CN110025506B - Frosted color-changing lip balm and preparation method thereof - Google Patents
Frosted color-changing lip balm and preparation method thereof Download PDFInfo
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- CN110025506B CN110025506B CN201910264185.XA CN201910264185A CN110025506B CN 110025506 B CN110025506 B CN 110025506B CN 201910264185 A CN201910264185 A CN 201910264185A CN 110025506 B CN110025506 B CN 110025506B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/001—Preparations for care of the lips
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a frosted color-changing lip balm and a preparation method thereof, wherein the lip balm comprises the following components: thickening agent, adhesive, film forming agent, humectant, emollient, emulsifier, colorant, scrub agent, preservative, wherein the emollient comprises jojoba seed oil, Aralia mandshurica kernel oil and phytosterol isostearate. The frosted color-changing lip balm can repair damaged epidermis, enhance the barrier function of horny layer, has anti-inflammatory effect, can improve the dry and water-deficient state of skin, is convenient to use, can lock skin moisture, reduces irritation, and has attractive appearance and good use effect.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a frosted color-changing lip balm and a preparation method thereof.
Background
The main function of lip balm is to provide a barrier to moisture lock on the lips, as well as cosmetic purposes. The currently marketed lip balms are various in types and rich and diverse in color, and can be used for modifying lip shapes and lip colors, so that the lip balms are more and more popular with people; the frosted product is generally made of plastic frosted particles, and the plastic frosted particles can cause environmental pollution. The sucrose particles are not uniform in size, and the sucrose is not uniformly distributed in the paste body, so that the lips are easily scratched; the appearance is not beautiful, sucrose particles are on the surface, and the repair function of the lip is not obvious.
Disclosure of Invention
The invention aims to overcome the problems and provide a frosted color-changing lip balm with moisturizing and repairing effects and a preparation method thereof.
In order to achieve the purpose, the technical scheme adopted by the invention is that the frosted color-changing lip balm is characterized by comprising the following components: thickening agent, adhesive, film forming agent, humectant, emollient, emulsifier, colorant, scrub agent, preservative, wherein the emollient comprises jojoba seed oil, Aralia mandshurica kernel oil and phytosterol isostearate.
The jojoba seed oil is derived from one ester of jojoba and has the function of moisturizing the skin. Is not easy to be oxidized, and has high temperature resistance, high pressure resistance and small viscosity change. The jojoba oil is also rich in vitamin D and protein, is a good moisturizing and moisture-preserving oil, can maintain skin moisture, prevent wrinkles and soften skin.
Aralia spinosa kernel oil is a nut oil extracted from the fruit of the Argania spinosa tree. The oil is rich in fatty acids, vitamin E, squalene, sterol, etc., and is commonly used for treating skin diseases. The Aralia spinosa kernel oil is an important cosmetic oil and can improve good nourishing property and skin feeling. Has better oxidation resistance to human bodies, repairs lipid barriers of the skin and has certain repairing effect on sensitive skin.
The phytosterol is regarded as a 'life key' by scientists, the phytosterol mainly comprises beta-sitosterol, campesterol, stigmasterol, campesterol, corresponding alkanol and the like, wherein the beta-sitosterol is superior to other sterols in many effects, even has the effects which other sterols do not have, the phytosterol ester and the cholesterol have similar structures and can be mutually substituted, so that the homology of the phytosterol ester and the skin is very good, the compatibility and the skin sticking performance of the phytosterol ester and the skin are good, the skin feeling which is not comparatively moist and sticky is not generated is realized, the phytosterol isostearate has very high permeability to the skin, the surface moisture of the skin can be kept, the metabolism of the skin is promoted, the inflammation of the skin is inhibited, the sunburn erythema and the skin aging can be prevented, and the effects of growing and nourishing the hair are realized; has the characteristics of good use skin feeling (good spreadability, smoothness and no stickiness), good durability, difficult deterioration and the like.
The inventor of the application finds that the jojoba seed oil, the argania spinosa kernel oil and the phytosterol isostearate are combined for use, and the jojoba seed oil, the argania spinosa kernel oil and the phytosterol isostearate have excellent moisturizing and repairing effects.
In a preferred embodiment of the frosted color-changing lip balm, the skin moisturizer comprises 5-25 parts of jojoba seed oil, 2-10 parts of argania spinosa seed oil and 1-10 parts of phytosterol isostearate by weight. The moisture-preserving repair effect can be influenced by the weight part ratio of each component, and a large amount of experimental researches show that the moisture-preserving repair effect is better under the specific weight part ratio of each component.
In a preferred embodiment of the frosted color-changing lip balm, the skin moisturizer comprises 10-18 parts of jojoba seed oil, 3-6 parts of argania spinosa seed oil and 3-6 parts of phytosterol isostearate. The inventor of the application finds that the moisture-preserving repair effect is influenced by the weight part ratio of each component under the condition of the same addition amount, and a large number of experimental researches find that the moisture-preserving repair effect is better under the specific weight part ratio of each component.
In a preferred embodiment of the frosted color-change lip balm, the skin moisturizer comprises 14 parts of jojoba seed oil, 4 parts of argania spinosa seed oil and 5 parts of phytosterol isostearate by weight. Particularly, when the components are matched according to the weight part ratio, the best moisturizing and repairing effect can be obtained.
The preferred embodiment of the frosted color-changing lip balm comprises the following coloring agents, namely CI 45410, CI45370, CI 15850, CI 45410 and CI 19140, wherein the content of each ingredient in the coloring agents in the lip balm is CI 454100.01-1 part by weight, CI 453700.01-1 part by weight, CI 158500.01-1 part by weight, CI 454100.01-1 part by weight and CI 191400.01-1 part by weight.
According to the preferred embodiment of the frosted color-changing lip balm, the frosting agent is cane sugar, and the content of the cane sugar in the lip balm is 3-10 parts by weight; preferably, the frosting agent is sucrose treated by a 200-mesh screen. The invention sieves the cane sugar once by a 200-mesh sieve, so that the cane sugar becomes the grain size with the same grain size, the use feeling and the appearance are better, and the cane sugar can be uniformly distributed in the paste.
In a preferred embodiment of the frosted color-change lip gloss of the present invention, at least one of the following (a) to (g) is used:
(a) the thickening agent is microcrystalline wax or synthetic wax; the weight parts of the components in the thickening agent in the lip balm are 1-8 parts of microcrystalline wax and 1-8 parts of synthetic wax;
(b) the adhesive is candelilla wax, beeswax and hydrogenated polyisobutene; the weight parts of each component in the adhesive in the lip balm are 0.5-5 parts of candelilla wax, 1-10 parts of beeswax and 1-10 parts of hydrogenated polyisobutene;
(c) the film forming agent is polyethylene; the weight part content of the polyethylene in the lip balm is 1-8 parts;
(d) the humectant is a compound consisting of dipentaerythritol hexahydroxystearate, hexastearate and hexaabietate, and tridecyl alcohol trimellitate; the weight parts of all components in the moisturizer in the lip balm are 2-8 parts of a compound consisting of dipentaerythritol hexahydroxystearate, hexastearate and hexaabietate and 5-15 parts of tridecyl alcohol trimellitate;
(e) the emollient further comprises diisostearyl malate, glycerol tri (ethyl hexanoate); the components in the emollient comprise 5-20 parts by weight of glycerol tri (ethyl hexanoate) and 5-20 parts by weight of lip balm;
(f) the emulsifier is polyglycerol-2 triisostearate; the weight part content of the polyglycerol-2 triisostearate in the lip balm is 1-8 parts;
(g) the preservative is 0.05-0.8 part of glyceryl caprylate.
As a preferred embodiment of the frosted color-changing lip balm, the lip balm further comprises a pigment dispersant, an aromatizer and an antioxidant; the pigment dispersing agent comprises 5-20 parts by weight of pentaerythritol tetraisostearate; the aromatizing agent comprises 0.1-1 part of menthol, and the antioxidant comprises 0.1-1 part of pomegranate flower oil, 0.05-1 part of bisabolol and 0.05-1 part of tocopherol.
The frosted color-changing lip balm comprises the following components in parts by weight: 2.5 parts of microcrystalline wax, 5 parts of polyethylene, 5 parts of synthetic wax, 2.5 parts of beeswax, 1.5 parts of candelilla wax, 13 parts of diisostearyl malate, 4 parts of a compound consisting of dipentaerythritol hexahydroxystearate, hexastearate and hexaabietate, 10 parts of glycerol tri (ethyl hexanoate), 14 parts of jojoba seed oil, 3 parts of polyglycerol-2 triisostearate, 4 parts of argania spinosa kernel oil, 4 parts of hydrogenated polyisobutene, 5 parts of phytosterol isostearate, 10.17 parts of pentaerythritol tetraisostearate, 8.5 parts of tridecanol trimellitate, CI 454100.02 parts, CI 453700.08 parts, CI 158500.05 parts, CI 454100.03 parts, CI 191400.05 parts, 0.3 part of titanium dioxide, 6 parts of sucrose, 0.4 part of menthol, 0.2 part of pomegranate flower oil, 0.2 part of bisabolol, 0.2 part of tocopherol and 0.3 part of glycerol caprylate.
The invention also provides a preparation method of the frosted color-changing lip balm, which comprises the following steps:
1) heating microcrystalline wax, polyethylene, synthetic wax, beeswax, candelilla wax, and glycerol tri (ethyl hexanoate) to 95 deg.C until completely melted;
2) adding diisostearyl malate, dipentaerythritol hexahydrostearate/hexastearate/hexaabietate, jojoba seed oil, polyglycerol-2 triisostearate, argania spinosa oil, hydrogenated polyisobutene, phytosterol isostearate, pentaerythritol tetraisostearate and tridecanol trimellitate into the mixture in sequence 1), stirring and dissolving uniformly, and controlling the temperature to be 85-90 ℃;
3) mixing a proper amount of dissolved material body with CI 45410, CI45370, titanium dioxide, silica, alumina, CI 15850, CI 45410 and CI 19140 in the formula uniformly, grinding the mixture by using a grinder, adding the mixture into a main pot 1) for uniformly stirring and dispersing, and controlling the temperature to be 85 ℃;
4) sieving sucrose with 200 mesh sieve, adding into a pot, stirring, adding Mentholum, flos Granati oil, bisabolol, tocopherol, and glyceryl caprylate, stirring, and dispersing at 85 deg.C.
The invention has the beneficial effects that: the frosted color-changing lip balm can repair damaged epidermis, enhance the barrier function of horny layer, improve the dry and water-deficient state of skin, is convenient to use, can lock skin moisture, reduces irritation, and has beautiful appearance and good use effect.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
The raw materials in the following examples are all commercially available general-purpose materials unless otherwise specified.
The COSMOL 168ARV is a compound composed of dipentaerythritol hexahydroxystearate, hexastearate and hexaabietate.
Examples 1 to 7 and comparative examples 1 to 4
Examples 1 to 7 are examples of the frosted color-change lip gloss of the present invention, and the components and the weight parts of the examples 1 to 7 and the comparative examples 1 to 4 are shown in table 1:
TABLE 1
The method of making frosted color change lip gloss of examples 1-7 and comparative examples 1-4 includes the steps of:
1) heating microcrystalline wax, polyethylene, synthetic wax, beeswax, candelilla wax, and glycerol tri (ethyl hexanoate) to 95 deg.C until completely melted;
2) adding diisostearyl malate, dipentaerythritol hexahydrostearate/hexastearate/hexaabietate, jojoba seed oil, polyglycerol-2 triisostearate, argania spinosa oil, hydrogenated polyisobutene, phytosterol isostearate, pentaerythritol tetraisostearate and tridecanol trimellitate into the mixture in sequence 1), stirring and dissolving uniformly, and controlling the temperature to be 85-90 ℃;
3) mixing a proper amount of dissolved material body with CI 45410, CI45370, titanium dioxide, silica, alumina, CI 15850, CI 45410 and CI 19140 in the formula uniformly, grinding the mixture by using a grinder, adding the mixture into a main pot 1) for uniformly stirring and dispersing, and controlling the temperature to be 85 ℃;
4) sieving sucrose with 200 mesh sieve, adding into a pot, stirring, adding Mentholum, flos Granati oil, bisabolol, tocopherol, and glyceryl caprylate, stirring, and dispersing at 85 deg.C.
Comparative example 5
The lip balm of comparative example 5 has the same contents as those of example 1 except that the difference is that the preparation method comprises the step 4) of adding sucrose into a pot and stirring uniformly, adding menthol, pomegranate flower oil, bisabolol, tocopherol and caprylic glyceride and stirring uniformly to disperse, and controlling the temperature at 85 ℃.
Example 8
The physical and chemical properties of the lip balms prepared in examples 1 to 7 and comparative examples 1 to 4 were measured.
(first) Room temperature standing test
The lip balms prepared in examples 1 to 7 and comparative examples 1 to 4 were placed in a lipstick tube, and after standing at room temperature for 6 months, no delamination occurred, no change in feeling after use, and no change in odor.
(II) irritation and allergy test
The back of the white mouse was shaved, and the lip balms according to examples 1 to 7 and comparative examples 1 to 4 were applied to the shaved back, and compared with the portion without the lip balm, no irritation such as redness, rash, blister and the like occurred after 30 min.
Example 9
Evaluation of lip gloss Effect
The moisture contents of the lip balms prepared in examples 1 to 7 and comparative examples 1 to 4 in a silica gel drying environment were respectively tested for moisture retention rates of 4h, 8h, 16h and 24h according to the change with time, and the test results are shown in table 2:
(II) experimental method: human volunteers were randomly selected 220, with the age between 20-40 years. The lip balms of examples 1 to 7 and comparative examples 1 to 4 were applied to 20 persons per group for 1 month in the evening for each face washing. The volunteers were subjected to questionnaires and the experience of the evaluation items before and after use was compared. Grading standard: very good 5 points: good 4 points are: slightly better for 3 minutes: and 2, common score: slightly worse by 1 point: the difference 0, the evaluation results are shown in table 3:
TABLE 2
TABLE 3
As can be seen from tables 2 and 3, the frosted color-change lip gloss of the present invention has good moisturizing and repairing effects, wherein the best effect is obtained in example 1, and the difference between examples 4 to 7 and example 1 is that the content of jojoba seed oil, argan nut oil and phytosterol isostearate is different, and as a result, the moisturizing and repairing effect is changed, and the repairing effect is better when the content of jojoba seed oil is 10 to 18 parts by weight, the content of argan nut oil is 3 to 6 parts by weight, and the content of phytosterol isostearate is 3 to 6 parts by weight. Comparative examples 1 to 4 are different from example 1 only in that one or two components of jojoba seed oil, argania spinosa kernel oil and phytosterol isostearate are respectively absent, and as can be seen from tables 2 and 3, the repairing and moisturizing effects are reduced compared with example 1, and as can be seen, the moisturizing effect is reduced due to the absence of any one component, indicating that the moisturizing effect is better than that of one or two components when only one component is used in the three cases. In comparative example 5, the sucrose particles are different in size, and the sucrose is unevenly distributed in the paste, so that the lips are easily scratched, and the use feeling is greatly influenced.
Example 10
Color change effect test
The frosted color-change lipstick prepared in example 1 was subjected to an experiment, wherein 60 healthy women within age 45 years were randomly selected, 6 groups of healthy women were divided into 6 groups in each 10 people, 3 groups (numbered 1, 2 and 3) were randomly selected to apply the lip gloss of example 1, and the other three groups (numbered 4, 5 and 6) were selected without adding the colorant components of CI 45410, CI45370, CI 15850, CI 45410 and CI 19140, and the rest of the components were the same as in example 1, wherein the color development time was averaged, and the experimental results are shown in table 4:
TABLE 4
The frosted color-changing lip balm has a good color-changing effect, changes according to the pH value and the body temperature of each person, such as skin acid, strong alkalinity, quick color-changing time, high body temperature color-changing time, both high color-changing time and high color-changing thickness, and the color concentration is changed, the thicker the smearing is, the darker the color is, and the lighter the color is.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the scope of the present invention.
Claims (9)
1. The frosted color-changing lip balm is characterized by comprising the following components: thickening agent, adhesive, film forming agent, humectant, emollient, emulsifier, colorant, scrub agent, preservative, wherein the emollient comprises jojoba oil, argania spinosa oil and phytosterol isostearate; the skin moisturizer comprises, by weight, 10-18 parts of jojoba seed oil, 3-6 parts of argania spinosa kernel oil and 3-6 parts of phytosterol isostearate.
2. The frosted color-change lip balm according to claim 1, wherein the skin moisturizer comprises 14 parts of jojoba seed oil, 4 parts of argania spinosa kernel oil and 5 parts of phytosterol isostearate by weight.
3. The frosted color-change lip balm according to claim 1, wherein the colorant is CI 45410, CI45370, CI 15850, CI 45410 and CI 19140, and the content of each component in the colorant in the lip balm is CI 454100.01-1 part, CI 453700.01-1 part, CI 158500.01-1 part, CI 454100.01-1 part and CI 191400.01-1 part by weight.
4. The matte color-changing lip balm according to claim 1, wherein the frosting agent is sucrose, and the sucrose is contained in the lip balm by 3-10 parts by weight.
5. The frosted color-change lip balm according to claim 4, wherein the frosting agent is sucrose treated by a 200-mesh screen.
6. The frosted color-change lip balm according to claim 1, wherein at least one of the following (a) - (g):
(a) the thickening agent is microcrystalline wax or synthetic wax; the weight parts of the components in the thickening agent in the lip balm are 1-8 parts of microcrystalline wax and 1-8 parts of synthetic wax;
(b) the adhesive is candelilla wax, beeswax and hydrogenated polyisobutene; the weight parts of each component in the adhesive in the lip balm are 0.5-5 parts of candelilla wax, 1-10 parts of beeswax and 1-10 parts of hydrogenated polyisobutene;
(c) the film forming agent is polyethylene; the weight part content of the polyethylene in the lip balm is 1-8 parts;
(d) the humectant is dipentaerythritol hexahydroxy stearate/hexastearate/hexaabietate, tridecyl alcohol trimellitate; the weight parts of the components in the moisturizer in the lip balm are 2-8 parts of dipentaerythritol hexahydroxystearate/hexastearate/hexaabietate and 5-15 parts of tridecyl alcohol trimellitate;
(e) the emollient further comprises diisostearyl malate, glycerol tri (ethyl hexanoate); the emollient comprises the components of 5-20 parts by weight of diisostearyl malate and 5-20 parts by weight of glycerol tri (ethyl hexanoate) in the lip balm;
(f) the emulsifier is polyglycerol-2 triisostearate; the weight part content of the polyglycerol-2 triisostearate in the lip balm is 1-8 parts;
(g) the preservative is 0.05-0.8 part by weight of glyceryl caprylate.
7. The frosted color-change lip balm according to claim 1, further comprising a colorant dispersant, a fragrance, an antioxidant; the pigment dispersing agent comprises 5-20 parts by weight of pentaerythritol tetraisostearate; the aromatizing agent comprises 0.1-1 part of menthol, and the antioxidant comprises 0.1-1 part of pomegranate flower oil, 0.05-1 part of bisabolol and 0.05-1 part of tocopherol.
8. The frosted color-change lip balm according to claim 1, which comprises the following components in parts by weight: 2.5 parts of microcrystalline wax, 5 parts of polyethylene, 5 parts of synthetic wax, 2.5 parts of beeswax, 1.5 parts of candelilla wax, 13 parts of diisostearyl malate, 4 parts of dipentaerythritol hexahydroxystearate/hexastearate/hexaabietate, 10 parts of glycerol tri (ethyl hexanoate), 14 parts of jojoba seed oil, 3 parts of polyglycerol-2 triisostearate, 4 parts of argania spinosa kernel oil, 4 parts of hydrogenated polyisobutene, 5 parts of phytosterol isostearate, 10.17 parts of pentaerythritol tetraisostearate, 8.5 parts of tridecanol trimellitate, CI 454100.02 parts, CI 453700.08 parts, CI 158500.05 parts, CI 454100.03 parts, CI 191400.05 parts, 0.3 part of titanium dioxide, 6 parts of sucrose, 0.4 part of menthol, 0.2 part of flower oil, 0.2 part of bisabolol, 0.2 part of tocopherol and 0.3 part of glyceryl caprylate.
9. A method of making a frosted color-shifting lip gloss according to claim 8, comprising the steps of:
1) heating microcrystalline wax, polyethylene, synthetic wax, beeswax, candelilla wax, and glycerol tri (ethyl hexanoate) to 95 deg.C until completely melted;
2) adding diisostearyl malate, dipentaerythritol hexahydrostearate/hexastearate/hexaabietate, jojoba seed oil, polyglycerol-2 triisostearate, argania spinosa oil, hydrogenated polyisobutene, phytosterol isostearate, pentaerythritol tetraisostearate and tridecanol trimellitate into the mixture in sequence 1), stirring and dissolving uniformly, and controlling the temperature to be 85-90 ℃;
3) mixing a proper amount of dissolved material body with CI 45410, CI45370, titanium dioxide, silica, alumina, CI 15850, CI 45410 and CI 19140 in the formula uniformly, grinding the mixture by using a grinder, adding the mixture into a main pot 1) for uniformly stirring and dispersing, and controlling the temperature to be 85 ℃;
4) sieving sucrose with 200 mesh sieve, adding into a pot, stirring, adding Mentholum, flos Granati oil, bisabolol, tocopherol, and glyceryl caprylate, stirring, and dispersing at 85 deg.C.
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| CN112535647A (en) * | 2020-12-14 | 2021-03-23 | 广州艾蓓生物科技有限公司 | Degradable flash lip glaze and preparation method thereof |
| CN115778858B (en) * | 2022-12-21 | 2024-06-11 | 广州多多化妆品有限公司 | Nourishing lip balm and preparation method thereof |
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| CN103462816A (en) * | 2013-09-06 | 2013-12-25 | 珀莱雅化妆品股份有限公司 | Exfoliating lip balm containing frosted particles |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103462816A (en) * | 2013-09-06 | 2013-12-25 | 珀莱雅化妆品股份有限公司 | Exfoliating lip balm containing frosted particles |
Non-Patent Citations (1)
| Title |
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| 曼秀雷敦天然植物精华油润唇膏-无香料;曼秀雷敦（中国）药业有限公司;《国产非特殊用途化妆品备案信息服务平台》;20160111;第1-2页 * |
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