CN107260641B

CN107260641B - Male refreshing lotion and preparation method thereof

Info

Publication number: CN107260641B
Application number: CN201710489318.4A
Authority: CN
Inventors: 熊延靖; 熊峰; 汪大伟; 陈雨婷; 陶枫; 方毓楠; 刘安; 赵晓苇; 臧开林; 尚昌懿
Original assignee: Wannan Medical College
Current assignee: Wannan Medical College
Priority date: 2017-06-24
Filing date: 2017-06-24
Publication date: 2020-04-21
Anticipated expiration: 2037-06-24
Also published as: CN107260641A

Abstract

The invention discloses a male skin refreshing lotion and a preparation method thereof, and the male skin refreshing lotion comprises the following raw materials, by weight, 20-40 parts of glycerin, 2-15 parts of β -glucan, 5-15 parts of betaine, 15-25 parts of hydrolyzed rice bran protein, 15-25 parts of hydrolyzed wheat protein, 5-15 parts of sodium hyaluronate, 2-10 parts of ceramide, 4-10 parts of propolis, 10-15 parts of lemon extract, 20-25 parts of mint extract, 5-15 parts of cherry extract, 20-30 parts of wormwood extract, 30-35 parts of mung bean extract and 60-100 parts of distilled water.

Description

Male refreshing lotion and preparation method thereof

Technical Field

The invention relates to a male skin refreshing lotion and a preparation method thereof.

Background

With the gradual improvement of the living standard of substances, the pursuit of beauty is continuously improved, the concept of skin care of men is gradually changed, more and more men begin to pay attention to their instrument decoration and external quality, and become consumers of cosmetics. However, most skin care products are for women at present, and the skin care products special for men are few.

The difference between the skin of a male and the skin of a female is large, the horny layer of the skin of the male is usually thicker, the elasticity of the corium layer is more flexible than that of the skin of the female, and the sebaceous glands are more active and developed, so that most of the male belongs to the skin with mixed partial oil to oily skin and is very easy to be disturbed by oily light and acne, and the male is not suitable for using the skin care product of the female.

At present, the domestic male skin care product market is still in the initial development stage, the product formula, the product function and the positioning are still insufficient, and particularly, the product formula is rarely designed according to the skin characteristics of men, so that the using effect is poor.

Disclosure of Invention

In order to solve the technical problems, the invention provides a male refreshing lotion and a preparation method thereof. The skin care product has good absorbability and strong permeability, and can wake up bright and transparent skin, brighten skin color, control oil and keep moisture, effectively increase skin moisture, effectively repair skin wrinkles and increase immunity of skin to aging.

The technical scheme provided by the invention is as follows:

the male skin refreshing lotion comprises the following raw materials in parts by weight:

preferably, the feed comprises the following raw materials in parts by weight:

the lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil.

The supercritical CO₂The extraction conditions were: the temperature is 34-40 ℃; the pressure is 13-15 MPa; CO 2₂The circulation flow rate is 15-19 kg/min.

The preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 10-15 mL, heating and extracting at 55-65 ℃ for 6-8 hours, and concentrating and drying the product to obtain the mint extract.

The preparation method of the cherry extract comprises the following steps: squeezing fresh cherries, mixing the fresh cherries with 70% ethanol which is 3-5 times of the fresh cherries, extracting for 3-5 hours at 65-75 ℃, and sequentially extracting with ethyl acetate and petroleum ether in a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

The preparation method of the wormwood extract comprises the following steps: the wormwood is crushed, soaked in 70% ethanol for 1-2 hours according to the material-liquid ratio of 1g: 30-35 mL, then extracted at 95-100 ℃ for 2.5-3 hours, and the product is concentrated and dried to obtain the wormwood extract.

The preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding the mung beans into water according to the material-liquid ratio of 1g to 20-35 mL, heating and stirring at 60-75 ℃ for 3-5 hours, centrifuging, and concentrating and drying supernatant to obtain the mung bean extract.

The invention also provides a preparation method of the male skin-refreshing lotion, which comprises the following steps:

(a) dissolving 4-10 parts of propolis in 20-40 parts of glycerol, mixing and stirring uniformly, adding 10-15 parts of lemon extract, and mixing and stirring uniformly for later use to obtain a first mixture;

(b) adding 15-25 parts of hydrolyzed rice bran protein, 15-25 parts of hydrolyzed wheat protein, 2-15 parts of β -glucan, 5-15 parts of betaine, 2-10 parts of ceramide and 5-15 parts of sodium hyaluronate into 30-40 parts of distilled water in sequence, and stirring while adding to fully dissolve and uniformly mix to obtain a second mixture;

(c) adding 20-25 parts of mint extract, 5-15 parts of cherry extract, 20-30 parts of wormwood extract and 30-35 parts of mung bean extract into 30-50 parts of distilled water in sequence, and stirring while adding to fully dissolve and uniformly mix to obtain a third mixture;

(d) and adding the mixture I into the mixture III, stirring and mixing uniformly, adding the mixture II into the mixture, and stirring and mixing uniformly to obtain the male skin-refreshing lotion.

The male skin-refreshing lotion comprises the following components:

lemon extract: the lemon extract contains various nutrient components such as vitamin B1, vitamin B2, vitamin C and the like, and also contains rich organic acid and citric acid, and the lemon is a highly alkaline food, has strong antioxidation, and is very effective in promoting the metabolism of skin, delaying aging, inhibiting pigmentation and the like.

And (3) mint extract: the herba Menthae extract is rich in Mentholum and menthol, and has effects of refreshing, relieving itching and refreshing.

Cherry extract: the cherry extract is rich in anthocyanin, has the capacity of removing free radicals and oxidation resistance, has the effects of resisting aging, whitening skin, lightening spots and tightening skin, is beneficial to resisting allergy, avoiding melanin generation, softening food connective tissues and avoiding melanin generation, has excellent oxidation resistance, can prevent the oxidation of skin caused by sunshine or environmental pollution, accelerates skin metabolism and keeps the skin healthy.

The wormwood extract: the wormwood extract contains elements such as flavone, calcium, iron, vitamin ABC and the like, has the capacity of removing free radicals and oxidation resistance, can help to keep skin ruddy and cell metabolism and keep the skin in a viable state, and also has the effects of resisting bacteria, controlling oil and removing freckles.

Mung bean extract: the mung bean extract is rich in mung bean protein, has the effects of tightening skin, fading skin lines and preventing skin aging, and can supply sufficient moisture to skin and effectively strengthen the moisture-retaining capacity of the skin due to the specific moisture-retaining components and mineral substances of mung beans.

Propolis: the propolis is a colloidal solid with aromatic odor, which is processed by mixing resin and wax substances collected by bees from plants with secretions of palatine glands and wax glands on the bees, has good cosmetic effects of broad-spectrum antibiosis, antiphlogosis, antivirus, pain relief, antioxidation, tissue regeneration promotion, immunity enhancement and the like, can prevent chloasma, remove skin grease, antibiosis, antiphlogosis and acne removal, and has good antioxidation function and free radical removal function given by propolis as a marked component flavonoid compound.

β -dextran has effects of keeping moisture, resisting inflammation, resisting aging, removing wrinkle, and increasing skin elasticity, and is a powerful free radical scavenger.

Betaine belongs to an amphoteric compound, and the aqueous solution of the betaine is neutral and has strong moisture retention and oxidation resistance. Tests show that the moisture retention of betaine is about 12 times that of glycerin and 3 times that of sorbitol, and the betaine can be used as an additive of daily chemical products. Since betaine has excellent moisture-retaining and penetrating properties, it rapidly enters the skin, and makes the skin smooth and moist.

Hydrolyzed rice bran protein and hydrolyzed wheat protein: has effects in keeping moisture, removing wrinkle, resisting oxidation, softening and refining skin, and whitening skin.

Sodium hyaluronate: the unique property of having moisturizing effect, the highest moisture absorption at low relative humidity (33%) and the lowest moisture absorption at high relative humidity (75%), is just adapting to the requirements of skin on moisturizing effect in different seasons, different environmental humidities, such as dry winter and wet summer; in addition, the sodium hyaluronate is an inherent biological substance of the skin, and the exogenous sodium hyaluronate can supplement endogenous sodium hyaluronate of the skin, promote the supply of skin nutrition and the excretion of waste, thereby preventing skin aging and playing the roles of beautifying and nourishing the skin; in addition, the sodium hyaluronate belongs to a high molecular polymer, has strong lubricating feeling and film forming property, and the skin care product containing the sodium hyaluronate has obvious lubricating feeling and good hand feeling when being smeared. After being applied to the skin, a layer of film can be formed on the surface of the skin, so that the skin can generate good smooth feeling and moist feeling, and the protective effect on the skin is achieved.

Ceramide: ceramide is a latest generation humectant developed in recent years, has a structure similar to that of substances forming the horny layer of the skin, can quickly permeate into the skin, is combined with water in the horny layer to form a net structure to lock water, forms a protective film on the surface of the skin to lock water, has good skin permeability, and can help to lock water in the deep layer of the skin.

The glycerol has good moisturizing effect.

The male skin-refreshing lotion disclosed by the invention contains cherry extract, wormwood extract, mung bean extract, propolis, β -glucan, betaine, mint extract with skin-refreshing effect, β -glucan, betaine, hydrolyzed rice bran protein, hydrolyzed wheat protein, sodium hyaluronate, ceramide with moisturizing effect, hydrolyzed rice bran protein, hydrolyzed wheat protein and cherry extract with whitening effect, and all the components interact with each other, so that the male skin-refreshing lotion disclosed by the invention has excellent effects of whitening, freckle removing, ageing resisting, moisturizing and moisturizing.

The male skin refreshing lotion disclosed by the invention is designed for the skin of a male, has good absorptivity and strong permeability, has strong moisturizing capability, awakens the skin vitality, brightens the skin color, can effectively increase the skin moisture, effectively repairs skin wrinkles and delays skin aging.

Detailed Description

The present invention will be described in detail with reference to specific examples.

The weight parts of the raw materials in each example are shown in table 1:

TABLE 1

	Example 1	Example 2	Example 3	Example 4
					Glycerol	26 portions of	32 portions of	20 portions of	38 portions of
β dextran	8 portions of	10 portions of	4 portions of	14 portions of
					Betaine	8 portions of	12 portions of	5 portions of	15 portions of
Hydrolyzed rice bran protein	18 portions of	20 portions of	15 portions of	25 portions of
					Hydrolyzed wheat protein	18 portions of	20 portions of	15 portions of	25 portions of
Hyaluronic acid sodium salt	8 portions of	12 portions of	5 portions of	15 portions of
					Ceramide	4 portions of	7 portions of	2 portions of	10 portions of
Propolis (propolis)	6 portions of	8 portions of	4 portions of	10 portions of
					Lemon extract	12 portions of	15 portions of	10 portions of	13 portions of
Mint extract	22 portions of	24 portions of	20 portions of	25 portions of
					Cherry extract	8 portions of	12 portions of	5 portions of	15 portions of
Artemisia princeps extract	25 portions of	28 portions of	20 portions of	30 portions of
					Mung bean extract	31 portions of	34 portions of	32 portions of	35 portions of
Distilled water	70 portions of	85 portions of	60 portions of	100 portions of

Example 1

The male skin refreshing lotion comprises the raw materials in parts by weight shown in example 1 of Table 1, and the preparation method comprises the following steps:

(a) dissolving propolis in the formula amount in glycerol, mixing and stirring uniformly, adding the lemon extract, and mixing and stirring uniformly for later use to obtain a mixture I;

(b) adding hydrolyzed rice bran protein, hydrolyzed wheat protein, β -glucan, betaine, ceramide and sodium hyaluronate into 30 parts of distilled water in sequence, stirring while adding to fully dissolve and uniformly mix to obtain a mixture II;

(c) adding the mint extract, the cherry extract, the wormwood extract and the mung bean extract into 40 parts of distilled water in sequence, stirring while adding to fully dissolve the mint extract, the cherry extract, the wormwood extract and the mung bean extract, and uniformly mixing to obtain a third mixture;

The lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil. The supercritical CO₂The extraction conditions were: the temperature is 40 ℃; the pressure is 13 MPa; CO 2₂The circulation flow rate was 16 kg/min.

The preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 10mL, heating and extracting at 60 ℃ for 8 hours, concentrating and drying the product to obtain the mint extract.

The preparation method of the cherry extract comprises the following steps: squeezing fresh cherry, mixing with 4 times of 70% ethanol, extracting at 70 deg.C for 5 hr, sequentially extracting with ethyl acetate, petroleum ether at a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

The preparation method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, soaking in 70% ethanol at a ratio of 1g to 35mL for 2 hr, extracting at 100 deg.C for 2.5 hr, concentrating, and drying to obtain folium Artemisiae Argyi extract.

The preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding water according to the material-liquid ratio of 1g to 35mL, heating and stirring at 60 ℃ for 5 hours, centrifuging, concentrating supernatant, and drying to obtain the mung bean extract.

Example 2

The male skin refreshing lotion comprises the raw materials in parts by weight shown in example 2 of Table 1, and the preparation method comprises the following steps:

(b) adding hydrolyzed rice bran protein, hydrolyzed wheat protein, β -glucan, betaine, ceramide and sodium hyaluronate into 35 parts of distilled water in sequence, stirring while adding to fully dissolve and uniformly mix to obtain a mixture II;

(c) adding the mint extract, the cherry extract, the wormwood extract and the mung bean extract into 50 parts of distilled water in sequence, stirring while adding to fully dissolve the mint extract, the cherry extract, the wormwood extract and the mung bean extract, and uniformly mixing to obtain a third mixture;

The lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil. The supercritical CO₂The extraction conditions were: the temperature is 34 ℃; the pressure is 15 MPa; CO 2₂The circulation flow rate was 18 kg/min.

The preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 15mL, extracting for 6 hours at 65 ℃, concentrating and drying the product to obtain the mint extract.

The preparation method of the cherry extract comprises the following steps: squeezing fresh cherry, mixing with 3 times of 70% ethanol, extracting at 65 deg.C for 5 hr, sequentially extracting with ethyl acetate, petroleum ether at a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

The preparation method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, soaking in 70% ethanol at a ratio of 1g to 30mL for 1.5 hr, extracting at 95 deg.C for 3 hr, concentrating, and drying to obtain folium Artemisiae Argyi extract.

The preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding water according to the ratio of material to liquid of 1g to 30mL, heating and stirring at 65 ℃ for 4 hours, centrifuging, concentrating supernatant, and drying to obtain the mung bean extract.

Example 3

The male skin refreshing lotion comprises the raw materials in parts by weight shown in example 3 of Table 1, and the preparation method comprises the following steps:

(c) adding the mint extract, the cherry extract, the wormwood extract and the mung bean extract into 30 parts of distilled water in sequence, stirring while adding to fully dissolve the mint extract, the cherry extract, the wormwood extract and the mung bean extract, and uniformly mixing to obtain a third mixture;

The lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil. The supercritical CO₂The extraction conditions were: the temperature is 38 ℃; the pressure is 14 MPa; CO 2₂The circulation flow rate was 18 kg/min.

The preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 12mL, heating and extracting at 60 ℃ for 7 hours, concentrating and drying the product to obtain the mint extract.

The preparation method of the cherry extract comprises the following steps: squeezing fresh cherry, mixing with 5 times of 70% ethanol, extracting at 75 deg.C for 3 hr, sequentially extracting with ethyl acetate, petroleum ether at a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

The preparation method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, soaking in 70% ethanol at a ratio of 1g to 35mL for 1 hr, extracting at 100 deg.C for 3 hr, concentrating, and drying to obtain folium Artemisiae Argyi extract.

The preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding water according to the material-liquid ratio of 1g to 25mL, heating and stirring at 75 ℃ for 3 hours, centrifuging, concentrating supernatant, and drying to obtain the mung bean extract.

Example 4

The male skin refreshing lotion comprises the raw materials in parts by weight shown in example 4 of Table 1, and the preparation method comprises the following steps:

(b) adding hydrolyzed rice bran protein, hydrolyzed wheat protein, β -glucan, betaine, ceramide and sodium hyaluronate into 40 parts of distilled water in sequence, stirring while adding to fully dissolve and uniformly mix to obtain a mixture II;

(c) adding the mint extract, the cherry extract, the wormwood extract and the mung bean extract into 60 parts of distilled water in sequence, stirring while adding to fully dissolve the mint extract, the cherry extract, the wormwood extract and the mung bean extract, and uniformly mixing to obtain a third mixture;

The lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil. The supercritical CO₂The extraction conditions were: the temperature is 36 ℃; the pressure is 15 MPa; CO 2₂The circulation flow rate was 15 kg/min.

The preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 10mL, extracting for 6 hours at 65 ℃, concentrating and drying the product to obtain the mint extract.

The preparation method of the cherry extract comprises the following steps: squeezing fresh cherry, mixing with 4 times of 70% ethanol, extracting at 70 deg.C for 3 hr, sequentially extracting with ethyl acetate, and petroleum ether at a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

The preparation method of the wormwood extract comprises the following steps: pulverizing folium Artemisiae Argyi, soaking in 70% ethanol at a ratio of 1g to 35mL for 2 hr, extracting at 95 deg.C for 2.5 hr, concentrating, and drying to obtain folium Artemisiae Argyi extract.

The preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding water according to the material-liquid ratio of 1g to 20mL, heating and stirring at 60 ℃ for 5 hours, centrifuging, concentrating supernatant, and drying to obtain the mung bean extract.

The efficacy of the obtained men lotions of examples 1 to 4 was evaluated by the feeling of trial use. Selecting 400 men with the age of 18-50 years as trial objects by adopting a civil survey grading method, dividing the trial objects into four groups, and respectively using the male skin-refreshing lotion obtained in the embodiments 1-4 to care skin, wherein the male skin-refreshing lotion is used once a day, and the trial time is two months. The using effects of the ingredients are divided into 5 points: the score of 5 is the highest score, which represents good and very satisfactory; 4, the classification is better and satisfactory; 3 is acceptable; when the amount is less than 3 points, the results are not acceptable. The following are

Each item is scored evenly. The results are shown in Table 2:

TABLE 2 examination of the Effect of the skin lotion for men obtained in the examples

As can be seen from the table, the male refreshing lotion disclosed by the invention has ideal effects of removing freckles, whitening, moisturizing, resisting aging and wrinkles, fading fine wrinkles and refreshing skin.

The above detailed description of the men's refreshing lotion and the method for preparing the same with reference to the examples is illustrative and not restrictive, and several examples are listed according to the limited scope, therefore, variations and modifications without departing from the general concept of the present invention shall fall within the protection scope of the present invention.

Claims

1. The male skin refreshing lotion is characterized by comprising the following raw materials in parts by weight:

the preparation method of the male skin refreshing lotion comprises the following steps:

2. The male skin refreshing lotion as claimed in claim 1, which is characterized by comprising the following raw materials in parts by weight:

3. the male skin refreshing lotion according to claim 1 or 2, wherein the lemon extract is lemon essential oil, and the preparation method comprises the following steps: crushing lemon peel to 0.5-1.5 mm, and performing supercritical CO₂Extracting to obtain the lemon essential oil.

4. The male skin-refreshing lotion for relieving skin inflammation according to claim 3, wherein the supercritical CO is₂The extraction conditions were: the temperature is 34-40 ℃; the pressure is 13-15 MPa; CO 2₂The circulation flow rate is 15-19 kg/min.

5. The male skin-refreshing lotion according to claim 1 or 2, characterized in that the preparation method of the mint extract comprises the following steps: drying mint in the sun, grinding the mint into powder, and taking normal hexane as a solvent, wherein the ratio of material to liquid is 1g: 10-15 mL, heating and extracting at 55-65 ℃ for 6-8 hours, and concentrating and drying the product to obtain the mint extract.

6. The male skin-refreshing lotion according to claim 1 or 2, wherein the preparation method of the cherry extract comprises the following steps: squeezing fresh cherries, mixing the fresh cherries with 70% ethanol which is 3-5 times of the fresh cherries, extracting for 3-5 hours at 65-75 ℃, and sequentially extracting with ethyl acetate and petroleum ether in a ratio of 3: 1: extracting with water and ethyl acetate, concentrating, and drying to obtain fructus Pruni Pseudocerasi extract.

7. The male skin-refreshing lotion for the men according to claim 1 or 2, wherein the preparation method of the wormwood extract comprises the following steps: the wormwood is crushed, soaked in 70% ethanol for 1-2 hours according to the material-liquid ratio of 1g: 30-35 mL, then extracted at 95-100 ℃ for 2.5-3 hours, and the product is concentrated and dried to obtain the wormwood extract.

8. The male skin-refreshing lotion as claimed in claim 1 or 2, wherein the preparation method of the mung bean extract comprises the following steps: crushing mung beans to 70-80 meshes, adding the mung beans into water according to the material-liquid ratio of 1g to 20-35 mL, heating and stirring at 60-75 ℃ for 3-5 hours, centrifuging, and concentrating and drying supernatant to obtain the mung bean extract.