CN111317673A - Isolation cream added with cyperus esculentus root oil and preparation method thereof - Google Patents

Isolation cream added with cyperus esculentus root oil and preparation method thereof Download PDF

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CN111317673A
CN111317673A CN201811559513.0A CN201811559513A CN111317673A CN 111317673 A CN111317673 A CN 111317673A CN 201811559513 A CN201811559513 A CN 201811559513A CN 111317673 A CN111317673 A CN 111317673A
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skin
cyperus esculentus
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root oil
cyperus
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宋超
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/23Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25Silicon; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/26Aluminium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/29Titanium; Compounds thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36Carboxylic acids; Salts or anhydrides thereof
    • A61K8/361Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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  • Cosmetics (AREA)

Abstract

The invention discloses a moisturizer added with cyperus esculentus root oil and a preparation method thereof, wherein cyperus esculentus root oil rich in vitamin E and linoleic acid is compatible with whitening, moisturizing and anti-aging components, and the moisturizer added with the cyperus esculentus root oil is prepared by adopting a modern technology.

Description

Isolation cream added with cyperus esculentus root oil and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to a make-up base added with cyperus oil and a preparation method thereof.
Background
With the improvement of living standard, people's pursuit of beauty is continuously improved, so more and more people choose to achieve instant effect of beauty through makeup, but people also want the efficacy of skin care and skin care of cosmetics. At present, most of the common makeup creams in the market are prepared by adding silicon compounds, mica, light modification particles and other components and pigment particles which can improve the smooth texture of skin, so that the makeup creams have the effects of pore modification, skin color adjustment and the like, but the method cannot solve the original problems of skin, such as dull skin color, color spots, wrinkles, skin barrier damage and the like, and further causes the deterioration of skin problems after long-term use.
Research shows that the roots of the cyperus rotundus contain rich grease, the cyperus rotundus root oil extracted from the cyperus rotundus roots is rich in vitamin E and linoleic acid, can prevent skin damage, can be used as a skin conditioner to be added into skin care products and cosmetics, can enhance the barrier function of the skin, has the effects of moisturizing, improving the glossiness of the skin and tendering the skin, and enables the skin to be kept in a healthy state. The applicant plants a large amount of cyperus esculentus, and root tubers of the cyperus esculentus can extract cyperus esculentus root oil, so the applicant invents the isolation cream added with the cyperus esculentus root oil to solve the problems that the existing isolation cream cannot fundamentally solve the skin color dullness, color spots, wrinkles, skin barrier damage, skin condition deterioration caused by long-term use and the like.
Disclosure of Invention
The invention aims to provide a barrier cream added with cyperus rotundus root oil and a preparation method thereof, wherein cyperus rotundus root oil rich in vitamin E and linoleic acid is compatible with whitening, moisturizing and anti-aging components, and the barrier cream added with the cyperus rotundus root oil is prepared by adopting a modern technology, has stable performance, has the effects of isolating, whitening, concealing blemishes, adjusting skin color and preventing sunlight, also has the functions of moisturizing, improving skin glossiness and caring skin, can repair damaged skin barriers, improve the conditions of dry, rough and aging of the skin, and fundamentally solves the skin problem.
In order to achieve the purpose, the invention provides the following scheme:
the invention provides a makeup base added with cyperus oil, which comprises the following components in percentage by weight: 0.5-9% of cyperus esculentus root oil, 2-4% of titanium dioxide, 6-12% of polydimethylsiloxane, 2-12% of a softening agent, 8-16% of a humectant, 2-4% of an emulsifier, 1-7% of isododecane, 1.5-3.5% of an isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, 0.02-0.2% of tocopheryl acetate, 0.5-1.5% of ethylhexyl palmitate, 0.6-1.2% of magnesium sulfate, 0.1-0.6% of silica, 0.01-0.2% of mica, 1.5-3.5% of magnesium stearate, 0.15-1% of phenoxyethanol, 0.05-0.3% of ethylhexylglycerin, 0.05-0.2% of an essence, and the balance of deionized water.
Preferably, the emulsifier is one or two of polyglycerol-2 dipolyhydroxystearate and polyglycerol-3 diisostearate.
Preferably, the humectant is one or a mixture of more than two of glycerin, propylene glycol and glyceryl polyether-26.
Preferably, the softening agent is one or a mixture of more than two of mineral oil, C12-15 alcohol benzoate and isohexadecane.
Preferably, the titanium dioxide is surface treated with triethoxycaprylylsilane.
The invention also provides a preparation method of the foundation cream added with cyperus oil, which comprises the following steps:
s1: mixing the emulsifier and the emollient, heating to 55-80 ℃, and uniformly stirring to completely dissolve the emulsifier in the emollient to prepare an emulsion A;
s2: adding the polydimethylsiloxane, the ethylhexyl palmitate, the isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, the magnesium sulfate, the tocopherol acetate, the magnesium stearate, the silica and the titanium dioxide treated by the triethoxyoctylsilane into the emulsion A, uniformly stirring, and homogenizing to obtain an emulsion B;
s3: adding the humectant and the deionized water into the emulsion B while stirring, and homogenizing after uniformly stirring to obtain an emulsion C;
s4: adding the cyperus esculentus root oil, the phenoxyethanol, the ethylhexyl glycerol, the alumina, the mica and the essence into the emulsion C while stirring, homogenizing after uniformly stirring, and performing vacuum defoamation to obtain the isolation cream added with the cyperus esculentus root oil.
The main components and the effects of the invention are as follows:
1. cyperus oil: the essential oil extracted from the cyperus esculentus roots is rich in vitamin E and linoleic acid, can prevent skin damage, can be added into skin care products and cosmetics as a skin conditioner, can enhance the barrier function of skin, has the effects of moisturizing, improving the glossiness of the skin and tendering the skin, and keeps the skin in a healthy state.
2. Titanium dioxide: the whitening powder has higher whiteness, belongs to inert mineral substances, has no activity, thus having good safety and no anaphylactic reaction, and is commonly added into foundation make-up and sun screen to be used as white powder for color matching, thereby having the effect of whitening skin color. In addition, titanium dioxide has the efficacy of a sunscreen.
3. Polydimethylsiloxane: the lubricant has good lubricating property, can form a layer of uniform protective film with water resistance after being coated on skin, does not have any sticky or greasy feeling, and has good glossiness. The performance of resisting ultraviolet radiation is good: it is not oxidized and deteriorated under ultraviolet rays to cause skin irritation. The antistatic performance is good: tests show that the skin static electricity after being wiped by the skin care cream containing polysiloxane is completely eliminated, and the skin care cream has obvious dustproof effect. The air permeability is good: even the formation of a silicone film on the skin does not affect sweat discharge. It has the functions of slowly releasing and fixing fragrance, so that it has long fragrance-retaining period, high stability, chemical inertia and good compatibility with other components of cosmetics, especially active component. Has no toxicity, odor or taste, no irritation or allergy to skin, and high safety.
4. Mineral oil: the oil extracted from petroleum is colorless, odorless and low in sensitivity. Has antistatic effect, and can be used as solvent and emollient in cosmetics. The mineral oil is divided into cosmetic grade and medicinal grade, and the cosmetic grade mineral oil has high safety and small irritation, and can also achieve the effect of resisting oxidation.
5. Ethylhexyl palmitate: belongs to synthetic ester, is widely used in skin care products and cosmetics, has stable property, and is not easy to oxidize or generate peculiar smell. The component has small molecule, and can easily penetrate into pore and penetrate into keratinocyte, but excessive application can cause skin to have phenomena of keratinization, yellow wax, coarse yellow, etc.
6. Glycerol: also known as glycerin, a softening, moisturizing, makeup removing solvent and a lubricant. Undiluted 100% pure glycerol can never be used directly, which would have adverse effects. Glycerol has a water-absorbing effect, and is often used in moisturizing skin care products to absorb water molecules in the air, so that the stratum corneum of the skin covered by the moisturizing skin care product is kept moist.
7. Propylene glycol: propylene oxide derived from petrochemical sources belongs to small molecular moisture-retaining components. Is one kind of polyol, is almost colorless, odorless and non-greasy, is completely dissolved in water, and also has antiseptic effect. Propylene glycol, which has high permeability when used as a slip agent, helps other ingredients spread and penetrate on the skin surface, but is often used in combination with glycerin because of its low water-holding ratio when used as a moisturizer.
8. C12-15 alcohol benzoates: can be used as softening agent, and has refreshing effect when added into product. And the emulsion is easy to emulsify, can be used in cream, emulsion skin care products and cosmetics, and has moistening and non-greasy using effects.
9. Isohexadecane: can be used as emollient and solvent in cosmetics, and has effect in improving texture of product.
10. Polyglyceryl-2 dipolyhydroxystearate: the water-in-oil emulsifier can be used for preparing a low-viscosity water-in-oil emulsion, and can be added into cosmetics as a film forming agent, so that the skin has good adsorption and spreadability, and is clean, white and bright.
11. Isododecane: it is commonly used as an emulsifier and solvent in skin care and cosmetic products, and is a hydrocarbon, which acts as a solvent to provide a product with a fresh texture, which is easy to apply, and which reduces or avoids loss of skin moisture.
12. Isobutyl methacrylate/bis-hydroxypropyl dimethicone acrylate copolymer: has excellent film forming, dispersing, adsorbing and lubricating abilities, is used as a film forming agent, a conditioner and the like, and is applied to the field of personal care products.
13. Polyglyceryl-3 diisostearate: can be used as emulsifier in cosmetic.
14. Glyceryl polyether-26: is glycerin adduct of 26 mol of epoxy ethylene, and is used as a humectant and a lubricant. Are stable over a wide range of pH values for cosmetic and cleaning products, have good compatibility with cationic, nonionic and anionic surfactants, and are very effective moisturizers in creams and lotions. The glyceryl polyether-26 greatly improves the sticky and skin-friendly feeling of the product in a semi-dry state, and is particularly suitable for products containing macromolecular polymers such as essence, gel and the like.
15. Magnesium sulfate: the external preparation can improve rough skin, and can be used as filler and viscosity control agent in cosmetic, fill depression and pores, and smooth skin.
16. Silica: is commonly used in foundation and makeup base, has slight coverage, and can increase skin smoothness. And silica is highly safe in cosmetics and non-irritating to the skin.
17. Alumina: the product can be used as adsorbent and thickener in cosmetic, has high safety on skin, and can make mica surface show soft pearl luster.
18. Tocopherol acetate: the vitamin E derivative belongs to vitamin E derivatives, is commonly used as an antioxidant in cosmetics, has good antioxidant effect, is an oil-soluble natural substance, is a good nutritional moistening agent for skin, can avoid rancidity oxidation of oil and stabilize the oil when being added into skin care products and cosmetics. The composition has good effects in moisturizing and maintaining connective tissues, and protecting skin from ultraviolet rays, and can soften skin touch and retain skin moisture, promote wound healing, prevent inflammation, prevent skin from rough and chapped, improve black spots, and has a low safety risk index, thus being widely used.
19. Mica: belongs to natural mineral substances, has luster, and can be made into matt shape. The cosmetic is mainly used as a coloring agent, and the brightness of the cosmetic is increased, so that the skin texture and the touch feeling are increased after the cosmetic is used. The mica can not be absorbed by skin, and can not cause any damage to skin due to mineral substances, and is mainly used for enhancing the shiny visual effect of cosmetics.
20. Triethoxyoctylsilane: is a silicone resin, and is mainly used as a binder and an emulsifier. The product is used as surface treating agent for inorganic filler or pigment such as titanium dioxide, and has improved affinity and wettability with paint, adhesive, sealant, etc.
21. Magnesium stearate: can be used as self-emulsifying matrix of water-in-oil type cosmetic emulsion, can be used as colorant in various cosmetics and other daily chemical products, can effectively inhibit degradation of DHA in the product, and has good antiaging and moisturizing effects.
22. Phenoxyethanol: it is a low-grade skin sensitive preservative, and the most widely used preservative in cosmetics. Has slight aromatic smell, has certain emulsification effect and has great influence on the viscosity of the product.
23. Ethyl hexyl glycerin: has the functions of moisturizing, antibacterial property and strong stability, is often used as a solvent or an additive, can improve the moisturizing effect of the product, and has the effect of smoothing skin. The component can also enhance the antiseptic effect of phenoxyethanol, reduce the dosage of antiseptic components in the product, and increase the safety of the product.
24. Essence: although the amount of the essence used in the cosmetics is small, the essence can provide pleasant smell, cover the smell of the product matrix, help the product to establish brand-new image and enhance the attraction of the product to customers.
The invention achieves the following beneficial technical effects:
1. the barrier cream added with the cyperus esculentus root oil provided by the invention is prepared by matching the cyperus esculentus root oil rich in vitamin E and linoleic acid with whitening, moisturizing and anti-aging components and adopting a modern technology, has stable performance, not only has the effects of isolating, whitening, concealing flaws, adjusting skin color and preventing sun, but also has the skin care functions of moisturizing, improving the glossiness of skin and softening skin, can repair damaged skin barriers, improves the conditions of dry, rough and aging skin and fundamentally solves the skin problem.
2. The moisturizer added with the cyperus esculentus root oil provided by the invention is simple in material components, reasonable in formula, low in cost and easy to popularize, and has small irritation to skin.
3. The moisturizer added with the cyperus esculentus root oil widens the new application field of cyperus esculentus and brings great economic and social benefits.
4. The preparation method of the foundation cream added with the cyperus esculentus root oil provided by the invention is simple in process, easy to operate and easy to realize large-scale production.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention aims to provide a barrier cream added with cyperus rotundus root oil and a preparation method thereof, wherein cyperus rotundus root oil rich in vitamin E and linoleic acid is compatible with whitening, moisturizing and anti-aging components, and the barrier cream added with cyperus rotundus root oil is prepared by adopting a modern technology, has stable performance, has the effects of isolating, whitening, covering blemishes and adjusting skin color, also has the functions of moisturizing, improving the glossiness of skin and caring the skin of tender skin, can repair the damaged skin barrier, improve the conditions of dry, rough and aging of the skin, and fundamentally solves the problem of the skin.
The present invention will be described in further detail with reference to specific embodiments in order to make the above objects, features and advantages more apparent and understandable.
Example 1:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: cyperus oil 0.5%, titanium dioxide 2%, polydimethylsiloxane 6%, mineral oil 2%, glycerol 4%, propylene glycol 4%, polyglycerol-2-dipolyhydroxystearate 2%, isododecane 1%, isobutyl methacrylate/bis-hydroxypropyl polydimethylsiloxane acrylate copolymer 1.5%, tocopherol acetate 0.02%, ethylhexyl palmitate 0.5%, magnesium sulfate 0.6%, silica 0.1%, mica 0.01%, magnesium stearate 1.5%, phenoxyethanol 0.15%, ethylhexylglycerol 0.05%, essence 0.05%, and the balance of deionized water.
A base cream with added cyperus oil having the composition of the example was prepared according to the following procedure:
s1: mixing the emulsifier and the emollient, heating to 55 ℃, and uniformly stirring to completely dissolve the emulsifier in the emollient to prepare an emulsion A;
s2: adding the polydimethylsiloxane, the ethylhexyl palmitate, the isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, the magnesium sulfate, the tocopherol acetate, the magnesium stearate, the silica and the titanium dioxide treated by the triethoxyoctylsilane into the emulsion A, uniformly stirring, and homogenizing to obtain an emulsion B;
s3: adding the humectant and the deionized water into the emulsion B while stirring, and homogenizing after uniformly stirring to obtain an emulsion C;
s4: adding the cyperus esculentus root oil, the phenoxyethanol, the ethylhexyl glycerol, the alumina, the mica and the essence into the emulsion C while stirring, homogenizing after uniformly stirring, and performing vacuum defoamation to obtain the isolation cream added with the cyperus esculentus root oil.
Example 2:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: cyperus oil 9%, titanium dioxide 4%, polydimethylsiloxane 12%, C12-15 alcohol benzoate 12%, glycerol 10%, glycerol polyether-26 6%, polyglycerol-2-dihydroxystearate 2%, polyglycerol-3-diisostearate 2%, isododecane 7%, isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer 3.5%, tocopheryl acetate 0.2%, ethylhexyl palmitate 1.5%, magnesium sulfate 1.2%, silica 0.6%, mica 0.2%, magnesium stearate 3.5%, phenoxyethanol 1%, ethylhexylglycerin 0.3%, essence 0.2%, and the balance of deionized water.
The preparation method of the makeup base containing cyperus rotundus essential oil in this example is the same as that of example 1 except that the heating is carried out to 57 ℃ in step S1.
Example 3:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: cyperus oil 2%, titanium dioxide 2%, polydimethylsiloxane 8%, isohexadecane 6%, glycerol 4%, propylene glycol 4%, glyceryl polyether-26 of 2%, polyglycerol-3 diisostearate 2.5%, isododecane 4%, isobutyl methacrylate/dihydroxypropylpolydimethylsiloxane acrylate copolymer 2%, tocopheryl acetate 0.1%, ethylhexyl palmitate 1%, magnesium sulfate 0.9%, silica 0.4%, mica 0.1%, magnesium stearate 2%, phenoxyethanol 0.5%, ethylhexylglycerin 0.2%, essence 0.1%, and the balance of deionized water.
The preparation method of the makeup base containing cyperus rotundus essential oil in this example is the same as that of example 1 except that the heating is carried out to 61 ℃ in step S1.
Example 4:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: cyperus oil 5%, titanium dioxide 3%, polydimethylsiloxane 9%, mineral oil 5%, C12-15 alcohol benzoate 5%, glycerol 12%, polyglycerol-2-dipolyhydroxystearate 3%, isododecane 5%, isobutyl methacrylate/bis-hydroxypropyl polydimethylsiloxane acrylate copolymer 2.5%, tocopherol acetate 0.05%, ethylhexyl palmitate 0.8%, magnesium sulfate 0.7%, silica 0.2%, mica 0.15%, magnesium stearate 3%, phenoxyethanol 0.7%, ethylhexylglycerin 0.15%, essence 0.15%, and the balance of deionized water.
The preparation method of the makeup base containing cyperus rotundus essential oil in this example is the same as that of example 1 except that the heating is performed to 69 ℃ in step S1.
Example 5:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: 7% of cyperus oil, 3.5% of titanium dioxide, 11% of polydimethylsiloxane, 2.5% of mineral oil, 1.5% of isohexadecane, 6% of propylene glycol, 8% of glyceryl polyether-26, 3.5% of polyglycerol-3 diisostearate, 3% of isododecane, 3% of isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, 0.15% of tocopheryl acetate, 1.2% of ethylhexyl palmitate, 1% of magnesium sulfate, 0.5% of silica, 0.13% of mica, 2.5% of magnesium stearate, 0.26% of phenoxyethanol, 0.1% of ethylhexylglycerin, 0.08% of essence and the balance of deionized water.
The preparation method of the makeup base containing cyperus rotundus essential oil in this example is the same as that of example 1 except that the heating is carried out to 72 ℃ in step S1.
Example 6:
the embodiment provides a makeup base added with cyperus esculentus essential oil, which comprises the following components in percentage by weight: 8% of cyperus oil, 2.5% of titanium dioxide, 10% of polydimethylsiloxane, 4% of C12-15 alcohol benzoate, 4% of isohexadecane, 10.5% of glyceryl polyether-26, 1.4% of polyglyceryl-2-dipolyhydroxystearate, 1.4% of polyglyceryl-3-diisostearate, 6% of isododecane, 1.8% of isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, 0.08% of tocopherol acetate, 1.3% of ethylhexyl palmitate, 0.8% of magnesium sulfate, 0.3% of silica, 0.04% of mica, 1.8% of magnesium stearate, 0.83% of phenoxyethanol, 0.24% of ethylhexylglycerol, 0.11% of essence, and the balance of deionized water.
The preparation method of the makeup base containing cyperus esculentus essential oil in this example is the same as that of example 1 except that the heating temperature is increased to 76 ℃ in step S1.
Example 1:
the embodiment provides a foundation cream added with cyperus esculentus root oil, which comprises the following components in percentage by weight: cyperus oil 3.5%, titanium dioxide 4%, polydimethylsiloxane 7%, mineral oil 2%, C12-15 alcohol benzoate 1.5%, isohexadecane 1.5%, propylene glycol 5%, glyceryl polyether-26 6%, polyglycerol-2-dihydroxystearate 1.7%, polyglycerol-3-diisostearate 1.5%, isododecane 2%, isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer 2.6%, tocopherol acetate 0.17%, ethylhexyl palmitate 0.6%, magnesium sulfate 1.1%, silica 0.35%, mica 0.08%, magnesium stearate 2.7%, phenoxyethanol 0.9%, ethylhexylglycerin 0.08%, essence 0.19%, and the balance of deionized water.
The preparation method of the makeup base containing cyperus rotundus essential oil in this example is the same as that of example 1 except that the heating is carried out to 80 ℃ in step S1.
The surface treatment method of the titanium dioxide in the above embodiments 1 to 7 is:
s1: uniformly mixing triethoxyoctylsilane and 95 vt% ethanol solution to obtain surface treatment liquid for later use; the addition ratio of the triethoxyoctylsilane to the ethanol solution is (0.85-1.15) to (1.8-2.2) by mass, and preferably the addition ratio of the triethoxyoctylsilane to the ethanol solution is 1: 2;
s2: adding titanium dioxide powder into a high-speed stirrer, adding the surface treatment liquid prepared in the step S1 into the titanium dioxide powder while stirring at a high speed, and fully stirring to uniformly mix the titanium dioxide powder and the titanium dioxide powder;
s3: taking the titanium dioxide powder uniformly mixed with the surface treatment liquid out of the stirrer, putting the titanium dioxide powder into an oven for baking, setting the baking time to be 3-5 h, setting the baking temperature to be 90-110 ℃, and naturally cooling after baking is finished to obtain titanium dioxide treated by triethoxycaprylylsilane; preferably, the baking time is set to 4.5h and the baking temperature is set to 100 ℃.
Test example 1:
50ml of the base cream added with cyperus oil prepared in example 2 was used as a sample, and the sample was tested according to GB/T1857-2013 and technical Specification for cosmetic safety (2015), and the results were as follows:
TABLE 1
Figure BSA0000176255500000091
Figure BSA0000176255500000101
Figure BSA0000176255500000111
From the test results in table 1, it can be seen that the base cream containing cyperus oil prepared in example 2 meets the standard requirements of GB/T1857-2013 and technical specifications for cosmetic safety (2015 edition). The single evaluation obtained by detecting the embodiments 3 to 8 is the same as that of the embodiment 2, and all the detection items are qualified, namely the standard requirements of national standards and specifications are met.
Test example 2:
campaign propaganda is carried out through the internet, a trial report can be submitted in one month for free trial, 150 parts of the sun screen prepared in each embodiment is provided and randomly distributed to 1050 female users participating in the campaign, 1044 parts of the trial report are recovered after the deadline of one month, 140 parts of the trial report in each embodiment is randomly selected, the 980 trial reports are sorted and summarized, and the summary result is as follows:
TABLE 2
Figure BSA0000176255500000112
TABLE 3
Figure BSA0000176255500000121
TABLE 4
Figure BSA0000176255500000122
TABLE 5
Figure BSA0000176255500000131
As can be seen from tables 2 to 5, for examples 2 to 8, more than 85% of users had good or better evaluations of the barrier cream added with cyperus esculentus root oil, skin color adjustment, skin color brightening, makeup fitting, skin moisturizing, sun protection and skin barrier repair effects, and no one had reflected the occurrence of an allergic phenomenon in the use process.
Therefore, the foundation cream added with the cyperus oil has stable performance, not only has the effects of isolating, whitening, concealing, adjusting skin color and preventing sun, but also has the functions of moisturizing, improving the glossiness of skin and caring the tender skin, can repair the damaged skin barrier, improves the conditions of dry, rough and aged skin, and fundamentally solves the skin problem.
The principle and the implementation mode of the invention are explained by applying specific examples, and the description of the above examples is only used for helping understanding the method and the core idea of the invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, the specific embodiments and the application range may be changed. In summary, this summary should not be construed to limit the present invention.

Claims (6)

1. A foundation cream added with cyperus esculentus root oil is characterized in that: comprises the following components in percentage by weight: 0.5-9% of cyperus esculentus root oil, 2-4% of titanium dioxide, 6-12% of polydimethylsiloxane, 2-12% of a softening agent, 8-16% of a humectant, 2-4% of an emulsifier, 1-7% of isododecane, 1.5-3.5% of an isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, 0.02-0.2% of tocopheryl acetate, 0.5-1.5% of ethylhexyl palmitate, 0.6-1.2% of magnesium sulfate, 0.1-0.6% of silica, 0.01-0.2% of mica, 1.5-3.5% of magnesium stearate, 0.05-0.5% of aluminum oxide, 0.15-1% of phenoxyethanol, 0.05-0.3% of ethylhexylglycerin, 0.05-0.2% of essence and the balance of deionized water.
2. The base cream with added cyperus esculentus root oil according to claim 1, wherein: the emulsifier is one or two of polyglycerol-2 dipolyhydroxystearate and polyglycerol-3 diisostearate.
3. The base cream with added cyperus esculentus root oil according to claim 1, wherein: the humectant is one or a mixture of more than two of glycerol, propylene glycol and glycerol polyether-26.
4. The base cream with added cyperus esculentus root oil according to claim 1, wherein: the softening agent is one or a mixture of more than two of mineral oil, C12-15 alcohol benzoate and isohexadecane.
5. The base cream with added cyperus esculentus root oil according to claim 1, wherein: the titanium dioxide is subjected to surface treatment by triethoxyoctylsilane.
6. The method for preparing a base cream containing cyperus rotundus oil according to any of claims 1 to 5, comprising the following steps:
s1: mixing the emulsifier and the emollient, heating to 55-80 ℃, and uniformly stirring to completely dissolve the emulsifier in the emollient to prepare an emulsion A;
s2: adding the polydimethylsiloxane, the ethylhexyl palmitate, the isobutyl methacrylate/dihydroxypropyl polydimethylsiloxane acrylate copolymer, the magnesium sulfate, the tocopherol acetate, the magnesium stearate, the silica and the titanium dioxide treated by the triethoxyoctylsilane into the emulsion A, uniformly stirring, and homogenizing to obtain an emulsion B;
s3: adding the humectant and the deionized water into the emulsion B while stirring, and homogenizing after uniformly stirring to obtain an emulsion C;
s4: adding the cyperus esculentus root oil, the phenoxyethanol, the ethylhexyl glycerol, the alumina, the mica and the essence into the emulsion C while stirring, homogenizing after uniformly stirring, and performing vacuum defoamation to obtain the isolation cream added with the cyperus esculentus root oil.
CN201811559513.0A 2018-12-13 2018-12-13 Isolation cream added with cyperus esculentus root oil and preparation method thereof Pending CN111317673A (en)

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