CN109528539A - A kind of compact shining skin effect application of ganoderma lucidum Radix Codonopsis and facial mask and preparation method - Google Patents
A kind of compact shining skin effect application of ganoderma lucidum Radix Codonopsis and facial mask and preparation method Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
Compact shining skin effect application and facial mask and preparation method the invention discloses a kind of ganoderma lucidum Radix Codonopsis.The present invention is using ganoderma lucidum as monarch drug in a prescription, Radix Codonopsis is ministerial drug, lotus flower is adjutant, and the pure plants antioxygen grease such as print plus fruit seed oil, camellia seed oil and peony seed oil of arranging in pairs or groups, pass through the assurance to key component ratio, playing Traditional Chinese Medicine " monarch " thought is guidance, in conjunction with skin care application target scientific design prescription, it obtains and effectively removes free radical, anti-lipid peroxidation, delay skin aging, keeps the tender glossiness beneficial effect of skin, it is applied in facial mask, releive promoting blood circulation, compact shining skin can be played the role of.
Description
Technical field
The present invention relates to cosmetic technical fields, more particularly, to a kind of compact shining skin effect application of ganoderma lucidum Radix Codonopsis
And facial mask and preparation method.
Background technique
Radix Codonopsis is the beneficial tonic of tradition in China, and it is living to mainly contain a variety of natural pharmacology such as polysaccharide, saponin(e, alkaloid, flavones
Property ingredient.Modern pharmacology research show Radix Codonopsis can strengthen immunity, the effects of anti-aging is anti-oxidant, anticancer.Wherein, party
It is significant to join saponin(e antioxidation, Codonopsis pilosula polysaccharide has obvious anti-aging effects.Ganoderma lucidum is that a kind of medical value is very high rare
Fungi, modern medicine is the study found that there is ganoderma lucidum enhancing to be immunized, boost metabolism, delay senescence, neurasthenia etc. is made
With.
Skin aging is to be determined by inherent cause and continued gradual physiology mistake by a kind of of a variety of such environmental effects
Journey, skin aging are formed, characterized by cutis laxa and pigmentary disturbances by rough surface, wrinkle in appearance.Skin aging is nature
Aging and the coefficient result of light aging action.Wherein, light aging is mainly since skin is under ultraviolet light irradiation, in skin
Active oxygen radical is generated, oxygen radical makes collagen cross-linking, and skin follows the string, and generates wrinkle.On the other hand, free radical
The damage of protein, DNA etc. can also be caused, there are also the effects for promoting Apoptosis to form brown plain spot, generate with albumen qualitative response
Pigmentation causes premature skin ageing.Therefore, in order to be effectively prevented the aging of skin, various antisenility skin care products at
For hot spot concerned by people.
Wherein, anti-ageing face mask is one of existing most common anti-aging skin care product.Facial mask is using being covered on face
The of short duration time is temporarily isolating extraneous air and pollution, improves skin temperature, the pore expansion of skin, promote sweat gland secretion with
Metabolism rises the oxygen content of skin, is conducive to skin and excludes the product of epidermal cell metabolism and the grease of accumulation
A kind of product of substance, the moisture in facial mask penetrate into the cuticula of epidermis, and skin becomes soft, and skin nature light has bullet
Property.And existing anti-ageing face mask is mostly to add artificial synthesized antioxidant, and it is big to skin irritation, even with person face
Allergic symptom can occur for portion.
Summary of the invention
For deficiency existing for anti-ageing face mask in the prior art, the purpose of the present invention is to provide one kind to have compact shine
The composition of skin effect, the composition with Chinese medicine " monarch " thought be guidance carry out prescription, also containing print plus fruit seed oil,
Camellia seed oil and peony seed oil etc. have the natural component of anti-oxidation efficacy, can remove free radical, be applied in facial mask,
Can effective delay skin aging, keep skin it is tender glossy.
Another technical problem to be solved by the present invention is that providing the preparation side of the composition with compact shining skin effect
Method.
It is anti-in preparation that a present invention also technical problems to be solved are to provide the composition with compact shining skin effect
Application in aging face mask of traditional Chinese medicine.
The purpose of the present invention is achieved through the following technical solutions:
A kind of compact shining skin effect application of ganoderma lucidum Radix Codonopsis is provided, being specifically applied to preparation has compact shining skin effect
Composition, the composition includes each component of following parts by weight: lotus flower flower 90~130 parts of water, Ganodenna Lucidum P.E 0.4~1
Part, 0.4~1 part of Radix Codonopsis extract, print plus 0.09~0.16 part of fruit seed oil, 0.09~0.16 part of camellia seed oil, peony seed oil
0.09~0.16 part.
Preferably, the composition includes each component of following parts by weight: lotus flower flower 90~120 parts of water, Ganodenna Lucidum P.E
0.45~0.8 part, 0.45~0.7 part of Radix Codonopsis extract, print plus 0.09~0.12 part of fruit seed oil, camellia seed oil 0.09~0.13
Part, 0.09~0.15 part of peony seed oil.
It is further preferred that the composition includes each component of following parts by weight: lotus flower flower 90~100 parts of water, ganoderma lucidum
0.45~0.6 part of extract, 0.5~0.6 part of Radix Codonopsis extract, print plus 0.09~0.1 part of fruit seed oil, camellia seed oil 0.1~
0.12 part, 0.11~0.13 part of peony seed oil.
The composition with compact shining skin effect is that guidance carries out prescription with Chinese medicine " monarch " thought, with ganoderma lucidum
For monarch drug in a prescription, Radix Codonopsis is ministerial drug, and lotus flower is adjutant, wherein is rich in polysaccharide component in ganoderma lucidum, can eliminate interior free yl, protects
Cell and cell delay senescence；Radix Codonopsis blood-nourishing skin-moisturizing, has delaying senility function concurrently；Contain the factor of invigorating blood circulation of releiving in lotus flower flower water,
On the one hand it can improve blood circulation with activating microcirculation and removing stasis medicinal, increase skin gloss, on the other hand, also have and delay senescence, improve skin
Appearance keeps skin emolliency and increases elasticity, eliminates and reduce the booster actions such as wrinkle of skin.The present invention passes through long term test,
The components compatibility is formed to the composition with compact shining skin effect according to reasonable dosage, and is applied in facial mask,
It can play the role of releive promoting blood circulation, compact shining skin.
Further to play collaboration antioxidation, the composition also includes print plus fruit seed oil, camellia seed oil and tree peony
The natural anti-oxidations grease such as seed oil can delay senescence with " monarch " Chinese prescription compatibility, keep skin emolliency, have light
Pool, wherein camellia seed oil contains vitamin E and antioxidant content, it can protect skin, and skin is made to have gloss, and peony seeds
The rich content of vitamin, niacin, carrotene, unsaturated fatty acid in oil can obviously improve skin epidermal cells circulation
Function, the progress of anti-lipid peroxidation effect, improves metabolism, and delay skin aging process has crease-resistant, moisturizing to brighten work
With；Tocopherol content is high in print plus fruit seed oil, on the one hand, vitamin E has good free radical scavenging ability, with superoxides
Mutase, glutathione peroxidase constitute internal antioxidant system together, protect cell membrane and intracellular nucleic acid from certainly
By the attack of base；On the other hand, after vitamin E is absorbed by the skin, it not only can be reduced the mistake of lipid and lipoprotein on cell membrane
Oxidation, moreover it is possible to keep subcutaneous fat, elastomer and the connection being coupled between collagen tissue, further suppress lipid peroxy
Change, skin is made to keep elasticity.
The composition with compact shining skin effect can be existing using this field under the essential idea of compatibility of the present invention
There is achievable technological means to be prepared.
Present invention simultaneously provides the preferred preparation method of the composition with compact shining skin effect, the ganoderma lucidum is extracted
Object, Radix Codonopsis extract are to extract the extracting solution being obtained by filtration through boiling respectively by ganoderma lucidum, Radix Codonopsis；By print plus fruit seed oil, tea seed
Lotus flower flower water and Ganodenna Lucidum P.E, Radix Codonopsis extract is added in oil, peony seed oil mixing, be thoroughly mixed uniformly to get.
Wherein, the lotus flower flower water in the present invention can be made by conventional method in that art, and the present invention provides a kind of optional
Method is made: after lotus flower and solvent are mixed, extracting by conventional method in that art.The solvent can be conventional for this field
Extraction solvent, preferably one of water, ethyl alcohol and 1,3-BDO or a variety of.The method of the extraction can for infusion process,
Percolation, decocting method, reflux extraction or ultrasonic extraction etc..Preferably, after the lotus flower flower water is by lotus flower and ethyl alcohol mixing,
It is obtained using ultrasonic extraction.
Present invention simultaneously provides application of the composition with compact shining skin effect in delay aging drug facial mask.
It is further preferred that the delay aging drug facial mask includes base fabric and film Essence, the base fabric is three stratus mists
Facial mask cloth contains the composition with compact shining skin effect in the Essence.
Cloud and mist facial mask of the invention is three layers composite structured, and upper and lower two germinal layer is to hold high and Delicate fibers, middle layer are
Special oil suction does not absorb water superfine fibre, using newest Hydroentangled technology, three layers of fiber are lossless entangled, both guarantees
Fibre structure is not destroyed, and greatly improves the density of fiber, is enabled facial mask sufficiently flexible, is unlikely to deform, liquid absorption amount is up to
1923%.The present invention is arranged in pairs or groups using three stratus mist facial mask cloths and Essence of the present invention, and being adapted property is very good, and Essence is carried on
Seaweed mask cloth, load effect is good, and moisture-regulating effect complements each other.Preferably, three stratus mist facial mask cloths of the invention
Many nonwoven cosmetics Co., Ltd is closed purchased from Guangzhou.
Further, the facial mask essence is made of A phase and B phase raw material, has in the B phase raw material comprising described
The composition of compact shining skin effect；
The A phase includes: 0.9~2 part of glycerol, 0.95~1.8 part of butanediol, 0.25~0.5 part of Sodium Hyaluronate, seaweed
0.8~1.5 part of sugar, 0.27~0.48 part of dipotassium glycyrrhizinate, 0.7~1.3 part of methyl gluceth -20, allantoin 0.2~
0.5 part, 0.4~0.9 part of Scleroglucan, 0.08~0.15 part of laruyl alcohol phosphate potassium, acrylic acid (ester) class/C10-30 alkanol third
0.09~0.15 part of olefin(e) acid ester cross-linked polymer, 0.15~0.4 part of parahydroxyacet-ophenone；
The B phase includes: 0.08~0.2 part of 90~133 parts of composition, arginine, decoyl with compact shining skin effect
0.025~0.048 part of hydroximic acid, 0.04~0.08 part of glycerol caprylate, 0.36~0.64 part of 1,2- pentanediol.
Further, the A phase include: 1~1.6 part of glycerol, 1.2~1.5 parts of butanediol, Sodium Hyaluronate 0.27~
0.36 part, 0.9~1.2 part of trehalose, 0.3~0.45 part of dipotassium glycyrrhizinate, methyl gluceth -200.8~1 part, allantois
0.27~0.36 part of element, 0.45~0.8 part of Scleroglucan, 0.09~0.12 part of laruyl alcohol phosphate potassium, acrylic acid (ester) class/
0.1~0.13 part, 0.18~0.3 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
The B phase includes: 0.09~0.15 part of 91~102 parts of composition, arginine, decoyl with compact shining skin effect
0.03~0.04 part of hydroximic acid, 0.05~0.06 part of glycerol caprylate, 0.45~0.55 part of 1,2- pentanediol.
The present invention selects minimum 2000 molecular weight hyaluronic acids of molecular weight on the market, can prevent the production of some enzymes in cell
It is raw, the formation of free radical is reduced, is preventing free radical from the side such as destroying eucaryotic cell structure, generating lipid peroxidation and cause senility of humanbody
Face plays an important role, and has the function of that anti-inflammatory, inhibition germ generates, keeps skin bright and clean；Dipotassium glycyrrhizinate is good
Anti-freckle agent and anti-allergic agent, it can prevent the release of histamine, have removing toxic substances, disinfection, anti-allergic effects.Facial mask of the invention utilizes
The composition with compact shining skin effect of Chinese prescription acts synergistically with nutritional ingredients such as dipotassium glycyrrhizinate, Sodium Hyaluronates,
It is blending the east and the west, it can effectively improve the oxidation resistance of skin, avoid face skin accelerated ageing, reduce facial wrinkles, promote
Skin metabolism enhances the vigor and antimicrbial power of skin.
The present invention provides a kind of preparation method of preferred Essence, and the preparation method of the Essence includes following step
It is rapid:
S1. above-mentioned A phase raw material is sequentially added in water phase pot, stirring is warming up to 80~90 DEG C, stirs, and keeps the temperature
It is spare；
S2. after mixing evenly, homogeneous 1~10 minute, vacuumizes, and constant temperature 10~20 minutes；
When being S3. cooled to 40~45 DEG C, above-mentioned B phase raw material is sequentially added, stirs, every a raw material of addition,
A raw material under stirring adds again to after dissolving；
When being S4. cooled to 32~38 DEG C, discharging is stood to get the facial mask essence.
Further, in step S1, the temperature is 80~85 DEG C；Preferably, the temperature is 85 DEG C.
Further, in step S2, the homogenizing time is 2~5 minutes；Preferably, the homogenizing time is 3 minutes.
Further, in step S3, when being cooled to 45 DEG C, above-mentioned B phase raw material is sequentially added, stirs, often adds
A raw material under adding a raw material, stirring to add again to after dissolving.
Further, in step S4, when being cooled to 38 DEG C, discharging is stood to get the Essence.
Compared with prior art, the beneficial effects of the present invention are:
The present invention provides a kind of composition with compact shining skin effect, with Chinese medicine " monarch " thought be instruct into
Row prescription, using ganoderma lucidum as monarch drug in a prescription, Radix Codonopsis is ministerial drug, and lotus flower is adjutant, wherein is rich in polysaccharide component in ganoderma lucidum, can eliminate body
Interior free radical, protection cell and cell delay senescence；Radix Codonopsis blood-nourishing skin-moisturizing, has delaying senility function concurrently；Contain in lotus flower flower water
It releives the factor of invigorating blood circulation, on the one hand can improve blood circulation with activating microcirculation and removing stasis medicinal, increase skin gloss, on the other hand, also have and delay
Aging improves skin appearance, keeps skin emolliency and increases elasticity, eliminates and reduce the booster actions such as wrinkle of skin.The present invention
By long term test, the components compatibility forms to the composition with compact shining skin effect according to reasonable dosage, and by its
Applied to releive promoting blood circulation, compact shining skin in facial mask, can be played the role of.
Also containing the pure natural inhibited oil such as print plus fruit seed oil, camellia seed oil and peony seed oil in composition of the invention
Rouge can effectively clear free radical using rational proportion and " monarch " Chinese prescription compatibility, and anti-lipid peroxidation delays
Skin aging keeps skin tender glossy.
From the point of view of overall composition, the present invention provides a kind of full-featured green face pack, by key component ratio
It holds, containing a variety of antioxidant contents such as vitamin, tocopherols in product, and by Chinese prescription and dipotassium glycyrrhizinate, hyalomitome
Sour sodium synergistic effect, it is blending the east and the west, it can effectively improve the oxidation resistance of skin, avoid face skin accelerated ageing, reduce
Facial wrinkles promote skin metabolism, enhance the vigor and antimicrbial power of skin.
Delay aging drug facial mask of the invention does not add a drop secondary water using pure lotus flower flower water, without essence, without anti-corrosion
Agent had not only remained the effect of lotus flower spends water activating microcirculation and removing stasis medicinal, but also be added to a variety of pure natural under the collocation of pure plant ingredient
Beauty plant component, makes it complement each other, and skin is allowed to fully absorb nutrition.
The present invention uses three stratus mist facial mask cloths, and deposited sense is tender, imbibition rate is high, docile is elastic, and collocation is melted into rich in antioxygen
Point facial mask essence, can effective delay skin aging, keep skin it is tender flexible, eliminate and reduce wrinkle of skin.
Specific embodiment
To facilitate the understanding of the present invention, present invention work more comprehensively, is meticulously described below in conjunction with embodiment, but this hair
Bright protection scope is not limited to embodiment in detail below.
Unless otherwise defined, all technical terms used hereinafter and the normally understood meaning of those skilled in the art
It is identical.Technical term used herein is intended merely to the purpose of description specific embodiment, it is no intended to limit of the invention
Protection scope.
For convenience of description, it is exemplified below heretofore described primary raw material as follows, unless stated otherwise its preparation side
Method is commercially available.Specifically:
Ganodenna Lucidum P.E, GANODERMA SINENSIS EXTRACT, in the present invention, Ganodenna Lucidum P.E are by ganoderma lucidum water
It boils, it is extracted, filter de- slag and obtain corresponding filtrate, it then will leave after its boiling and extracted again, by the extracting solution and the
No. one time extracting solution merges to obtain.
Radix Codonopsis extract, CODONOPSIS PILOSULA EXTRACT, in the present invention, Radix Codonopsis extract is by Radix Codonopsis
Boiling, it is extracted, filter de- slag and obtain corresponding filtrate, then will leave after its boiling and extracted again, by the extracting solution and
First time extracting solution merges to obtain.
Lotus flower spends water, and NELUMBO NUCIFERA FLOWER WATER, in the present invention, the lotus flower flower water is by lotus
Flower smashes it through 80 meshes, according to the solid-liquid ratio (g:mL) of 1:15, extracts 70min with the EtOH Sonicate of volume fraction 85% and obtains
It arrives, wherein the frequency of ultrasonic extraction is 50kHz, power 900W.
Print plus fruit seed oil, PLUKENETIA VOLUBILIS SEED OIL are purchased from bright Ji Ya.
Camellia seed oil, CAMELLIA OLEIFERA SEED OIL are purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd.
Peony seed oil, LINUM USITATISSIMUM (LINSEED) SEED OIL are purchased from bright Ji Ya.Scleroglucan (water
Solve Scleroglucan), Hydrolyzed Sclerotium Gum (HSG), regular market purchase, the chemical component for hydrolyzing Scleroglucan is
Scleroglucan is the hydrolysis natural small molecule amount beta glucan decomposited by the white beautiful bacterium of a fungi plant, has splendid lock
Outlet capacity and skin care bioactivity, can prevent the invasion of extraneous bacterial virus, stop the loss of intradermal nutriment, in machinery
Property, it is physical, chemically and the protection of biological skin injury in terms of also have remarkable efficacy, in addition, hydrolysis Scleroglucan
It is a kind of skin care item skin sense " modifying agent ", the tender sense of cunning of facial mask essence velvet can be assigned.
Dipotassium glycyrrhizinate, regular market purchase, No. CAS: 68797-35-3, structural formula is as follows:
Dipotassium glycyrrhizinate is the effect of Radix Glycyrrhizae proposes neutralization acquisition through water ingredient, is extensively answered in medicine food and daily chemicals field
With in the present invention, being cooperateed with Sodium Hyaluronate and play antibacterial removing toxic substances, anti-inflammatory antiallergic and other effects, and corticosteroid can be activated
The effect of closing object, preventing cosmetic allergic contact dermatitis from reacting, promotes the absorption of skin care item.
Allantoin, regular market purchase, CAS 97-59-6, structural formula are as follows:
Allantoin is a kind of hydantoin derivatives as made from glyoxalic acid, urea synthesizing, and allantoin can promote cell raw
Long, quickening wound healing, cutin-softening albumen simultaneously alleviate xerodermia, and in the present invention, it is just right that allantoin can play
Sterilization and anticorrosion, nourish moisturizing, it is anti-oxidant convergence etc. multi-efficiencies.
Decoyl hydroximic acid, regular market purchase, No. CAS: 7377-03-9.
Glycerol caprylate, regular market purchase, No. CAS: 26402-26-6.
1,2- pentanediol, regular market purchase, No. CAS: 5343-92-0.
Parahydroxyacet-ophenone, regular market purchase, No. CAS: 99-93-4.
Butanediol, regular market purchase, No. CAS: 107-88-0.
Methyl gluceth -20, regular market purchase, No. CAS: 68239-42-9.
Sodium Hyaluronate, regular market purchase, No. CAS: 9067-32-7.
Trehalose, regular market purchase, No. CAS: 99-20-7.
Arginine, regular market purchase, No. CAS: 74-79-3.
Glycerol, regular market purchase, No. CAS: 56-81-5.
Laruyl alcohol phosphate potassium, regular market purchase, structural formula are as follows:
Laruyl alcohol phosphate potassium have class phosphatide characteristic, it is natural, highly-safe, it is nontoxic it is non-stimulated have excellent emulsification,
The performances such as dispersion, softness are not only able to play certain emulsification in the present invention, moreover it is possible to assist with Sodium Hyaluronate, allantoin
With moisture-keeping function is played, keep skin is long-acting to moisten.
Acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer, regular market purchase is by multiple at being grouped as
Copolymer has excellent emulsification, dispersion, thickening power, is cooperateed with Scleroglucan as skin care item skin sense " modifying agent ", can be assigned
It gives facial mask essence and comfortably slides tender sense.
In addition, the base fabric that delay aging drug facial mask of the invention uses closes many nothings for three stratus mist facial mask cloths, purchased from Guangzhou
Spin cosmetics Co., Ltd.
Embodiment 1
The present embodiment provides a kind of delay aging drug facial mask, including base fabric and Essence, mask substrate is three stratus cloudy surfaces
Film cloth, Essence are made of A phase and B phase raw material, are specifically prepared by the component of following parts by weight:
A phase includes: 0.9 part of glycerol, 0.95 part of butanediol, 0.25 part of Sodium Hyaluronate, 1.5 parts of trehalose, glycyrrhizic acid two
0.27 part of potassium, 1.3 parts of methyl gluceth -20,0.5 part of allantoin, 0.4 part of Scleroglucan, laruyl alcohol phosphate potassium 0.15
Part, acrylic acid (ester) class/0.15 part, 0.4 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
B phase includes: 0.048 part of 0.2 part of 91 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect, sweet
0.04 part of oily caprylate, 0.36 part of 1,2- pentanediol.
The present embodiment prepares the Essence according to following processing step:
S1. above-mentioned A phase raw material is added in water phase pot, stirring is warming up to 85 DEG C, stirs, and keeps the temperature spare；
S2. after mixing evenly, homogeneous 3 minutes, vacuumize, and constant temperature 15 minutes；
When being S3. cooled to 45 DEG C, above-mentioned B phase raw material is added, stirs；
When being S4. cooled to 38 DEG C, discharging is stood to get the facial mask essence.
Composition in the present embodiment B phase raw material with compact shining skin effect includes each component of following parts by weight: lotus flower
90 parts of water of flower, 0.4 part of Ganodenna Lucidum P.E, 0.4 part of Radix Codonopsis extract, print plus fruit seed oily 0.16 part, 0.09 part of camellia seed oil, tree peony
0.09 part of seed oil；
The preparation method of the above-mentioned composition with compact shining skin effect, include the following steps: to print plus fruit seed oil, oil tea
Seed oil, peony seed oil mixing, are added lotus flower flower water and Ganodenna Lucidum P.E, Radix Codonopsis extract, are thoroughly mixed uniformly, i.e.,
?.
Embodiment 2
The present embodiment provides a kind of delay aging drug facial mask, including base fabric and Essence, mask substrate is three stratus cloudy surfaces
Film cloth, Essence are made of A phase and B phase raw material, are specifically prepared by following parts by weight of component:
A phase includes: 2 parts of glycerol, 1.8 parts of butanediol, 0.5 part of Sodium Hyaluronate, 0.8 part of trehalose, dipotassium glycyrrhizinate
0.48 part, 0.7 part of methyl gluceth -20,0.2 part of allantoin, 0.9 part of Scleroglucan, laruyl alcohol phosphate potassium 0.08
Part, acrylic acid (ester) class/0.09 part, 0.15 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
B phase include: 0.025 part of 0.08 part of 133 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect,
0.08 part of glycerol caprylate, 0.64 part of 1,2- pentanediol
The processing step of Essence is prepared with embodiment 1.
Composition in the present embodiment B phase raw material with compact shining skin effect includes each component of following parts by weight: lotus flower
130 parts of water of flower, 1 part of Ganodenna Lucidum P.E, 1 part of Radix Codonopsis extract, print plus fruit seed oily 0.09 part, 0.16 part of camellia seed oil, peony seeds
0.16 part of oil；The preparation method of the above-mentioned composition with compact shining skin effect, referring to the operating procedure of embodiment 1.
Embodiment 3
The present embodiment provides a kind of delay aging drug facial mask, including base fabric and Essence, mask substrate is three stratus cloudy surfaces
Film cloth, Essence are made of A phase and B phase raw material, are specifically prepared by following parts by weight of component:
A phase includes: 1.6 parts of glycerol, 1.2 parts of butanediol, 0.27 part of Sodium Hyaluronate, 1.2 parts of trehalose, dipotassium glycyrrhizinate
0.3 part, 1 part of methyl gluceth -20,0.36 part of allantoin, 0.45 part of Scleroglucan, 0.12 part of laruyl alcohol phosphate potassium,
Acrylic acid (ester) class/0.1 part, 0.18 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
B phase include: 0.03 part of 0.15 part of 122 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect,
0.45 part of glycerol caprylate, 0.4 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
The composition with compact shining skin effect in the present embodiment B phase raw material includes each component of following parts by weight: lotus
120 parts of Hua Huashui, 0.8 part of Ganodenna Lucidum P.E, 0.45 part of Radix Codonopsis extract, print plus fruit seed oil 0.12 part, 0.15 part of camellia seed oil,
0.13 part of peony seed oil；The preparation method of the above-mentioned composition with compact shining skin effect, referring to the operating procedure of embodiment 1.
Embodiment 4
The present embodiment provides a kind of delay aging drug facial mask, including base fabric and Essence, mask substrate is three stratus cloudy surfaces
Film cloth, Essence are made of A phase and B phase raw material, are specifically prepared by following parts by weight of component:
A phase includes: 1 part of glycerol, 1.5 parts of butanediol, 0.36 part of Sodium Hyaluronate, 0.9 part of trehalose, dipotassium glycyrrhizinate
0.45 part, 0.8 part of methyl gluceth -20,0.27 part of allantoin, 0.8 part of Scleroglucan, laruyl alcohol phosphate potassium 0.09
Part, acrylic acid (ester) class/0.13 part, 0.3 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
B phase include: 0.045 part of 0.09 part of 102 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect,
0.06 part of glycerol caprylate, 0.45 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
The composition with compact shining skin effect in the present embodiment B phase raw material includes each component of following parts by weight: lotus
100 parts of Hua Huashui, 0.45 part of Ganodenna Lucidum P.E, 0.7 part of Radix Codonopsis extract, print plus fruit seed oil 0.15 part, 0.13 part of camellia seed oil,
0.15 part of peony seed oil；The preparation method of the above-mentioned composition with compact shining skin effect, referring to the operating procedure of embodiment 1.
Embodiment 5
The present embodiment provides a kind of delay aging drug facial mask, including base fabric and Essence, mask substrate is three stratus cloudy surfaces
Film cloth, Essence are made of A phase and B phase raw material, are specifically prepared by following parts by weight of component:
A phase includes: 1.2 parts of glycerol, 1.3 parts of butanediol, 0.3 part of Sodium Hyaluronate, 1 part of trehalose, dipotassium glycyrrhizinate
0.42 part, 0.9 part of methyl gluceth -20,0.32 part of allantoin, 0.6 part of Scleroglucan, laruyl alcohol phosphate potassium 0.1
Part, acrylic acid (ester) class/0.12 part, 0.25 part of parahydroxyacet-ophenone of C10-30 alkylol acrylamide acid esters cross-linked polymer；
B phase includes: 0.04 part of 0.1 part of 94 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect, sweet
0.05 part of oily caprylate, 0.5 part of 1,2- pentanediol.
The processing step of facial mask essence is prepared with embodiment 1.
The composition with compact shining skin effect in the present embodiment B phase raw material includes each component of following parts by weight: lotus
It is 0.1 part of 92 parts of Hua Huashui, 0.6 part of Ganodenna Lucidum P.E, 0.5 part of Radix Codonopsis extract, print plus fruit seed oil, 0.12 part of camellia seed oil, male
Red 0.11 part of seed oil；The preparation method of the above-mentioned composition with compact shining skin effect, referring to the operating procedure of embodiment 1.
Embodiment 6
Indices detection, detection are carried out to the facial mask that Examples 1 to 5 is prepared according to standard QB/T 2872-2017
As a result as follows:
(1) organoleptic indicator
Appearance: translucent liquid shape；
Fragrance: without essence addition, the natural fragrance of raw material lotus flower meet regulation fragrance.
(2) physical and chemical index
PH value (25 DEG C): 5.99；
Viscosity (2#, 6rpm): 1777mpas；
Heat-resistant stability: kept at 40 ± 1 DEG C for 24 hours, restore to after room temperature with test before no significant difference；
Cold-resistant stability: keeping for 24 hours at -8 ± 2 DEG C, after restoring to room temperature with test before no significant difference；
Photostability: it is kept under ultraviolet light for 24 hours, with no significant difference before test.
(3) hygienic chemistry index
Mask product prepared by the present invention is detected by the method for " cosmetics health specification " 2015, testing result is shown in Table 1.
Table 1
| Sanitary index | Standard requirements | Testing result | Single item evaluation |
| Total plate count, CFU/g | ≤1000 | ≤432 | It is qualified |
| Yeast and mold sum, CFU/g | ≤100 | ≤42 | It is qualified |
| Heat-resisting coliform, g | It must not detect | It is not detected | It is qualified |
| Staphylococcus aureus, g | It must not detect | It is not detected | It is qualified |
| Pseudomonas aeruginosa, g | It must not detect | It is not detected | It is qualified |
| Mercury, mg/kg | ≤1 | ≤1 | It is qualified |
| Lead, mg/kg | ≤10 | ≤4 | It is qualified |
| Arsenic, mg/kg | ≤2 | ≤2 | It is qualified |
| Cadmium, mg/kg | ≤5 | ≤4 | It is qualified |
| Methanol, mg/kg | ≤2000 | ≤468 | It is qualified |
| Dioxanes, mg/kg | ≤30 | ≤24 | It is qualified |
| Asbestos, mg/kg | It must not detect | It is not detected | It is qualified |
(4) application method
After face cleaning, facial mask of the invention is lain on the face, smooths facial mask with hand.
(5) specified risk material safety evaluation
Each raw material for preparing facial mask to the present invention carries out specified risk material security evaluation, and specific assessment result is shown in Table 2.
Table 2
7 skin irritation test of embodiment
By taking delay aging drug facial mask prepared by the method for Examples 1 to 5 as an example, delay aging drug facial mask is observed to skin
Irritation and allergic reaction provide reference to evaluate its safety.
(1) skin irritation test is carried out using rabbit, divides intact skin group and damage skin group, for 24 hours by rabbit before test
Back backbone diamond wool shaves off, and the delay aging drug facial mask and rabbit skin and mucosa prepared respectively with the embodiment of the present invention 1~5 is protected
After holding contact 1d, continuous 7d, whether there is or not the stimulate the reactions such as erythema, oedema for observation skin.
(2) skin allergy experiment is carried out using cavy, the delay aging drug face prepared with the embodiment of the present invention 1~5 weekly
Film and guinea pig skin mucous membrane are kept in contact 2 times, contact 4h or more every time, continuous 3 weeks, whether there is or not erythema, oedema to wait for observation skin
Quick reaction.
Experimental result:
The intact skin and damaged skin of rabbit, remove after being intended for single use or be used for multiple times for 24 hours, respectively at 1,24,48,
72h observation, is showed no erythema and oedema, and stimulate the reaction mean scores are < 0.5, nonirritant.
In guinea pig skin allergic experiment, does not occur the cutaneous anaphylaxises such as the obvious erythema of skin, oedema and other are systemic
Allergic reaction.
Therefore, delay aging drug facial mask of the invention will not cause irritation anti-rabbit intact skin and damage skin
It answers, to guinea pig skin without allergic reaction, there is good cutaneous safety.
Comparative example 1
The process conditions of this comparative example reference embodiment 5, the main distinction are: using deionized water substitution lotus flower flower water.
Comparative example 2
The process conditions of this comparative example reference embodiment 5, the main distinction are: the composition with compact shining skin effect is not
Containing Ganodenna Lucidum P.E.
Comparative example 3
The process conditions of this comparative example reference embodiment 5, the main distinction are: the composition with compact shining skin effect is not
Containing Radix Codonopsis extract.
Comparative example 4
The process conditions of this comparative example reference embodiment 5, the main distinction are: the composition with compact shining skin effect is not
Containing print plus fruit seed oil, camellia seed oil, peony seed oil.
Comparative example 5~8
The process conditions of 5~8 reference embodiment 5 of comparative example, the main distinction are there is the composition of compact shining skin effect
Respectively include following parts by weight of component:
Remove free radical test
Free radical test is purged to Essence prepared by Examples 1 to 5 and comparative example 1~8, and calculates its inhibition
Rate；Specific detection method is as follows: the Essence of above-described embodiment and comparative example being configured to concentration respectively with dimethyl sulfoxide
For the concentration of mass volume ratio 1%, then take sample solution 2mL and concentration for the diphenyl picryl phenylhydrazine of 100 μm of ol/L
(DPPH) solution (solvent of the solution is water) 2mL is first added in same tool plug test tube, shakes up, and stands 30 minutes at room temperature, with
Solvent is blank, measures sample absorbance under 510nm wavelength.Specific testing result is shown in Table 3.
The calculation formula of inhibiting rate (k%) is as follows:
K%=[1- (Ai-Aj)/AC] × 100%；
Wherein, Ai is the absorbance of 2mL DPPH solution+2mL sample solution；
Aj is the absorbance of 2mL D sample solution+2mL sample solvent (i.e. dimethyl sulfoxide)；
Ac is the absorbance of 2mL DPPH solution+2mL sample solvent (i.e. dimethyl sulfoxide)；
Table 3
| Inhibiting rate, % | |
| Embodiment 1 | 89.4 |
| Embodiment 2 | 93.7 |
| Embodiment 3 | 92.5 |
| Embodiment 4 | 92.2 |
| Embodiment 5 | 93.6 |
| Comparative example 1 | 88.9 |
| Comparative example 2 | 78.3 |
| Comparative example 3 | 89.5 |
| Comparative example 4 | 80.1 |
| Comparative example 5 | 79.7 |
| Comparative example 6 | 81.4 |
| Comparative example 7 | 80.5 |
| Comparative example 8 | 84.6 |
It is above-mentioned the experimental results showed that, delay aging drug facial mask of the invention can effectively inhibit the generation of free radical, and effect
Significantly.
Anti-aging evaluation test
Using total number born (SOD), glutathione peroxidase (GSH-PX), malonaldehyde (MDA) as anti-
The evaluation index of aging investigates the anti-aging effects of Examples 1 to 5 and the Essence in comparative example 1~8 respectively.
1. material and reagent
Material: SPF grades of SD rat, 180 ± 10g of weight, male female fifty-fifty.
Reagent: SOD assay kit, MDA assay kit, GSH-PX assay kit.
2. animal model constructs
The present invention is using D- gal Aging model and is aided with ultraviolet light, specifically by each group rat skin lower injection
60mg/ (kg.d) D- galactolipin, all experimental animals are injected weekly twice, and continuous seven weeks.Back hits exactly skin depilatory, exposure
2cm*2cm2Skin, test group give smear Examples 1 to 5 in Essence (4%w/w), comparative example group give smearing comparison
Essence (4%w/w), control group in example 1~8 give smearing distilled water, and all experimental animals are smeared once daily, and continuous seven
Week.
Ultraviolet light is with the following method: with the UVB lamp of 80w to each group rat in distance about 60cm place's irradiation, every
Primary, each 1h every irradiation in two days, continuous seven weeks.
After 7th week last day smeared Essence, from animal orbital venous plexus venous blood sampling, according to SOD, MDA, GSH-
PX kit illustrates to be operated, and log, and concrete outcome is shown in Table 4.
Table 4
| SOD,U/ml | MDA,nmol/ml | GSH-PX,Uml/min | |
| Embodiment 1 | 158.27±2.42** | 8.02±0.57** | 16.23±1.45** |
| Embodiment 2 | 164.15±1.37** | 7.84±1.24** | 18.12±0.64** |
| Embodiment 3 | 162.26±0.94** | 7.94±1.36** | 17.48±1.02** |
| Embodiment 4 | 168.34±0.87** | 7.75±1.12** | 19.06±0.86** |
| Embodiment 5 | 171.34±1.35** | 7.53±1.61 | 21.22±1.05** |
| Comparative example 1 | 150.36±2.51* | 8.69±1.53* | 13.32±1.40* |
| Comparative example 2 | 142.21±0.66 | 9.89±1.48 | 10.36±0.56 |
| Comparative example 3 | 150.67±1.23* | 8.45±0.55* | 13.27±1.04* |
| Comparative example 4 | 145.28±1.07 | 9.21±1.16 | 11.38±0.87 |
| Comparative example 5 | 148.34±0.64* | 9.23±1.27* | 12.02±1.13* |
| Comparative example 6 | 148.26±0.76* | 9.30±1.19* | 11.98±1.24* |
| Comparative example 7 | 153.21±1.25* | 8.52±1.68* | 14.72±1.39* |
| Comparative example 8 | 150.04±1.36* | 8.71±2.01* | 13.05±2.12* |
Note: the * P < 0.05 compared with comparative example 1,3 and comparative example 5~8, the * * P < compared with comparative example 2 and comparative example 4
0.01。
As can be seen from Table 4, for intracorporal SOD, GSH-PX activity of rat is compared with control group in Examples 1 to 5, measurement
It is worth higher, significant difference (P < 0.05), the effect in These parameters evaluation of embodiment 5 is best, extremely significant (the P < of difference
0.01).The Essence of comparative example 1~8 still has an obvious gap compared with Examples 1 to 5, and comparative example 2 and comparative example 4 with
Gap of the embodiment of the present invention is larger, especially the disparity of comparative example 2 and the embodiment of the present invention, has also confirmed ganoderma lucidum from side
Extract plays a major role, and lotus flower Hua Shui, print plus fruit seed oil, camellia seed oil, peony seed oil play synergistic effect.
Using effect experiment
The delay aging drug facial mask that above-described embodiment 1~5 and comparative example 1~8 are prepared carries out effect performance test,
Select several 30~40 years old people as volunteer, application method are as follows: after cleaning face, to take each test group of same size and right
It is pasted on face skin according to a group facial mask, gently pats and absorb, it is each using primary daily morning and evening, stick 20 every time~
30min adhered to using 2 months.Given a mark respectively to disparity items according to change of skin, disparity items include wrinkle variation,
Skin elasticity, tightening effect, skin overall condition, each project full marks are 100 points, and score value is higher, shows that effect is better.Statistics
Marking obtains final appraisal result as a result, then average.Concrete outcome is shown in Table 5.
Table 5
Experimental result is shown: delay aging drug facial mask disclosed by the invention for guiding theory prescription, is adopted with " monarch "
With rational proportion and pure natural anti-oxidant grease compatibility, it can effectively improve the oxidation resistance of skin, face skin avoided to add
Fast aging, eliminates and reduces facial wrinkles, and delay skin aging keeps skin tender flexible.
Obviously, above-described embodiment is only intended to clearly illustrate technical solution of the present invention example, and is not
Restriction to embodiments of the present invention.For those of ordinary skill in the art, on the basis of the above description also
It can make other variations or changes in different ways.There is no necessity and possibility to exhaust all the enbodiments.It is all
Made any modifications, equivalent replacements, and improvements etc. within the spirit and principles in the present invention should be included in right of the present invention and want
Within the protection scope asked.
Claims (10)
1. a kind of compact shining skin effect application of ganoderma lucidum Radix Codonopsis, which is characterized in that there is compact shining skin effect applied to preparation
Composition, the composition include each component of following parts by weight: lotus flower flower 90 ~ 130 parts of water, 0.4 ~ 1 part of Ganodenna Lucidum P.E, party
0.4 ~ 1 part of conopsea extraction, print plus 0.09 ~ 0.16 part of fruit seed oil, 0.09 ~ 0.16 part of camellia seed oil, peony seed oil 0.09 ~ 0.16
Part.
2. application according to claim 1, which is characterized in that the composition with compact shining skin effect, including with
The each component of lower parts by weight: lotus flower flower 90 ~ 120 parts of water, 0.45 ~ 0.8 part of Ganodenna Lucidum P.E, 0.45 ~ 0.7 part of Radix Codonopsis extract,
Print plus 0.09 ~ 0.12 part of fruit seed oil, 0.09 ~ 0.13 part of camellia seed oil, 0.09 ~ 0.15 part of peony seed oil.
3. application according to claim 1 or 2, which is characterized in that the composition with compact shining skin effect, including
The each component of following parts by weight: lotus flower flower 90 ~ 100 parts of water, 0.45 ~ 0.6 part of Ganodenna Lucidum P.E, 0.5 ~ 0.6 part of Radix Codonopsis extract,
Print plus 0.09 ~ 0.1 part of fruit seed oil, 0.1 ~ 0.12 part of camellia seed oil, 0.11 ~ 0.13 part of peony seed oil.
4. described in any item applications according to claim 1 ~ 3, which is characterized in that the composition with compact shining skin effect
The preparation method is as follows: print plus fruit seed oil, camellia seed oil, peony seed oil are mixed, be added lotus flower spend water and Ganodenna Lucidum P.E,
Radix Codonopsis extract, be thoroughly mixed uniformly to get；Wherein, the Ganodenna Lucidum P.E, Radix Codonopsis extract are by ganoderma lucidum, Radix Codonopsis
The extracting solution being obtained by filtration is extracted through boiling respectively.
5. a kind of delay aging drug facial mask, which is characterized in that containing described in any one of claim 1 ~ 4 have compact shining skin effect
Composition.
6. delay aging drug facial mask according to claim 5, which is characterized in that including base fabric and Essence, the facial mask base
Cloth is three stratus mist facial mask cloths, contains the group described in any one of claim 1 ~ 4 with compact shining skin effect in the Essence
Close object.
7. delay aging drug facial mask according to claim 6, which is characterized in that the Essence is by A phase and B phase raw material system
At comprising having the composition of compact shining skin effect described in any one of claim 1 ~ 4 in the B phase raw material；
The A phase include: 0.9 ~ 2 part of glycerol, 0.95 ~ 1.8 part of butanediol, 0.25 ~ 0.5 part of Sodium Hyaluronate, trehalose 0.8 ~
1.5 parts, 0.27 ~ 0.48 part of dipotassium glycyrrhizinate, 0.7 ~ 1.3 part of methyl gluceth -20,0.2 ~ 0.5 part of allantoin, small nut
0.4 ~ 0.9 part of bacterium glue, 0.08 ~ 0.15 part of laruyl alcohol phosphate potassium, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters crosslinking
0.09 ~ 0.15 part of polymer, 0.15 ~ 0.4 part of parahydroxyacet-ophenone；
The B phase includes: 0.08 ~ 0.2 part of 90 ~ 133 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect
0.025 ~ 0.048 part, 0.04 ~ 0.08 part of glycerol caprylate, 0.36 ~ 0.64 part of 1,2- pentanediol.
8. delay aging drug facial mask described according to claim 6 or 7, which is characterized in that the A phase include: 1 ~ 1.6 part of glycerol,
1.2 ~ 1.5 parts of butanediol, 0.27 ~ 0.36 part of Sodium Hyaluronate, 0.9 ~ 1.2 part of trehalose, 0.3 ~ 0.45 part of dipotassium glycyrrhizinate, first
- 20 0.8 ~ 1 parts of base glucitol polyethers, 0.27 ~ 0.36 part of allantoin, 0.45 ~ 0.8 part of Scleroglucan, laruyl alcohol phosphate potassium
0.09 ~ 0.12 part, acrylic acid (ester) class/0.1 ~ 0.13 part of C10-30 alkylol acrylamide acid esters cross-linked polymer, parahydroxyacet-ophenone
0.18 ~ 0.3 part；
The B phase includes: 0.09 ~ 0.15 part of 91 ~ 102 parts of composition, arginine, decoyl hydroximic acid with compact shining skin effect
0.03 ~ 0.04 part, 0.05 ~ 0.06 part of glycerol caprylate, 0.45 ~ 0.55 part of 1,2- pentanediol.
9. according to any one of the claim 5 ~ 8 delay aging drug facial mask, which is characterized in that the preparation method of the Essence
The following steps are included:
S1. above-mentioned A phase raw material is sequentially added in water phase pot, stirring is warming up to 80 ~ 90 DEG C, stirs, and keeps the temperature spare；
S2. after mixing evenly, homogeneous 1 ~ 10 minute, vacuumizes, and constant temperature 10 ~ 20 minutes；
When being S3. cooled to 40 ~ 45 DEG C, above-mentioned B phase raw material is sequentially added, stirs, every a raw material of addition, stirring is extremely
A raw material under adding again after dissolution；
When being S4. cooled to 32 ~ 38 DEG C, discharging is stood to get the Essence.
10. delay aging drug facial mask according to claim 9, which is characterized in that in step S2, the homogenizing time is 2 ~ 5
Minute；Preferably, the homogenizing time is 3 minutes.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115778865A (en) * | 2022-12-30 | 2023-03-14 | 水羊化妆品制造有限公司 | Fluid face cream and preparation method thereof |
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| CN104305180A (en) * | 2014-10-09 | 2015-01-28 | 张璧云 | Edible and applicable ingredient |
| CN105411960A (en) * | 2015-12-30 | 2016-03-23 | 广州环亚化妆品科技有限公司 | Mask with acne inhibition effect and preparation method thereof |
| CN107233263A (en) * | 2017-08-04 | 2017-10-10 | 遵义医学院 | A kind of Radix Codonopsis sleep mask and preparation method thereof |
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| CN101966141A (en) * | 2010-10-14 | 2011-02-09 | 珈侬生化科技(中国)有限公司 | Composite containing ginseng extracts and ganoderma extracts and application thereof |
| CN104305180A (en) * | 2014-10-09 | 2015-01-28 | 张璧云 | Edible and applicable ingredient |
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Application publication date: 20190329 |