CN108938508A - A kind of fig fruit extract and application thereof with sun-proof synergistic effect - Google Patents
A kind of fig fruit extract and application thereof with sun-proof synergistic effect Download PDFInfo
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- CN108938508A CN108938508A CN201811196187.1A CN201811196187A CN108938508A CN 108938508 A CN108938508 A CN 108938508A CN 201811196187 A CN201811196187 A CN 201811196187A CN 108938508 A CN108938508 A CN 108938508A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention relates to a kind of fig fruit extracts and application thereof.The fig fruit extract makes an addition to the sun-proof building capability in sunscreen product with wide spectrum as natural plant raw material, can suitably reduce physical, chemically sun-screening agent dosage.The sunscreen product stability, safety are preferable, possess good concealing and highlight effect, and skin sense, smell are good, and irritation risk reduces, and have a vast market application prospect.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of fig fruit extraction with sun-proof synergistic effect
Object and application thereof.
Background technique
Because current commercial sunscreen product is with physics, chemically sun-screening agent is leading, the usage amount layers such as to skin sense and safely
There are many influences in face, and with pursuit of the people to green safe theory, natural plant raw material is applied to the sunscreen product general trend of events
Become.Plant-derived sun-prevention component mainly has alkaloid, fatty acid, steroids, polyphenol, polysaccharide and polypeptide, individually makes
Used time, sun protection factor (SPF) is lower, thus is unable to reach ideal sun-proof result.
As the fig of integration of drinking and medicinal herbs, because being praised rich in a variety of nutritional factors such as fiber, polyphenol, vitamin, organic acids
For " patron saint of 21 century human health ".Its present Research is mainly for common fig leaf juice, it is preferred that emphasis is assessment antibacterial, anticancer,
The field of medicaments such as cytotoxicity, cosmetics aspect, which stresses to adjust as odor type, to be made an addition in product.
Paper Khan, H., Akhtar, N., &Ali, A. (2014) .Effects of Cream Containing Ficus
carica L.Fruit Extract on Skin Parameters:In vivo Evaluation.Indian Journal
Of Pharmaceutical Sciences, 76 (6), 560-564. have studied the lotion of the extract containing fig fruit in formula
Influence to human skin parameter comprising dermal melanin, erythema, epidermis aquation and sebum secretion amount.4% nothing will be contained
The basic components of flowers and fruits berry extract are compared as test reagent, basic components, are applied to random volunteer's cheek skin, are gone through
When 8 weeks.Test result shows that the water-in-oil emulsion of the berry extract containing fig in formula can effectively reduce dermal melanin
Content reduces lost transepidermal water, reduction fat secretion, enhancing skin hydration effect.Thus it is not difficult to find out that, very few nothing
Flowers and fruits extract is also only to have studied its moisturizing and whitening effect in the prior art for cosmetics；And it has not focused on
Fig fruit extract is applied in cosmetics and its synergistic effect to sun-screening agent, that is, its use in sunscreen product
On the way.
Application No. is 201711499544.7 patents to disclose a kind of novel sunscreen synergistic composition.The composition includes
Radix Arnebiae extract, ginger-root extract, bisabolol and more Gallate catechol Gallate esters acid, itself can be added without sun-proof function
In conventional sunscreen agent, SPF is increased substantially.The ingredient in composition with synergistic effect has mainly been screened in the invention
And the most suitable additive amount of tie element, sun-proof synergistic effect of the composition in different base is inquired into, but do not study nothing
Synergistic effect of the flowers and fruits fruit extract to different sunscreen formulas.
Therefore, in view of the foregoing, fig fruit extract is applied in sunscreen product, probes into it to different sun-proof
The synergistic effect of agent prescription, for reduce the additive amount of cosmetic formulations sun-screening agent, reduce cosmetics to the irritation of skin, reach
It is had a very important significance to green safe sun-proof theory.
The present invention exactly proposed under the above technical background, it is significantly different with the prior art, the present invention by fig, without flower
Fruits extract is used for the preparation of sunscreen product, has been surprisingly found that it has apparent synergistic effect to different types of sun-screening agent.
Summary of the invention
For the market demand and the deficiencies in the prior art, the present invention is directed to by fig, fig fruit extract gradient
Make an addition to it is physical, chemically and physical chemistry compounding sunscreen formula in, develop its sun-proof synergistic effect.
The present invention provides a kind of figs to prepare the purposes in sunscreen product.
Further, the present invention implements fig different parts and is preparing the purposes in sunscreen product.
Hereinafter, illustrating technical solution of the present invention by representative of fig fruit, but it is not meant to other portions of fig
Position is not achieved that fig fruit is achieved same or similar effect.That is, the extract at other positions of fig plant can
Reach and the same or similar effect of fig fruit extract set forth below.
As one group specifically, the embodiment of particularization, the present invention provides a kind of fig fruit extracts to make
Purposes in standby sunscreen product.
The present invention uses in implementation process: according to masses such as paper, the patents published
The fig fruit extract that extracting method disclosed in the legal open approach that would know that is extracted；It is obtained by legal approach of giving
The fig fruit extract taken；The fig fruit extract obtained by legal commercially available approach.
The above various approach obtain fig fruit extract can reach the same or similar in this group of embodiment
Technical effect.
Below by taking the fig fruit extract that commercially available approach obtains as an example, this group of embodiment is illustrated.
The fig fruit extract that the commercially available approach obtains is purchased from Shaanxi Xi'an health raw material mill, product goods
Number be F6008, lot number 201803001A.
The present invention is determined above-mentioned commercially available fig fruit extract in implementation process, includes no flower
Fruits general flavone, fig fruit total starches and fig fruit total polyphenols, the content of three are respectively 0.0064mg/
ML, 1.46mg/mL and 0.0047mg/mL.
The fig fruit extract of the above content reaches certain skill for a certain technical problem in this group of embodiment
Art effect；The fig fruit extract of other compositions content in other respects the technical issues of when also can get relevant art effect
Fruit.
In the implementation process of this group of embodiment, it is provided commonly in preparation using fig fruit extract and sun-screening agent
State sunscreen product.
That is, the sunscreen product includes sun-screening agent and fig fruit extract.
The sun-screening agent is that physical sun-screening agent, chemically sun-screening agent or physical chemistry compound sun-screening agent.
The physical sun-screening agent includes but is not limited to titanium dioxide.
The chemically sun-screening agent includes but is not limited to ethylhexyl methoxy cinnamate.
Physical chemistry compounding sun-screening agent mixture of sun-screening agent for physical sun-screening agent and chemically；
The physical chemistry compounding sun-screening agent includes but is not limited to ethylhexyl methoxy cinnamate and titanium dioxide.
In some specific embodiments, the physical sun-screening agent includes titanium dioxide.
In other specific embodiments, the chemically sun-screening agent includes ethylhexyl methoxy cinnamate.
In still other specific embodiment, the physical chemistry compounding sun-screening agent is methoxy cinnamic acid ethyl hexyl
Ester and titanium dioxide.
In some more specifically embodiments, the physical sun-screening agent is titanium dioxide, in sunscreen product
Account for 4%-25%, fig fruit extract weight percent shared in sunscreen product
For 0.01%-1.13%.
In other more particular embodiments, the chemically sun-screening agent is ethylhexyl methoxy cinnamate,
It accounts for 4%-10%, fig fruit extract institute in sunscreen product in sunscreen product
The weight percent accounted for is 0.01%-1.11%.
In still other more specifically embodiment, the physical chemistry compounding sun-screening agent is methoxy cinnamic acid ethyl
Own ester and titanium dioxide, the titanium dioxide account for 5%-25%, the first in sunscreen product
Oxygroup 2-Ethylhexyl cinnamate accounts for 5%-10% in sunscreen product, and the fig fruit extracts
Object accounts for 0.01%-1.07% in sunscreen product.
The sunscreen product can also include that commonly used in the art any can be used for additive therein.
Compared with prior art, beneficial effect obtained by the present invention is:
(1) present invention is surprised to find that for fig fruit extract to be mixed for sun-screening agent in implementation process sun-proof
In product and the weight percent of fig fruit extract and sun-screening agent is controlled, can effectively increase the sun-proof of sunscreen product
Effect.
(2) fig fruit extract is used for sunscreen product as natural plant raw material has antibacterial, anti-oxidant, anti-ageing
Always, the potential ability of whitening has concealing and the ocular effect without adding essence, can suitably reduce physics, chemically prevent
The dosage for shining agent reduces sun-screening agent usage amount to a certain extent and increases the irritating risk of bring cosmetics, has wide
Big market application prospect.
Specific embodiment
Fig fruit extract (hereinafter referred to as fruit extract A) used herein is purchased from Shaanxi Xi'an health raw material mill
(extract is that 10 kilograms of raw material extract 1 kilogram of product, and the additives such as preservative free are water-soluble, and fig fruit comes
Source is the collective fruits of moraceae plants fig).Such as table 1 of instrument and reagent used in the present invention.
1 test apparatus of table and reagent
1. extract dissolubility test
1.1 fat-soluble tests
1.00g fruit extract A is weighed in 10mL dehydrated alcohol, is stirred evenly, a large amount of precipitatings of appearance slightly stand and divide
Layer.
1.2 soluble test
1.00g fruit extract A is weighed in 10mL deionized water, is added by every 10mL deionized water gradient, 70 DEG C add
Thermal agitation 10min, ultrasonic 5min (ultrasound condition is 28 DEG C, 70% power) when deionized water is always added to 60mL, are presented clear
Clearly, bright, special odor brown color uniform solution, standing beaker bottom has a small amount of finely ground particle substance.Every 1g glycerol compounding is molten
When liquid is by gradient addition fruit extract A to 6g, bottom of a cup little particle almost dissolves.
In summary, 1.00g fruit extract A highest is fully soluble in 60mL deionized water in the present invention and 6g glycerol is multiple
With in solution.
2. the preparation of sunscreen product
To exclude the interference that fig fruit extract itself may have sun-proof ability, by the fruit of highest addition concentration
Extract A makes an addition in the formula without any component of sun, is set as blank group.Table 2 is blank group component.
2 blank group component of table
Different content fig fruit extract and heterogeneity sun-screening agent are mixed with out sunscreen product respectively, obtained
Following 3 groups of embodiments.
Embodiment group 1
Effect of the table 3 to titanium dioxide
Embodiment group 2
The effect of 4 ethylhexyl-p-methoxycinnamate of table
Embodiment group 3
The effect of the compounding (ethylhexyl methoxy cinnamate+titanium dioxide) sun-proof to physical chemistry of table 5
Comparative example group 1
Effect of the table 6 to benzophenone-3
Comparative example 2
The thin sunlight lotion of the new clear water of Mentholatum (SPF=25).
2.1 preparation process
Above-mentioned blank group, embodiment group 1-3 and comparative example group 1 are with the preparation of following technique:
(1) A phase and B phase are weighed according to formula and dosage respectively, are separately heated to 85 DEG C；
(2) A phase is poured into B phase, polysorbate -60 is added in 5600r/min homogeneous 5min, and homogeneous 1min is cooled to 40
DEG C, Phenoxyethanol, 1,2 hexylene glycols is added, 300r/min stirring is cooled to 28 DEG C, dispenses to 10mL centrifuge tube, obtain sun-proof production
Product.
The test of 2.2SPF value
Currently, the method for test sunscreen product SPF index has human body method of testing and external instrument test method, the two both at home and abroad
Respectively restricted by different factors.But human test's method exists, and time-consuming, troublesome in poeration, costly, individual difference is big, test population
The disadvantages of selection is difficult.Compared to this, external instrument test rule wants slightly better.Yan Shuxian etc. demonstrates sunscreen cosmetic
The degree of association of SPF index external instrument test method and human test's method.Itself the result shows that, the two has good correlation (r=
0.9616), there was no significant difference (0.40 < P < 0.50) for the surveyed spf value of two methods.Therefore, this test will use external instrument
Device method of testing to sample above carry out SPF index assessment, SPF analyzer can calculate automatically spf value, Boots Star,
MPF value and trap will completely show UVA/UVB test value, the test report that can print and curve graph.Testing environment is that constant temperature is permanent
Moist chamber, temperature are controlled in (20 ± 2) DEG C, relative humidity (50 ± 5) %.
2.2.1 coating carrier is investigated
Before formal measurement, medical adhesive tape and polymethyl methacrylate are used respectively to a sample according to determination step
(PMMA) plate carries out the stability that two kinds of carriers are investigated in 3 groups of parallel tests.The results show that the numerical value measured using PMMA plate is compared with glue
Band method deviation is smaller, therefore used carrier is PMMA plate in following tests.
2.2.2 test procedure
Coated sample: with each sample 2mg/cm in dedicated sample applicator Example group 1-3 and comparative example group 12In PMMA plate
On, it puts on finger-cover for medical use and uniformly smears, smear on the fingerstall of front and back without visible sample, all samples are all made of same procedure and are applied
It covers, each sample carries out 3 groups of parallel tests.Sample panel after smearing is placed in dark surrounds the 20min that forms a film naturally, it is to be measured.
It rectifies an instrument: before test, scanning PMMA hollow plate under the continuous xenon source of 125W with the correction filter disc that instrument carries
6 points at edge and center are corrected, it is ensured that the accuracy of test.
Test sample: with the mode to rectify an instrument, each sample SPF-290s SPF analyzer is tested.Instrument needle
6 optical wavelength MPF (Monochromatic Protection Factor, monochromatic light protection index) is respectively described to each sample,
The index of correlation of sample is calculated by instrument software kit.
To reduce evaluated error as far as possible, sample obtained by formula gradient test is placed in room temperature dark situation 48h to guarantee cream
Body is solution-stabilized, obtains table 7.
Table 7 surveys spf value
Note: being obtained by detection, and the spf value of blank group is 0.67.
A0, B0 and C0 are contrasted with the other embodiments in corresponding embodiment group in embodiment group.According to blank group with
Table 7 surveys spf value and is such as drawn a conclusion:
(1) fig fruit extract itself is without anti-sunlight function；
(2) the sun-proof synergy object of fig fruit extract is selective, and its synergistic effect is mentioned in fig fruit
The weight percent for taking object and sun-screening agent shared in sunscreen product within a certain range when effect it is optimal, fig fruit extracts
Object has sun-proof synergy linear as a result, to benzophenone-3 without sun-proof synergy line titanium dioxide or ethylhexyl methoxy cinnamate
Property result；
(3) sunscreen composition (ethylhexyl methoxy cinnamate+titanium dioxide of the fig fruit extract to linear synergy
Titanium) there are linear synergistic results, and its synergistic effect is shared in sunscreen product in fig fruit extract and sun-screening agent
Weight percent within a certain range when effect it is optimal.
The estimation of stability of 3 sunscreen products
The present invention investigated embodiment group 1-3, in comparative example group 1 and comparative example 2 sunscreen product stability.By embodiment
Group 1-3, comparative example group 1 and 2 gained sample of comparative example are respectively placed in that room temperature, room temperature dark situation, illumination, (45 ± 1 DEG C impermeable for thermal environment
Light air dry oven), refrigeration 4 DEG C, freezing environment (- 15 ± 1 DEG C), hot and cold alternation (- 15 ± 1 DEG C and 45 ± 1 DEG C for 24 hours alternately into
Row) under the conditions of 7, its changing features is observed after a period of time, investigation the results are shown in Table 8 and table 9.
Table 8 sunscreen product, 28 days Stability Observation results
Table 9 sunscreen product, 78 days Stability Observation results
Note: "-" indicates more unchanged with original state；" 1 " indicates a little floccule；" 2 " indicate in special odor
Sweet taste slightly weakens；" 3 " indicate that bottom colors upper layer is slightly deep；Wherein 1 and 3 shake up after restore original state.
By carrying out stability observing to fig sunscreen product the results show that Fructus Fici extract is used for sunscreen product
In, which has good stability, the change of no floccule, smell, color etc..Equally, the stability of comparative example 2 also compared with
It is good.And the sunscreen product stability in comparative example group 1 is relatively poor, occurs a little floccule, special at 28 days and 78 days
Sweet taste slightly weakens or the problems such as bottom colors upper layer is slightly deep in smell.
4 fig fruit extract safety evaluatios
Safety through erythrocyte hemolysis thrombotest detection fig fruit extract.
Erythrocyte hemolysis test (Red blood cell test, RBC) is one of Draize test alternative, is led to
The damage of measurement hemoglobin seepage discharge and deformation degree with evaluating chemical product to ocular tissue's cell is crossed, in the world mainly by RBC
Eye irritation research of the test for chemicals such as cosmetic product and raw materials.
Agents useful for same of the present invention is fig fruit extract combination solution, and method therefor is the blood coagulation of normal erythrocytes haemolysis
Test method.As shown in Table 10, the extract solution is nonirritant, good security.
10 fig fruit extract combination solution erythrocyte hemolysis of table tests (RBC) result
5 sunscreen product Efficiency assessments
5.1 test reagent
A1, B4, C3, A0, B0 and C0 group in embodiment group 1-3 are randomly selected, D1 group and comparative example 2 in comparative example group 1
Product.
5.2 test method
It looks for satisfactory 18 volunteers to try out, takes Blind Test (blank) mode, product sample is applied to
Human skin (such as inboard arm, the positions such as the back of the hand), to the overall feeling of product, specific assimilation effect, moistens effect at stretchability
Corresponding evaluation is given in terms of the subjective sensations such as fruit, exquisiteness, glossiness, viscosity, concealing, salubrious degree.The evaluation of each is real
Row scoring mechanism: fine 9-10 points；Preferable 7-8 points；General 5-6 points；Poor 3-4 points；Very poor 1-2 points.
5.3 test data
Human trial combines the crowd of different skin quality, their sense organ in-service evaluation is as shown in table 11:
11 product sensory evaluation table of table
Note: sensory evaluation data is the average value of 18 volunteer's evaluations point in table.
5.4 conclusion (of pressure testing)
Experiments have shown that the exquisiteness of cosmetics, concealing scoring are 9 points or more after addition fig fruit extract,
Satisfaction is good；Stretchability and salubrious degree are more satisfied at 7-8 points；Assimilation effect, moisturizing effect, glossiness, viscosity are equal
At 8-10 points, selected crowd is good to the common sensation of target product, better than the sun-proof production for being not added with fig fruit extract
Product.Although the thin sunlight lotion spf value of the new clear water of Mentholatum is relatively high, stability is preferable, its product efficacy is in contrast
It is weaker than the present invention.
In conclusion the sunscreen product in the present invention meets cosmetics listing requirement by stability and security test,
And there is the sunscreen product good concealing to highlight effect, skin sense, smell are good, have broad application prospects.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than limiting the scope of the invention, ability
The simple modification or equivalent replacement that the those of ordinary skill in domain carries out technical solution of the present invention, all without departing from skill of the present invention
The spirit and scope of art scheme.
Claims (10)
1. fig is preparing the purposes in sunscreen product.
2. purposes according to claim 1, it is characterised in that: fig fruit extract is preparing the use in sunscreen product
On the way.
3. purposes according to claim 2, it is characterised in that: the fig fruit extract includes fig fruit
General flavone, fig fruit total starches and fig fruit total polyphenols.
4. purposes according to claim 2, it is characterised in that: fig fruit extract and sun-screening agent to be provided commonly for making
Standby sunscreen product.
5. purposes according to claim 4, it is characterised in that: the sun-screening agent is physical sun-screening agent, chemically prevents
It shines agent or physical chemistry compounds sun-screening agent.
6. purposes according to claim 5, it is characterised in that: the physical sun-screening agent is titanium dioxide.
7. purposes according to claim 5, it is characterised in that: the chemically sun-screening agent is methoxy cinnamic acid ethyl
Own ester.
8. purposes according to claim 5, it is characterised in that: the described physical chemistry compounding sun-screening agent be titanium dioxide and
The mixture of ethylhexyl methoxy cinnamate.
9. purposes according to claim 6, it is characterised in that: wherein the fig fruit extract is in sun-proof production
0.01%-1.13% is accounted in product.
10. purposes according to claim 7, it is characterised in that: wherein the fig fruit extract is sun-proof
0.01%-1.11% is accounted in product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811196187.1A CN108938508B (en) | 2018-10-15 | 2018-10-15 | Fig fruit extract with sun-screening and synergistic effects and application thereof |
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|---|---|---|---|
| CN201811196187.1A CN108938508B (en) | 2018-10-15 | 2018-10-15 | Fig fruit extract with sun-screening and synergistic effects and application thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112107533A (en) * | 2020-09-27 | 2020-12-22 | 广州妮趣化妆品有限公司 | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof |
| TWI740107B (en) * | 2019-02-22 | 2021-09-21 | 大江生醫股份有限公司 | Use of unripe fig fruit extracts for reducing skin collagen loss |
| CN114600913A (en) * | 2020-12-07 | 2022-06-10 | 王殿丰 | Ecological pesticide based on fig leaves and preparation method thereof |
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| JP2015034131A (en) * | 2013-08-07 | 2015-02-19 | 片倉チッカリン株式会社 | Fermented fig extract, method for producing the same, and cosmetic in which fermented fig extract is blended |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| TWI740107B (en) * | 2019-02-22 | 2021-09-21 | 大江生醫股份有限公司 | Use of unripe fig fruit extracts for reducing skin collagen loss |
| CN112107533A (en) * | 2020-09-27 | 2020-12-22 | 广州妮趣化妆品有限公司 | Composition with effects of controlling oil, tendering skin and collecting fine pores and preparation method and application thereof |
| CN114600913A (en) * | 2020-12-07 | 2022-06-10 | 王殿丰 | Ecological pesticide based on fig leaves and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN108938508B (en) | 2021-03-30 |
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