense, but moisture retention is fabulous, and also after often using, face makes use good than No. 2 products, and the colour of skin is more moistened, and is brighter.And there is not the people that allergic phenomena is arranged in the questionnaire that reclaims.
As shown in Table 5,86.67% people recommends to use product No. 1, has only 13.33% people to recommend to use product No. 2.
Claims (1)
- One kind contain Herba Violae Hortensis flower extract, guava extract and hydrolyzed pearl wink saturating granulation promoting water composition preparation method, it is characterized in that this method is made of following step:1) deionized water after the sterilization, adds carbomer and hyaluronate sodium when being cooled to 70 ℃, stir;2) to about 45 ℃, add phase 2, stir discharging; Described phase 2 is by weight percentage by glycerol 15%, Radix Hamamelidis Mollis extract 8%, 1,2-hexanediol/caprylyl glycol 1%, glycyrrhizic acid dipotassium 1%, triethanolamine 1%, solubilizing agent 0.4%, essence 0.2%, antiseptic 0.4%, Herba Violae Hortensis flower extract 2%, guava extract 2% and hydrolyzed pearl 2% constitute;3) storage → inspection of semifinished product → fill → product inspection → warehouse-in.
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| CN201310156431.2A CN103222943B (en) | 2011-09-27 | 2011-09-27 | Preparation method for instantaneous penetration skin regeneration water composition containing pansy flower extract, guava extract and hydrolyzed pearl |
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| CN201110289426.XA Division CN102370606B (en) | 2011-09-27 | 2011-09-27 | skin penetration and tissue regeneration lotion composition and preparation method thereof |
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Effective date of registration: 20151119 Address after: 313200 Zhejiang province Deqing County Wukang Center Road No. 518 Patentee after: Zhejiang OSM Group Co.,Ltd. Address before: 313200 Zhejiang city of Huzhou province Deqing County Wukang Town Center Road No. 518 Patentee before: Shen Zhirong |
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Effective date of registration: 20230106 Address after: 313200 No. 99, Pearl Street, Moganshan high tech Industrial Development Zone, Deqing County, Huzhou City, Zhejiang Province Patentee after: OSMUN BIOLOGICAL Co.,Ltd. Address before: No. 518, Zhongxin North Road, Wukang Town, Deqing County, Zhejiang Province, 313200 Patentee before: Zhejiang OSM Group Co.,Ltd. |