CN105326668B - A kind of transparent lipstick and preparation method thereof - Google Patents

A kind of transparent lipstick and preparation method thereof Download PDF

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Publication number
CN105326668B
CN105326668B CN201510777692.5A CN201510777692A CN105326668B CN 105326668 B CN105326668 B CN 105326668B CN 201510777692 A CN201510777692 A CN 201510777692A CN 105326668 B CN105326668 B CN 105326668B
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parts
seed oil
oil
transparent lipstick
natural
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CN105326668A (en
Inventor
王飞
王一飞
马婧
王巧利
廖晓凤
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Guangzhou Jinan Biomedicine Research and Development Base Co Ltd
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Guangzhou Jinan Biomedicine Research and Development Base Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Emergency Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to cosmetic technical fields, and in particular to a kind of transparent lipstick and preparation method thereof.The transparent lipstick includes the raw material of following parts by weight:0.1 ~ 0.5 part of diisooctadecanol malate and in pairs 35 ~ 45 parts of the mixture of octadecylamine dimerized linoleic acid/ethylenediamine copolymer, 15 ~ 25 parts of two isostearic acid malate, 8 ~ 20 parts of olive oil, 1 ~ 8 part of grape seed oil, 6 ~ 15 parts of green tea seed oil, 5 ~ 10 parts of Queensland nut seed oil, 2 ~ 5 parts of vitamin E, 0.1 ~ 0.5 part of natural perfume material, 0.005 ~ 0.05 part of natural pigment and Nipasol.Transparent lipstick of the present invention is safe and non-stimulating, and clear appearance, transparency are high, moistens and spends, bright-colored, bright using rear lip.

Description

A kind of transparent lipstick and preparation method thereof
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of transparent lipstick and preparation method thereof.
Background technology
Lip skin is different from the skin at other positions, and lip skin keratin is relatively thin, without appendicles such as hair follicle, sebaceous glands Official, and it is distributed in cuticula there are many salivary gland, cuticula, stratum granulosum are thin, and particle melanin is fewer than common skin.
Current market sales of cosmetics lipstick product, main component are lanolin, wax and dyestuff, lanolin have compared with Strong adsorptivity, can be by dust, bacterium, virus and some heavy metal ion adsorbed on lip mucous membrane, wax sources in air In oil, such as paraffin, white oil, ceresine;And lanolin is complicated with wax component, allergic reaction is easily caused, such as lip mucous membrane It is dry and cracked, peel off, feel that lip is itched or mild pain etc. sometimes;Show to suffer from young women cancer according to data from abroad In person, there is 18.2% cause of disease related with way lipstick, lipstick.Lipstick contains the heavy metals such as the lead of higher amount, cadmium, and lead has accumulation Property, long-term sucking human body probably can lead to chronic lead poisoning, anaemia, abdominal pain, acute renal failure and brain neuroblastoma lesion etc. is caused to be asked Topic;Artificial color in lipstick may be converted into Mutagen, lead to cancer under ultraviolet light irradiation.People is drinking water, is eating east When western, lipstick and its those above substance harmful to health can be taken in the mouth, it is made to be directly entered in vivo.
All the time, the cosmetics of appearance transparent are well received by consumers, because opaque products can be carried to consumer For a kind of pure safe subjective feeling of product.102688162 B of Chinese patent CN disclose a kind of pure natural components profit lip Cream comprising natural oil, wax and auxiliary material, wherein natural oil are selected from caprylic/capric triglyceride, hydrogenated coco glycerine The acid courage of ester, glycerol caprylate, sunflower oil, jojoba oil, shea butter, macadimia nut oil, olive oil, soybean oil, C10~30 At least one of sterol/lanosterol mixed ester, grape seed oil;Natural wax is selected from beeswax, candelila wax, Brazil wax At least one of;Natural auxiliary material is selected from pure water, vitamin E, pentanediol, aloe extract, chamomile extracting solution, hyalomitome At least one of acid.The lip gloss is naturally safe, is free of synthetic dyestuff, fragrance and preservative.
Invention content
For overcome the deficiencies in the prior art, the purpose of the present invention is to provide a kind of transparent lipsticks, safe and non-stimulating, Clear appearance, transparency are high, moisten and spend, bright-colored, bright using rear lip.
To achieve the goals above, technical scheme is as follows:
A kind of transparent lipstick includes the raw material of following parts by weight:Diisooctadecanol malate and double-dioctadecylamine 35~45 parts of the mixture of dimerized linoleic acid/ethylenediamine copolymer, 15~25 parts of two isostearic acid malate, olive oil 8~ 20 parts, 1~8 part of grape seed oil, 6~15 parts of green tea seed oil, 5~10 parts of Queensland nut seed oil, 2~5 parts of vitamin E, natural perfume 0.1 part of 0.1~0.5 part of material, 0.005~0.05 part of natural pigment and Nipasol.
As the preferred embodiment of the present invention, the transparent lipstick is made of the raw material of following parts by weight:Two is different hard 40 parts of mixture, the two isostearic acid apples of lipidol malate and double-dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer 20 parts of tartaric acid ester, 15 parts of olive oil, 5 parts of grape seed oil, 10 parts of green tea seed oil, Queensland nut seed oily 7 parts, vitamin E 3 part, day 0.15 part of right 0.1 part of fragrance, 0.01 part of natural pigment and Nipasol.
Further, the natural perfume material is at least one in Rosa Damascana, sweet orange oil, Peppermint essential oil and osmanthus essential oil Kind.
Further, the natural pigment is at least one of lycopene, lutein, lutein ester and carrotene.
The present invention also provides the preparation methods of above-mentioned transparent lipstick, include the following steps:
S1, by the mixing of diisooctadecanol malate and double-dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer In object, two isostearic acid malates, olive oil, grape seed oil, green tea seed oil and Queensland nut seed oil input heating and stirring pot, It stirs and is warming up to 80~85 DEG C, stirring to material is completely dissolved;
S2 and then addition vitamin E, natural perfume material, natural pigment and Nipasol stir controlled at 75~80 DEG C It mixes to being completely dissolved, obtains mixed material;
S3, material to be mixed temperature be reduced to 70~75 DEG C, by mixed material inject mold in, be cooled to 4~10 DEG C, Demoulding is to get transparent lipstick.
The present invention is total using diisooctadecanol malate and double-dioctadecylamine dimerized linoleic acid/ethylenediamine simultaneously The weight ratio of the base-material of the mixture of polymers and two isostearic acid malates as transparent lipstick, the two is (7~9):(3~ 5) so that product is not only with the transparent characteristic of clear appearance, but also has good moist degree, colouring ability and higher fusing point. Olive oil, grape seed oil, green tea seed oil, Queensland nut seed oil and vitamin E are reused simultaneously, further increase moistening for product Degree, effective nourishing is provided for lip.
Therefore, compared with prior art, advantage of the invention is that:
(1) the present invention provides a kind of novel transparent lipsticks, use diisooctadecanol malate and double-bis- octadecanes Base-material of the mixture and two isostearic acid malates of base amine dimerized linoleic acid/ethylenediamine copolymer as transparent lipstick, makes Product is obtained not only with the transparent characteristic of clear appearance, but also with good moist degree, colouring ability and higher fusing point;
(2) transparent lipstick of the present invention is safe, nonirritant, stay in grade, contains olive oil, grape seed oil, green tea seed The natural components such as oil, Queensland nut seed oil and vitamin E, can provide effective nourishing, while using natural perfume material, day for lip Right pigment so that product has light fragrance, and bright-colored, bright using rear lip;
(3) formula of transparent lipstick of the present invention is simple, raw material is easy to get, while preparation method is simple, process stabilizing, can promote Using.
Specific implementation mode
The present invention is further described below by way of specific implementation mode, but the present invention is not limited only to following embodiment. It in the scope of the present invention or is not departing from present disclosure, in spirit and scope, transparent lipstick of the present invention is being carried out It is suitably modified, replaces the identical component of effect, it will become apparent to those skilled in the art that they are considered as wrapping It includes within the scope of the present invention.
The producer of part material of the embodiment of the present invention and article No. are as follows:
The formula of the embodiment of the present invention 1 and 2 transparent lipsticks:
The preparation method of the embodiment of the present invention 1 and 2 transparent lipsticks:
S1, by the mixing of diisooctadecanol malate and double-dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer In object, two isostearic acid malates, olive oil, grape seed oil, green tea seed oil and Queensland nut seed oil input heating and stirring pot, It stirs and is warming up to 80 DEG C, stirring to material is completely dissolved;
S2 and then addition vitamin E, natural perfume material, natural pigment and Nipasol, controlled at 75 DEG C, stirring is extremely It is completely dissolved, obtains mixed material;
S3, material to be mixed temperature be reduced to 70 DEG C, mixed material is injected in mold, is cooled to 5 DEG C, demoulding, i.e., Obtain transparent lipstick.
The formula of one~tri- transparent lipstick of comparative example:
The preparation method of comparative example refers to the preparation method of the embodiment of the present invention 1 and 2 transparent lipsticks.
The performance test of test example one, transparent lipstick of the present invention
The transparent lipstick that gained is prepared to Examples 1 to 2 and comparative example one~tri- using following methods is tested, and is detected Its fusing point, colouring ability, moistens degree, transparency and stability at breaking force.
(1) fusing point:Using 2010 editions annex VIC melting point determinations of Chinese Pharmacopoeia;
(2) breaking force:Using lipstick fracture instrument test.Under normal conditions, the lipstick of 12.7mm diameters, breaking force is 400 ~800g ranges, just can guarantee and are not easily broken in use;
(3) colouring ability and moist degree:Using actual use sensory evaluation, 5 points indicate, 4 points indicate preferable, 3 points of tables Show that generally 2 points of expressions are poor, and 1 point of expression is poor;Data are recorded after 20 people evaluation, are averaged;
(4) transparency:Using visual evaluation;
(5) stability:Refer to 25 DEG C, it is 18 DEG C subzero, 48 DEG C, it is subzero 18 DEG C with 48 DEG C cycle four kinds under the conditions of test 3 Month, restore unchanged, energy normal use, in this, as evaluation criteria after room temperature.
Test result is as follows shown in table:
Trial target Fusing point (DEG C) Breaking force Colouring ability Moisten degree Transparency Stability
Embodiment 1 69 546 4.4 4.6 It is good It is qualified
Embodiment 2 75 612 4.8 4.9 It is good It is qualified
Comparative example one 52 402 3.0 3.0 It is good It is unqualified
Comparative example two 48 408 2.4 2.6 It is good It is unqualified
Comparative example three 58 423 3.5 3.2 It is good It is qualified
As seen from the above table, the embodiment of the present invention 1 and 2 transparent lipsticks are had excellent performance, and fusing point is high, breaking force is strong, colouring Effect is spent with moist, has obtained the consistent favorable comment of subject, while its transparency is high, stability is good.With reality in Examples 1 and 2 Each performance for applying 2 transparent lipstick of example is the most excellent, therefore embodiment 2 is highly preferred embodiment of the present invention.
The base-material of comparative example one contains only diisooctadecanol malate and double-dioctadecylamine dimerized linoleic acid/second two The mixture of amine copolymer object, comparative example two and three isooctadecanol malate of comparative example and the sub- oil of double-dioctadecylamine dimerization The use ratio of the mixture of acid/ethylenediamine copolymer and two isostearic acid malates not within the scope of the present invention, melts Point, colouring ability, moistens the performances such as degree, stability compared with the embodiment of the present invention at breaking force, there is apparent gap, explanation There is synergistic effect in the present invention.
The security test of test example two, transparent lipstick of the present invention
The transparent lipstick that Examples 1 and 2 are prepared with gained carries out security test, and test result is as follows shown in table:
As seen from the above table, transparent lipstick safety of the present invention, it is non-stimulated.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment Limitation, it is other it is any without departing from the spirit and principles of the present invention made by changes, modifications, substitutions, combinations, simplifications, Equivalent substitute mode is should be, is included within the scope of the present invention.

Claims (5)

1. a kind of transparent lipstick, which is characterized in that be made of the raw material of following parts by weight:Diisooctadecanol malate and double- 15 ~ 25 parts of 35 ~ 45 parts of mixture, the diisooctadecanol malate of dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer, 8 ~ 20 parts of olive oil, 1 ~ 8 part of grape seed oil, 6 ~ 15 parts of green tea seed oil, 5 ~ 10 parts of Queensland nut seed oil, vitamin E 2 ~ 5 part, day 0.1 part of right 0.1 ~ 0.5 part of fragrance, 0.005 ~ 0.05 part of natural pigment and Nipasol.
2. a kind of transparent lipstick, which is characterized in that be made of the raw material of following parts by weight:Diisooctadecanol malate and double- 20 parts of 40 parts of mixture, diisooctadecanol malate, the olive oil of dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer 15 parts, it is 5 parts of grape seed oil, 10 parts of green tea seed oil, 7 parts of Queensland nut seed oil, 3 parts of vitamin E, 0.1 part of natural perfume material, natural 0.15 part of 0.01 part of pigment and Nipasol.
3. transparent lipstick as claimed in claim 1 or 2, which is characterized in that the natural perfume material is Rosa Damascana, sweet orange essence At least one of oil, Peppermint essential oil and osmanthus essential oil.
4. transparent lipstick as claimed in claim 1 or 2, which is characterized in that the natural pigment be lycopene, lutein, At least one of lutein ester and carrotene.
5. a kind of method preparing transparent lipstick as claimed in claim 1 or 2, which is characterized in that include the following steps:
S1, by the mixture of diisooctadecanol malate and double-dioctadecylamine dimerized linoleic acid/ethylenediamine copolymer, In diisooctadecanol malate, olive oil, grape seed oil, green tea seed oil and Queensland nut seed oil input heating and stirring pot, stir It mixes and is warming up to 80 ~ 85 DEG C, stirring to material is completely dissolved;
S2 and then addition vitamin E, natural perfume material, natural pigment and Nipasol stir controlled at 75 ~ 80 DEG C to complete Fully dissolved obtains mixed material;
S3, material to be mixed temperature be reduced to 70 ~ 75 DEG C, mixed material is injected in mold, is cooled to 4 ~ 10 DEG C, demoulding, Up to transparent lipstick.
CN201510777692.5A 2015-11-11 2015-11-11 A kind of transparent lipstick and preparation method thereof Active CN105326668B (en)

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Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106727227A (en) * 2016-12-19 2017-05-31 郑州市嘉蓓丽生物科技有限公司 A kind of lipstick containing teas and Chinese medicine and preparation method thereof
CN106798657A (en) * 2017-03-14 2017-06-06 广州暨北生物科技有限公司 A kind of U.S. face jelly lipstick
KR102038681B1 (en) * 2018-02-13 2019-10-30 충북대학교 산학협력단 Cosmetic composition containing citrus oil and method for producing same
CN109394573A (en) * 2018-12-27 2019-03-01 唯客乐化妆品(杭州)有限公司 A kind of transparent lipstick and its preparation process

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1465335A (en) * 2002-07-04 2004-01-07 克利尔德科技公司 Transparent lipstick
CN102413809A (en) * 2009-05-08 2012-04-11 乐敦制药株式会社 Oily composition and rod-shaped medicinal preparation
CN102811697A (en) * 2011-04-05 2012-12-05 雅芳产品公司 Clear or Translucent Composition
CN102885699A (en) * 2012-09-28 2013-01-23 珀莱雅化妆品股份有限公司 Transparent lipstick
FR2975296B1 (en) * 2011-05-18 2013-05-10 Oreal FLUID COSMETIC COMPOSITION COMPRISING A PARTICULAR POLYESTER, A NON-VOLATILE SILICONE OIL AND A SPECIFIC ORGANOGELER
FR2984150A1 (en) * 2011-12-20 2013-06-21 Oreal Transparent, anhydrous and solid composition, useful for making up skin, comprises fatty phase comprising nonvolatile polar hydrocarbon oil, polyamide resin, and gelling system comprising combination of lipophilic gelling agent

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Publication number Priority date Publication date Assignee Title
FR2958159B1 (en) * 2010-03-31 2014-06-13 Lvmh Rech COSMETIC OR PHARMACEUTICAL COMPOSITION

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1465335A (en) * 2002-07-04 2004-01-07 克利尔德科技公司 Transparent lipstick
CN102413809A (en) * 2009-05-08 2012-04-11 乐敦制药株式会社 Oily composition and rod-shaped medicinal preparation
CN102811697A (en) * 2011-04-05 2012-12-05 雅芳产品公司 Clear or Translucent Composition
FR2975296B1 (en) * 2011-05-18 2013-05-10 Oreal FLUID COSMETIC COMPOSITION COMPRISING A PARTICULAR POLYESTER, A NON-VOLATILE SILICONE OIL AND A SPECIFIC ORGANOGELER
FR2984150A1 (en) * 2011-12-20 2013-06-21 Oreal Transparent, anhydrous and solid composition, useful for making up skin, comprises fatty phase comprising nonvolatile polar hydrocarbon oil, polyamide resin, and gelling system comprising combination of lipophilic gelling agent
CN102885699A (en) * 2012-09-28 2013-01-23 珀莱雅化妆品股份有限公司 Transparent lipstick

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