CN106726683A - A kind of Multifunctional mask liquid and its preparation technology - Google Patents

A kind of Multifunctional mask liquid and its preparation technology Download PDF

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Publication number
CN106726683A
CN106726683A CN201611238698.6A CN201611238698A CN106726683A CN 106726683 A CN106726683 A CN 106726683A CN 201611238698 A CN201611238698 A CN 201611238698A CN 106726683 A CN106726683 A CN 106726683A
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CN
China
Prior art keywords
mask liquid
multifunctional mask
buffer
multifunctional
superoxide dismutase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
CN201611238698.6A
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Chinese (zh)
Inventor
夏国顺
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Anhui Tan Xin Technology Co Ltd
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Anhui Tan Xin Technology Co Ltd
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Application filed by Anhui Tan Xin Technology Co Ltd filed Critical Anhui Tan Xin Technology Co Ltd
Priority to CN201611238698.6A priority Critical patent/CN106726683A/en
Publication of CN106726683A publication Critical patent/CN106726683A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/66Enzymes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

Abstract

The invention belongs to cosmetic technical field, the problems such as in order to solve skin water shortage, sunburn and age mark, the invention provides a kind of Multifunctional mask liquid and its preparation technology, mainly it is made up of following components and its mass fraction:Superoxide dismutase 0.2 ‰ 1 ‰, Isin glue collagen 0.8% 3%, hyaluronic acid 0.5% 2%, edible preservative 0.1 ‰ 0.8 ‰, glycerine 5 20%, pH buffer 0.1 2% and water 75 95%.There are moisturizing, anti-aging, the good effects such as nti-freckle in the facial mask liquid, and facial mask composition is all edible, and safety coefficient is high, and effect is good.

Description

A kind of Multifunctional mask liquid and its preparation technology
Technical field
The present invention relates to cosmetic field, and in particular to a kind of Multifunctional mask liquid and its preparation technology.
Background technology
With advancing age, skin histology can slowly degenerate, and main cause has the old of natural cause and non-natural factor Change, such as human skin keratinocyte's oxidation, for a long time in face of computer screen, smoke, expose to the open air in the environment of air pollution, have not enough sleep, Will allow generation free radical, make skin aging;Dry skin caused by water shortage;And color spot caused by precipitation of colored materials;Make Breath is abnormal to cause body metabolism ability to decline, and influence melanin is generated and metabolism, the reduction of epidermis maintenance ability.Skin is hindered Evil is nearly ubiquitous in living now.Currently for skin problem, skin care item on the market are more and more, and wherein facial mask is Most effective fruit skin care item.
Notification number discloses a kind of preparation of the toner containing superoxide dismutase for the Chinese patent of 101732172B Method, although the superoxide dismutase of addition plays a role to anti-aging, due to the activity that toner is carried Component is few, and is easy to run off, and the composition that active component is really absorbed to inside skin is few, does not reach real skin effect, needs Further to improve, it is to avoid the loss of activearm component.
Notification number discloses a kind of hydrosol moisture saver mask and preparation method thereof for the Chinese patent of CN102935055B, and it is Hydrosol with moisture-keeping efficacy is put into a container, then by hyaluronic acid, Isin glue collagen, water soluble vitamin and bay Sour Modified Superoxide Dismutase is added in container, stirring, until being completely dissolved;Again by extract solution from aloe and Jie Ma BP preservatives In addition solution, and stir, the liquid of gained is uniformly added dropwise on ground non-woven fabrics facial mask.The outstanding horse BP that the patent is used prevents Rotten agent easily makes allergic, long-term use facial mask injury skin, and effect is unstable.
The content of the invention
In order to solve the deficiency of prior art presence, the invention discloses a kind of Multifunctional mask liquid and its preparation technology, The facial mask has preferable moisturizing freckle effect, and the component part for using is that life entity exists in itself, and a part is Edible, harmless component, safety coefficient are high.
A kind of Multifunctional mask liquid that the present invention is provided, key component:It is superoxide dismutase, Isin glue collagen, transparent Matter acid, glycerine, edible preservative, pH buffer and water;Hyaluronic acid CAS.9004-61-9.
Further, described Multifunctional mask liquid, is mainly made up of following components and its mass fraction:Superoxides discrimination Change enzyme 0.2 ‰ -1 ‰, Isin glue collagen 0.8%-3%, hyaluronic acid 1%-3%, edible preservative 0.1 ‰ -0.8 ‰, sweet Oily 5-20%, pH buffer 0.1-2% and water 75-95%.
Preferably, described Multifunctional mask liquid, is made up of following components and its mass fraction:Superoxide dismutase 0.5 ‰, Isin glue collagen 1%, hyaluronic acid 2%, edible preservative 0.3 ‰, glycerine 10%, pH buffer 1% and water 85.92%.
Further, described edible preservative is the one kind in sodium dehydroacetate, calcium propionate and Nisin.
Preferably, described edible preservative is sodium dehydroacetate.
Further, described pH buffer is citric acid, potassium hydroxide, lactic acid, sodium citrate, sodium lactate and glycine In one kind.
Preferably, described pH buffer is the one kind in citric acid, potassium hydroxide and glycine.
Further, described pH buffer is glycine.
Present invention also offers the preparation technology of described Multifunctional mask liquid, step is as follows:
S1, with after water dissolves glycerine, 105-120 DEG C of high-temperature sterilization, after cooling glycerite A;
S2, superoxide dismutase, Isin glue collagen, hyaluronic acid, edible preservative are added in step S1 To glycerite A in, heating, stir to being completely dissolved, obtain mixed liquid B;
S3, the mixed liquid B that step S2 is obtained is cooled to 25-35 DEG C, adds pH buffer to adjust pH to 5.0-6.0, stir Mix uniform, obtain final product.
Further, in described Multifunctional mask liquid preparing process, step S2 mixing speeds are 40-50r/min, heating Temperature is 65-80 DEG C.
Superoxide dismutase (SOD, CAS.9054-89-1) is antioxidase important in organism, is distributed widely in In the organisms such as animal, plant, microorganism.SOD has special physiologically active, is the primary thing that free radical is removed in organism Matter.SOD level height in vivo means the index directly perceived of aging and death, and it can be resisted with blocking because of oxygen radical The infringement caused to cell, and damaged cell is repaired in time, restore caused by free radical to the injury of cell.Due to the modern life Pressure, environmental pollution, various radiation and excess motion can all cause oxygen radical largely to be formed;Therefore, biological antioxidant mechanism The status of middle SOD is more and more important.
Hyaluronic acid (CAS.99004-61-9)) it is a kind of acid mucopolysaccharide, the preferable water retention of hyaluronic acid, the mankind Skin maturation and ageing process change also with content and the metabolism of hyaluronic acid, and it can improve skin-nourishing generation Thank, make that skin is tender, smooth, go to wrinkle, increase elasticity, prevent aging, be again good Transdermal absorption promotion while moisturizing Agent, with other compositions with sharing, promotes ingredient draws.
Compared with prior art, the invention has the advantages that:
Preferable moisture-retaining capacity:Containing abundant hyaluronic acid in Multifunctional mask, using supplementing moisture of skin after facial mask, Moisturizing elite can be pinned with deep layer;
Nti-freckle ability:Contain superoxide dismutase, dispel Skin Cell free radical, prevent color spot from being formed, protect skin Hold younger state;
Security:A component part is to be directly present in organism in Multifunctional mask, and another part is grade-safe Composition, it is ensured that the security of Multifunctional mask.
Specific embodiment
Below to further detailed description of the invention, with make those skilled in the art with reference to specification word can be according to this Implement, present component belongs to conventional products, wherein, Isin glue collagen (CAS.9064-67-9):Wuhan is remote to be had into creating science and technology Limit company.
Embodiment 1
A kind of Multifunctional mask liquid, is made up of following component and its mass fraction:Superoxide dismutase 0.5 ‰, fish glue Former albumen 1%, hyaluronic acid 2%, edible preservative sodium dehydroacetate 0.3 ‰, glycerine 10%, pH buffer glycine 1% With water 85.92%.
The preparation technology of Multifunctional mask liquid is as follows in the present embodiment:
S1, use water dissolves glycerine, 110 DEG C of high-temperature sterilizations, after cooling glycerite A;
S2, superoxide dismutase, Isin glue collagen, hyaluronic acid, edible preservative are added in step S1 To glycerite A in, after being heated to 70 DEG C stir, mixing speed is 45rpm, until being completely dissolved, obtains mixed liquid B;
S3, the mixed liquid B that step S2 is obtained is cooled to 30 DEG C, adds pH buffer to adjust pH value of solution to 5.6, stirring is equal It is even, obtain final product.
Embodiment 2
A kind of Multifunctional mask liquid, is made up of following component and its mass fraction:Superoxide dismutase 0.2 ‰, fish glue Former albumen 3%, hyaluronic acid 1%, edible preservative calcium propionate 0.1 ‰, glycerine 20%, pH buffer citric acid 2% and water 73.97%.
The preparation technology of described Multifunctional mask liquid is similar to Example 1.
Embodiment 3
A kind of Multifunctional mask liquid, is made up of following component and its mass fraction:Superoxide dismutase 1 ‰, collagen Albumen 0.8%, hyaluronic acid 3%, edible preservative Nisin 0.8 ‰, glycerine 5%, pH buffer potassium hydroxide 0.1% With water 90.92%.
The preparation technology of described Multifunctional mask liquid is similar to Example 1.
Comparative example 1
A kind of Multifunctional mask liquid, is made up of following component and its mass fraction:Isin glue collagen 1%, hyaluronic acid 2%th, edible preservative sodium dehydroacetate 0.3 ‰, glycerine 10%, pH buffer glycine 1% and water 85.97%.
It is, without superoxide dismutase, to increase the content of water in being formulated with the difference of embodiment 1;
The preparation technology of described facial mask liquid is similar to Example 1.
Comparative example 2
A kind of Multifunctional mask liquid, is made up of following component and its mass fraction:Superoxide dismutase 0.5 ‰, fish glue Former albumen 1%, edible preservative sodium dehydroacetate 0.3 ‰, glycerine 12%, pH buffer glycine 1% and water 85.92%.
It is, without hyaluronic acid, to increase the content of glycerine in being formulated with the difference of embodiment 1;
The preparation technology of described many facial mask liquids is similar to Example 1.
The moisturizing moisturizing effect of test example 1
Experiment facial mask:One silk film cloth is immersed into 25mL Multifunctional masks liquid (Multifunctional mask prepared by embodiment 1-3 Liquid, facial mask liquid prepared by comparative example 1-2), facial mask is obtained.
Subjects:Each 25 people of men and women, random point 5 groups, every group uses a kind of facial mask.
Test method:The moisture for testing forehead, left face, right face and chin skin respectively using skin moisture detector contains Amount, and takes arithmetic mean of instantaneous value, respectively test using after preceding, first time use, the continuous facial moisture using after 60 days.Survey Test result such as table 1 below.
The moisture result table of table 1
Skin moisture content Using preceding After first time use Continuously using after 60 days
Embodiment 1 20.1% 29.8% 29.6%
Embodiment 2 20.3% 29.1% 29.0%
Embodiment 3 20.5% 29.3% 29.2%
Comparative example 1 20.4% 25.4% 24.8%
Comparative example 2 20.3% 25.2% 23.5%
The replenishing water and preserving moisture effect of the Multifunctional mask liquid for being prepared using embodiment 1-3 as can be seen from Table 1 is become apparent from, its Multifunctional mask liquid replenishing water and preserving moisture best results prepared by middle embodiment 1, illustrate that Multifunctional mask moisturizing disclosed by the invention is protected Wet effect is good, and still fine using moisturizing effect after 60 days.
The sunburn of test example 2 is dispelled
Subjects:Male 25 people, the people of female 25 is randomly divided into 5 groups, every group of 10 people.
Age:25~35 years old.
Health status:Skin has sunburn, without skin disease allergies, meets subject's aspiration inclusion criteria.
Test method:Every 5 days use a facial mask, used before sleeping, each use time be 15 minutes, using 15 times after, Record result of variations, every group is only used a kind of facial mask, and concrete outcome is as shown in table 2.
The sunburn freckle effect test result of table 2
Use Multifunctional mask species Sunburn dispels effect
Embodiment 1 It is very good
Embodiment 2 It is very good
Embodiment 3 It is very good
Comparative example 1 It is medium
Comparative example 2 It is medium
" very good " represents that sunburn is wholly absent or spot only stays slight trace, and speck area reduces more than 90%;" in Deng " represent it is effective, but spot or it is obvious that speck area reduce 50-90%, from Table 2, it can be seen that the present invention implement Example 1-3 compared to comparative example 1-2 have preferably dispel sunburn effect.
The age mark of test example 3 is dispelled
Subjects:Male 25 people, the people of female 25 is randomly divided into 5 groups, every group of 10 people.
Age:40~50 years old.
Health status:Skin has age mark, without skin disease allergies, meets subject's aspiration inclusion criteria.
Test method:Every 5 days use a facial mask, used before sleeping, each use time be 15 minutes, using 15 times after, Record result of variations, every group is only used a kind of facial mask.Result is as shown in table 3.
The age mark freckle effect test result of table 3
Sunburn dispels effect Age mark dispels effect
Embodiment 1 It is excellent
Embodiment 2 It is excellent
Embodiment 3 It is excellent
Comparative example 1 Typically
Comparative example 2 Typically
" excellent " represents that age mark is wholly absent or spot only stays slight trace, and speck area reduces more than 70%;" general " Represent it is effective, but spot or it is obvious that speck area reduce 30-70%.
It is fine that the age mark of the Multifunctional mask liquid for being prepared using embodiment 1-3 as can be seen from Table 3 dispels effect.
In sum, Multifunctional mask disclosed by the invention has preferable replenishing water and preserving moisture and spot-removing function.
The above-described embodiments merely illustrate the principles and effects of the present invention, not for the limitation present invention.It is any ripe The personage for knowing this technology all can carry out modifications and changes under without prejudice to spirit and scope of the invention to above-described embodiment.Cause This, those of ordinary skill in the art is complete with institute under technological thought without departing from disclosed spirit such as Into all equivalent modifications or change, should be covered by claim of the invention.

Claims (8)

1. a kind of Multifunctional mask liquid, it is characterised in that be mainly made up of following components and its mass fraction:Superoxide dismutase Enzyme 0.2 ‰ -1 ‰, Isin glue collagen 0.8%-3%, hyaluronic acid 1%-3%, edible preservative 0.1 ‰ -0.8 ‰, glycerine 5-20%, pH buffer 0.1-2% and water 75-95%.
2. Multifunctional mask liquid according to claim 1, it is characterised in that be made up of following components and its mass fraction: Superoxide dismutase 0.5 ‰, Isin glue collagen 1%, hyaluronic acid 2%, edible preservative 0.3 ‰, glycerine 10%, pH delay Electuary 1% and water 85.92%.
3. Multifunctional mask liquid according to claim 1 and 2, it is characterised in that described edible preservative is dehydrogenation One kind in sodium acetate, calcium propionate and Nisin.
4. Multifunctional mask liquid according to claim 3, it is characterised in that described edible preservative is dehydroacetic acid Sodium.
5. Multifunctional mask liquid according to claim 1 and 2, it is characterised in that described pH buffer is citric acid, hydrogen One kind in potassium oxide, lactic acid, sodium citrate, sodium lactate and glycine.
6. Multifunctional mask liquid according to claim 5, it is characterised in that described pH buffer is citric acid, hydrogen-oxygen Change the one kind in potassium and glycine.
7. the preparation technology of the Multifunctional mask liquid according to claim any one of 1-6, it is characterised in that step is as follows:
S1, with after water dissolves glycerine, 105-120 DEG C of high-temperature sterilization, after cooling glycerite A;
S2, superoxide dismutase, Isin glue collagen, hyaluronic acid, edible preservative are added to what is obtained in step S1 In glycerite A, heating, stirring obtain mixed liquid B to being completely dissolved;
S3, the mixed liquid B that step S2 is obtained is cooled to 25-35 DEG C, adds pH buffer regulation pH to 5.0-6.0, stirring is equal It is even, obtain final product.
8. Multifunctional mask liquid preparing process according to claim 7, it is characterised in that step S2 mixing speeds are 40- 50r/min, heating-up temperature is 65-80 DEG C.
CN201611238698.6A 2016-12-28 2016-12-28 A kind of Multifunctional mask liquid and its preparation technology Withdrawn CN106726683A (en)

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Application Number Priority Date Filing Date Title
CN201611238698.6A CN106726683A (en) 2016-12-28 2016-12-28 A kind of Multifunctional mask liquid and its preparation technology

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375045A (en) * 2017-08-02 2017-11-24 万允志 Edible delicious food cosmetics of the All Pure Nature without any chemical addition agent

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102935055A (en) * 2012-12-04 2013-02-20 深圳市妍倩科技有限公司 Hydrolat moisturizing facial mask

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102935055A (en) * 2012-12-04 2013-02-20 深圳市妍倩科技有限公司 Hydrolat moisturizing facial mask

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
徐阳等: "《化妆品质量检验》", 30 June 2016, 中国质检出版社 *
李安平等: "《食品添加剂原理与安全使用》", 30 September 2011, 国防科技大学出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375045A (en) * 2017-08-02 2017-11-24 万允志 Edible delicious food cosmetics of the All Pure Nature without any chemical addition agent

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