CN106955246A - A kind of active crystallite dew of suspension oil droplet and preparation method thereof - Google Patents
A kind of active crystallite dew of suspension oil droplet and preparation method thereof Download PDFInfo
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- CN106955246A CN106955246A CN201710128680.9A CN201710128680A CN106955246A CN 106955246 A CN106955246 A CN 106955246A CN 201710128680 A CN201710128680 A CN 201710128680A CN 106955246 A CN106955246 A CN 106955246A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/044—Suspensions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
Abstract
Reveal the invention discloses a kind of active crystallite of suspension oil droplet and preparation method thereof, belong to cosmetic technical field, the active crystallite dew includes the component of following parts by weight：71.99 ~ 99.697 parts of A phases, 0.001 ~ 10 part of B phases, 0.1014 ~ 4.01 part of C phases, 0.2 ~ 6 part of D phases.Oil phase in formula is dispersed in suspension within the aqueous phase of this product by the active crystallite dew of the present invention using the network macromolecular structure of gellan gum；Meanwhile, a variety of natural plant extracts are added in crystallite dew, organic assembling is carried out to these extracts, crystallite dew is highlighted with good moisturizing, whitening, sensitive skin maintenance and the effects such as keep skin elasticity.
Description
Technical field
The invention belongs to cosmetic technical field, more particularly to a kind of active crystallite dew of suspension oil droplet and its preparation side
Method.
Background technology
In the market skin care item are had by formulation classification：Aqua, emulsion, cream, gel, Essence, facemask powder etc., wherein aqua
Product has a single-layer type and the class product of multi-layered type two, wherein multi-layered type aqua be Yi Shui, oil, powder or containing functional particles composition,
The toner of multilayer liquid is presented in outward appearance.Toner divides and has two types according to whether there is addition emulsifying agent in formula components again：
1）With the addition of the toner of emulsifying agent in product, oil is wrapped in water to be emulsified in the form of emulsifying, product in outward appearance visually
Very common, feel and effect are relatively conventional when using；Wherein, the toner that oil droplet is formed in the way of commonly emulsifying, this cosmetic
Water outward appearance is creamy white liquid, and denseness is very low and stability is bad, it is easy to water-oil separating phenomenon occur；Oil droplet is with microemulsified side
The toner of formula formation, this toner outward appearance is transparent slightly light blue；2）Without the toner of emulsifying agent in product, this change
Oil is swum in above product in adornment water, will firmly be shaken before use, so that oil is quickly dispersed in water, it is fast again afterwards
Speed, which is poured out, to be used, and uses very inconvenient and oil mixing with water is uneven, and the effect used is not also fine.Meanwhile, in the market
The toner of release highlights effect and shown as typically in moisturizing, whitening.
Therefore, need badly develop in a kind of new cosmetic water, the toner oil droplet can for a long time and ratio relatively evenly divides
Cloth in toner, and good moisturizing can be obtained, the effect that whitening is highlighted.
The content of the invention
Present invention aims to overcome that the deficiency that prior art is present, and a kind of oil droplet is provided and is uniformly distributed and with guarantor
Wet, whitening highlights the active crystallite dew of effect.To achieve the above object, the technical scheme taken of the present invention is：A kind of suspended oil
The active crystallite dew of drop, the active crystallite dew includes the component of following parts by weight：71.99 ~ 99.697 parts of A phases, B phases
0.001 ~ 10 part, 0.1014 ~ 4.01 part of C phases, 0.2 ~ 6 part of D phases.
The raw material that the A phases include is：Water, butanediol, glycerine, glycerine polymethacrylates, propane diols, vinyl first
Ether/copolymer-maleic anhydride（PVM/MA copolymers）, glycine betaine, beta glucan, gellan gum, Sodium Hyaluronate, xanthans and hydroxyl
Benzene methyl.
Butanediol, glycerine, propane diols are used as NMF；Glycerine polymethacrylates promotes aqueous phase A and oil phase B to be blended altogether
Melt, during aqueous phase and oil phase are while penetrate to the skin when using, play good moisture-keeping function；Gellan gum is the polysaccharide of plant origin
Family macromolecule, the ad hoc network macromolecular structure of gellan gum can by oil suspensions in formula in the cyberspace of itself, from
Without allowing oil droplet drift to float, therefore oil droplet can disperse to be suspended in the aqueous phase of this product for a long time and than more uniform, this
Sample both ensure that oil can be uniformly dispersed in water this product when in use, and this product can be also used well without firmly shaking,
The relative stability of product is can guarantee that again.
The raw material that the B phases include is：Magnolia cortex P.E, Fructus Schisandrae Sphenantherae extract, burdock extract, Fructus Cucumidis sativi extract,
Green-tea extract, Gotu Kola P.E, Gentrin Knotweed P.E, Scutellaria baicalensis extract, glycyrrhiza glabra extract and german chamomile extract.
The active component of Magnolia cortex P.E includes magnolol, and magnolol can suppress skin photoage, can play protection skin
The effect of skin；The active component of Fructus Schisandrae Sphenantherae extract includes lignin composition, and lignin composition has good anti-purple
Outer effect；The active component of burdock extract includes arctigenin, and arctigenin can maintain skin clean, can cutin-softening
Layer, removes dirt in pore, and can maintenance small pox, improvement topical skin tone；The active component of Fructus Cucumidis sativi extract includes polysaccharide, dimension life
Element, amino acid etc., these nutritional ingredients have effects that moist, convergence, gloss skin and beauty；Green-tea extract activity into
Dividing includes Tea Polyphenols, aromatic oil, protein and vitamin, and these active components can remove greasy, the convergence pore of skin of face
And resisting age of skin；The active component of Gotu Kola P.E includes triterpenes components, such as Asiaticoside and madecassoside, product
The careless glucoside of snow and madecassoside have desalination scar, healing wounds, repair impaired skin, enhance metabolism, compact, it is anti-ageing
Always, the effects such as anti-acne acne print is repaired；Gentrin Knotweed P.E is water extract, and the water extract of giant knotweed can reduce melanin content, and
Suppress the activity of elastoser；The active component of Scutellaria baicalensis extract includes scutellaria glycosides, flavones, Wogonin etc., these activity
Composition can suppress the activity of melanocyte, with anti-oxidant and antianaphylactic effect；The active component of glycyrrhiza glabra extract
Determine including glycyrrhiza glabra and glycyrrhiza glabra element, glycyrrhiza glabra is fixed and glycyrrhiza glabra element has the desalination color spot and skin of inoxidizability by force
The effects such as skin is dehydrated；German chamomile extract is water extract, and the water extract of german chamomile can adjust facial epidermis and cuticula new old generation
Thank, there is anti-aging and wrinkle is removed.The B phases are organically combined the extract of natural plants, make the present invention
Active crystallite dew highlighted with good moisturizing, whitening, sensitive skin maintenance and the effects such as keep skin elasticity.
The raw material that the C phases include is：Cremophor RH40, essence, methylisothiazolinone, sodium chloride, lemon
Sour sodium and citric acid.The Cremophor RH40 has the effect of moisturizing, and methylisothiazolinone can be used as preservative, lemon
Lemon acid, sodium citrate are from can be used as pH adjusting agent.
The raw material that the D phases include is：Diphenyl dimethicone and the poly- front three of diphenyl silicon phenyl
Radical siloxane.The diphenyl dimethicone and the poly- trimethicone conduct of the diphenyl silicon phenyl
Organic silicone oil, its compatibility is preferably.
As the improvement of above-mentioned technical proposal, the A phases include the raw material of following parts by weight：Water 28.19 ~ 97.2709
Part, 1 ~ 10 part of butanediol, 1 ~ 10 part of glycerine, 0.1 ~ 5 part of glycerine polymethacrylates, 0.1 ~ 5 part of propane diols, vinyl first
0.1 ~ 5 part of ether/copolymer-maleic anhydride, 0.1 ~ 5 part of glycine betaine, 0.0001 ~ 3 part of beta glucan, 0.001 ~ 0.2 part of gellan gum,
0.01 ~ 0.3 part of 0.005 ~ 0.1 part of Sodium Hyaluronate, 0.01 ~ 0.2 part of xanthans and methyl hydroxybenzoate.
As the improvement of above-mentioned technical proposal, the B phases include the raw material of following parts by weight：Magnolia cortex P.E 0.0001
~ 1 part, 0.0001 ~ 1 part of Fructus Schisandrae Sphenantherae extract, 0.0001 ~ 1 part of burdock extract, 0.0001 ~ 1 part of Fructus Cucumidis sativi extract, green tea
0.0001 ~ 1 part of extract, 0.0001 ~ 1 part of Gotu Kola P.E, 0.0001 ~ 1 part of Gentrin Knotweed P.E, Scutellaria baicalensis extract 0.0001
0.0001 ~ 1 part of ~ 1 part, 0.0001 ~ 1 part of glycyrrhiza glabra extract and german chamomile extract.
As the improvement of above-mentioned technical proposal, the C phases include the raw material of following parts by weight：Cremophor RH40
0.0001 ~ 0.4 part, 0.0001 ~ 0.2 part of essence, 0.0001 ~ 0.01 part of methylisothiazolinone, 0.1 ~ 3 part of sodium chloride, lemon
0.0001 ~ 0.2 part of 0.001 ~ 0.2 part of sour sodium and citric acid.
As the improvement of above-mentioned technical proposal, the D phases include the raw material of following parts by weight：Diphenyl poly dimethyl silicon
0.1 ~ 3 part of 0.1 ~ 3 part of oxygen alkane and the poly- trimethicone of diphenyl silicon phenyl.
In addition, the present invention also provides a kind of preparation method of the active crystallite dew, the preparation method includes following step
Suddenly：
1）Raw material in the A phases is added sequentially in agitated kettle, stirring is warming up to after 85 ~ 95 DEG C, constant temperature stirs 30 min, so
Cooling is handled afterwards；
2）After temperature is down to 42 ~ 45 DEG C, raw material in the B phases is added sequentially in agitated kettle, is stirred；
3）It will add in agitated kettle, be stirred after sodium chloride in the C phases and sodium citrate water dissolves；Again by the C phases
The mixture of middle essence and Cremophor RH40 is added in agitated kettle together with methylisothiazolinone, is stirred evenly, obtained
Obtain solution I；By sodium citrate in the C phases with agitated kettle is added after water dissolves, the pH value of the solution I is adjusted；
4）To step 3）Adjust the solution I after pH and carry out cooling processing, after temperature is down to 42 DEG C, raw material in the D phases is added
Enter in agitated kettle, the active crystallite dew can be obtained after stirring.
It is used as the improvement of above-mentioned technical proposal, the step 3）The pH value of middle solution I is 5.0 ~ 7.0.The activity of the present invention
In the pH of crystallite dew is interval 5.0 ~ 7.0, the absorption for being easy to skin of face to reveal crystallite.
The beneficial effects of the present invention are：The present invention provides crystallite dew of a kind of suspension oil droplet and preparation method thereof, this hair
Oil phase in formula is dispersed in suspension within this product by bright active crystallite dew using the network macromolecular structure of gellan gum
In aqueous phase；A variety of natural plant extracts are added in the crystallite dew of the present invention, organic assembling is carried out to these extracts（Including original
Expect species and content）, crystallite dew is highlighted with good moisturizing, whitening, sensitive skin maintenance and keep skin elasticity etc.
Effect；Crystallite reveals the absorption that suitable pH value is easy to skin of face.
Embodiment
For the object, technical solutions and advantages of the present invention are better described, below in conjunction with specific embodiment and subordinate list pair
The present invention is described further.
Embodiment 1
A kind of active crystallite dew of suspension oil droplet, for the transparency liquid of suspension oil droplet, the active crystallite dew of the embodiment include with
The component of lower parts by weight：71.99 parts of A phases, 0.001 part of B phases, 0.1014 part of C phases, 0.2 part of D phases；
The A phases include the raw material of following parts by weight：28.19 parts of water, 10 parts of butanediol, 10 parts of glycerine, the poly- methyl-prop of glycerine
5 parts of olefin(e) acid ester, 5 parts of propane diols, 5 parts of methoxy ethylene/copolymer-maleic anhydride, 5 parts of glycine betaine, 3 parts of beta glucan, gellan gum
0.3 part of 0.2 part, 0.1 part of Sodium Hyaluronate, 0.2 part of xanthans and methyl hydroxybenzoate；
The B phases include the raw material of following parts by weight：0.0001 part of Magnolia cortex P.E, 0.0001 part of Fructus Schisandrae Sphenantherae extract,
0.0001 part of burdock extract, 0.0001 part of Fructus Cucumidis sativi extract, 0.0001 part of green-tea extract, Gotu Kola P.E 0.0001
Part, 0.0001 part of Gentrin Knotweed P.E, 0.0001 part of Scutellaria baicalensis extract, 0.0001 part of glycyrrhiza glabra extract and german chamomile extract
0.0001 part；
The C phases include the raw material of following parts by weight：0.0001 part of Cremophor RH40,0.0001 part of essence, methyl
0.0001 part of 0.0001 part of OIT, 0.1 part of sodium chloride, 0.001 part of sodium citrate and citric acid；
The D phases include the raw material of following parts by weight：0.1 part of diphenyl dimethicone and diphenyl silicon epoxide
0.1 part of phenyl trimethicone.
The preparation method of embodiment activity crystallite dew comprises the following steps：
1）Raw material in the A phases is added sequentially in agitated kettle, stirring is warming up to after 85 DEG C, constant temperature stirs 30 min, then
Cooling is handled；
2）After temperature is down to 42 DEG C, raw material in the B phases is added sequentially in agitated kettle, is stirred；
3）It will add in agitated kettle, be stirred after sodium chloride in the C phases and sodium citrate water dissolves；Again by the C phases
The mixture of middle essence and Cremophor RH40 is added in agitated kettle together with methylisothiazolinone, is stirred evenly, obtained
Obtain solution I；By sodium citrate in the C phases with agitated kettle is added after water dissolves, the pH value for adjusting the solution I is 5.0；
4）To step 3）Adjust the solution I after pH and carry out cooling processing, after temperature is down to 42 DEG C, raw material in the D phases is added
Enter in agitated kettle, the active crystallite dew can be obtained after stirring.
Embodiment 2
A kind of active crystallite dew of suspension oil droplet, for the transparency liquid of suspension oil droplet, the active crystallite dew of the embodiment include with
The component of lower parts by weight：99.697 parts of A phases, 10 parts of B phases, 4.01 parts of C phases, 6 parts of D phases；
The A phases include the raw material of following parts by weight：97.2709 parts of water, 1 part of butanediol, 1 part of glycerine, the poly- methyl-prop of glycerine
0.1 part of olefin(e) acid ester, 0.1 part of propane diols, 0.1 part of methoxy ethylene/copolymer-maleic anhydride, 0.1 part of glycine betaine, beta glucan
0.01 part of 0.0001 part, 0.001 part of gellan gum, 0.005 part of Sodium Hyaluronate, 0.01 part of xanthans and methyl hydroxybenzoate；
The B phases include the raw material of following parts by weight：1 part of Magnolia cortex P.E, 1 part of Fructus Schisandrae Sphenantherae extract, burdock extract 1
Part, 1 part of Fructus Cucumidis sativi extract, 1 part of green-tea extract, 1 part of Gotu Kola P.E, 1 part of Gentrin Knotweed P.E, 1 part of Scutellaria baicalensis extract, light
1 part of 1 part of fruit licorice and german chamomile extract；
The C phases include the raw material of following parts by weight：0.4 part of Cremophor RH40,0.2 part of essence, methyl-isothiazol
0.2 part of 0.01 part of quinoline ketone, 3 parts of sodium chloride, 0.2 part of sodium citrate and citric acid；
The D phases include the raw material of following parts by weight：3 parts of diphenyl dimethicone and diphenyl silicon epoxide benzene
3 parts of the poly- trimethicone of base.
The preparation method of embodiment activity crystallite dew comprises the following steps：
1）Raw material in the A phases is added sequentially in agitated kettle, stirring is warming up to after 95 DEG C, constant temperature stirs 30 min, then
Cooling is handled；
2）After temperature is down to 45 DEG C, raw material in the B phases is added sequentially in agitated kettle, is stirred；
3）It will add in agitated kettle, be stirred after sodium chloride in the C phases and sodium citrate water dissolves；Again by the C phases
The mixture of middle essence and Cremophor RH40 is added in agitated kettle together with methylisothiazolinone, is stirred evenly, obtained
Obtain solution I；By sodium citrate in the C phases with agitated kettle is added after water dissolves, the pH value for adjusting the solution I is 7.0；
4）To step 3）Adjust the solution I after pH and carry out cooling processing, after temperature is down to 42 DEG C, raw material in the D phases is added
Enter in agitated kettle, the active crystallite dew can be obtained after stirring.
Embodiment 3
A kind of active crystallite dew of suspension oil droplet, for the transparency liquid of suspension oil droplet, the active crystallite dew of the embodiment include with
The component of lower parts by weight：80.4 parts of A phases, 5.2 parts of B phases, 1.464 parts of C phases, 3 parts of D phases；
The A phases include the raw material of following parts by weight：60 parts of water, 5 parts of butanediol, 5 parts of glycerine, glycerine polymethacrylates
2 parts, 2 parts of propane diols, 2 parts of methoxy ethylene/copolymer-maleic anhydride, 3 parts of glycine betaine, 1 part of beta glucan, 0.1 part of gellan gum,
0.15 part of 0.05 part of Sodium Hyaluronate, 0.1 part of xanthans and methyl hydroxybenzoate；
The B phases include the raw material of following parts by weight：0.5 part of Magnolia cortex P.E, 0.4 part of Fructus Schisandrae Sphenantherae extract, burdock are carried
Take 0.6 part of thing, 0.3 part of Fructus Cucumidis sativi extract, 0.8 part of green-tea extract, 0.5 part of Gotu Kola P.E, 0.5 part of Gentrin Knotweed P.E,
0.5 part of 0.4 part of Scutellaria baicalensis extract, 0.7 part of glycyrrhiza glabra extract and german chamomile extract；
The C phases include the raw material of following parts by weight：0.2 part of Cremophor RH40,0.005 part of essence, the different thiophene of methyl
0.1 part of 0.009 part of oxazoline ketone, 1 part of sodium chloride, 0.15 part of sodium citrate and citric acid；
The D phases include the raw material of following parts by weight：1 part of diphenyl dimethicone and diphenyl silicon epoxide benzene
2 parts of the poly- trimethicone of base.
The preparation method of embodiment activity crystallite dew comprises the following steps：
1）Raw material in the A phases is added sequentially in agitated kettle, stirring is warming up to after 90 DEG C, constant temperature stirs 30 min, then
Cooling is handled；
2）After temperature is down to 44 DEG C, raw material in the B phases is added sequentially in agitated kettle, is stirred；
3）It will add in agitated kettle, be stirred after sodium chloride in the C phases and sodium citrate water dissolves；Again by the C phases
The mixture of middle essence and Cremophor RH40 is added in agitated kettle together with methylisothiazolinone, is stirred evenly, obtained
Obtain solution I；By sodium citrate in the C phases with agitated kettle is added after water dissolves, the pH value for adjusting the solution I is 6.0；
4）To step 3）Adjust the solution I after pH and carry out cooling processing, after temperature is down to 42 DEG C, raw material in the D phases is added
Enter in agitated kettle, the active crystallite dew can be obtained after stirring.
Embodiment 4
A kind of active crystallite dew of suspension oil droplet, for the transparency liquid of suspension oil droplet, the active crystallite dew of the embodiment include with
The component of lower parts by weight：80.4 parts of A phases, 3 parts of B phases, 1.464 parts of C phases, 3 parts of D phases；
The A phases include the raw material of following parts by weight：60 parts of water, 5 parts of butanediol, 5 parts of glycerine, glycerine polymethacrylates
2 parts, 2 parts of propane diols, 2 parts of methoxy ethylene/copolymer-maleic anhydride, 3 parts of glycine betaine, 1 part of beta glucan, 0.1 part of gellan gum,
0.15 part of 0.05 part of Sodium Hyaluronate, 0.1 part of xanthans and methyl hydroxybenzoate；
The B phases include the raw material of following parts by weight：0.5 part of Magnolia cortex P.E, 0.4 part of Fructus Schisandrae Sphenantherae extract, cucumber carry
Take 0.5 part of 0.3 part of thing, 0.8 part of green-tea extract, 0.4 part of Scutellaria baicalensis extract and german chamomile extract；
The C phases include the raw material of following parts by weight：0.2 part of Cremophor RH40,0.005 part of essence, the different thiophene of methyl
0.1 part of 0.009 part of oxazoline ketone, 1 part of sodium chloride, 0.15 part of sodium citrate and citric acid；
The D phases include the raw material of following parts by weight：1 part of diphenyl dimethicone and diphenyl silicon epoxide benzene
2 parts of the poly- trimethicone of base.
The preparation method be the same as Example 3 of embodiment activity crystallite dew.
Embodiment 5
Stability test
1）Resistance to Thermal test：The active crystallite dew for implementing embodiment 1 ~ 4 is put into constant incubator, carried out heat-resisting（40±1℃）
Experiment, is placed after 24 h, recovers to room temperature, the generation of water-oil separating phenomenon and metachromatism is not found；
2）Cold-resistant test：The active crystallite dew for implementing embodiment 1 ~ 4 is put into refrigerator, carried out（-15±1℃）Cold-resistant experiment,
Place after 24 h, recover to room temperature, the generation of water-oil separating phenomenon and metachromatism is not found.
Embodiment 6
Experimental animal：The kunming mice 24 of health is taken, body weight is 18 ~ 24 g, is randomly divided into 6 groups, every group of 4 mouse：One group
For blank group（Do not apply toner）, one group is contrast groups（Smear the toner A that market is bought）, four groups are experimental group（Apply respectively
Smear the active crystallite dew of embodiment 1 ~ 4）.
Experimental method：Each group mouse carries out back depilation with 0.8% sodium sulphate, the cm of 4 cm of sudden and violent leakage × 4 test section.Apply
Skin first is cleaned with warm water before smearing toner, the mouse for being coated with toner is placed on culture in experimental box, daily to smear 3 times,
4 weeks are carried out continuously, the mouse hair newly grown is during which shaved off in time.Finally, moisture value and elasticity are determined with CK skinanalysis apparatus
Value.Experimental result, is shown in Table 1.
Table 1 is influence of the toner to mouse skin moisture value and elasticity number
| Group | Moisture value | Elasticity number |
| Blank group | 54.2 | 70.1 |
| Toner A | 60.3 | 80.6 |
| The active crystallite dew of embodiment 1 | 66.6 | 87.9 |
| The active crystallite dew of embodiment 2 | 65.8 | 88.5 |
| The active crystallite dew of embodiment 3 | 70.2 | 93.7 |
| The active crystallite dew of embodiment 4 | 62.1 | 84.0 |
From table 1, it can be seen that the toner A and the active crystallite dew of the embodiment of the present invention 1 ~ 4 that market is bought have moisturizing
With put forward elastomeric effect；Meanwhile, show one's true colours and compare with the active crystallite of embodiment 1 ~ 3, the active crystallite dew of embodiment 4 with the addition of less
Burdock extract, Gotu Kola P.E, Gentrin Knotweed P.E and glycyrrhiza glabra extract, it is seen that effect that its moisturizing, elasticity are maintained
Declined.Therefore, the natural extract in B phases of the present invention, which is mutually cooperateed with, strengthens moisturizing, effect of elasticity maintenance.
Embodiment 7
The test of skin elasticity and moistening effect
Experimental subjects：The sensitive volunteer of 180 skin of face is chosen, 5 groups, every group of 36 volunteers are randomly divided into：One group is
Blank group（Do not apply toner）, one group is contrast groups（Smear the toner A that market is bought）, four groups are experimental group（Smear respectively
The active crystallite dew of embodiment 1 ~ 4）.1 toner is used within every 3 days, altogether using 4 weeks.Finally, by doctor to face
Colour of skin whitening is highlighted, moisturizing water lock, effect of sensitive skin maintenance are evaluated.Experimental result, is shown in Table 1.
Table 2 is using after toner, colour of skin whitening is highlighted, moisturizing water lock, the improvement rate of sensitive skin maintenance
| Group | Whitening is highlighted | Moisturizing water lock | Sensitive skin maintenance |
| Toner A | 30.9% | 62.1% | 8.1% |
| The active crystallite dew of embodiment 1 | 52.5% | 73.5% | 44.8% |
| The active crystallite dew of embodiment 2 | 55.7% | 74.6% | 45.5% |
| The active crystallite dew of embodiment 3 | 58.8% | 77.8% | 46.3% |
| The active crystallite dew of embodiment 4 | 48.5% | 68.8% | 39.5% |
From table 2, it can be seen that the toner A and the active crystallite dew energy whitening of the embodiment of the present invention 1 ~ 4 that market is bought are carried
Bright, moisturizing water lock and maintenance sensitive skin；Meanwhile, show one's true colours and compare with the active crystallite of embodiment 1 ~ 3, the active crystallite of embodiment 4
Dew with the addition of burdock extract, Gotu Kola P.E, Gentrin Knotweed P.E and glycyrrhiza glabra extract less, it is seen that its whitening highlights,
Moisturizing water lock and effect of sensitive skin maintenance are declined.Therefore, the natural extract in B phases of the present invention, which is mutually cooperateed with, adds
Strong whitening is highlighted, effect of moisturizing water lock and sensitive skin maintenance.
It is last to should be noted that above example to illustrate technical scheme rather than to present invention protection
The limitation of scope, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should manage
Solution, technical scheme can be modified or replaced on an equal basis, without departing from technical solution of the present invention essence and
Scope.
Claims (7)
1. a kind of active crystallite dew of suspension oil droplet, it is characterised in that：The active crystallite dew includes the group of following parts by weight
Point：71.99 ~ 99.697 parts of A phases, 0.001 ~ 10 part of B phases, 0.1014 ~ 4.01 part of C phases, 0.2 ~ 6 part of D phases；
The raw material that the A phases include is：Water, butanediol, glycerine, glycerine polymethacrylates, propane diols, methoxy ethylene/
Copolymer-maleic anhydride, glycine betaine, beta glucan, gellan gum, Sodium Hyaluronate, xanthans and methyl hydroxybenzoate；
The raw material that the B phases include is：Magnolia cortex P.E, Fructus Schisandrae Sphenantherae extract, burdock extract, Fructus Cucumidis sativi extract, green tea
Extract, Gotu Kola P.E, Gentrin Knotweed P.E, Scutellaria baicalensis extract, glycyrrhiza glabra extract and german chamomile extract；
The raw material that the C phases include is：Cremophor RH40, essence, methylisothiazolinone, sodium chloride, sodium citrate
And citric acid；
The raw material that the D phases include is：Diphenyl dimethicone and the poly- trimethyl silicane of diphenyl silicon phenyl
Oxygen alkane.
2. activity crystallite dew as claimed in claim 1, it is characterised in that：The A phases include the raw material of following parts by weight：Water
28.19 ~ 97.2709 parts, 1 ~ 10 part of butanediol, 1 ~ 10 part of glycerine, 0.1 ~ 5 part of glycerine polymethacrylates, propane diols 0.1 ~ 5
Part, 0.1 ~ 5 part of methoxy ethylene/copolymer-maleic anhydride, 0.1 ~ 5 part of glycine betaine, 0.0001 ~ 3 part of beta glucan, gellan gum
0.01 ~ 0.3 part of 0.001 ~ 0.2 part, 0.005 ~ 0.1 part of Sodium Hyaluronate, 0.01 ~ 0.2 part of xanthans and methyl hydroxybenzoate.
3. activity crystallite dew as claimed in claim 1, it is characterised in that：The B phases include the raw material of following parts by weight：It is thick
Plain 0.0001 ~ 1 part of extract, 0.0001 ~ 1 part of Fructus Schisandrae Sphenantherae extract, 0.0001 ~ 1 part of burdock extract, Fructus Cucumidis sativi extract
0.0001 ~ 1 part, 0.0001 ~ 1 part of green-tea extract, 0.0001 ~ 1 part of Gotu Kola P.E, 0.0001 ~ 1 part of Gentrin Knotweed P.E,
0.0001 ~ 1 part of 0.0001 ~ 1 part of Scutellaria baicalensis extract, 0.0001 ~ 1 part of glycyrrhiza glabra extract and german chamomile extract.
4. activity crystallite dew as claimed in claim 1, it is characterised in that：The C phases include the raw material of following parts by weight：
0.0001 ~ 0.4 part of Cremophor RH40,0.0001 ~ 0.2 part of essence, 0.0001 ~ 0.01 part of methylisothiazolinone, chlorine
Change 0.0001 ~ 0.2 part of 0.1 ~ 3 part of sodium, 0.001 ~ 0.2 part of sodium citrate and citric acid.
5. activity crystallite dew as claimed in claim 1, it is characterised in that：The D phases include the raw material of following parts by weight：Two
0.1 ~ 3 part of 0.1 ~ 3 part of phenyl dimethicones and the poly- trimethicone of diphenyl silicon phenyl.
6. it is a kind of such as the preparation method of any one of the claim 1 ~ 5 active crystallite dew, it is characterised in that：Including following step
Suddenly：
1）Raw material in the A phases is added sequentially in agitated kettle, stirring is warming up to after 85 ~ 95 DEG C, constant temperature stirs 30 min, so
Cooling is handled afterwards；
2）After temperature is down to 42 ~ 45 DEG C, raw material in the B phases is added sequentially in agitated kettle, is stirred；
3）It will add in agitated kettle, be stirred after sodium chloride in the C phases and sodium citrate water dissolves；Again by the C phases
The mixture of middle essence and Cremophor RH40 is added in agitated kettle together with methylisothiazolinone, is stirred evenly, obtained
Obtain solution I；By sodium citrate in the C phases with agitated kettle is added after water dissolves, the pH value of the solution I is adjusted；
4）To step 3）Adjust the solution I after pH and carry out cooling processing, after temperature is down to 42 DEG C, raw material in the D phases is added
Enter in agitated kettle, the active crystallite dew can be obtained after stirring.
7. the preparation method that activity crystallite reveals as claimed in claim 6, it is characterised in that：The step 3）The pH value of middle solution I
For 5.0 ~ 7.0.
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Application publication date: 20170718 |