CN103893065B - De-etiolation lightening compositions and its preparation method and application - Google Patents
De-etiolation lightening compositions and its preparation method and application Download PDFInfo
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Abstract
The present invention discloses a kind of de-etiolation lightening compositions and its preparation method and application, and described de-etiolation lightening compositions comprises hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119, Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, formula Seaweed Extract difficult to understand, PEG-4000, niacinamide, neutralizing agent, wetting Agent for Printing Inks and deionized water. Above-mentioned de-etiolation lightening compositions is by Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, ramie extract combination together, mutually promote between each composition, collaborative performance effect, the formation of effective check melanin, make skin dark yellow, obscure recover pale, reach better de-etiolation whitening effect.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to de-etiolation lightening compositions and its preparation method and application.
Background technology
With the quickening pace of modern life, economic fast growth, the operating pressure of people is also increasing, adds the irregular of rest so that skin is old and feeble too early, various skin problem occurs. Spot as long in skin, flavescence, dimmed. These skin problems have seriously perplexed the psychology of liking to be beautiful of the personage that likes to be beautiful. In recent years, people are finding fast always, skin skin care products effective, efficient, and facial mask becomes first-selected undoubtedly.
The principle of facial mask, utilize the of short duration time covering face exactly, the air in the temporarily isolation external world and pollution, improving skin temperature, the pore expansion of skin, promotes sweat gland secretion and metabolism, the oxygen level of skin is made to increase, being conducive to skin to get rid of the oil substances of the metabolic product of epidermic cell and accumulation, the moisture content in facial mask infiltrates the stratum corneum of skin epidermis, and skin becomes soft. Effective constituent in facial mask can continue to enter epiderm skin fast, and skin is better absorbed.
But, the big multicomponent of the facial mask in existing market is single, and effect is not obvious. More notably produce side effect, produce anaphylaxis.
Summary of the invention
Based on this, it is necessary to provide a kind of can de-etiolation whitening and the de-etiolation cleawhite pack that has no side effect and its preparation method and application.
A kind of de-etiolation lightening compositions, by weight, comprises following component:
Wherein in an embodiment, the weight ratio of described Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract and Ramie Root extract is 8-10:2-5:1-3.
Wherein in an embodiment, it is 10:2:2 that described shizandra berry shifts to an earlier date the weight ratio of thing, Herba Houttuyniae extract and Ramie Root extract.
Wherein in an embodiment, described de-etiolation lightening compositions also comprises the formula Seaweed Extract difficult to understand of 1-3 weight part, the sanitas of 0.3-0.7 weight part and the essence of 0.01-0.05 weight part.
Wherein in an embodiment, described wetting Agent for Printing Inks to be 1,2-hexylene glycol/pungent glycol, described sanitas be Phenoxyethanol/Sensiva SC50, described neutralizing agent are trolamine. Wetting Agent for Printing Inks is possible to prevent skin because of Exposure to Sunlight high temperature and causes the loss of skin moisture, and has certain water supplement function, can be replenish water for skin in time, reduce xerosis cutis, can skin care, increase the skinfeel of makeup. The main effect adding sanitas in de-etiolation lightening compositions is protection product, makes it from microbial contamination, extends the shelf-life of product, it is ensured that the security of product, prevents human consumer from causing possible infection because using the product by microbial contamination.
Wherein in an embodiment, weight percentage, comprising:
Wherein in an embodiment, weight percentage, comprising:
The preparation method of above-mentioned de-etiolation lightening compositions, comprises the following steps:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119 and deionized water mixing, soak and it is warming up to 80-85 DEG C in 1.5-2 hour, homogeneous 5-8 minute, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, PEG-4000 and niacinamide mixing, steep 20-30 minute, it is warming up to 50-60 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50-60 DEG C, B is added in A phase, mixing and stirring;
When 40-50 DEG C, add neutralizing agent, stir evenly, then add wetting Agent for Printing Inks, stir evenly, obtain de-etiolation lightening compositions.
Above-mentioned de-etiolation lightening compositions in the application in skin care kind, the particularly application in facial mask. De-etiolation lightening compositions is soaked silk facial mask paste, it is possible to obtain facial mask finished product.
Shizandra berry selects Schizandra leaf to be raw material, is the total flavones composition that Extraction solvent extracts with ethanol. Shizandra berry is described as plant soft gold, taking Schisandra chinensis as top grade. Schisandra chinensis whole body is all precious, and its fruit can be used as medicine, it is possible to cooks beverage, fruit wine, fruit tea; Its stem skin, bud can make condiment, spices; Its tender stem, leaf can eat or tea making. At present, the research and apply of shizandra berry is concentrated on fruit mostly, the research and apply of its leaf is very few. The total flavones that the present invention mainly applies in Folium Schisandrae Chinensis extract is applied in face pack prescription as activeconstituents. Shizandra berry total flavones has certain Scavenging ability, removes hydroxyl radical free radical effect and is better than superoxide radical. Can the generation of effective check melanin, make obscure skin recover delicate.
Herba Houttuyniae is Rhizoma Saururi (Herba Saururi) section heartleaf houttuynia, the dry aerial parts of platymiscium heartleaf houttuynia and fresh full grass. Compendium of Material Medica is carried: " its leaf stink smell, therefore popular name Herba Houttuyniae. " another name pig nostril, chicken root etc. Herba Houttuyniae is hidden and pungent, micro-trembles with fear, returns lung channel. There is the multiple functions such as clearing heat and detoxicating, inducing diuresis for treating stranguria syndrome, hemostasis, expelling phlegm for arresting cough, analgesia, clinical tell purulence for lung carbuncle, phlegm heat breath with cough, hot dysentery, heat is drenched, carbuncle sore tumefacting virus, is one of China's tradition common drug. Herba Houttuyniae rich in proteins, grease, vitamins and other nutritious components, nutritive value is very high, is one of conventional wild vegetable. At present, Herba Houttuyniae by health ministry one of resource of great exploitation potential for its being formally defined as " being medicine, be again food ". The present invention adopts alcohol extraction process to obtain Herba Houttuyniae extract, and plasminogen and trypsinase are had good restraining effect by it, can improve skin function and prevention contact dermatitis. The growth of neurocyte also there is is good restraining effect, can effectively prevent allergic, and contribute to suppressing the undue expansion of blood vessel, the symptom such as ecchymosis, red blood streak is had prophylactic effect. Also have it that tyrosine oxidase has good restraining effect, there is whitening effect fast and efficiently.
Ramie is Urticaceae ramie, belongs to per nnial herb. According to made, China is among the people utilizes the history of ramie disease therapy very long, and the part medicinal function of ramie, in famous medical literature Compendium of Material Medica, has been done detailed record and elaboration by Ming Dynasty's LI Shi-Zhen. The medicinal function of ramie, effective component etc. have also been carried out some researchs by modern medicine, it has been found that the root of ramie and leaf have higher health care and medicinal Development volue. The Ramie Root extract of the present invention is ethanol extraction, has extraordinary super oxyradical scavenging capacity, it is possible to promote cell metabolism.
The facial mask adopting above-mentioned de-etiolation lightening compositions to prepare has the following advantages:
1, by Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract combination together, mutually promoting between each composition, collaborative performance effect, the formation of effective check melanin, makes skin dark yellow, obscure recover pale, reaches better de-etiolation whitening effect.
2, the appearance of microgroove, obscure, comedo can effectively be suppressed.
3, whitening effect profit skin, nourishes skin, it is possible to pins moisture, has humidity-holding effect.
4, epiderm skin, fast absorption can be infiltrated rapidly, have no side effect.
Embodiment
For enabling above-mentioned purpose, the feature and advantage of the present invention more become apparent, below the specific embodiment of the present invention is described in detail. Set forth a lot of detail in the following description so that fully understanding the present invention. But the present invention can implement to be much different from alternate manner described here, and those skilled in the art can do similar improvement when not running counter to intension of the present invention, therefore the present invention is not by the restriction of following public concrete enforcement.
Composition title used in following examples is international cosmetic material name (InternationalNomenclatureCosmeticIngredient, INCI) title of defined: glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119,1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50.
The Fructus Schisandrae Chinensis extrat used in embodiment is purchased from sky, Xi'an one Bioisystech Co., Ltd; Herba Houttuyniae extract is purchased from Hao Yang bio tech ltd, Shaanxi; Ramie Root extract is purchased from Xi'an Sen Ran biotechnology company limited.
Embodiment 1
A kind of de-etiolation lightening compositions, weight percentage, comprising:
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate or propylene glycol glycerine polymethacrylate, propylene glycol or methoxy ethylene and copolymer-maleic anhydride and deionized water mixing, soak and it is warming up to 85 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 60 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 60 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence when 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Embodiment 2
A kind of de-etiolation lightening compositions, weight percentage, comprising:
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate or propylene glycol glycerine polymethacrylate, propylene glycol or methoxy ethylene and copolymer-maleic anhydride and deionized water mixing, soak and it is warming up to 85 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 60 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 60 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence at 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Embodiment 3
A kind of de-etiolation lightening compositions, weight percentage, comprising:
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate or propylene glycol glycerine polymethacrylate, propylene glycol or methoxy ethylene and copolymer-maleic anhydride and deionized water mixing, soak and it is warming up to 80 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 50 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence at 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Comparative example 1
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119 and deionized water mixing, soak and it is warming up to 80 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 50 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence at 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Comparative example 2
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119 and deionized water mixing, soak and it is warming up to 80 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Herba Houttuyniae extract, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 50 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence at 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Comparative example 3
The preparation method of above-mentioned de-etiolation lightening compositions is:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119 and deionized water mixing, soak and it is warming up to 80 DEG C in 2 hours, homogeneous 5 minutes, stir, dissolve completely, obtain A phase;
By Ramie Root extract, formula Seaweed Extract difficult to understand, PEG-4000 and niacinamide mixing, soak 30 minutes, it is warming up to 50 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50 DEG C, B is added in A phase, mixing and stirring;
When 50 DEG C, add trolamine, stir evenly, then add 1,2-hexylene glycol/pungent glycol, Phenoxyethanol/Sensiva SC50 and essence at 45 DEG C, stir evenly, obtain de-etiolation lightening compositions.
Embodiment 4 testing performance index
The de-etiolation lightening compositions of embodiment 1-3 carries out the performance test of outward appearance, pH value, viscosity, heat-resistant stability and cold-resistant stability, and test result is as follows:
Outward appearance: transparent flow liquid;
PH value: 5.0-6.5;
Viscosity: 1000-10000mpa.s;
Heat-resistant stability investigates (depositing 24 hours at 50 DEG C): qualified;
Cold-resistant study on the stability (depositing 24 hours at-15 DEG C): qualified.
The de-etiolation lightening compositions of embodiment 1-3 is carried out result of use assessment experiment by embodiment 5
Respectively the de-etiolation lightening compositions of embodiment 1-3 being soaked silk face and paste film, every sheet soaks de-etiolation lightening compositions 25g, obtains facial mask finished product 1,2 and 3 respectively.
In use, the careful facial mask that takes out fits on face, applies 20 minutes, and facial mask is without the need to cleaning, and facial mask uses 2-3 time weekly.
Research object: select dark yellow, obscure, microgroove, acne print and responsive five kinds of skin triers, often kind of problem skin chooses 80 people, it is divided into 4 groups, each group 20 people, group 1 facial mask finished product 1, group 2 facial mask finished product 2, group 3 facial mask finished product 3, the group 4 blank facial mask not adding Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, uses 2 times weekly, use 3 months continuously, record trier's skin. Experimental result is in table 1.
The result of use evaluation form of the de-etiolation lightening compositions of table 1 embodiment 1-3
Experimental result:
What dark yellow skin obviously improved shows as: skin is obvious pale bright.
What dark yellow skin symptom was alleviated shows as: skin dark yellow subtracts light, slightly turns white.
Dark yellow skin is without showing as of improving: skin is dark yellow, without turning white also dark yellow without the intensification colour of skin.
What obscure skin obviously improved shows as: skin is obvious pale bright.
What obscure skin symptom was alleviated shows as: the obscure look of skin subtracts light, slightly turns white.
Obscure skin is without showing as of improving: skin gloss, but the colour of skin is light also without deterioration without subtracting.
What microgroove skin obviously improved shows as: microgroove disappears.
What microgroove skin symptom was alleviated shows as: lines becomes shallow.
Microgroove skin is without showing as of improving: skin gloss, and microgroove is shallow also without intensification without change.
What acne print skin obviously improved shows as: acne print disappears.
What acne print skin symptom was alleviated shows as: acne print becomes shallow.
Acne print skin is without showing as of improving: acne print is without becoming shallow also without intensification.
What sensitive skin obviously improved shows as: red and swollen allergic phenomena major part disappears.
Showing as of sensitive skin remission: red and swollen allergic phenomena major part alleviates, and small portion disappears.
Sensitive skin is without showing as of improving: red and swollen allergic phenomena is without alleviating also without deterioration.
As can be seen from Table 1, dark yellow, microgroove, acne print and sensitive skin problem are had good curative effect by the facial mask adopting the de-etiolation lightening compositions of embodiment 1-3 to make. Shown in trial effect according to record trier, after being finished the facial mask of the de-etiolation lightening compositions making adopting embodiment 1-3, skin has improvement faster, skin sliding tender, flexible, moistening, various skin problem has and alleviates, and adheres to life-time service, and better effects if is more stable.
The result of use of the de-etiolation lightening compositions of embodiment 6 embodiment 1-3 and the de-etiolation lightening compositions of comparative example 1-3
1, tested object: choose the age be 20-30 year women, often organize 100.
2, testing tool: VISA digital skin analyser (U.S.), Aomei health moisture of skin tester (China) and MinoltaCR300 colour-difference meter (China);
3, test zone: face;
4, duration of service: weekly twice, continue to use 4 weeks;
5, test event: whitening, humidity of skin and skin delicacy degree.
The result of use of the de-etiolation lightening compositions of embodiment 1-3 and the composition of comparative example 1-3 is as shown in table 2:
The result of use table of the de-etiolation lightening compositions of table 2 embodiment 1-3 and the de-etiolation lightening compositions of comparative example 1-3
As shown in Table 2, the facial mask that the de-etiolation lightening compositions of embodiment 1-3 makes has in the improvement of humidity of skin, skin delicacy degree, whitening effect relative to the de-etiolation lightening compositions of comparative example 1-3 and very significantly improves. Wherein, it is the most obvious that the de-etiolation lightening compositions of embodiment 1 improves effect, taking second place of embodiment 2. Illustrate Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract three combination get up additive effect more independent than three well a lot.
The above embodiment only have expressed several enforcement modes of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to patent scope of the present invention. , it is also possible to make some distortion and improvement, it should be appreciated that for the person of ordinary skill of the art, without departing from the inventive concept of the premise these all belong to protection scope of the present invention. Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (10)
1. a de-etiolation lightening compositions, it is characterised in that, by weight, it is prepared from by following component:
2. de-etiolation lightening compositions according to claim 1, it is characterised in that, the weight ratio of described Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract and Ramie Root extract is 8-10:2-5:1-3.
3. de-etiolation lightening compositions according to claim 2, it is characterised in that, the weight ratio of described Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract and Ramie Root extract is 10:2:2.
4. a de-etiolation lightening compositions, it is characterised in that, by weight, it is prepared from by following component:
5. de-etiolation lightening compositions according to claim 4, it is characterised in that, described wetting Agent for Printing Inks to be 1,2-hexylene glycol/pungent glycol, described sanitas be Phenoxyethanol/Sensiva SC50, described neutralizing agent are trolamine.
6. de-etiolation lightening compositions according to claim 4, it is characterised in that, by weight, it is prepared from by following component:
7. de-etiolation lightening compositions according to claim 6, it is characterised in that, by weight, it is prepared from by following component:
8. the preparation method of a de-etiolation lightening compositions according to claim 1, it is characterised in that, comprise the following steps:
By hyaluronate sodium, carbomer, EDETATE SODIUM, glycerine, glycerine polymethacrylate/propylene glycol, glycerine polymethacrylate/propylene glycol/Gantrez AN-119 and deionized water mixing, soak and it is warming up to 80-85 DEG C in 1.5-2 hour, homogeneous 5-8 minute, stir, dissolve completely, obtain A phase;
By Fructus Schisandrae Chinensis extrat, Herba Houttuyniae extract, Ramie Root extract, PEG-4000 and niacinamide mixing, soak 20-30 minute, it is warming up to 50-60 DEG C, stir, dissolve completely, obtain B phase;
When A phase is cooled to 50-60 DEG C, B is added in A phase, mixing and stirring;
When 40-50 DEG C, add neutralizing agent, stir evenly, then add wetting Agent for Printing Inks, stir evenly, obtain de-etiolation lightening compositions.
9. de-etiolation lightening compositions described in the arbitrary item of claim 1-7 is in the application prepared in skin care product.
10. de-etiolation lightening compositions according to claim 9 is in the application prepared in skin care product, it is characterised in that, described skin care product are facial mask.
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| CN104382833B (en) * | 2014-10-28 | 2015-11-18 | 广东碧嫄化妆品有限公司 | Plant protein peptide stock solution and its preparation method and application |
| CN106860088B (en) * | 2017-02-09 | 2021-04-13 | 曼秀雷敦(中国)药业有限公司 | Skin care product for whitening and removing scars and preparation method thereof |
| CN106955246A (en) * | 2017-03-06 | 2017-07-18 | 广州奥蓓斯化妆品有限公司 | A kind of active crystallite dew of suspension oil droplet and preparation method thereof |
| CN107693448A (en) * | 2017-10-31 | 2018-02-16 | 徐鹂 | A kind of facial mask for going obscure moisturizing and preparation method thereof |
| CN109394561B (en) * | 2018-12-14 | 2021-11-02 | 完美（中国）有限公司 | Composition for removing yellow and whitening skin, application and preparation method thereof |
| CN111728887B (en) * | 2020-08-06 | 2023-08-04 | 上海阿睿索生物科技有限公司 | Moisturizing mask and preparation method thereof |
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| CN102430024B (en) * | 2011-11-29 | 2013-11-06 | 青岛阳光海川医药科技发展有限公司 | Traditional Chinese medicine composition, traditional Chinese medicinal preparation and traditional Chinese medicinal face mask |
| KR20130085012A (en) * | 2012-01-18 | 2013-07-26 | 주식회사 엘지생활건강 | Cosmetic composition comprising fermented material and manufacturing method thereof |
| KR20130087938A (en) * | 2012-01-30 | 2013-08-07 | (주)해피콜 | Cosmetic composition for reducing skin wrinkle comprising schizandra chinensis fruit extracts |
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