CN111821247A

CN111821247A - Lip plumping glaze containing pepper peel extract and preparation method thereof

Info

Publication number: CN111821247A
Application number: CN202010881151.8A
Authority: CN
Inventors: 蒙宇; 夏洁; 李春煌; 胡根华; 吴知情
Original assignee: Guangzhou Nabion Biotechnology Co ltd
Current assignee: Guangzhou Nabion Biotechnology Co ltd
Priority date: 2020-08-27
Filing date: 2020-08-27
Publication date: 2020-10-27

Abstract

The invention relates to a lip plumping glaze containing pepper peel extract and a preparation method thereof, wherein the lip plumping glaze comprises lip plumping components, grease, a thickening agent, a bacteriostatic agent and a film forming agent; the lip plumping component comprises a pepper peel extract. The lip plumping glaze contains lip plumping components containing pepper peel extracts, and pepper serving as rutaceae plants is rich in unsaturated fatty acid, can improve blood rheology, is commonly used in edible seasonings and is natural and edible. The fruit and pericarp extract is mild and safe for application to the skin, and does not cause strong burning sensation like capsaicin. The invention adds the zanthoxylum peel extract into the lip-rounding product for the first time, and achieves the effect of 'instantly rounding lips' by enhancing the blood circulation of the lips.

Description

Lip plumping glaze containing pepper peel extract and preparation method thereof

Technical Field

The invention belongs to the technical field of cosmetics, and particularly relates to lip plumping glaze and a preparation method thereof, in particular to lip plumping glaze containing pepper peel extract and a preparation method thereof.

Background

The lips are organs around the mouth, with thick folds and a form of pounding outward. The lips are the transition from the oral mucosa to the skin, and unlike normal facial skin, the lip skin is not only free of sebaceous glands and sebaceous membranes, but also has a very rapid rate of stratum corneum metabolism, with thin stratum corneum and immature cells exposed on the surface of the lips. Therefore, moisture on the skin of the lips is relatively more easily evaporated, and particularly, when the lips need to be breathed by mouth during exercise or nasal obstruction, the moisture loss rate of the lips through the skin is higher, and the lips show a dry, rough, dull and dull shape.

Among a plurality of lip care products, a product with unique characteristics is closely related to fashion popularity, namely a lip care product with lip plumping effect, and the series of products occupy a place in the color cosmetic market.

CN108014026A discloses a lip plumping composition, which comprises the following components in parts by weight: 0.6 to 2 parts of first active component and 1 to 4 parts of second active component; the first active component comprises: ethylhexyl palmitate, behenyl trisilicate, sorbitan isostearate and palmitoyl tripeptide-1; the second active component comprises: isohexadecane, ethylene/propylene/styrene copolymer, butene/ethylene/styrene copolymer, sodium hyaluronate, xanthan gum, phenoxyethanol and tripeptide-1. The lip plumping composition has the effects of lip plumping and lip wrinkle removing while the moistening degree is ensured. The lip plumping composition comprises palmitoyl tripeptide-1 for promoting synthesis of collagen and glycosaminoglycan, sodium hyaluronate for high moisturizing capability and tripeptide-1 for promoting skin repair, and is mainly used for plumping lips by virtue of ingredients with conditioning function.

For another example, CN110538129A discloses a lip plumping lipstick, which comprises efficacy additives and pigment additives, wherein the efficacy additives comprise a class i efficacy additive and a class ii efficacy additive; the I-type efficacy additive comprises palmitoyl tripeptide lip plumping factor, jojoba seed oil, tocopherol, stearoyl glycyrrhizic acid, propyl hydroxybenzoate, shea butter, dog rose hip oil, ascorbyl dipalmitate, shea butter, almond oil, isooctyl palmitate tribehenate, sorbitan isostearyl and lactic acid; the II-class functional additive comprises collagen nourishing components, phytosterol, hyaluronic acid, methylparaben and honey. It also relies on ingredients with conditioning functions to plump the lips.

However, the active ingredients can achieve a good lip plumping effect only after being used for a long time, and more young consumers are expected to bring an instant lip plumping effect to lip plumping products for the young of the current color cosmetic market.

In conclusion, the research and development ideas of the existing commercially available lip plumping products are single, the lip plumping effect is achieved mostly from long-term continuous physiological effects, and the sensory perception and psychological expectation of 'instant lip plumping' are ignored to a great extent.

Disclosure of Invention

Aiming at the defects of the prior art, the invention aims to provide a lip plumping glaze and a preparation method thereof, and particularly provides the lip plumping glaze containing pepper peel extract and the preparation method thereof.

In order to achieve the purpose, the invention adopts the following technical scheme:

in a first aspect, the invention provides a lip plumping glaze containing pepper peel extract, which comprises lip plumping components, grease, a thickening agent, a bacteriostatic agent and a film forming agent; the lip plumping component comprises a pepper peel extract.

The lip plumping glaze contains lip plumping components containing pepper peel extracts, and pepper serving as rutaceae plants is rich in unsaturated fatty acid, can improve blood rheology, is commonly used in edible seasonings and is natural and edible. The fruit and pericarp extract is mild and safe for application to the skin, and does not cause strong burning sensation like capsaicin. The invention adds the zanthoxylum peel extract into the lip-rounding product for the first time, and achieves the effect of 'instantly rounding lips' by enhancing the blood circulation of the lips.

Preferably, the lip plumping glaze comprises 1-5 parts by weight of lip plumping components, 25-50 parts by weight of grease, 1-5 parts by weight of thickening agent, 0.1-1 part by weight of bacteriostatic agent and 40-70 parts by weight of film forming agent; the lip plumping component comprises a pepper peel extract.

The lip plumping glaze disclosed by the invention has a better effect on the lip plumping effect by combining the components according to the weight ratio.

The lip plumping component can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts by weight.

The weight portion of the grease can be 25, 28, 30, 32, 35, 40 or 50.

The weight portion of the thickening agent can be 1 part, 2 parts, 3 parts, 4 parts or 5 parts and the like.

The bacteriostatic agent can be 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part or 1 part by weight and the like.

The film forming agent can be 40 parts, 50 parts, 52 parts, 55 parts, 58 parts, 60 parts, 65 parts or 70 parts by weight.

The specific values in the above range can be selected, and are not described in detail herein.

Preferably, the lip plumping component comprises a zanthoxylum peel extract, a ginger root extract, bisabolol, vanillyl butyl ether, moisturizing microspheres, a lip plumping factor and a filler.

The lip plumping glaze creatively selects the combination of seven components of zanthoxylum bungeanum pericarp extract, ginger root extract, bisabolol, vanillyl butyl ether, moisturizing microspheres, lip plumping factors and fillers as the lip plumping component of the lip plumping glaze. The vanillyl butyl ether can permeate under the skin surface to slowly emit heat from inside to outside, the provided thermal sensation effect is multiple times that of a common pepper extract, the thermal sensation is mild, the thermal sensation is kept for several hours, the pepper extract is not red, hot, spicy and allergic to the skin, the pepper extract is combined with the pepper peel extract to increase the skin temperature of lips and improve the blood circulation, namely the pepper peel extract and the vanillyl butyl ether which are excellent skin warming agents are combined to synergistically increase the skin temperature and improve the blood circulation of the lips, so that the lip-rich thermal sensation effect is achieved. And mild non-irritating ginger root extract and bisabolol, and as soothing components, can reduce skin inflammation.

The filler can also synergize the visual effect of the instant lip plumping effect by increasing the coating thickness of the lip plumping product on the skin of the lips, and the normal stress (the best known stress in the polymer field is the climbing rod effect and the entrance effect) appears in the paste in the lip rubbing process due to the existence of polymers, and the 'traction series' caused by the normal stress enables the lip product to obtain higher consumer evaluation in the sensory test of the instant lip plumping when the lip is rubbed.

The moisturizing microspheres penetrate the upper layer of epidermis based on the dehydrated crosslinked spheres and absorb water evaporated from deep dermis to rapidly increase and expand the volume of the spheres, and the skin is tightened by the hydration to adhere to the skin of lips, so that an elastic skin surface is left.

The hydration of the lips depends to a large extent on the quality of the extracellular matrix, the reticular structure made up of hydrated macromolecules, in particular glycosaminoglycans and hyaluronic acid, promotes the swelling and elasticity of the dermis, collagen also plays a key role in the three-dimensional structure of the connective tissue, and lip plumping factors are able to stimulate the synthesis of collagen and glycosaminoglycans, achieving a skin-filling effect in macroscopic manifestations.

Preferably, the lip plumping component comprises 0.01-0.5 part of pepper peel extract, 0.001-0.5 part of ginger root extract, 0.05-0.3 part of bisabolol, 0.05-0.5 part of vanillyl butyl ether, 0.1-3 parts of moisturizing microspheres, 0.1-2 parts of lip plumping factor and 0.5-3 parts of filler in parts by weight.

When the components in the lip plumping component are combined according to the numerical value ranges, the lip plumping effect is better.

The weight parts of the pepper peel extract can be 0.01 part, 0.05 part, 0.1 part, 0.2 part, 0.3 part, 0.4 part or 0.5 part and the like.

The weight portion of the ginger root extract can be 0.001 portion, 0.01 portion, 0.05 portion, 0.1 portion, 0.2 portion, 0.3 portion, 0.4 portion or 0.5 portion, etc.

The weight portion of the bisabolol may be 0.05 portion, 0.08 portion, 0.1 portion, 0.15 portion, 0.2 portion, 0.25 portion, 0.3 portion, or the like.

The weight portion of the vanillyl butyl ether can be 0.05 portion, 0.1 portion, 0.2 portion, 0.3 portion, 0.4 portion or 0.5 portion, etc.

The moisture-keeping microspheres can be 0.1 part, 0.5 part, 0.8 part, 1 part, 1.5 parts, 2 parts, 2.5 parts or 3 parts by weight.

The weight portions of the lip plumping factor can be 0.1 portion, 0.5 portion, 0.8 portion, 1 portion, 1.5 portions, 2 portions and the like.

The filler may be present in an amount of 0.5, 0.8, 1, 1.5, 2, 2.5, or 3 parts by weight.

Preferably, the bulking agent comprises selamethamine bentonite and/or selamethamine hectorite.

When the saralamin bentonite and/or the saralamin hectorite are used as the filling agent, the structure of a 'card palace' formed on the skin of the lips can be formed, the thickness of a film covered on the lips by lip glaze is increased, obvious 'plump feeling' is provided, and the psychological expectation of 'plump lips' of a user is met.

Preferably, the moisturizing microspheres comprise Ultra FillingSphere manufactured by BASF (China) Inc. Ultra Filling Sphere (moisturizing microsphere) is realized by that dehydrated cross-linked spheres permeate the upper layer of epidermis and absorb moisture evaporated from deep dermis to rapidly increase and expand the volume of the spheres, and the skin is tightened by the hydration to adhere to the lip skin, so that an elastic skin surface is left.

Preferably, the Lip plumping factor comprises Maxi-Lip produced by Heda chemical (Shanghai) Inc. Maxi-Lip is able to stimulate the synthesis of collagen and glycosaminoglycans. The effect of skin filling is achieved on macroscopic expression.

Preferably, the oil or fat comprises any one or a combination of at least two of octyldodecanol, hydrogenated polyisobutene, diisostearyl malate, isononyl isononanoate, caprylic/capric triglyceride, ethylhexyl palmitate, cetyl ethylhexanoate, bis-diglycerol polyacyladipate-2, isopropyl palmitate, isopropyl myristate, C12-15 alcohol benzoate, isohexadecane, pentaerythritol tetrakis (ethylhexanoate), polyglycerol-3 triisostearate, pentaerythritol tetraisostearate, phenyl trimethicone, polydimethylsiloxane, trimethylpentaphenyl trisiloxane, or isododecane.

The combination of at least two of the above-mentioned compounds, such as octyldodecanol, hydrogenated polyisobutene and diisostearyl malate, caprylic/capric triglyceride and ethylhexyl palmitate, and isopropyl palmitate and isopropyl myristate, can be selected according to any combination, and thus, the details are not repeated herein.

Preferably, the thickener comprises any one of dimethylsilylated silica, ethylene/propylene/styrene copolymer, butylene/ethylene/styrene copolymer, hydrogenated (styrene/butadiene) copolymer, dibutylethylhexanoylglutamine, dibutyllauroylglutamine or hydrogenated (styrene/isoprene) copolymer, or a combination of at least two thereof.

The combination of at least two of the above-mentioned compounds, for example, the combination of dimethylsilylated silica and hydrogenated (styrene/butadiene) copolymer, the combination of dibutylethylhexanoylglutamine and dibutyllauroylglutamine, and the like, can be selected in any combination, and will not be described in detail herein.

Preferably, the bacteriostatic agent comprises any one or a combination of at least two of phenoxyethanol, caprylyl glycol, ethylhexyl glycerin, or caprylic glyceride.

The combination of at least two of the above-mentioned compounds, such as the combination of phenoxyethanol and caprylyl glycol, the combination of ethylhexyl glycerin and caprylic glyceride, etc., can be selected in any other combination manner, and thus, the details are not repeated herein.

Preferably, the film former comprises polybutylene.

Preferably, the polybutene has a kinematic viscosity at 100 ℃ of 200-.

Preferably, the refractive index of the polybutene ranges from 1.494 to 1.502, such as 1.494, 1.495, 1.496, 1.497, 1.498, 1.499, 1.500, 1.501, 1.502, etc.

The polybutylene increases the visual brightness of the lips by adjusting the refractive index of the lip glaze, and the brightness stimulation can lead the neurons to generate nonlinear amplification effect, thereby achieving the amplification effect of visual illusion and realizing the instant lip plumping.

Preferably, the lip plumping glaze further comprises a coloring agent.

Preferably, the colorant comprises any one of CI 77499, CI 42090, CI 15850, or a combination of at least two of pearlescent powders.

The combination of at least two of the above components, for example, the combination of CI 77499, CI 42090 and CI 15850, the combination of CI 15850 and pearl powder, the combination of CI 42090 and pearl powder, and the like, can be selected in any other combination manner, and thus, the details are not repeated herein.

In a second aspect, the invention provides a preparation method of the lip plumping glaze containing the zanthoxylum peel extract, which comprises the following steps:

(1) mixing lip plumping ingredients with 20-60% of grease according to the formula amount, and dispersing to obtain a dispersion liquid Q1; mixing the thickening agent with grease with the formula amount of 5-50%, and dispersing to obtain a dispersion liquid Q2;

(2) and mixing the dispersion liquid Q1, the dispersion liquid Q2, a bacteriostatic agent, a film-forming agent and the residual formula amount of grease, and dispersing to obtain the lip plumping glaze containing the pepper peel extract.

The preparation method of the lip plumping glaze provided by the invention has the advantages of simple process flow, easiness in operation, no need of heating, energy conservation and emission reduction, conforms to the current environmental protection regulations and requirements, and is suitable for industrial large-scale energy-saving production.

Preferably, the dispersing in step (1) is carried out at least three times by using a three-roll mill.

Preferably, the dispersing manner in step (2) is stirring for 10-40min, for example, 10min, 15min, 20min, 25min, 30min, 35min or 40min, and the specific values in the above range can be selected, and are not described herein again.

Preferably, in the step (2), the dispersion liquid Q1, the dispersion liquid Q2, the bacteriostatic agent, the film-forming agent and the color paste are mixed with the grease with the rest formula amount and dispersed.

Preferably, the preparation method of the color paste comprises the following steps: mixing the colorant with 20-40% of grease according to the formula amount, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the mixture by a particle size analyzer to ensure that the particle size of the color paste is below 7 mu m.

Compared with the prior art, the invention has the following beneficial effects:

the invention can not only increase the visual brightness of the lips, achieve the amplification effect of visual illusion and realize the instant lip plumping; meanwhile, the lip plump feeling is provided, the psychological expectation of consumer groups is met, and the user obviously feels that the lips slowly become plump. The skin warming agent with excellent compatibility can synergistically raise the skin temperature, improve the blood circulation of lips and achieve the lip plumping effect by the pepper peel extract and the vanillic butyl ether, and is mild and non-irritating by being matched with the ginger root extract and the bisabolol; the moisturizing microspheres and lip plumping factors are matched, and the effects of moisturizing lips and plumping double lips can be achieved after long-term use; the filler increases the coating thickness of the product on the skin of the lips and can also synergize the visual effect of 'instant lip plumping'; the film forming agent component added in the formula can increase the visual brightness of the lips, achieve the amplification effect of visual illusion and realize instant lip plumping.

Drawings

Figure 1 is a visual effect of lips before and after application of the product of example 1 (a before application and b after application).

Detailed Description

The technical solution of the present invention is further explained by the following embodiments. It should be understood by those skilled in the art that the examples are only for the understanding of the present invention and should not be construed as the specific limitations of the present invention.

Unless otherwise indicated, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The reagents and apparatus used are conventional products commercially available from normal sources, not indicated by the manufacturer.

Ultra Filling Sphere, to which the following examples refer, was purchased from basf (china) limited;

Maxi-Lip is purchased from Heda chemical (Shanghai) Inc.;

the extract of pericarpium Zanthoxyli is from research institute of Guangzhou Huanya cosmetics science and technology;

the ginger root extract is from research institute of Guangzhou Huanya cosmetics science and technology;

hydrogenated (styrene/isoprene) copolymers were purchased from KRATON corporation;

ethylene/propylene/styrene copolymers were purchased from calimet Specialty Products Partners, l.p.;

butene/ethylene/styrene copolymers were purchased from Calumet Specialty Products Partners, L.P..

Example 1

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(1) mixing and wetting the selamexane hectorite in the lip plumping component, caprylic/capric triglyceride and hydrogenated polyisobutene, grinding and dispersing by a three-roll grinder, adding other components in the lip plumping component, and stirring and dispersing uniformly to obtain a dispersion liquid Q1 containing the lip plumping component;

(2) mixing a colorant with 50% diisostearyl malate, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the particle size of the color paste by a particle sizer to be less than 7 microns to obtain the color paste Q3 meeting the requirements;

(3) mixing a thickening agent and 50% diisostearyl malate, and grinding and dispersing for three times by using a three-roll grinder until the material body is uniform to obtain a dispersion liquid Q2;

(4) and sequentially adding the dispersion liquid Q1, the color paste Q3, the dispersion liquid Q2, the bacteriostatic agent and the film forming agent, and mixing and stirring for 30min until the mixture is uniformly stirred to obtain the lip plumping glaze.

The visual effect of lips before and after application of the product of example 1 is shown in fig. 1 (a is before application and b is after application), and it can be seen that: the lip glaze provided by the invention has a remarkable instant lip plumping effect.

Example 2

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(1) mixing and wetting the salamin bentonite in the lip plumping component with caprylic/capric triglyceride, grinding and dispersing by a three-roll grinder, then adding other components in the lip plumping component, and then stirring and dispersing uniformly to obtain a dispersion liquid Q1 containing the lip plumping component;

(2) mixing a colorant with 50% cetyl ethyl hexanoate, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the particle size of the color paste by a particle sizer to be below 7 microns to obtain the color paste Q3 meeting the requirements;

(3) mixing a thickening agent and 50% cetyl ethyl hexanoate, and grinding and dispersing for three times by a three-roll grinder until the material body is uniform to obtain a dispersion liquid Q2;

(4) and sequentially adding the dispersion liquid Q1, the color paste Q3, the dispersion liquid Q2, the bacteriostatic agent, the film-forming agent and the residual oil, and mixing and stirring for 30min until the mixture is uniformly stirred to obtain the lip plumping glaze.

Example 3

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(2) mixing a colorant with 50% ethylhexyl palmitate, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the particle size of the color paste by a particle size analyzer to be less than 7 microns to obtain a color paste Q3 meeting the requirements;

(3) mixing a thickening agent and 50% ethylhexyl palmitate, and grinding and dispersing for three times by using a three-roll grinder until the material body is uniform to obtain a dispersion liquid Q2;

Example 4

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(4) and sequentially adding the dispersion liquid Q1, the color paste Q3, the dispersion liquid Q2, the bacteriostatic agent, the film-forming agent and the residual oil, and mixing and stirring for 20min until the mixture is uniformly stirred to obtain the lip plumping glaze.

Example 5

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(1) mixing and wetting the salamin bentonite in the lip plumping component with octyl dodecanol, grinding and dispersing by a three-roll grinder, adding other components in the lip plumping component, and stirring and dispersing uniformly to obtain a dispersion liquid Q1 containing the lip plumping component;

(2) mixing a colorant with 50% isopropyl palmitate, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the particle size of the color paste by a particle size analyzer to be less than 7 microns to obtain the color paste Q3 meeting the requirements;

(3) mixing a thickening agent with 50% isopropyl palmitate, and grinding and dispersing for three times by using a three-roll grinder until the material body is uniform to obtain a dispersion liquid Q2;

Example 6

This example provides a lip plumping glaze, which has the following formula:

the preparation method comprises the following steps:

(2) mixing a colorant with 50 percent of octyl dodecanol, grinding the mixture by a three-roll grinder for three times, uniformly dispersing the mixture, and analyzing the particle size of the color paste by a particle sizer to be less than 7 microns to obtain the color paste Q3 meeting the requirements;

(3) mixing a thickening agent with 50% of octyldodecanol, and grinding and dispersing for three times by using a three-roll grinder until the material body is uniform to obtain a dispersion liquid Q2;

Example 7

This example provides a lip plumping glaze, which is prepared according to a formula that is different from that of example 1 only in that the lip plumping glaze does not contain vanillyl butyl ether, and the weight percentage of the pepper peel extract is 0.5%, and the rest are kept unchanged.

Example 8

This example provides a lip plumping glaze which differs from example 1 only in that it does not contain the filler salamine hectorite and the hydrogenated polyisobutene is 6.5 weight percent, the dimethylsilylated silica is 5 weight percent, and the rest remains the same.

Example 9

This example provides a lip plumping glaze whose formulation differs from that of example 1 only in that the amount of selectamine hectorite was replaced with the same amount of kaolin, all other things remaining the same.

Example 10

This example provides a lip glaze which is formulated in a manner similar to that described in example 1 except that it does not comprise UltraFilling Sphere and the hydrogenated polyisobutene is present in an amount of 6.2% by weight, all other things remaining unchanged.

Example 11

This example provides a Lip plumping glaze which is formulated in the same manner as in example 1 except that Maxi-Lip is not included and hydrogenated polyisobutene is present in an amount of 6.5% by weight, all other things remaining unchanged.

Example 12

This example provides lip plumping glaze, which is prepared according to the following formula except that the lip plumping glaze does not contain ginger root extract, and the weight percentage of bisabolol is 0.35%, and the rest is kept unchanged.

Example 13

This example provides a lip plumping glaze which is formulated in the same manner as in example 1 except that it does not contain bisabolol and hydrogenated polyisobutene has a weight percentage of 6.3%, all other components remaining unchanged.

Comparative example 1

The comparative example provides lip plumping glaze, and the formula of the lip plumping glaze is different from that of the lip plumping glaze in example 1 only in that the lip plumping glaze does not contain pepper peel extract, the weight percentage of the vanillyl butyl ether is 0.5 percent, and the rest remains unchanged.

Comparative example 2

The comparative example provides a lip plumping glaze, which is different from the formula of example 1 in that the lip plumping component only contains the selectamine hectorite and does not contain other lip plumping components, and the formula is as follows:

the preparation process is as in example 1.

Evaluation test:

(1) single open smear test

The experiment is specifically operated according to modern cosmetics science and technology: volunteers 150 with healthy skin and an age between 25 and 55 years were selected as subjects, 10 per group. The lip gloss provided in examples 1 to 13 and comparative examples 1 to 2 was applied to the inner side of the left forearm of the volunteer as a test site, and the placebo cream was applied to the same site on the inner side of the right forearm, and the change in the appearance of the skin of the subject was observed and recorded, and the judgment criteria for skin reaction grade were as shown in the following table:

the results of the single open-paint lip glaze test provided in application examples 1-13 and application comparative examples 1-2 are shown in table 1:

TABLE 1

Test sample	Grade of reaction
		Example 1	Has no irritation
Example 2	Has no irritation
		Example 3	Has no irritation
Example 4	Has no irritation
		Example 5	Has no irritation
Example 6	Has no irritation
		Example 7	Has no irritation
Example 8	Has no irritation
		Example 9	Has no irritation
Example 10	Has no irritation
		Example 11	Has no irritation
Example 12	Has no irritation
		Example 13	Has no irritation
Comparative example 1	Has no irritation
		Comparative example 2	Has no irritation

As can be seen from the table above, the lip plumping glaze containing the zanthoxylum peel extract is safe and non-irritant to skin and can be used with confidence.

(2) Human body test and results of "instant lip plumping feeling" effect

(2.1) test method:

the lip gloss prepared according to examples 1, 7-13 and comparative examples 1-2 was tested by 20 persons. After cleaning the lips with the eye-lip makeup remover, the lips were left to stand in a room at constant temperature and humidity for 30 minutes, and the lip gloss provided in example 1 and comparative example 1 was used for comparison. After several days, lip enamels provided in example 1 and comparative example 2, example 1 and example 7, example 1 and example 8, example 1 and example 9, example 1 and example 10, example 1 and example 11, example 1 and example 12, example 1 and example 13, respectively, were used and compared. The test dimension was set as "instant lip plumping", and the control was scored at 5 points in this dimension, which was used as a control in example 1 to score (instant lip plumping was 1, 2, 3, 4 points lower than in example 1, 6, 7, 8, 9 higher than in example 1, and was 5 in the same way as in example 1.

To ensure uniformity, all examples and comparative examples provide the following specific application method of lip glaze:

the product of example 1 was applied to the left lower lip and the left upper lip first, i.e. the product was applied from the middle of the lip to the left lip corner in a horizontal stroke (1 time), then rapidly applied from the left lip corner along the left lower lip line (1 time), then applied at the left lip peak of the upper lip in an inclined stroke, then applied from the left lip peak of the upper lip along the left upper lip line to the left lip corner (1 time), and finally the blank part of the upper lip was filled up (1 time). The lip gloss provided by the other groups was applied to the right upper lip half and the right lower lip half with the same force and times.

(2.2) the test results are shown in Table 2:

TABLE 2

As can be seen from the data in Table 2:

example 7 was equally divided into 4.75 points, and 5 subjects had diminished feedback sensations, thus perceived less "instant lip plumping" than example 1. The feedback for example 12 and comparative examples 1 and 2 are similar to the feedback for example 1 in that the sensation of "instant lip plumping" is perceived as less than the sensation of reduced heat. The average score of example 12 was 4.95, with 1 subject having a slightly diminished sensation of feedback, and therefore perceived less "instant lip plumping" than example 1. The average score of comparative example 1 was 4.9. There were 2 subjects with diminished sensory feedback, and the "instant lip plumping" of example 1 was better. In comparative example 2, the average score was 4.7, and 4 scores were given to 6 subjects because "lip plumping" was not perceived at all. Thus, we have found that heat sensation is one of the important factors affecting whether the consumer obtains an "instant lip plumping" feeling. For most consumers, lip plumping products should be somewhat hot.

Example 8 was divided on average into 4.1 points, and more than half of the subjects felt a reduction in coating thickness on the upper lip of the body to varying degrees, and thus felt less "instant lip plumping" than example 1, although the sensation of heat and shine was not very different. Whereas the subject feedback in example 9 was due to a significant reduction in coating thickness and a slight reduction in lightness, resulting in most subjects being given a score of 5 points, an average score of 3.75, below the standard score of example 1. Thus, while seralatame bentonite and/or seralatame bentonite are able to increase coating thickness, kaolin in this system does not exhibit significant coating thickness-increasing properties and is likely to affect shine, thereby reducing the "instant lip plumping" experience when used by a subject.

In examples 10, 11 and 13, the average score was 5, and it was found that Ultra Filling Sphere, Maxi-Lip and bisabolol did not affect the evaluation of "instant Lip plumping" by the subjects.

(3) Evaluation of sensory Effect by consumers

150 volunteers aged 30-40 and having normal lip status were selected as subjects, and randomized into 15 groups of 10 persons each. The test method comprises the following steps: the subjects applied lips with the lip gloss of examples 1 to 13 and comparative examples 1 to 2 times a day for 30 consecutive days, recorded the state of the lip striae before use and the state of the lip striae after 30 days of use, and after the use, the subjects evaluated the "lip plumping" effect before and after the use of lipstick, and the evaluation results were classified into three grades, i.e., better, ordinary and no effect of lip plumping, and the evaluation results are shown in table 3.

TABLE 3

As can be seen from the data in Table 3:

in examples 1-6, there was good feedback, and in examples 3-4, all subjects had a significant improvement in lip area after 30 days of use, with good lip plumping effect.

In example 7, 6 subjects had better feedback effect, 3 subjects had general feedback effect, 1 subject had general feedback, and example 7 did not contain vanillyl butyl ether compared to example 1. It is hypothesized that when ingredients that provide a sensation of warmth and promote blood circulation are reduced in the formulation, the synergistic effect of other active ingredients on improving the condition of the lips so that they become engorged is reduced.

Example 8 has 8 subjects with better feedback effect, 2 subjects with general feedback effect, and the lip plumping effect after long-term use is the same as the test result of example 1, which shows that the filler in the lip plumping component does not affect the lip plumping effect after long-term use.

Example 9 also showed that 8 subjects had better feedback, and 2 subjects had a general feedback, indicating that the filler in the lip plumper had no effect on the lip plumper after long-term use.

Examples 10 to 11, wherein 6 of the examples 10 had no effect on feedback, 3 had a general effect on feedback, and 1 had a good effect on feedback, and it can be seen that the moisturizing microspheres had a great effect on the lip plumping effect after long-term use. Similarly, the lip plumping factor also has a great influence on the improvement of the lip filling state after long-term use.

Examples 12 to 13 showed the same overall feedback effect as example 1, and thus showed that the ginger root extract and bisabolol had no effect on improving the lip fullness after long-term use, but only for reducing the external irritation to the lips.

In comparative example 1, the feedback of 6 subjects is better, and the feedback of 4 subjects is general, which shows that the zanthoxylum peel extract has larger synergistic effect in the process of improving the lip plumpness.

In comparative example 2, 2 persons had general feedback effect, and 8 persons had no effect, indicating that the filler in the lip plumping composition did not bring about the lip plumping effect after long-term use.

The applicant states that the invention is illustrated by the above examples, but the invention is not limited to the above examples, i.e. the invention is not limited to the above examples. It should be understood by those skilled in the art that any modification of the present invention, equivalent substitutions of the raw materials of the product of the present invention, addition of auxiliary components, selection of specific modes, etc., are within the scope and disclosure of the present invention.

The preferred embodiments of the present invention have been described in detail, however, the present invention is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present invention within the technical idea of the present invention, and these simple modifications are within the protective scope of the present invention.

It should be noted that the various technical features described in the above embodiments can be combined in any suitable manner without contradiction, and the invention is not described in any way for the possible combinations in order to avoid unnecessary repetition.

Claims

1. A lip plumping glaze containing pepper peel extract is characterized in that the lip plumping glaze comprises lip plumping components, grease, a thickening agent, a bacteriostatic agent and a film forming agent; the lip plumping component comprises a pepper peel extract.

2. The lip plumping glaze containing the pepper peel extract as claimed in claim 1, wherein the lip plumping glaze comprises 1-10 parts by weight of lip plumping components, 25-50 parts by weight of grease, 1-5 parts by weight of thickening agent, 0.1-1 part by weight of bacteriostatic agent and 40-70 parts by weight of film forming agent; the lip plumping component comprises a pepper peel extract.

3. The lip plumping glaze containing the zanthoxylum peel extract according to claim 1 or 2, wherein the lip plumping component comprises zanthoxylum peel extract, ginger root extract, bisabolol, vanillyl butyl ether, moisturizing microspheres, lip plumping factor and filler.

4. The lip plumping glaze containing the pepper peel extract as claimed in claim 3, wherein the lip plumping component comprises 0.01-0.5 part of pepper peel extract, 0.001-0.5 part of ginger root extract, 0.05-0.3 part of bisabolol, 0.05-0.5 part of vanillyl butyl ether, 0.1-3 parts of moisturizing microspheres, 0.1-2 parts of lip plumping factor and 0.5-3 parts of filler in parts by weight.

5. The lip plumping glaze comprising the zanthoxylum bungeanum peel extract according to claim 3 or 4, wherein the filler comprises salami bentonite and/or salami hectorite;

preferably, the moisturizing microspheres comprise Ultra Filling Sphere manufactured by basf ltd;

preferably, the Lip plumping factor comprises Maxi-Lip manufactured by Dacron Chemicals, Inc.

6. The lip plumping glaze containing the prickly ash peel extract according to any one of claims 1 to 5, wherein the oil comprises any one or a combination of at least two of octyldodecanol, hydrogenated polyisobutene, diisostearyl malate, isononyl isononanoate, caprylic/capric triglyceride, ethylhexyl palmitate, cetyl ethylhexanoate, bis-diglycerol polyacyladipate-2, isopropyl palmitate, isopropyl myristate, C12-15 alcohol benzoate, isohexadecane, pentaerythritol tetrakis (ethylhexanoate), polyglycerol-3 triisostearate, pentaerythritol tetraisostearate, phenyl trimethicone, polydimethylsiloxane, trimethylpentaphenyl trisiloxane or isododecane.

7. The lip plumping glaze containing the pepper peel extract as claimed in any one of claims 1 to 6, wherein the thickener comprises any one or a combination of at least two of dimethylsilylated silica, ethylene/propylene/styrene copolymer, butylene/ethylene/styrene copolymer, hydrogenated (styrene/butadiene) copolymer, dibutylethylhexanoylglutamine, dibutyllauroylglutamine or hydrogenated (styrene/isoprene) copolymer;

8. The lip plumping glaze containing the zanthoxylum peel extract according to any one of claims 1 to 7, wherein the film forming agent comprises polybutene;

preferably, the polybutene has a kinematic viscosity at 100 ℃ of 200-;

preferably, the refractive index of the polybutene ranges from 1.494 to 1.502;

preferably, the lip plumping glaze further comprises a colorant;

9. The preparation method of lip plumping glaze containing zanthoxylum peel extract according to any one of claims 1 to 8, which comprises the following steps:

10. The method for preparing lip plumping glaze containing zanthoxylum peel extract according to claim 9, wherein the dispersing manner in the step (1) is to grind and disperse at least three times by using a three-roll grinder;

preferably, the dispersing mode in the step (2) is stirring for 10-40 min;

preferably, the step (2) is to mix and disperse the dispersion liquid Q1, the dispersion liquid Q2, the bacteriostatic agent, the film-forming agent and the color paste with the grease with the rest formula amount;