CN115778858B - Nourishing lip balm and preparation method thereof - Google Patents
Nourishing lip balm and preparation method thereof Download PDFInfo
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- CN115778858B CN115778858B CN202211653171.5A CN202211653171A CN115778858B CN 115778858 B CN115778858 B CN 115778858B CN 202211653171 A CN202211653171 A CN 202211653171A CN 115778858 B CN115778858 B CN 115778858B
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- Cosmetics (AREA)
Abstract
The invention belongs to the field of cosmetics, and particularly discloses a nourishing lip balm and a preparation method thereof. The nourishing lip balm comprises the following raw material components in parts by mass: 3-12 parts of berhard walnut seed oil, 3-12 parts of phytosterol isostearate, 0-25 parts of diisostearyl malate, 0-20 parts of jojoba seed oil, 0-16 parts of sunflower seed oil, 0-15 parts of hydrogenated vegetable oil, 0-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 0-8 parts of PEG-12 carnauba wax, 0-10 parts of candelilla wax, 0-8 parts of wild lacquer fruit wax, 0-6 parts of ceresin wax, 0-2 parts of Rosa canina oil and 0-0.2 parts of hydroxypropyl. The nourishing lip balm disclosed by the invention has good stability, can be light and thin in use, has strong moistening property, can keep the moistening property for a long time, and can not generate sensitization and adverse reaction after use.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a nourishing lip balm and a preparation method thereof.
Background
Lipstick is a lip cosmetic that has the primary function of imparting a hue to the lips, emphasizing or changing the contours of the lips, and exhibiting more vitality and vitality. Compared with the skin, the cuticle of the lips is very thin, the moisture is easy to evaporate, especially in autumn and winter dry weather, the moisture of the lips is very easy to evaporate, and the phenomena of dry lips, roughness, sensitivity, dry cracks and the like often occur. In order to improve and even avoid phenomena such as dry, rough, sensitive and chapped lips, lip balm is often used for coating the lips to play a role in moistening and protecting the lips. With the development of lip cosmetics, the lip balm has various formulas and processes, and has the functions of preventing dry cracking, fading lip marks, providing cool feeling, enlarging lips and the like.
However, the existing lip products still have poor moisturizing property, poor moisturizing durability, sticky feel and even possible sensitization and adverse reactions.
Disclosure of Invention
Aiming at the problems of poor moisturizing property, poor moisturizing persistence, sticky feeling and the like of the nourishing lip balm related to the prior art, the invention provides the nourishing lip balm and the preparation method thereof.
In order to achieve the above purpose, the method specifically comprises the following technical scheme:
The nourishing lip balm comprises the following raw material components in parts by mass:
3-12 parts of berhard walnut seed oil, 3-12 parts of phytosterol isostearate, 0-25 parts of diisostearyl malate, 0-20 parts of jojoba seed oil, 0-16 parts of sunflower seed oil, 0-15 parts of hydrogenated vegetable oil, 0-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 0-8 parts of PEG-12 carnauba wax, 0-10 parts of candelilla wax, 0-8 parts of wild lacquer fruit wax, 0-6 parts of ceresin wax, 0-2 parts of Rosa canina oil and 0-0.2 parts of hydroxypropyl.
As a preferred embodiment of the invention, the material comprises the following raw material components in parts by mass: 6-12 parts of berhard walnut seed oil, 6-12 parts of phytosterol isostearate, 10.5-20 parts of diisostearyl malate, 12.5-20 parts of jojoba seed oil, 12.5-16 parts of sunflower seed oil, 10.5-15 parts of hydrogenated vegetable oil, 8.5-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 5.5-8 parts of PEG-12 carnauba wax, 4.5-10 parts of candelilla wax, 4.5-8 parts of wild lacquer fruit wax, 3-6 parts of ozokerite, 0.5-2 parts of dog rose fruit oil and 0.05-0.15 part of hydroxypropyl.
As a further preferred embodiment of the invention, the material comprises the following raw material components in parts by mass: 6 parts of berhard walnut seed oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of laspi wax, 3.9 parts of ceresin wax, 1 part of Rosa canina fruit oil and 0.1 part of propyl hydroxybenzoate.
The berl hard walnut seed oil is a vegetable oil with rich nutrition and high nutrition, can soften blood vessels, reduce the cholesterol content of human bodies, prevent arteriosclerosis and thrombosis, promote the regeneration, eliminate fatigue, invigorate qi and enrich blood, and has stronger tissue repair capability; and is rich in vitamin E, has strong oxidation resistance, and has moisture keeping function.
The plant sterol isostearate has stronger absorption and anti-inflammatory effects on human bodies, and can inhibit the absorption of cholesterol by human bodies, promote the degradation metabolism of the cholesterol, inhibit the biochemical synthesis of the cholesterol and the like; can promote wound healing, prevent lip chapping, enhance capillary circulation, and also can be used as inhibitor for cholelithiasis; has high permeability to lip, and can maintain lip moisture, promote lip metabolism, and inhibit lip inflammation.
The inventor of the invention discovers that the compound of the berl hard walnut seed oil and the phytosterol isostearate has obvious moisturizing and repairing effects on the skin of lips, can accelerate the healing of the chapped wounds, enables the skin damage to be restored to be smooth, does not have sensitization and adverse use reaction, and has good stability.
In the invention, the diisostearyl malate can quickly permeate, absorb and soften skin cutin, so that the skin becomes soft and elastic.
As a preferred embodiment of the present invention, the mass ratio of the berhard walnut seed oil to the phytosterol isostearate is 1: (0.5-5).
As a preferred embodiment of the present invention, the mass ratio of the berhard walnut seed oil to the phytosterol isostearate is 1:1.
Under the mass ratio, the blending effect of the primary hard walnut seed oil and the plant sterol isostearate is better.
A preparation method of a nourishing lip balm comprises the following steps:
(1) Uniformly mixing diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, lacquer fruit wax and ceresin, adding the berl hard walnut seed oil and the phytosterol isostearate, and uniformly mixing to obtain a premix;
(2) And adding the Rosa canina fruit oil and the propyl hydroxybenzoate into the premix, uniformly mixing, discharging, and cooling to room temperature to obtain the nourishing lip balm.
As a preferred embodiment of the present invention, the uniform mixing in the step (1) is performed by stirring.
As a preferred embodiment of the present invention, the temperature of the mixing in step (1) is 80-100 ℃.
As a further preferred embodiment of the present invention, the temperature of the mixing in step (1) is 90 ℃.
As a preferred embodiment of the present invention, the temperature of the mixing in step (2) is 75-85 ℃.
As a further preferred embodiment of the present invention, the temperature of the dissolution in step (2) is 80 ℃.
As a preferred embodiment of the invention, the temperature of the discharge in step (2) is 65-75 ℃.
As a further preferred embodiment of the invention, the temperature of the discharge in step (2) is 70 ℃.
Compared with the prior art, the invention has the following beneficial effects:
(1) In the nourishing lip balm disclosed by the invention, the berl hard walnut seed oil and the phytosterol isostearate are compounded, so that the synergistic effect is achieved, the moistening and repairing effects on the skin of lips are very obvious, the healing of the chapped wounds can be accelerated, the skin loss is restored to be smooth, and the sensitization and adverse use reactions are avoided.
(2) The nourishing lip balm disclosed by the invention has good stability, can be light and thin, has strong moistening property, can keep the moistening property for a long time, and can not generate sensitization and adverse reaction after being used.
Detailed Description
For a better description of the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to specific comparative examples and examples. The raw materials used in the following are commercially available unless otherwise specified.
Example 1
The nourishing lip balm comprises the following raw material components in parts by mass:
6 parts of berhard walnut seed oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of laspi wax, 3.9 parts of ceresin wax, 1 part of Rosa canina fruit oil and 0.1 part of propyl hydroxybenzoate.
The raw material components of this example are shown in Table 1, wherein the mass ratio of the primary hard walnut seed oil to the plant sterol isostearate is 1:1.
The preparation method of the nourishing lip balm comprises the following steps:
(1) The diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, lacquer fruit wax and ceresin are stirred, mixed and dissolved uniformly at 90 ℃, and then the berl hard walnut seed oil and the phytosterol isostearate are added, stirred, mixed and dissolved uniformly to obtain a premix;
(2) And (3) reducing the temperature of the premix to 80 ℃, adding the Rosa canina fruit oil and the propyl hydroxybenzoate into the premix, stirring and mixing uniformly, reducing the temperature to 70 ℃, discharging, and finally reducing the temperature to room temperature to obtain the nourishing lip balm.
Table 1 Components and contents of nourishing lip gloss of example 1
Examples 2 to 7
Examples 2-7 preparation of lip balm the amounts of the raw material components are shown in Table 2, wherein the same kind of raw materials as in example 1 was used, and the specific preparation method was described in the preparation procedure of example 1.
Comparative example 1
The only difference of this comparative example compared to example 1 is that no berl hard walnut seed oil was added.
The method of preparing a nourishing lip balm product of this comparative example is described in example 1.
Comparative example 2
The only difference between this comparative example and example 1 is that no phytosterol isostearate was added.
The method of preparing a nourishing lip balm product of this comparative example is described in example 1.
Comparative example 3
The only difference between this comparative example compared to example 1 is that no burl's hard walnut seed oil and no phytosterol isostearate were added.
The method of preparing a nourishing lip balm product of this comparative example is described in example 1.
Comparative example 4
The only difference between this comparative example and example 1 is that the parts of the added primary hard walnut seed oil and the plant sterol isostearate are all 2 parts.
The method of preparing a nourishing lip balm product of this comparative example is described in example 1.
Comparative example 5
The only difference between this comparative example and example 1 is that the parts of the added primary hard walnut seed oil and the plant sterol isostearate are 13 parts.
The method of preparing a nourishing lip balm product of this comparative example is described in example 1.
TABLE 2 Components and contents of nourishing lip balms of examples 1-7 and comparative examples 1-5
Example nourishing lip gloss appearance and physicochemical index:
Appearance: the nourishing lip balm is white paste.
PH (1:10 aqueous solution): 4.8-6.0.
Heat resistance (45.+ -. 2 ℃ C.). The nourishing lip balm provided by the invention is placed at 45+/-2 ℃ for 2 months and is restored to room temperature without abnormality.
Cold-resistant (-18±2 ℃). The nourishing lip balm provided by the invention is placed at the temperature of-18+/-2 ℃ for 2 months and is recovered to room temperature without abnormality.
Cycle test (45 ℃, normal temperature, -18 ℃): the nourishing lip balm provided by the invention is sequentially placed at 45 ℃, normal temperature and-18 ℃ and circulated for 3 times, and is qualified.
Stability test: the stability test means that the nourishing lip balm is respectively tested at the temperature of minus 5 ℃ and the temperature of 40 ℃ and the temperature of 45 ℃ for three months in an acceleration way, then tested at the temperature of 50 ℃ for one month, and finally the nourishing lip balm is recovered to normal temperature, and the nourishing lip balm can be used normally, and the nourishing lip balm is judged to be qualified according with the regulations, and if the nourishing lip balm is deteriorated, the condition that the nourishing lip balm cannot be used normally is regarded as unqualified.
PH value test method: N/A.
The testing method of the toxic substance content (lead, arsenic, mercury and cadmium) refers to the physicochemical testing method of the 2015 edition of Chinese cosmetic safety technical specification.
TABLE 3 hygienic chemistry index
TABLE 4 stability, pH test and toxic substance content test results of the nourishing lip balms prepared in examples and comparative examples
Microbial challenge experiment: microbial challenge experiments for nourishing lip balm were tested with reference to USP51, 52, 62.
Table 5 microbial challenge results for nourishing lip balm
Nourishing lip gloss product test:
(1) Moisturizing effect: the method comprises the steps of testing by a moisture tester, measuring the moisture and oil content data of lips of a human body (voluntary tester) when no lipstick is coated by the moisture tester, coating a lipstick product, and respectively testing the moisture and oil content of lips after the lipstick product is coated for one minute; a good lipstick with moisturizing effect has moisture content of above 15%, and is considered as moisturizing, otherwise is considered as dry or drier; the fluctuation of the oil content is controlled within 10%, so that the oil content is not too greasy and is regarded as light and thin, and conversely, is regarded as heavy.
(2) Moisture retention time test: the method comprises the steps of testing by a moisture tester, measuring the moisture and oil content data of lips of a human body (voluntary tester) when no lipstick is coated by the moisture tester, coating a lipstick product, and respectively testing the moisture and oil content of lips after the lipstick product is coated for one minute; then after waiting for 2 hours, respectively testing the moisture and oil content of lips;
Test standard: after 2 hours, if the moisture content of the lips is lower than the normal moisture content (20%), the lips are disqualified; the moisture retention time of the product is finally determined by measuring for 4 hours, 6 hours and 8 hours by the same method.
(3) Testing of the tackiness: coating lipstick products on the palm, and after waiting for 30 seconds, lightly placing the palm on the crushed paper scraps, wherein the palm is not stuck or hardly stuck with the paper scraps, namely, the palm is good in lipstick, namely, is not sticky; if the palm is stuck with a small amount of broken paper scraps, the palm is sticky, namely sticky; if the palm sticks more crushed paper scraps, the palm is sticky, namely sticky and greasy. A lipstick, if very sticky, can be uncomfortable to apply to the lips.
(4) Irritation: the evaluation is performed according to whether or not the individual of the test person has an allergy phenomenon.
TABLE 6 lipstick Performance test results for examples and comparative examples
The commercial lipstick (oiliness) 1 is a DHC lipstick, has higher lanolin content, is sticky in material body and is easy to cause allergic cheilitis; the commercially available lipstick 2 is another DIOR lipstick, and has a heavy sticky feeling when used.
The nourishing lip balm disclosed by the invention is a white pasty product, can be light and thin, has strong moistening property, can keep the moistening property for a long time, and can not generate sensitization and adverse reaction after being used.
The berhard walnut seed oil has low viscosity, the berhard walnut seed oil and the phytosterol isostearate are compounded, the synergistic effect is realized, the moistening and repairing effects on the skin of lips are very obvious, the healing of the chapped wounds can be quickened, the skin loss is restored to be smooth, and the sensitization and adverse use reactions do not exist.
From example 1 and comparative example 4, it is understood that the moisturizing degree and the moisturizing durability are decreased when the addition amount of the burl nut seed oil and the phytosterol isostearate is small; the addition of the Bull hard walnut seed oil and the plant sterol isostearate is excessive, the oil taste is relatively large, and the vegetable oil is easy to oxidize when being added, so that the product has sticky feel when being smeared.
Finally, it should be noted that the above embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.
Claims (6)
1. The nourishing lip balm is characterized by comprising the following raw material components in parts by mass: 6 parts of Berl hard walnut seed oil, 6 parts of phytosterol isostearate, 10.5-20 parts of diisostearyl malate, 12.5-20 parts of jojoba seed oil, 12.5-16 parts of sunflower seed oil, 10.5-15 parts of hydrogenated vegetable oil, 8.5-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 5.5-8 parts of PEG-12 carnauba wax, 4.5-10 parts of candelilla wax, 4.5-8 parts of wild lacquer fruit wax, 3-6 parts of ceresin wax, 0.5-2 parts of dog rose fruit oil and 0.05-0.15 part of hydroxypropyl.
2. The nourishing lip balm according to claim 1, which is composed of the following raw material components in parts by mass: 6 parts of berhard walnut seed oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of laspi wax, 3.9 parts of ceresin wax, 1 part of Rosa canina oil and 0.1 part of propyl hydroxybenzoate.
3. The method for preparing the nourishing lip balm according to claim 1 or 2, characterized by comprising the following steps:
(1) Uniformly mixing diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, lacquer fruit wax and ceresin, adding the berl hard walnut seed oil and the phytosterol isostearate, and uniformly mixing to obtain a premix;
(2) And adding the Rosa canina fruit oil and the propyl hydroxybenzoate into the premix, uniformly mixing, discharging, and cooling to room temperature to obtain the nourishing lip balm.
4. The method for preparing a lip balm according to claim 3, wherein the temperature of the mixing in the step (1) is 80-100 ℃.
5. The method for preparing a lip balm according to claim 3, wherein the temperature of the mixing in the step (2) is 75-85 ℃.
6. The method for preparing a lip balm according to claim 3, wherein the temperature of the discharged material in the step (2) is 65-75 ℃.
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| CN114028268A (en) * | 2021-10-21 | 2022-02-11 | 曼秀雷敦(中国)药业有限公司 | Natural plant component lip balm and preparation method thereof |
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| NZ575991A (en) * | 2006-10-11 | 2012-02-24 | Wyeth Corp | Stick lip balm comprising carnauba wax, candelilla wax, jojoba esters and botanical butters |
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