CN108938497B

CN108938497B - High-gloss moisturizing solid lip gloss rich in natural plant extracts and production process thereof

Info

Publication number: CN108938497B
Application number: CN201811112097.XA
Authority: CN
Inventors: 楼彪; 陈榕洪; 石蓓君; 从云玲
Original assignee: Hangzhou Weikela Investment Co ltd; Yu Qiongfei
Current assignee: Hangzhou Weikela Investment Co., Ltd.; Yu Qiongfei
Priority date: 2018-09-21
Filing date: 2018-09-21
Publication date: 2021-07-06
Anticipated expiration: 2038-09-21
Also published as: CN108938497A

Abstract

The invention discloses a high-gloss moisturizing solid lip gloss rich in natural plant extracts and a production process thereof, belonging to the technical field of cosmetics, and the solid lip gloss comprises the following components: 1-15 parts of a plastic forming agent; 1-6 parts of ethylene/propylene/styrene copolymer; 3-40 parts of a first emollient; 2-10 parts of petrolatum; 0.1-1 part of tocopherol acetate; 1-37 parts of a second emollient; 1-5 parts of propylene glycol dibenzoate; 0.005-0.015 parts of skin conditioner; 10-20 parts of a color paste composition; the plastic forming agent comprises at least two of synthetic wax, polyethylene and microcrystalline wax; the first emollient comprises at least two of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate; the second emollient comprises at least two of dipentaerythritol hexacaprylate/hexacaprylate, tridecyl trimellitate, tridecyl stearate, neopentyl glycol dicaprylate/dicaprate. The solid lip gloss disclosed by the invention has the advantages of being easy to coat on lips and enabling the lips to have better light feeling and coloring effect.

Description

High-gloss moisturizing solid lip gloss rich in natural plant extracts and production process thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to a high-gloss moisturizing solid lip gloss rich in natural plant extracts and a production process thereof.

Background

Conventional lip colors can be generally divided into liquid and paste textures.

The solid lip gloss, namely the cream lip gloss, has the advantages of good covering property after makeup, fresh and cool use experience, no greasiness and good durability; when makeup which is relatively close to skin is needed, a lip brush or fingers are used, the use is inconvenient, and after the solid lip gloss is coated on the lips, the brightness of the surfaces of the lips is poor. Although the liquid lip gloss has the effects of convenient and sanitary use and bright color by a lip brush, the lip brush is difficult to achieve uniform smearing effect during smearing, sticky and heavy feeling is easy to appear after smearing, and the liquid lip gloss is not only easy to remove makeup, but also difficult to accept by many consumers due to the heavy feeling.

Therefore, the solid lip gloss which is easier to apply on the lips and enables the lips to have the light feeling and the coloring effect is more accepted by more consumers and has better market prospect.

Disclosure of Invention

Aiming at the defects in the prior art, the invention aims to provide the high-gloss moisturizing solid lip gloss rich in natural plant extracts, which is easy to apply to lips during application and enables the lips to have good gloss and coloring effects.

In order to achieve the first purpose, the invention provides the following technical scheme:

the high-gloss moisturizing solid lip gloss rich in natural plant extracts comprises the following components in parts by weight:

1-15 parts of a plastic forming agent;

1-6 parts of ethylene/propylene/styrene copolymer;

3-40 parts of a first emollient;

2-10 parts of petrolatum;

0.1-1 part of tocopherol acetate;

1-37 parts of a second emollient;

1-5 parts of propylene glycol dibenzoate;

0.005-0.015 parts of skin conditioner;

10-20 parts of a color paste composition;

0.02-0.5 part of vegetable oil mixture;

the plasticizer comprises at least two of synthetic wax, polyethylene and microcrystalline wax;

the first emollient comprises at least two of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate;

the second emollient comprises at least two of dipentaerythritol hexacaprylate/hexadecanoate, tridecyl trimellitate, tridecyl stearate, neopentyl glycol dicaprylate/dicaprate;

the skin conditioner comprises at least four of caprylic/capric triglyceride, phytosterol, glyceryl stearate, tocopherol acetate, hydrogenated lecithin, bisabolol, and Glycyrrhrizae radix extract;

the color paste composition consists of a colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate;

the vegetable oil and fat mixture comprises at least two of sunflower seed oil, shea butter, olive fruit oil and rose oil.

Through the technical scheme, in the plastic forming agent, the synthetic wax, the polyethylene and the microcrystalline wax have thickening and bonding effects to a certain degree, and the synthetic wax also has antistatic and skin softening effects; the polyethylene has a good film forming effect and is also beneficial to improving the emulsification stability; the microcrystalline wax also has a certain effect of improving the stability of emulsification.

The ethylene/propylene/styrene copolymer has lipophilic and viscosity-increasing effects, contributes to a better intermixing effect with the components in the present application, and provides a sticky feeling between the components.

In the first emollient, hydrogenated dimeric decene and hydrogenated polyisobutene both have certain effects of increasing skin softness. Isononyl isononanoate is non-sticky and has a good emollient effect on the skin, helps to increase intermixing with other components, and helps to improve the smoothing effect of the solid lip gloss in the present application.

Petrolatum has antistatic and skin softening effects, and helps to retain moisture in the skin.

Therefore, through the mutual matching of the plasticizer, the ethylene/propylene/styrene copolymer, the first emollient and the petrolatum, the components in the application are fully dispersed, a proper sticky feeling is formed, and the formation of the solid lip gloss is facilitated.

In the second emollient, the dipentaerythritol hexacaprylate/hexadecanoate has better lipophilicity, better emulsification effect and certain concealing capacity. The tridecyl alcohol trimellitate has excellent skin-friendly and skin-moistening effects, heavy skin feel but no greasiness, and a good dispersing effect. The tridecyl alcohol stearate can make the skin smooth and soft; the neopentyl glycol dicaprylate/dicaprate not only can lock moisture and moisten skin, but also has no greasy feeling, can keep the air permeability of the skin, and is not easy to cause phenomena such as acne growth and the like on the skin.

The propylene glycol dibenzoate has good compatibility, and can form good compatibility effect with the components in the application, thereby being beneficial to improving the mixing effect of various components in the application.

Therefore, the second emollient and the propylene glycol dibenzoate are matched with each other, so that the solid lip gloss formed in the application can be used for enabling the surface of lips to have better mirror surface gloss after the lips are coated.

In the vegetable oil mixture, the sunflower seed oil contains abundant vitamin E and linoleic acid, has special fragrance, and also has effects of moistening skin, promoting epidermis defense ability, resisting oxidation, etc. The shea butter contains triterpene alcohol, vitamin E, vitamin A and allantoin, and is helpful for preventing water loss in tender lip skin, so as to keep the lip skin moist, promote wound healing on the lip skin, and increase defense ability and softness of the lip skin. The olive oil and the rose oil have the functions of moistening skin and keeping moisture, and can ensure that the tender lip skin locks moisture to achieve the moistening effect. The components are all extracted from natural plants, are natural and harmless, and are beneficial to the health of a user while the lip skin of the user is kept soft and moist.

In the skin conditioner, caprylic/capric triglyceride has pleasant fragrance, high refreshing degree, no greasy feeling, and good lubricating and dispersing effects. The phytosterol has mild odor, and can enter skin along with alcohol substances to improve skin moisturizing and nourishing effects. The glyceryl stearate and the hydrogenated lecithin have good emulsification effect, and the glyceryl stearate can also play a role in softening and lubricating the skin. The tocopherol acetate can play a good role in resisting oxidation and locking water, so that the skin is soft and moist, and has a certain ultraviolet resistance. The bisabolol has tranquilizing, antibacterial, and skin defense effects. The licorice root extract has good effect of enhancing the self-healing capability of skin.

Wherein the preparation process of the licorice root extract comprises the following steps:

pulverizing Glycyrrhrizae radix to obtain Glycyrrhrizae radix powder, mixing Glycyrrhrizae radix powder with ethanol water solution at a ratio of 1: 20, ultrasonic extracting at power of 150W, frequency of 40kHz and temperature of 25 deg.C for 30min, filtering with 0.45 μm microporous membrane, and vacuum rotary evaporating the filtrate under vacuum degree of 0.096MPa for 30min to obtain Glycyrrhrizae radix extract.

The vegetable fat blend interacts with the skin conditioner to help improve the moisturizing effect of the solid lip gloss formed herein and to provide a glossy finish to the solid lip gloss as occurs when applying a liquid lip gloss.

In the color paste composition, the tridecyl trimellitate and the diisostearyl malate have good skin softening effect. The ethylhexyl palmitate is a micromolecular substance, is easy to permeate pores and keratinocytes, has a good moistening effect, is fresh and cool in texture, has no greasy feeling, and is easy to push away. The caprylic/capric triglyceride has high freshness, is odorless, and has good lubricating and dispersing effects. The silica dimethyl silylate has a better anti-caking effect, and also has a certain defoaming effect and an enhanced emulsifying effect. Therefore, under the combined action of tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate, the coloring agent can be uniformly dispersed, the coloring effect of the coloring agent can be improved, and the solid lip gloss can endow bright and full color to the skin of lips when in use.

Thus, the combination of the skin conditioner and the color paste composition can help the solid lipstick formed in the application have better coloring effect on lips.

More preferably: the plasticizer consists of synthetic wax, polyethylene and microcrystalline wax in a weight part ratio of 4:3.5: 4.

Through above-mentioned technical scheme, synthetic wax, polyethylene, micrite wax form and mutually support, help improving the mixed effect of the component that adds in this application.

More preferably: the first emollient is composed of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate and petrolatum in a weight portion ratio of 2-2.5: 1-1.3:1.5-2: 1.

Through the technical scheme, the hydrogenated dimeric decene, the hydrogenated polyisobutene, the isononyl isononanoate and the petrolatum are matched with one another, so that the formed solid lip gloss has a moisturizing effect, lips can be kept moist and full after the lip gloss is applied, and phenomena such as chapping and lip wrinkle increase are not prone to occurring.

More preferably: the second emollient is composed of dipentaerythritol hexacaprylate/hexadecanoate, tridecanol trimellitate, tridecanol stearate and neopentyl glycol dicaprylate/dicaprate in a weight portion ratio of 10-10.1:8-8.1:2: 1.

Through the technical scheme, the dipentaerythritol hexacaprylate/hexacaprylate, the tridecanol trimellitate, the tridecanol stearate and the neopentyl glycol dicaprylate/dicaprate in the weight ratio range are used together, so that the formed solid lip gloss is favorably coated on lips, the lips have better mirror surface bright feeling, and the air color of the lips is better.

More preferably: in the color paste composition, the weight part ratio of the colorant, the tridecyl trimellitate, the ethylhexyl palmitate, the caprylic/capric triglyceride, the diisostearyl malate and the dimethyl silylated silica is 4.102-4.558: 5.051-5.566: 2.081-2.368: 2.011-2.352: 0.692-1.135: 0.185-0.321.

Through the technical scheme, the coloring agent, the tridecyl alcohol trimellitate, the ethylhexyl palmitate, the caprylic/capric triglyceride, the diisostearyl malate and the silica dimethyl silylate are matched with one another within the proportion range, so that the color is convenient to attach to lips, and the lips have a good coloring effect.

More preferably: the colorant includes at least four of CI15850, CI15985, CI16035, CI77499, CI77891, CI 77491.

Through above-mentioned technical scheme, help making the solid lipstick in this application have comparatively abundant color, can satisfy different consumers' diversified demand.

More preferably: in the colorant, the weight part ratio of CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 is 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Through the technical scheme, the pigments in the proportion are matched with each other, so that the formed solid lip gloss has rich and full color, and the lips can have full color and better layering after being smeared.

More preferably: also comprises 0.1 to 0.8 weight part of preservative, and the preservative consists of phenoxyethanol and caprylyl glycol according to the weight part ratio of 1:0.5 to 1.8.

According to the technical scheme, the phenoxyethanol and the caprylyl glycol are matched according to the weight part ratio, and the formed preservative has a mild preservative effect and is not easy to damage tender skin of lips.

The second purpose of the invention is to provide a production process of the high-gloss moisturizing solid lip gloss rich in natural plant extracts, which is beneficial to ensuring that the prepared solid lip gloss is fine and smooth in texture, free of agglomeration and good in forming effect.

In order to achieve the second purpose, the invention provides the following technical scheme:

a production process of a high-gloss moisturizing solid lip gloss rich in natural plant extracts comprises the following steps:

mixing an ethylene/propylene/styrene copolymer and a first emollient according to parts by weight, standing for 8-12h, heating to 110 +/-5 ℃, fully mixing until no impurity particles exist, cooling to 40 +/-5 ℃, and grinding to obtain a first mixture;

step two, adding a plastic forming agent, petrolatum, a second emollient and propylene glycol dibenzoate into the first mixture obtained in the step one according to parts by weight, mixing, heating to 95 +/-5 ℃, and fully mixing until no impurity particles exist to obtain a second mixture;

step three, adding a colorant, tridecyl alcohol trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate into the second mixture obtained in the step two according to the parts by weight, and fully mixing to obtain a third mixture;

step four, cooling the third mixture obtained in the step three to 75 +/-5 ℃, preserving heat, adding the tocopherol acetate, the skin conditioner and the vegetable oil mixture into the third mixture cooled to 75 +/-5 ℃ according to parts by weight, and fully mixing to obtain a fourth mixture;

and step five, filling and forming the fourth mixture obtained in the step four to obtain the solid lip gloss.

Through the technical scheme, in the first step, the temperature is adjusted to be higher, so that the ethylene/propylene/styrene copolymer and the first emollient can be fully mixed, and then the mixture is cooled and is convenient to grind, so that the first mixture has relatively fine texture. And the plastic forming agent, the petrolatum, the second emollient and the propylene glycol dibenzoate are added into the first mixture obtained after the temperature is reduced, and the temperature is raised, so that the added plastic forming agent, the petrolatum, the second emollient and the propylene glycol dibenzoate can be fully mixed with the first mixture to form a second mixture.

Then, the colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate are added into the second mixture, and under the combined action of tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate, the colorant can be smoothly and sufficiently mixed with the second mixture, so that the formed third mixture has uniform and full color.

And cooling the third mixture to 75 +/-5 ℃, and adding the tocopherol acetate, the skin conditioner and the vegetable oil mixture, so that the active ingredients in the tocopherol acetate, the skin conditioner and the vegetable oil mixture are not easily damaged, and the formed fourth mixture has good moistening and anti-aging effects.

Finally, the solid lipstick after filling and forming not only has bright and full appearance, but also has fine texture, and after being coated on the lips, the lip surface can have a glossy effect, and the lip lipstick has excellent moistening degree, and is not easy to cause the lip to crack.

More preferably: in the fourth step, the phenoxyethanol and the caprylyl glycol are fully mixed according to the parts by weight to form the preservative, and the preservative, the tocopheryl acetate, the skin conditioner and the vegetable oil mixture are added into the third mixture obtained in the third step and fully mixed.

Through above-mentioned technical scheme, mix phenoxyethanol, caprylyl glycol earlier and form the antiseptic, add to the third mixture in, help improving the mixing homogeneity between antiseptic and the third mixture, make the solid lipstick that finally obtains in this application have fine and smooth, even texture, the difficult phenomenon that appears agglomerating, caking.

In conclusion, the invention has the following beneficial effects:

1. the mutual matching of the plasticizer, the ethylene/propylene/styrene copolymer, the first emollient and the petrolatum is beneficial to enabling the formed solid lip gloss to be easily and uniformly smeared during use, so that the smearing operation is simpler;

2. the second emollient and the propylene glycol dibenzoate are matched with each other, so that the formed solid lip gloss can be applied to lips, and the surfaces of the lips have good mirror surface brightness;

3. the skin conditioner and the color paste composition are matched with each other, so that the formed solid lipstick has a good coloring effect on lips;

4. the vegetable oil mixture interacts with the skin conditioning agent, thereby helping to improve the moisturizing effect of the solid lip gloss formed in the present application.

Detailed Description

The present invention will be described in detail with reference to examples.

Example 1: the high-gloss moisturizing solid lip gloss rich in natural plant extracts comprises the components and the corresponding parts by weight shown in table 1, and is produced and obtained through the following steps:

mixing an ethylene/propylene/styrene copolymer and a first emollient, standing for 8-12h, heating to 110 +/-5 ℃, fully mixing until no impurity particles exist, cooling to 40 +/-5 ℃, and grinding to obtain a first mixture;

step two, adding a plasticizer, petrolatum, a second emollient and propylene glycol dibenzoate into the first mixture obtained in the step one, mixing, heating to 95 +/-5 ℃, and fully mixing until no impurity particles exist, so as to obtain a second mixture;

step three, adding a coloring agent, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate, and silica dimethyl silylate to the second mixture obtained in step two, and sufficiently mixing to obtain a third mixture;

step four, cooling the third mixture obtained in the step three to 75 +/-5 ℃, preserving heat, adding the tocopherol acetate, the skin conditioner and the vegetable oil mixture into the third mixture cooled to 75 +/-5 ℃, and fully mixing to obtain a fourth mixture;

Wherein the plasticizer consists of synthetic wax, polyethylene and microcrystalline wax with the weight portion ratio of 4:3.5: 4. The first emollient is composed of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate and petrolatum with the weight portion ratio of 2.312: 1.176: 1.6: 1. The second emollient is composed of dipentaerythritol hexacaprylate/hexadecanoate, tridecyl trimellitate, tridecyl stearate, neopentyl glycol dicaprylate/dicaprate in a weight ratio of 10: 8: 2: 1. In the color paste composition, the weight part ratio of the colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and dimethyl silylated silica is 4.357: 5.132: 2.121: 2.121: 1.067: 0.202; the colorant is composed of CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 in parts by weight of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17. The skin conditioner comprises caprylic/capric triglyceride, phytosterol, glycerol stearate, tocopheryl acetate, hydrogenated lecithin, bisabolol and Glycyrrhrizae radix extract at weight ratio of 1: 1. The vegetable oil comprises sunflower seed oil, shea butter, olive oil and rose oil in a weight ratio of 1: 1.

In addition, propylene glycol dibenzoate was purchased from INOLEX, usa.

Example 2: the highlight moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 1 in that the included components and the corresponding parts by weight are shown in the table 1. And a preservative is also added, wherein the preservative consists of phenoxyethanol and caprylyl glycol in a weight ratio of 1: 1. And in the production process, firstly, sufficiently mixing phenoxyethanol and caprylyl glycol to form a preservative, adding the preservative into the fourth step, adding the preservative, the tocopherol acetate, the skin conditioner and the vegetable oil mixture into the third mixture obtained in the third step, and sufficiently mixing.

Example 3: the highlight moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the components and the corresponding parts by weight are shown in table 1, and the preservative consists of phenoxyethanol and caprylyl glycol in a weight part ratio of 1: 0.5.

Examples 4 to 5: the highlight moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the components and the corresponding parts by weight are shown in table 1, and the preservative consists of phenoxyethanol and caprylyl glycol in a weight part ratio of 1: 1.8.

TABLE 1 Components and their corresponding parts by weight as included in examples 1-5

Example 6: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that a first emollient is composed of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate and petrolatum in a weight portion ratio of 2: 1.3: 1.5: 1.

Example 7: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that a first emollient is composed of hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate and petrolatum in a weight portion ratio of 2.5: 1:2: 1.

Example 8: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that a first emollient is composed of hydrogenated dimeric decene and hydrogenated polyisobutene in a weight portion ratio of 2.312: 1.176.

Example 9: a high light moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that the second emollient consists of dipentaerythritol hexacaprylate/hexacaprylate, tridecanol trimellitate, tridecanol stearate, neopentyl glycol dicaprylate/dicaprate in a weight ratio of 10.05: 8: 2: 1.

Example 10: a high light moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that the second emollient consists of dipentaerythritol hexacaprylate/hexacaprylate, tridecyl alcohol trimellitate, tridecyl alcohol stearate, neopentyl glycol dicaprylate/dicaprate in a weight ratio of 10.1: 8.1:2: 1.

Example 11: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the second emollient is composed of dipentaerythritol hexacaprylate/hexacaprylate, tridecyl alcohol trimellitate, and neopentyl glycol dicaprylate/dicaprate in a weight ratio of 10: 8: 1.

Example 12: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the second emollient is composed of dipentaerythritol hexacaprylate/hexacaprylate and tridecyl alcohol stearate in a weight ratio of 5: 1.

Example 13: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the color paste composition comprises a colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and dimethyl silylated silica in a weight part ratio of 4.102: 5.051: 2.081: 2.011: 0.692: 0.185; the colorant is composed of CI15850, CI15985, CI16035, C177499, CI77891 and CI77491 in the weight portion ratio of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Example 14: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the color paste composition comprises the colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and dimethyl silylated silica in a weight part ratio of 4.558: 5.566: 2.368: 2.352: 1.135: 0.321; the colorant is composed of CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 in parts by weight of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Example 15: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that a color paste composition is prepared from a colorant with the weight part ratio of 4.357: 5.132: 2.121: 2.121: 1.067, tridecyl alcohol trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride and diisostearyl malate; the colorant is composed of CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 in parts by weight of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Example 16: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the color paste composition comprises a colorant, tridecyl trimellitate, caprylic/capric triglyceride, diisostearyl malate and silica dimethyl silylate in a weight part ratio of 4.357: 5.132: 2.121: 1.067: 0.202; the colorant is composed of CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 in parts by weight of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Example 17: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that a skin conditioner consists of phytosterol, glycerol stearate, tocopherol acetate, hydrogenated lecithin, bisabolol and licorice root extracts in a weight ratio of 1: 3: 1:2: 1.

Example 18: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that a skin conditioner consists of caprylic acid/capric acid triglyceride, phytosterols, hydrogenated lecithin, bisabolol and licorice root extracts in a weight ratio of 1: 1.5: 1.2: 1: 1.1.

Example 19: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from example 2 in that a skin conditioner consists of tocopherol acetate, hydrogenated lecithin, bisabolol and licorice root extracts in a weight portion ratio of 1.3: 1.8: 1: 1.2.

Example 20: the highlight moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the plasticizer consists of synthetic wax and microcrystalline wax in a weight ratio of 1: 1.

Example 21: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that a plasticizer consists of synthetic wax and polyethylene in a weight ratio of 4: 3.5.

Example 22: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from that in example 2 in that the plant oil and fat consists of sunflower seed oil, shea butter, olive oil and rose oil in a weight ratio of 3: 1: 2.

Example 23: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from that in example 2 in that the plant oil and fat consists of sunflower seed oil, shea butter, olive oil and rose oil in a weight ratio of 2: 3:1.

Example 24: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the vegetable oil consists of shea butter, olive oil and rose oil in a weight ratio of 2: 1: 1.5.

Example 25: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the plant oil and fat consists of sunflower seed oil, shea butter and rose oil in a weight ratio of 1:2: 3.

Example 26: a high-gloss moisturizing solid lip gloss rich in natural plant extracts is different from the lip gloss in example 2 in that the vegetable oil and fat consist of sunflower seed oil and shea butter in a weight portion ratio of 2: 1.

Comparative example 1: the solid lip gloss is different from the solid lip gloss in example 2 in that the solid lip gloss is selected from example 1 in the light and thin matt lip gloss of Chinese invention patent with application publication number CN106913472A and application publication date of 2017, 07, 04.

Comparative examples 2 to 6: a solid lip gloss differs from example 2 in that the components included and their respective parts by weight are shown in Table 2.

TABLE 2 Included components of comparative examples 2-6 and their corresponding parts by weight

Comparative examples 7 to 9: a solid lip gloss differs from example 2 in that the components included and their respective parts by weight are shown in Table 3.

TABLE 3 Included components of comparative examples 7-9 and their corresponding parts by weight

Comparative examples 10 to 12: a solid lip gloss differs from example 2 in that the components included and their respective parts by weight are shown in Table 4.

TABLE 4 Components included in comparative examples 10-12 and their corresponding parts by weight

Comparative example 13: a solid lip gloss differs from example 2 in that the skin conditioner consists of caprylic/capric triglyceride, phytosterols, glyceryl stearate in a weight ratio of 1: 1.

Comparative example 14: a solid lip gloss differs from comparative example 10 in that the mill base composition is replaced by a colorant and the colorant is comprised of CI15850, CI15985, CI16035, CI77499, CI77891, and CI77491 in parts by weight of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

Comparative example 15: a solid lip gloss which differs from example 2 in the absence of both a skin conditioner and a vegetable oil mixture.

Comparative example 16: a solid lip gloss distinguished from example 2 by the absence of a vegetable oil mixture.

Comparative example 17: a solid lip gloss is different from the lip gloss in example 2 in that the weight part of the skin conditioner is 0.001 part, and the weight part of the vegetable oil and fat mixture is 0.005 part.

Test one: smearing test

Test samples: examples 1 to 21 were selected as test samples 1 to 21, and comparative examples 1 to 6 were selected as control samples 1 to 6.

The test method comprises the following steps: the method comprises selecting 270 female white collars (hereinafter referred to as subjects) with skin health, non-allergic constitution and age stage of 28-35 years in the same area, face and lip, and dividing into 27 groups of 10 persons; wherein, the test subjects of the 1 st to 21 st groups respectively adopt the test samples 1 to 21 to carry out the smearing test, the test subjects of the 22 nd to 27 th groups respectively adopt the comparison samples 1 to 6 to carry out the smearing test and then carry out the scoring, wherein, 5 points are that the smearing is very smooth and very even, 4 points are that the smearing is smooth and even, 3 points are that the smearing is comparatively smooth and comparatively even, 2 points are that the smearing is not very smooth and not very even, 1 point is that the smearing is very rough and uneven, the scoring record of each test subject is recorded, and the highest score and the lowest score in each group are removed and are subjected to average treatment, 2 decimal places are taken, and the average scoring value of each group of test subjects is recorded.

And (3) test results: the average score values of the subjects using test samples 1 to 21 and control samples 1 to 6 during the application are shown in Table 5.

TABLE 5 mean score values during application for subjects using test samples 1-21 and controls 1-6

Test sample used	Average score value	Test sample used	Average score value
				Test sample 1	4.89	Test specimen 15	4.92
Test sample 2	4.92	Test specimen 16	4.93
				Test sample 3	4.92	Test specimen 17	4.92
Test sample 4	4.93	Test specimen 18	4.92
				Test sample 5	4.93	Test specimen 19	4.93
Test sample 6	4.92	Test specimen 20	4.85
				Test sample 7	4.93	Test specimen 21	4.86
Test specimen 8	4.88	Control 1	3.82
				Test sample 9	4.93	Control 2	3.85
Test specimen 10	4.92	Control 3	3.16
				Test specimen 11	4.92	Control 4	2.52
Test specimen 12	4.92	Control 5	1.88
				Test specimen 13	4.92	Control 6	3.22
Test specimen 14	4.93	/	/

As can be seen from Table 5, the test subjects in groups 1-21 have higher average scores of test samples 1-21, which are all above 4.8, indicating that the test samples 1-21 are easier to spread evenly and are convenient to operate. The situation that the test subject using the control sample 1 scores the control sample 1 is not ideal, and the average score value is only 3.82, which indicates that the components and the corresponding amount used in the control sample 1 are not beneficial to the uniform smearing of the test samples 1-21; subjects using controls 2-6 scored controls 2-6 lower with an average score of 3.85 or even below, indicating controls 2-6 were more labourious and unevenly smeared during application due to the absence or improper amount of components of the plasticizer, ethylene/propylene/styrene copolymer, first emollient, petrolatum.

And (2) test II: test for light sensation

Test samples: examples 1 to 21 were selected as test samples 1 to 21, and comparative examples 7 to 9 were selected as control samples 7 to 9.

The test method comprises the following steps: selecting 240 female white collars (hereinafter referred to as subjects) with skin health, non-allergic constitution and age stage of 28-35 years in the same area, face and lip, and dividing into 24 groups of 10 persons in each group; wherein, the test subjects of the 1 st to 21 st groups respectively adopt test samples 1 to 21 to carry out smearing tests, the test subjects of the 22 nd to 24 th groups respectively adopt control samples 7 to 9 to carry out smearing tests, and then are scored, wherein, 5 is very bright, 4 is bright, 3 is relatively bright, 2 is not too bright, 1 is not bright, the scoring record of each test subject is recorded, the highest score and the lowest score in each group are removed and are subjected to average treatment, 1 decimal is taken, and the average scoring value of each test subject is recorded.

And (3) test results: the light sensation of the test samples 1 to 21 and the control samples 7 to 9 is shown in Table 6.

TABLE 6 light feeling of test samples 1 to 21 and control samples 7 to 9

Test sample	Mean average luminous sensation	Test sample	Mean average luminous sensation
				Test sample 1	4.5	Test specimen 13	4.6
Test sample 2	4.7	Test specimen 14	4.6
				Test sample 3	4.6	Test specimen 15	4.5
Test sample 4	4.7	Test specimen 16	4.6
				Test sample 5	4.7	Test specimen 17	4.6
Test sample 6	4.6	Test specimen 18	4.7
				Test sample 7	4.7	Test specimen 19	4.6
Test specimen 8	4.6	Test specimen 20	4.3
				Test sample 9	4.6	Test specimen 21	4.4
Test specimen 10	4.7	Control 7	2.8
				Test specimen 11	4.2	Control sample 8	3.2
Test specimen 12	4.1	Control 9	3.2

As is clear from Table 6, the test specimens 1 to 21 maintained a good mirror-like gloss on the lips after application, while the control specimens 7 to 9 all had a lower gloss than the test specimens 1 to 21. The main reasons for this phenomenon are: in controls 7-9, there was a corresponding reduction in the amount of second emollient and propylene glycol dibenzoate, resulting in a reduction in shine.

While test samples 11 and 12 had inferior shine compared to the other test samples, but were much better than the shine of control samples 7-9, mainly due to the reduced number of components in the second emollient, which also demonstrates that the second emollient and propylene glycol dibenzoate cooperate to improve the shine of the test samples.

And (3) test III: coloring effect test

Test samples: examples 1 to 21 were selected as test samples 1 to 21, and comparative examples 10 to 14 were selected as control samples 10 to 14.

The test method comprises the following steps: selecting 260 female white collars (hereinafter referred to as subjects) with skin health, non-allergic constitution and age stage of 28-35 years in the same area, face and lip, and dividing into 26 groups of 10 persons; wherein, the test subjects of the 1 st to 21 st groups respectively adopt the test samples 1 to 21 to carry out the smearing test, the test subjects of the 22 nd to 26 th groups respectively adopt the control samples 10 to 14 to carry out the smearing test, each test subject is evenly smeared with two layers, so that lips are fully covered by the corresponding test samples, the lip coloring effect of each group of test subjects is observed when the smearing is finished, and the record is carried out; after 30min after finishing smearing, each subject drinks water by adopting a white ceramic cup, the residual quantity of the lip gloss on the cup edge is observed and recorded; after 4h, lightly pressing and wiping the corresponding test sample smeared on the lips of each test subject by using a piece of facial tissue with a heart print, observing the coloring condition of the lips of each group of test subjects, recording and finally analyzing.

And (3) test results: the coloring effects of the test samples 1 to 21 and the control samples 10 to 14 are shown in Table 7.

TABLE 7 coloring effect of test samples 1 to 21 and control samples 10 to 14

Test sample	Just after application	Immediately after smearing for 30min	After the paint is applied for 4 hours
				Test sample 1	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test sample 2	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test sample 3	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test sample 4	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test sample 5	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test sample 6	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test sample 7	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test specimen 8	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test sample 9	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test specimen 10	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test specimen 11	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
Test specimen 12	Bright and full color	The residual quantity of the cup rim is very little	Is still bright and full
				Test specimen 13	Bright and full color	The cup rim has less residual quantity	Is still bright and full
Test specimen 14	Bright and full color	The cup rim has less residual quantity	Is still bright and full
				Test specimen 15	Has bright and full color	The residual quantity of the cup rim is small	Is bright and full
Test specimen 16	Has bright and full color	The residual quantity of the cup rim is small	Is bright and full
				Test specimen 17	Bright and full color	The cup rim has less residual quantity	Is still bright and full
Test specimen 18	Has bright and full color	The residual quantity of the cup rim is small	Is bright and full
				Test specimen 19	Has bright and full color	The residual quantity of the cup rim is small	Is bright and full
Test specimen 20	Bright and full color	The cup rim has less residual quantity	Is still bright and full
				Test specimen 21	Bright and full color	The cup rim has less residual quantity	Is still bright and full
Control sample 10	The color is not bright and full	The cup rim has much residue	The color is not bright and is not full
				Control sample 11	Colorful but not full enough	The cup rim has more residual quantity	The color is not bright and is not full
Control sample 12	The color is not bright enough and full	The cup rim has more residual quantity	The color is not bright and is not full
				Control 13	Has bright and full color	The cup rim has more residual quantity	The color is not bright and is not full
Control sample 14	Colorful but not full enough	The cup rim has much residue	The color is not bright and is not full

As can be seen from Table 7, the degrees of vividness and fullness of the colors of the test samples 1-21 immediately after application and after application for 4 hours are better than those of the control samples 10-14 immediately after application and after application for 4 hours, which indicates that the skin conditioner and the color paste composition are matched with each other and is helpful for improving the coloring effect of the test samples 1-21. The subjects used test samples 15, 16, 18, and 19, which were slightly less colorful and full than the other test samples, mainly caused the following phenomena: in test samples 15 and 16, the number of components in the colorant was reduced, which easily caused a reduction in the saturation and the degree of beauty of the color; in test samples 18-19, the reduction in the components used in the skin conditioner also resulted in a deterioration in the coloring effect of the colorant on the lips, mainly manifested in the saturation and gorgeous degree of color; furthermore, the lack of ingredients, whether in the colorant or skin conditioner, tends to result in a long-lasting coloration of the test sample on the lips, resulting in a tendency to stick to the cup or to be wiped off with a paper towel, i.e., a tendency to fade.

And (4) testing: moisturizing effect test

Test samples: examples 1-2 and examples 22-26 were selected as test samples 1-2 and 22-26, and comparative examples 15-17 were selected as control samples 15-17.

The test method comprises the following steps: : 100 subjects in the same area, 20-25 years old and healthy lip skin are selected and divided into 10 groups on average, and 10 subjects in each group are selected. Wherein, the 1 st to 7 th groups use the 1 st to 2 nd test samples 22 to 26 respectively, and the 8 th to 10 th groups use the 15 th to 17 th control samples respectively.

The lips of the testees in each group are cleaned by the same facial cleanser (no discomfort occurs in the testees), and after the lips are naturally dried, the lip skin moisture content data of the testees in each group is measured, namely X1; and smearing the corresponding test sample by using the corresponding test sample, wherein the using amount is 0.2 mL/person, after smearing and 3 hours, lightly wiping the test sample smeared on the lips by using the same cosmetic, and then testing the moisture content of the skin of the lips of each group of test subjects, namely X2. The average change of the moisture content of the lip skin of each group of testees before and after the application of the test sample for 3 hours is calculated (X2-X1 is calculated, and then each group is subjected to average treatment), recorded and analyzed.

And (3) test results: the average change in the moisture content of the skin of lips of the subjects using the test samples 1 to 2, the test samples 22 to 26 and the control samples 15 to 17 before and after the application of the test samples for 3 hours is shown in Table 8.

TABLE 8 average change in lip skin moisture content of test subjects using test samples 1-2, test samples 22-26, and control samples 15-17 before and after applying test sample for 3h

Test sample used	Average change rate of lip skin moisture content%
		Test sample 1	6.35
Test sample 2	6.28
		Test specimen 22	6.52
Test specimen 23	6.47
		Test specimen 24	6.08
Test specimen 25	5.95
		Test specimen 26	5.78
Control sample 15	2.16
		Control sample 16	2.81
Control sample 17	2.53

As can be seen from Table 8, the average change rate of the moisture content of the lip skin of each group was higher in the subjects using the test samples 1-2 and 22-26, which indicates that the moisture content of the lip skin was greatly increased after the test samples 1-2 and 22-26 were applied, and indicates that the effects of moisturizing and locking water and moisturizing the lip skin were better. The average change rate of the lip skin moisture content of each group of the subjects using the control samples 15 to 17 was much lower than that of the subjects using the test samples 1 to 2 and the test samples 22 to 26, indicating that the moisturizing effect of the control samples 15 to 17 was not good enough. The reasons for the above phenomenon are: the control sample 15 did not contain the skin conditioner and the vegetable oil and fat mixture, the control sample 16 did not contain the vegetable oil and fat mixture, and the control sample 17 added with the skin conditioner and the vegetable oil and fat mixture, but the addition amounts of the skin conditioner and the vegetable oil and fat mixture were all less than the addition amounts of the skin conditioner and the vegetable oil and fat mixture in the test samples 1-2 and 22-26. Therefore, the skin conditioner and the vegetable oil and fat mixture are mutually matched, which is helpful for improving the moisturizing effect of the formed test samples 1-2 and 22-26.

The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims

1. The high-gloss moisturizing solid lip gloss rich in natural plant extracts is characterized by comprising the following components in parts by weight:

1-15 parts of a plastic forming agent;

1-6 parts of ethylene/propylene/styrene copolymer;

3-40 parts of a first emollient;

2-10 parts of petrolatum;

0.1-1 part of tocopherol acetate;

1-37 parts of a second emollient;

1-5 parts of propylene glycol dibenzoate;

0.005-0.015 parts of skin conditioner;

10-20 parts of a color paste composition;

0.02-0.5 part of vegetable oil mixture;

the skin conditioner consists of caprylic acid/capric acid triglyceride, phytosterol, glycerol stearate, tocopheryl acetate, hydrogenated lecithin, bisabolol and licorice root extract in a weight part ratio of 1: 1;

the vegetable oil mixture consists of sunflower seed oil, shea butter, olive oil and rose oil in a weight ratio of 1: 1;

the plasticizer consists of synthetic wax, polyethylene and microcrystalline wax in a weight ratio of 4:3.5: 4;

the first emollient is prepared from the following components in parts by weight of 2-2.5: 1-1.3:1.5-2:1 hydrogenated dimeric decene, hydrogenated polyisobutene, isononyl isononanoate and petrolatum;

the second emollient is composed of dipentaerythritol hexacaprylate/hexadecanoate, tridecanol trimellitate, tridecanol stearate and neopentyl glycol dicaprylate/dicaprate in a weight ratio of 10-10.1:8-8.1:2: 1;

in the color paste composition, the ratio of the colorant, tridecyl trimellitate, ethylhexyl palmitate, caprylic/capric triglyceride, diisostearyl malate and dimethyl silylated silica in parts by weight is 4.102-4.558: 5.051-5.566: 2.081-2.368: 2.011-2.352: 0.692-1.135: 0.185-0.321;

the production process of the high-gloss moisturizing solid lip gloss rich in natural plant extracts comprises the following steps:

2. The natural plant extract-rich high gloss moisturizing solid lip gloss according to claim 1, wherein the colorant comprises at least four of CI15850, CI15985, CI16035, CI77499, CI77891 and CI 77491.

3. The natural plant extract-rich high-gloss moisturizing solid lip gloss according to claim 2, wherein the colorant comprises CI15850, CI15985, CI16035, CI77499, CI77891 and CI77491 in a weight ratio of 1.195: 0.148: 2.608: 0.023: 0.213: 0.17.

4. the high-gloss moisturizing solid lip gloss rich in natural plant extracts as claimed in claim 1, further comprising 0.1 part by weight of a preservative, wherein the preservative comprises phenoxyethanol and caprylyl glycol in a weight ratio of 1: 0.5-1.8.

5. The high-gloss moisturizing solid lip gloss rich in natural plant extracts as claimed in claim 1, wherein in the fourth step, phenoxyethanol and caprylyl glycol are fully mixed according to parts by weight to form a preservative, and the preservative, tocopherol acetate, a skin conditioner and a vegetable oil mixture are added into the third mixture obtained in the third step and fully mixed.