Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of antiallergic cosmetic water containing Folium Artemisiae Argyi extract and preparation method thereof.Antiallergic cosmetic water provided by the invention has antiallergic, antiinflammatory, effect of Lavender Extract, and gentle pro-skin is safe and non-stimulating, effective moisturizing, moisturizing, skin water is moistened smooth, flexible, can life-time service.
The present invention is by following technical solution to realize above-mentioned purpose:
A kind of antiallergic cosmetic water containing Folium Artemisiae Argyi extract, it is characterized in that, described cosmetic water is made up of the raw material of following weight percent meter: propylene glycol 2 ~ 5%, pyrrolidone sodium carboxylate 2 ~ 5%, glycerol 2 ~ 5%, Folium Artemisiae Argyi extract 2 ~ 4%, hyaluronate sodium 0.05 ~ 0.15%, Flos Lonicerae extractive solution 1 ~ 2%, menthol 0.01 ~ 0.05%, GelfestCH400.1 ~ 0.2%, chamomile essential oil 0.05 ~ 0.1%, and surplus is water.
Preferably, the described antiallergic cosmetic water containing Folium Artemisiae Argyi extract is made up of the raw material of following weight percent meter: propylene glycol 4%, pyrrolidone sodium carboxylate 4%, glycerol 4%, Folium Artemisiae Argyi extract 4%, hyaluronate sodium 0.1%, Flos Lonicerae extractive solution 2%, menthol 0.02%, GelfestCH400.2%, chamomile essential oil 0.08%, surplus is water.
Present invention also offers the preparation method of the above-mentioned antiallergic cosmetic water containing Folium Artemisiae Argyi extract, specifically comprise the following steps:
S1. by hyaluronate sodium and glycerol, add in agitated kettle, stir, add water, be heated to 40 ~ 50 DEG C, be stirred to hyaluronic acid and dissolve completely, cooling, for subsequent use;
S2. get menthol, chamomile essential oil mixes with GelfestCH40, fully stir, add propylene glycol, homogenizing 10-15min, then join in the agitated kettle of S1, stirring and evenly mixing;
S3. finally in agitated kettle, add Folium Artemisiae Argyi extract, Flos Lonicerae extractive solution and pyrrolidone sodium carboxylate, be stirred to system even, get final product discharging, obtained cosmetic water.
Further, the preparation method of described Folium Artemisiae Argyi extract is: get Folium Artemisiae Argyi, wash away impurity, crushed after being dried, cross 80-100 mesh sieve, adding medical material gross weight 8-10 times amount volume fraction is the ethanol of 60-80%, then adds the cellulase of medical material total amount 0.8-1.2%, lixiviate 2-3 hour at 40-45 DEG C, then at 80-90 DEG C of reflux, extract, 3-5 hour, filter, at filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05-1.15, obtains Folium Artemisiae Argyi extract.
Further, the preparation method of described Flos Lonicerae extractive solution is: extracting honeysuckle, pulverizes after cleaning, drying, and add Flos Lonicerae weight 4-8 water soaking 1-2 hour doubly, reflux, extract, 2-3 time, each 3-4 hour, filter, merging filtrate, obtains Flos Lonicerae extractive solution.
Folium Artemisiae Argyi extract of the present invention contain abundant volatile oil, flavonoid, triterpenes, by leaf alkanes like, trace element and the composition such as tannin, polysaccharide, its active component is mainly volatile oil and flavonoid, has antiallergic, antibacterial, calm grade for effect.Skin blood circulation can be promoted, improve the colour of skin, reduce the sensitivity of skin, Lavender Extract.
Described Flos Lonicerae extractive solution contains the compositions such as abundant procyanidin, bisflavone, polyphenol, organic acid, its active component is mainly chlorogenic acid and Luteolin, these compositions are except having antiinflammatory, antianaphylactic effect, also there is rapid osmotic and enter skin, mutual induction between active cell, dredge facial microcirculation, the function of reformation skin structure of fibrous tissue.By reducing free radical damage, to repair and filling is subsided, making skin obtain pile up similar to original structure, recovering skin compactness, thus reach and unfold coarse groove, desalination microgroove, the maintenance appearance youth is not old.
The main chemical compositions of described chamomile essential oil is sobrerone or pinene, camphene, sabinene, myrcene, eucalyptole, dipentene terpinene, Dianthus chinensis (terpene) alkene.Can alleviate anxiety, anxiety, indignation and frightened, people is loosened, soul is tranquil, has antiallergic and calm effect to skin, calms down broken the blood capillary of breaking, and enhancement elasticity of skin, the skin of easily itching to drying is splendid.
Therefore, compared with prior art, advantage of the present invention is:
(1) show in the test of product effect assessment, the present invention contain Folium Artemisiae Argyi extract, Flos Lonicerae extractive solution and chamomile essential oil three kinds of compositions in the antiallergic cosmetic water formula of Folium Artemisiae Argyi extract play antiallergic, antiinflammatory and calmness play collaborative effect on, the cosmetic water effect antiallergic simultaneously containing these three kinds of natural components, antiinflammatory, calm effect are best.In addition, the menthol that with the addition of trace in formula has the effect of refrigerant, antipruritic, antiinflammatory and promotion Transdermal absorption, increase the good opinion that consumer uses, in addition, the basic materials such as the glycerol added in formula, propylene glycol, hyaluronate sodium, GelfestCH40, the efficacy exertion of cosmetic water of the present invention is stablized, is easily absorbed by the skin, can life-time service.
(2) the present invention contains the antiallergic cosmetic water safety and stability of Folium Artemisiae Argyi extract, gentle pro-skin, does not stimulate, and skin easily absorbs, and uses rear face salubrious not sticky; And the cost of material that the present invention contains the antiallergic cosmetic water of Folium Artemisiae Argyi extract is low, preparation method is simple, and condition is controlled, process stabilizing, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, antiallergic cosmetic water of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
The information such as the producer containing part material in the antiallergic cosmetic water of Folium Artemisiae Argyi extract described in the embodiment of the present invention and article No. are as follows:
Raw material and the proportioning (by weight percentage) of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 3 antiallergic cosmetic water are as follows:
The preparation method of the antiallergic cosmetic water of the embodiment of the present invention 1 ~ 3 containing Folium Artemisiae Argyi extract is as follows:
S1. by hyaluronate sodium and glycerol, add in agitated kettle, stir, add water, be heated to 45 DEG C, be stirred to hyaluronic acid and dissolve completely, cooling, for subsequent use;
S2. get menthol, chamomile essential oil mixes with GelfestCH40, fully stir, add propylene glycol, homogenizing 10min, then join in the agitated kettle of S1, stirring and evenly mixing;
S3. finally in agitated kettle, add Folium Artemisiae Argyi extract, Flos Lonicerae extractive solution and pyrrolidone sodium carboxylate, be stirred to system even, get final product discharging, obtained cosmetic water.
Wherein, the preparation method of described Folium Artemisiae Argyi extract is: get Folium Artemisiae Argyi, wash away impurity, crushed after being dried, cross 100 mesh sieves, adding medical material gross weight 10 times amount volume fraction is the ethanol of 75%, then adds the cellulase of medical material total amount 1.0%, lixiviate 3 hours at 45 DEG C, then 90 DEG C of reflux, extract, 4 hours, filter, at filtrate reduced in volume to 60 DEG C, relative density is the extractum of 1.05, obtains Folium Artemisiae Argyi extract.
Wherein, the preparation method of described Flos Lonicerae extractive solution is: extracting honeysuckle, pulverizes after cleaning, drying, adds the water soaking 2 hours of Flos Lonicerae weight 6 times, reflux, extract, 3 times, each 3 hours, and filter, merging filtrate, obtains Flos Lonicerae extractive solution.
Meet the pertinent regulations requirement of QB/T1857-2013 through inspection embodiment 1 ~ 3 product, sense index (color and luster, fragrance, structure) meets industry regulation, and physical and chemical index (pH, heat-resisting, cold-resistant, active matter) meets industry regulation.
The preparation method of the preparation method reference embodiment of the present invention of comparative example 1 ~ 3.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, trial target: the antiallergic cosmetic water containing Folium Artemisiae Argyi extract that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare.
Two, tested crowd's data and grouping: 360 routine skin healths, the tested volunteer of the women without dermatosis allergies, 25 ~ 55 years old, 35 years old mean age, is divided into 6 groups at random, often organizes 60 people.
Three, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.015mL ~ 0.030mL drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Four, experimental result: human skin patch result shows: each group experimenter is by the patch test of the antiallergic cosmetic water of embodiment 1 ~ 3, comparative example 1 ~ 3, dermoreaction is observed at 0.5,6,12,24,48 hour, there is skin adverse reaction in equal nothing, the antiallergic cosmetic water use safety containing Folium Artemisiae Argyi extract described in explanation.
test example two, product effect assessment
One, trial target: the antiallergic cosmetic water containing Folium Artemisiae Argyi extract that embodiment 1 ~ 3, comparative example 1 ~ 3 prepare.
Two, tested crowd's data and grouping: 360 routine skin healths, the tested volunteer of the women without dermatosis allergies, 25 ~ 55
In year, 35 years old mean age, be divided into 6 groups at random, often organize 60 people.
Three, method of testing: experimenter uses Fes Kai Er SK-III skin moisture detector to test the moisture of forehead, left face, right face and chin skin respectively after using clean water face, and get arithmetic mean of instantaneous value, experimenter re-uses above-mentioned crease-resistant cosmetic water, uniform application is in face, pat gently, by the skin moisture content of skin moisture tester test forehead, left face, right face and the same position of chin after 30min, and get arithmetic mean of instantaneous value, re-use skin moisture tester after 6h and test one time.Often organize 10 experimenters and tested result is got arithmetic mean of instantaneous value.
Four, test result is as following table 1.
Wherein, skin average moisture before skin average moisture-use cosmetic water is used after cosmetic water 30min after skin moisture content gradient=use cosmetic water 30min;
To use after cosmetic water 6h after skin moisture content gradient=use cosmetic water 6h skin average moisture before skin average moisture-use cosmetic water.
Table 1 uses the test result of the skin moisture content after containing the antiallergic cosmetic water of Folium Artemisiae Argyi extract
From upper table 1: after the antiallergic cosmetic water 30min using embodiment 1 ~ 3 obtained, can not only skin moisture content be significantly improved, also can pin moisture, make skin keep long-acting water to moisten, still keep good water supplement function after 6h.And use the moisturizing that the obtained antiallergic cosmetic water of comparative example 1 ~ 3 produces, moistening effect is not as good as embodiment 1 ~ 3, illustrate and use antiallergic cosmetic water of the present invention can pin moisture of skin well, keep skin beauty water profit, and the antiallergic cosmetic water of comparative example 1,2 lacks Flos Lonicerae extractive solution in antiallergic cosmetic water formula of the present invention and chamomile essential oil respectively, its result of use all not as embodiment 1 ~ 3, in addition, comparative example 3 cosmetic water for want of solubilizing agent GelfestCH40, its result of use is the poorest.Above result shows, antiallergic cosmetic water formula of the present invention is not obtained by the simple combination of each component, then further illustrates between each component of formula of the present invention and there is synergism.As can be seen here, antiallergic cosmetic water of the present invention has the effect increasing skin elasticity, moisturizing moisturizing.
part II:
One, trial target: the antiallergic cosmetic water containing Folium Artemisiae Argyi extract prepared by embodiment 1 ~ 3, comparative example 1 ~ 3.
Two, tested crowd's data and grouping: 360 routine skin healths, the tested volunteer of the women without dermatosis allergies, 30 ~ 55 years old, 30 years old mean age, is divided into 6 groups at random, often organizes 60 people.
Three, method of testing: respectively use-case 1 ~ 3, antiallergic cosmetic water prepared by comparative example 1 ~ 3, observes and experiences result of use.Using method: after experimenter cleans face, by above-mentioned cosmetic water uniform application in face, pats gently to skin and all absorbs, the every day of each use sooner or later once, adhere to use one month, at least check weekly once to understand with or without whole body and local untoward reaction, and itemized record result.
Four, testing evaluation result is as follows:
(one month) on probation feedback conclusive table of table 2 embodiment 1 antiallergic cosmetic water
(one month) on probation feedback conclusive table of table 3 embodiment 2 antiallergic cosmetic water
(one month) on probation feedback conclusive table of table 4 embodiment 3 antiallergic cosmetic water
(one month) on probation feedback conclusive table of table 5 comparative example 1 antiallergic cosmetic water
(one month) on probation feedback conclusive table of table 6 comparative example 2 antiallergic cosmetic water
(one month) on probation feedback conclusive table of table 7 comparative example 3 antiallergic cosmetic water
From upper table 2 ~ 7, the gentle pro-skin of the antiallergic cosmetic water of embodiment 1 ~ 3, easily to absorb, replenishing water and preserving moisture Be very effective, the sensitivity of skin can be reduced after using, to skin, there is good antiallergic, antiinflammatory and sedation.Wherein the degree of recognition of embodiment 1 antiallergic cosmetic water is the highest, and therefore embodiment 1 is preferred embodiment.And comparative example 1 ~ 3 cosmetic water all lacks some component in antiallergic cosmetic water formula of the present invention, the effect of its antiallergic antiinflammatory, replenishing water and preserving moisture, all not as embodiment 1 ~ 3, illustrates that formula components of the present invention is worked in coordination with mutually, plays better effect.Therefore, the gentle safety of antiallergic cosmetic water of the present invention, can life-time service.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.