CN107028827A - A kind of natural anti-oxidation lipstick - Google Patents

A kind of natural anti-oxidation lipstick Download PDF

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Publication number
CN107028827A
CN107028827A CN201710252738.0A CN201710252738A CN107028827A CN 107028827 A CN107028827 A CN 107028827A CN 201710252738 A CN201710252738 A CN 201710252738A CN 107028827 A CN107028827 A CN 107028827A
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CN
China
Prior art keywords
parts
lipstick
oxidation
natural anti
natural
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710252738.0A
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Chinese (zh)
Inventor
不公告发明人
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Guangzhou Poly Green Chemical Technology Research Institute Co Ltd
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Guangzhou Poly Green Chemical Technology Research Institute Co Ltd
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Priority to CN201710252738.0A priority Critical patent/CN107028827A/en
Publication of CN107028827A publication Critical patent/CN107028827A/en
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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a kind of natural anti-oxidation lipstick, natural anti-oxidation lipstick of the present invention includes 0.02~4 part of plant composition, and plant composition is that citrus bark extract and green-tea extract are (0.01~2) by weight:(0.01~2) mixture of mixing, in addition to 8 15 parts of two isooctadecanol malates, 10 20 parts of beeswax, 3 10 parts of microwax, 0.01 0.1 parts of natural perfume material, 0.05 0.8 parts of preservative etc..Natural anti-oxidation lipstick of the present invention, which has, not to stimulate gently, and use feeling is good, and smear is good, and good permeability, film forming is good, moist and can protect lip skin, has no side effect, and foreign sense makes that lip is more soft, full, more flexible effect.

Description

A kind of natural anti-oxidation lipstick
Technical field
The present invention relates to daily cosmetics field, and in particular to a kind of natural anti-oxidation lipstick.
Background technology
Lipstick is most original, usually most common lipstick, solid, and quality is more dry and hard than lip gloss and lip honey.Lipstick is Into the conventional cosmetics of China's modern female.One layer of just right lipstick is applied on lip can make one to seem especially coquettish. Color saturation is high, and color mileage is strong, and due to being that solid is typically not easy because cheilogramma is too deep and excessive, commonly uses it and come Modify lip, lip color.
The endurance that lip Antagonistic Environment is invaded and harassed be in whole body skin it is most weak, be easiest to " aging ", its knot of tissue Structure layer is very thin, and only the 1/3 of body skin is thick.Because itself does not have pore, without sebaceous glands, so to dry and low temperature etc. Environment is especially sensitive, and the especially autumn and winter are dried and cold weather, often make Mucosa of lip damage serious, easily induce cheilitis.It is another Aspect, with the continuous improvement of people's quality of life, requirement of the people to lipstick is not only that can moisten lip, also to be used It is safer.
Therefore research and development one kind is badly in need of in contemporary society does not stimulate gently, and with antioxidant effect, use feeling is good, and smear is good, Good permeability, film forming is good, moistens and can protect lip skin, has no side effect, and foreign sense makes lip more soft, full, more Flexible lipstick.
The content of the invention
Present invention aims at a kind of natural anti-oxidation lipstick is provided, natural anti-oxidation lipstick of the present invention is not stimulated gently, Use feeling is good, and long-term use can make lip more soft, full, more flexible;Smear is good, and good permeability, film forming is good, moistens And lip skin can be protected, and have no side effect, foreign sense.
The present invention is realized by following scheme:
The lipstick includes 0.02~4 part of plant composition;Wherein, plant composition is that citrus bark extract and green tea are carried The mixing of thing is taken, the weight ratio of the citrus bark extract and green-tea extract is (0.01~2):(0.01~2).
The preparation method of the citrus bark extract includes:Orange peel is dried, 60~80 mesh sieves were crushed, by solid-liquid ratio 1:(10~30) absolute ethyl alcohol is added, 1~2h is extracted at 30~50 DEG C, is filtered while hot, concentrating filter liquor.
The preparation method of the green-tea extract includes:Green tea is dried, 40~60 mesh sieves were crushed, by solid-liquid ratio 1: (10~30) 70~95% ethanol are added, 60~80 DEG C of water-bath 2~3h of refluxing extraction are filtered, the rotated evaporimeter of filtrate while hot Concentration.
The lipstick also includes 2~10 parts of apricot kernel oil, 4~12 parts of avocado oil.
The lipstick also includes 8-15 parts of two isooctadecanol malate, 2-8 parts of caprylic/capric triglyceride, tridecane 2-8 parts of alcohol trimellitate, -25-10 parts of many acyl group adipate esters of double-two glycerine, 5-10 parts of polyisobutene, 10-20 parts of beeswax, 3-10 parts of microwax, 10-20 parts of stearine, 0.2-1 parts of tocopherol, 0.1-0.5 parts of allantoin, natural perfume material 0.01- 0.1 part, 0.05-0.8 parts of preservative.
The natural perfume material is at least one of Lavender, Rosa Damascana, orange oil, chamomile essential oil.
The preservative is at least one of potassium sorbate, sodium benzoate, methyl hydroxybenzoate, Nipasol.
The preparation method following steps of the natural anti-oxidation lipstick:Two isooctadecanol malates, caprylic/capric is sweet Oily three esters, tridecanol trimellitate, many acyl group adipate esters -2 of double-two glycerine, polyisobutene, beeswax, microwax, glycerine In stearate, apricot kernel oil and avocado oil input emulsification pot, heating stirring is simultaneously warming up to 80~85 DEG C, stirs completely molten to material Solution;Then tocopherol, natural perfume material, allantoin and preservative are added, it is 75~80 DEG C control temperature, stirred to being completely dissolved, Obtain mixed material;The temperature of material to be mixed is reduced to 50-60 DEG C of addition plant composition and is well mixed, and form takes off Mould.
Following introduction is done to the fractions of natural anti-oxidation lipstick of the present invention:
Citrus bark extract:Carotenoid has stronger antioxidation in citrus bark extract, to large biological molecule Also there is certain insured to act on, the normal structure of surrounding can be protected from being damaged caused by the inflammatory reaction of immune system Wound, strengthens the activity of NK, with antioxidation, prevents the oxidative damage of body;Exempting from for body can be activated Epidemic disease cell, strengthens the immunologic function of body;The signalling channels such as intracellular apoptosis regulation or propagation can be adjusted, control is adjusted and dies The gene low amounts expression of family or the overexpression for suppressing cancer gene.
Green-tea extract:Tea Polyphenols can close the metal ion of catalytic oxidation and cause oxidation in green-tea extract The material of reaction, so as to extend the induction period of oxidation, slows down reaction speed.
Portfolio ratio between its inoxidizability and its each component has anti-oxidant in the presence of cooperateing between substantial connection, each component Effect, Tea Polyphenols and carotenoid have the ability compared with strong anti-oxidation.Many studies have shown that, a variety of antioxidant connection effects, its Antioxidant capacity is often greater than the effect using the single antioxidant with dosage, so between antioxidant there is collaboration to make With its mechanism mainly includes complexation of metal ions, reparative regeneration, absorbs oxygen, the activity, the coupled oxidation that change enzyme etc..
Apricot kernel oil:Apricot kernel oil is excellent edible oil, and abundant unrighted acid, unsaturated fat are contained in apricot kernel oil Acid is a kind of aliphatic acid easily assimilated by human body, is that growth in humans develops indispensable element, in human body not Will not only produce Fat Accumulation, and can W reduction low-density lipoproteins (LDL) and serum cholesterol level, therefore, dessert almond Oil has anti-oxidant anti-aging physiological function.In addition, it has excellent skin-friendly, the cosmetics containing apricot kernel oil can quickly by Skin is absorbed.
Compared with prior art, the method have the advantages that:
(1) natural anti-oxidation lipstick of the present invention is not stimulated gently, and use feeling is good, and long-term use can make lip more soft, full It is full, more flexible.
(2) citrus bark extract is added in product as pigment in natural anti-oxidation mouthful in the present invention, and orange peel is extracted Thing is edible type additive, harmless, the Tea Polyphenols in carotenoid and green-tea extract in citrus bark extract There are the ability compared with strong anti-oxidation, carotenoid and Tea Polyphenols synergy, its antioxidant capacity is greater than using the class with dosage The effect of carrotene or Tea Polyphenols with dosage, citrus bark extract and green-tea extract have synergy, with more preferable Antioxidation.
(3) smear of this product is good, and good permeability, film forming is good, moistens and can protect lip skin, has no side effect, nothing Foreign body sensation.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.The following component title occurred in text is INCI (International Nomenclature Cosmetic Ingredient), i.e. international cosmetic raw material name institute are to regulation Title, including:Caprylic/capric triglyceride.The natural anti-oxidation lipstick formula of the present invention of embodiment 1~5 is shown in Table one
Table one
The preparation method of citrus bark extract includes described in embodiment 1~5:Orange peel is dried, 80 mesh sieves were crushed, By solid-liquid ratio 1:30 add absolute ethyl alcohol, and 2h is extracted at 50 DEG C, is filtered while hot, concentrating filter liquor.
The preparation method of green-tea extract includes described in embodiment 1~5:Green tea is dried, 60 mesh sieves were crushed, by material Liquor ratio 1:10 add 95% ethanol, and 60 DEG C of water-bath refluxing extraction 3h are filtered while hot, the rotated evaporimeter concentration of filtrate.
The preparation method of natural anti-oxidation lipstick comprises the following steps described in embodiment 1~5:By two isooctadecanol apples Acid esters, caprylic/capric triglyceride, tridecanol trimellitate, many acyl group adipate esters -2 of double-two glycerine, polyisobutene, In beeswax, microwax, stearine, apricot kernel oil and avocado oil input emulsification pot, heating stirring is simultaneously warming up to 85 DEG C, stirring It is completely dissolved to material;Then tocopherol, natural perfume material, allantoin and preservative are added, it is 80 DEG C to control temperature, is stirred to complete Fully dissolved, obtains mixed material;The temperature of material to be mixed is reduced to 60 DEG C of addition citrus bark extracts and green-tea extract is mixed Close uniform, form, the demoulding.
Comparative example 1
Difference with embodiment 1 is not add citrus bark extract, and other preparation conditions and method are same as Example 1.
Comparative example 2
Difference with embodiment 1 is not add green-tea extract, and other preparation conditions and method are same as Example 1.
Comparative example 3
Difference with embodiment 1 is to add 0.01 part of citrus bark extract and green-tea extract, other preparation conditions and side Method is same as Example 1.
Comparative example 4
Difference with embodiment 1 is to add 4.1 parts of citrus bark extracts and green-tea extract, other preparation conditions and method It is same as Example 1.
Comparative example 5
Difference with embodiment 1 is not add plant composition, and other preparation conditions and method are same as Example 1.
Antioxidative Activity Determination
Compound concentration is 1 × 10-4mol/L DPPH ethanol solutions.By embodiment 1~5 and comparative example 1~5 and Commercially available product (claiming the lipstick with good antioxidant effect on the market) be configured to 80% ethanol concentration be respectively 0.01, 0.04th, 0.08,0.10,0.12,0.16,0.20,0.24,0.26 testing sample solution.Take respectively 5mL sample solutions and DPPH solution, and be well mixed, avoid light place 30min, returned to zero with 80% ethanol, absorbance A i is determined at 517BITI;Together Quadrat method, takes 5mL80% alcohol solvents to be mutually mixed uniformly with sample solution, absorbance is determined after avoid light place 30min respectively Aj;5mL80% alcohol solvents add 5mLDPPH solution to mix, avoid light place 30min, determine absorbance A c.Finally according to following Formula calculates free radical scavenging activity:
IP%=[1 one (Ai-Aj)/Ac] × 100
Ai is the absorption values after sample is acted on DPPH in formula;
Aj is contribution of the sample itself to absorbance;Ac is DPPH itself absorption.
Two are shown in Table to the ability measurement result that embodiment 1~5 and comparative example 1~5 and commercially available product remove DPPH:
Table two
As seen from the above table, the removing of embodiment 1~5 DPPH ability is far above comparative example 1~5 and commercially available product, with very Strong oxidation resistance;Plant society scientific formulation of the present invention can be obtained by embodiment 1 and the contrast of embodiment 3,4, interval is taken most It is excellent;Contrasted by embodiment 1 and comparative example 5 can obtain it is of the invention in main functional component be plant composition.
Human body patch is tested
Organize 30 volunteers according to《Cosmetics health specification》The human body skin patch Experimental Standardization of (2007 editions) records, The natural anti-oxidation lipstick obtained by the embodiment of the present invention 1 is tested, as a result as shown in Table 3.
Table three
Performance of keeping humidity is assessed
In the present invention, test evaluation has been carried out to the performance of keeping humidity of embodiment 1 and the oxidation-resistant lipstick of comparative example 1,5, and Using claiming that the lip gloss with good moistening effect makees commercially available group of contrast on the market.
Subjects are 60 adult females for possessing dry lip, are randomly divided into 4 groups, every group of 15 people, and experiment position is Lip.Outer coating method is to apply 15 days outside altogether once a day.Behind 24 hours of the last day of outer painting, position is applied outside in the absence of outer Apply under conditions of sample, measure angle using SKICON200&corneometer thermostatic chamber (24 DEG C of room temperature, humidity 50%) is inner (SKICON200 is typically only capable to measure the moisture below epiderm skin near 20 μm to the moisture of matter layer; Corneometer can measure the moisture near 100 μm, two kinds of instruments be used simultaneously, it becomes possible to measure from skin Moisture of the epidermis to inside).Meanwhile, using the amino acid of transparent rubberized fabric skin without stratum corneum (under the 10th adhesive plaster is peeled off Cuticula, finally determines day), the amino acid content of cuticula is determined with fluorometric method.Logging such as following table four:
Table four
The present invention is described by way of example above, but the invention is not restricted to above-mentioned specific embodiment, it is all to be based on Any change or modification that the present invention is done belong to the scope of protection of present invention.

Claims (9)

1. a kind of natural anti-oxidation lipstick, it is characterised in that the lipstick includes 0.02~4 part of plant composition;Wherein, plant Composition is the mixing of citrus bark extract and green-tea extract.
2. a kind of natural anti-oxidation lipstick according to claim 1, it is characterised in that the citrus bark extract and green tea The weight ratio of extract is (0.01~2):(0.01~2).
3. a kind of natural anti-oxidation lipstick according to claim 1 or 2, it is characterised in that the citrus bark extract Preparation method includes:Orange peel is dried, 60~80 mesh sieves were crushed, by solid-liquid ratio 1:(10~30) absolute ethyl alcohol is added, 1~2h is extracted at 30~50 DEG C, is filtered while hot, concentrating filter liquor.
4. a kind of natural anti-oxidation lipstick according to claim 1 or 2, it is characterised in that the system of the green-tea extract Preparation Method includes:Green tea is dried, 40~60 mesh sieves were crushed, by solid-liquid ratio 1:(10~30) 70~95% ethanol, 60 are added ~80 DEG C of water-bath 2~3h of refluxing extraction, are filtered while hot, the rotated evaporimeter concentration of filtrate.
5. a kind of natural anti-oxidation lipstick according to claim 1, it is characterised in that the lipstick also includes apricot kernel oil 2 ~10 parts, 4~12 parts of avocado oil.
6. a kind of natural anti-oxidation lipstick according to claim 1, it is characterised in that the lipstick also includes two different tristearin 8-15 parts of alcohol malate, 2-8 parts of caprylic/capric triglyceride, 2-8 parts of tridecanol trimellitate, double many acyls of-two glycerine - 25-10 parts of base adipate ester, 5-10 parts of polyisobutene, 10-20 parts of beeswax, 3-10 parts of microwax, stearine 10-20 Part, 0.2-1 parts of tocopherol, 0.1-0.5 parts of allantoin, 0.01-0.1 parts of natural perfume material, 0.05-0.8 parts of preservative.
7. a kind of natural anti-oxidation lipstick according to claim 6, it is characterised in that the natural perfume material is lavender essence At least one of oil, Rosa Damascana, orange oil, chamomile essential oil.
8. a kind of natural anti-oxidation lipstick according to claim 6, it is characterised in that the preservative be potassium sorbate, At least one of sodium benzoate, methyl hydroxybenzoate, Nipasol.
9. a kind of preparation method of the natural anti-oxidation lipstick as described in any one of claim 1~8, it is characterised in that including with Lower step:Two isooctadecanol malates, caprylic/capric triglyceride, tridecanol trimellitate, double-two glycerine is more In acyl group adipate ester -2, polyisobutene, beeswax, microwax, stearine, apricot kernel oil and avocado oil input emulsification pot, Heating stirring is simultaneously warming up to 80~85 DEG C, and stirring to material is completely dissolved;Then add tocopherol, natural perfume material, allantoin and Preservative, it is 75~80 DEG C to control temperature, stirs to being completely dissolved, obtains mixed material;The temperature of material to be mixed is reduced to 50-60 DEG C adds plant composition and is well mixed, form, the demoulding.
CN201710252738.0A 2017-04-17 2017-04-17 A kind of natural anti-oxidation lipstick Withdrawn CN107028827A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375037A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 A kind of color-changing lipstick and preparation method thereof
CN109674706A (en) * 2019-02-18 2019-04-26 广州卡迪莲化妆品有限公司 A kind of green-tea extract and its preparation method and application, lipstick and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103222930A (en) * 2012-01-31 2013-07-31 株式会社爱茉莉太平洋 Skin external composition containing tangeretin and egcg
US20140179747A1 (en) * 2011-07-25 2014-06-26 Us Cosmeceutechs, Llc Botanical antioxidant compositions and methods of preparation and use thereof
CN105326671A (en) * 2015-12-02 2016-02-17 共聚生化科技(昆山)有限公司 Natural nourishing lip beautifying and protecting oil

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20140179747A1 (en) * 2011-07-25 2014-06-26 Us Cosmeceutechs, Llc Botanical antioxidant compositions and methods of preparation and use thereof
CN103222930A (en) * 2012-01-31 2013-07-31 株式会社爱茉莉太平洋 Skin external composition containing tangeretin and egcg
CN105326671A (en) * 2015-12-02 2016-02-17 共聚生化科技(昆山)有限公司 Natural nourishing lip beautifying and protecting oil

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375037A (en) * 2017-08-25 2017-11-24 漳浦彩露华化妆品有限公司 A kind of color-changing lipstick and preparation method thereof
CN109674706A (en) * 2019-02-18 2019-04-26 广州卡迪莲化妆品有限公司 A kind of green-tea extract and its preparation method and application, lipstick and preparation method thereof
CN109674706B (en) * 2019-02-18 2021-09-14 广州卡迪莲化妆品科技有限公司 Green tea extract, preparation method and application thereof, lipstick and preparation method thereof

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