CN115778858A - Nourishing lip balm and preparation method thereof - Google Patents
Nourishing lip balm and preparation method thereof Download PDFInfo
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- CN115778858A CN115778858A CN202211653171.5A CN202211653171A CN115778858A CN 115778858 A CN115778858 A CN 115778858A CN 202211653171 A CN202211653171 A CN 202211653171A CN 115778858 A CN115778858 A CN 115778858A
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Abstract
The invention belongs to the field of cosmetics, and particularly discloses a nourishing lip balm and a preparation method thereof. The nourishing lip balm comprises the following raw material components in parts by mass: 3-12 parts of Boer hard walnut seed oil, 3-12 parts of phytosterol isostearate, 0-25 parts of diisostearyl malate, 0-20 parts of jojoba seed oil, 0-16 parts of sunflower seed oil, 0-15 parts of hydrogenated vegetable oil, 0-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 0-8 parts of PEG-12 carnauba wax, 0-10 parts of candelilla wax, 0-8 parts of wild lacquer fruit wax, 0-6 parts of ozokerite, 0-2 parts of Rosa canina fruit oil and 0-0.2 part of propylhydroxybenzoate. The nourishing lip balm has good stability, can be light and thin when in use, has strong nourishing performance, can keep the nourishing performance for a long time, and does not have sensitization and adverse reaction after being used.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a nourishing lip balm and a preparation method thereof.
Background
Lipstick is a lip cosmetic, and has the main functions of giving color tone to lips, emphasizing or changing the contour of lips, and showing more vitality and vitality. Compared with the skin, the horny layer of the lips is very thin, the moisture is easy to evaporate, particularly in dry days in autumn and winter, the moisture of the lips is easy to evaporate, and the lips are often dry, rough, sensitive, dry and cracked and the like. In order to improve or even avoid the phenomena of dry, rough, sensitive, dry and cracked lips, people often use lip balm to coat the lips so as to achieve the effects of moistening and protecting the lips. With the development of lip cosmetics, the formula and the process thereof are diversified, and some lip balms have the functions of preventing chapping, fading lip wrinkles, providing cool feeling, enlarging lips and the like.
However, the existing lip products still have the defects of poor lip gloss moistening performance, poor moistening durability, sticky feeling and even possible sensitization and adverse reaction.
Disclosure of Invention
Aiming at the problems of poor moistening performance, poor moistening durability, sticky feeling and the like of the nourishing lip balm related to the prior art, the invention provides the nourishing lip balm and the preparation method thereof.
In order to achieve the purpose, the method specifically comprises the following technical scheme:
the nourishing lip balm comprises the following raw material components in parts by mass:
3-12 parts of Boer hard walnut seed oil, 3-12 parts of phytosterol isostearate, 0-25 parts of diisostearyl malate, 0-20 parts of jojoba seed oil, 0-16 parts of sunflower seed oil, 0-15 parts of hydrogenated vegetable oil, 0-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 0-8 parts of PEG-12 carnauba wax, 0-10 parts of candelilla wax, 0-8 parts of wild lacquer fruit wax, 0-6 parts of ozokerite, 0-2 parts of Rosa canina fruit oil and 0-0.2 part of propylhydroxybenzoate.
The preferable embodiment of the invention comprises the following raw material components in parts by mass: 6-12 parts of Boer hard walnut seed oil, 6-12 parts of phytosterol isostearate, 10.5-20 parts of diisostearyl malate, 12.5-20 parts of jojoba seed oil, 12.5-16 parts of sunflower seed oil, 10.5-15 parts of hydrogenated vegetable oil, 8.5-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 5.5-8 parts of PEG-12 carnauba wax, 4.5-10 parts of candelilla wax, 4.5-8 parts of wild lacquer fruit wax, 3-6 parts of ozokerite, 0.5-2 parts of Rosa canina fruit oil and 0.05-0.15 part of propylhydroxybenzoate.
The further preferable embodiment of the invention comprises the following raw material components in parts by mass: 6 parts of Boerhu walnut seed oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of jatropha wax, 3.9 parts of ozokerite, 1 part of Rosa canina fruit oil and 0.1 part of propylhydroxybenzoate.
The Boer hard walnut seed oil is vegetable oil with rich and high nutrition, can soften blood vessels, reduce the content of cholesterol in a human body, has the effects of preventing arteriosclerosis and thrombosis, can promote the regeneration, eliminate fatigue, tonify qi and enrich blood, and has strong tissue repair capacity; and is rich in vitamin E, and has strong oxidation resistance and moisturizing effect.
The phytosterol isostearate has strong absorption and anti-inflammatory effects on a human body, and can inhibit the absorption of the human body on cholesterol, promote the degradation and metabolism of the cholesterol, inhibit the biochemical synthesis of the cholesterol and the like; can promote wound healing, prevent lip chapping, enhance capillary circulation, and can be used as inhibitor for gallstone formation; has high permeability to lip, and can retain lip moisture, promote lip metabolism, and inhibit lip inflammation.
The inventor finds that the compound of the Boerhu walnut seed oil and the phytosterol isostearate has very obvious moistening and repairing effects on lip and mouth skin, can accelerate the healing of a chapped wound, enables the skin to be smooth, does not have sensitization and adverse use reaction, and has good stability.
In the invention, the diisostearyl malate can quickly permeate and absorb and soften skin cutin, so that the skin becomes soft and elastic.
As a preferred embodiment of the present invention, the mass ratio of the branchy walnut seed oil to the phytosterol isostearate is 1: (0.5-5).
As a preferred embodiment of the present invention, the weight ratio of the juglans boidinii seed oil to the phytosterol isostearate is 1:1.
in the mass ratio, the matching effect of the Boerhu walnut seed oil and the phytosterol isostearate is better.
A preparation method of the nourishing lip balm comprises the following steps:
(1) Uniformly mixing diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, elaeagnus mollis fruit wax and ozokerite, adding Boerhu walnut seed oil and phytosterol isostearate, and uniformly mixing to obtain a premix;
(2) Adding Rosa canina fruit oil and propyl hydroxybenzoate into the premix, mixing, discharging, and cooling to room temperature to obtain the nourishing lip balm.
In a preferred embodiment of the present invention, the mixing in step (1) is performed by stirring.
As a preferred embodiment of the present invention, the temperature of the mixing in the step (1) is 80 to 100 ℃.
As a further preferred embodiment of the present invention, the temperature of the mixing in step (1) is 90 ℃.
As a preferred embodiment of the present invention, the temperature of the mixing in the step (2) is 75 to 85 ℃.
As a further preferred embodiment of the present invention, the temperature of the dissolution in the step (2) is 80 ℃.
As a preferred embodiment of the present invention, the temperature of the discharge in step (2) is 65 to 75 ℃.
As a further preferred embodiment of the present invention, the temperature of the discharge in step (2) is 70 ℃.
Compared with the prior art, the invention has the following beneficial effects:
(1) In the nourishing and moistening lipstick, the Kelerya birica seed oil and the phytosterol isostearate are compounded, so that the nourishing and moistening lipstick has a synergistic effect, has very obvious moistening and repairing effects on lip and lip skin, can accelerate the healing of a chapped wound and restore the skin damage to be smooth, and does not have sensitization and adverse use reaction.
(2) The nourishing lip balm has good stability, light and thin feeling, strong moisturizing property, lasting moisturizing property and no sensitization and adverse reaction after use.
Detailed Description
To better illustrate the objects, technical solutions and advantages of the present invention, the present invention will be further illustrated by specific comparative examples and examples. The following starting materials were purchased from the market unless otherwise specified.
Example 1
The nourishing lip balm is prepared from the following raw materials in parts by mass:
6 parts of Boerhugu nut oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of wild lacquer fruit wax, 3.9 parts of ozokerite, 1 part of Rosa canina fruit oil and 0.1 part of propylhydroxybenzoate.
The raw material components of this example are shown in table 1, wherein the mass ratio of the branchy walnut seed oil to the phytosterol isostearate is 1.
The preparation method of the nourishing lip balm comprises the following steps:
(1) Stirring, mixing and dissolving diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, elaeagnus mollis wax and ozokerite at 90 ℃ uniformly, adding Boerhu walnut seed oil and phytosterol isostearate, stirring, mixing and dissolving uniformly to obtain a premix;
(2) And cooling the temperature of the premix to 80 ℃, adding the rosa canina fruit oil and the propylparaben into the premix, uniformly stirring and mixing, cooling to 70 ℃, discharging, and finally cooling to room temperature to obtain the nourishing lip balm.
Components and amounts of the nourishing lip balm of example 1
Examples 2 to 7
Examples 2-7 preparation of nourishing lip gloss the contents of the raw material components are shown in table 2, wherein the kinds of the raw materials used are the same as those in example 1, and the specific preparation method is as shown in the preparation procedure of example 1.
Comparative example 1
The comparative example differs from example 1 only in that no burl nut oil was added.
This comparative example is a method of preparing a nourishing lip gloss product according to the preparation method of example 1.
Comparative example 2
The comparative example differs from example 1 only in that no phytosterol isostearate was added.
This comparative example method of preparing a nourishing lip balm product is described in the preparation method of example 1.
Comparative example 3
The comparative example differs from example 1 only in that no burkholderia seed oil and no phytosterol isostearate are added.
This comparative example is a method of preparing a nourishing lip gloss product according to the preparation method of example 1.
Comparative example 4
The comparative example differs from example 1 only in that the parts of the seed oil and the phytosterol isostearate added are both 2 parts.
This comparative example method of preparing a nourishing lip balm product is described in the preparation method of example 1.
Comparative example 5
The comparative example differs from example 1 only in that the parts of the seed oil and the phytosterol isostearate added are both 13 parts.
This comparative example is a method of preparing a nourishing lip gloss product according to the preparation method of example 1.
TABLE 2 Components and contents of nourishing lip balm in examples 1 to 7 and comparative examples 1 to 5
The appearance and physical and chemical indexes of the nourishing lip balm are as follows:
appearance: the nourishing lip balm is a white cream body.
pH (1: 4.8-6.0.
Heat resistance (45 +/-2 ℃): the nourishing lip balm is placed at 45 +/-2 ℃ for 2 months, and is recovered to room temperature without abnormality.
Cold resistance (-18 +/-2 ℃): the nourishing lip balm is placed at the temperature of minus 18 +/-2 ℃ for 2 months, and returns to the room temperature without abnormality.
Cycle test (45 ℃, ambient temperature, -18 ℃): the nourishing lip balm is sequentially placed at 45 ℃, normal temperature and-18 ℃ for 3 times of circulation and is qualified.
And (3) stability testing: the stability test refers to that the nourishing lip balm is subjected to accelerated test at the temperature of minus 5 ℃, 40 ℃ and 45 ℃ for three months respectively, then is subjected to accelerated test at the temperature of 50 ℃ for one month, and finally is recovered to normal temperature, so that the nourishing lip balm can be normally used, and is qualified if the nourishing lip balm is judged to be in accordance with the specification, and if the nourishing lip balm is deteriorated, the lip balm cannot be normally used, the lip balm is not qualified.
Test of pH value experiment method: N/A.
The test method of toxic substance content (lead, arsenic, mercury, cadmium) refers to the physicochemical test method of the national cosmetic safety technical specification 2015 edition.
TABLE 3 index of sanitary chemistry
Table 4 stability, pH test and toxic substance content test results of nourishing lip gloss prepared in examples and comparative examples
Microbial challenge experiments: microbial challenge experiments with nourishing lip balm were tested with reference to USP51, 52, 62.
TABLE 5 microbial challenge results of nourishing lip balm
Testing of nourishing lip balm products:
(1) The moisturizing effect is as follows: testing by a moisture tester, firstly testing the moisture and oil content data of the lips of a human body (a voluntary tester) when no lipstick is coated by the moisture tester, then coating a lipstick product, and respectively testing the moisture and oil content of the lips after the lipstick product is coated for one minute; the lipstick with enough moisture retention is good in use, the moisture content reaches more than 15%, and is regarded as moist, otherwise, the lipstick is regarded as dry or relatively dry; the oil content is controlled within 10% to avoid excessive greasiness, which is regarded as light and heavy, otherwise, the feeling is regarded as heavy.
(2) Testing the moisture retention time: testing by a moisture tester, firstly testing the moisture and oil content data of the lips of a human body (a voluntary tester) when no lipstick is coated by the moisture tester, then coating a lipstick product, and respectively testing the moisture and oil content of the lips after the lipstick product is coated for one minute; then after waiting for 2 hours, respectively testing the water content and the oil content of the lips;
and (4) testing standard: after 2 hours, if the water content of the lips is lower than the normal water content (20 percent), the lips are unqualified; the moisture retention time of the product is finally determined by measuring 4 hours, 6 hours and 8 hours in the same way.
(3) And (3) testing the viscosity: the lipstick product is coated on the palm, and after the palm waits for 30 seconds, the palm is lightly placed on the shredded paper scraps and is not stuck or is hardly stuck with the shredded paper scraps, so that the lipstick is better, namely is not sticky; if the palm is stuck with a small amount of shredded paper, the palm is sticky, namely sticky; if the palm of the hand is stuck with more shredded paper, the palm of the hand is very sticky, namely sticky. If the lipstick is sticky, the lipstick can feel uncomfortable when being coated on the lips.
(4) Irritation: the assessment is made according to whether the test person individual has an allergic phenomenon.
TABLE 6 lipstick Performance test results of examples and comparative examples
The lipstick (oily) 1 sold in the market is a DHC lipstick, which contains lanolin in a high proportion, is relatively sticky in material and is easy to cause allergic cheilitis; lipstick 2 is another DIOR lipstick, which is thick and sticky when used.
The nourishing lip balm is a white paste product, can be light and thin, has strong moistening performance, can keep the moistening performance for a long time, and does not have sensitization and adverse reaction after being used.
The Boerhugu walnut seed oil has low viscosity, has a synergistic effect by compounding the Boerhugu walnut seed oil and the phytosterol isostearate, has very obvious effects of moistening and repairing lip skin, can accelerate the healing of a chapped wound, enables the skin to be restored to be smooth, and does not have sensitization and adverse use reaction.
As can be seen from example 1 and comparative example 4, the moisture retention and the moisture retention durability were reduced when the amounts of the burkholderia seed oil and the phytosterol isostearate were small; the taste of the oil is larger due to excessive addition of the Boerhugu nut oil and the phytosterol isostearate, the vegetable oil is easy to oxidize due to excessive addition, and the product has sticky feeling when being smeared.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (9)
1. The nourishing lip balm is characterized by comprising the following raw material components in parts by mass: 3-12 parts of Boer hard walnut seed oil, 3-12 parts of phytosterol isostearate, 0-25 parts of diisostearyl malate, 0-20 parts of jojoba seed oil, 0-16 parts of sunflower seed oil, 0-15 parts of hydrogenated vegetable oil, 0-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol esters, 0-8 parts of PEG-12 carnauba wax, 0-10 parts of candelilla wax, 0-8 parts of wild lacquer fruit wax, 0-6 parts of ozokerite, 0-2 parts of Rosa canina fruit oil and 0-0.2 part of propylhydroxybenzoate.
2. The nourishing lip balm according to claim 1, which comprises the following raw material components in parts by mass: 6-12 parts of Boerhugu nut oil, 6-12 parts of phytosterol isostearate, 10.5-20 parts of diisostearyl malate, 12.5-20 parts of jojoba oil, 12.5-16 parts of sunflower seed oil, 10.5-15 parts of hydrogenated vegetable oil, 8.5-12 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 5.5-8 parts of PEG-12 carnauba wax, 4.5-10 parts of candelilla wax, 4.5-8 parts of wild lacquer fruit wax, 3-6 parts of ozokerite, 0.5-2 parts of Rosa canina fruit oil and 0.05-0.15 part of propylhydroxybenzoate.
3. The nourishing lip balm according to claim 2, which comprises the following raw material components in parts by mass: 6 parts of Boerhu walnut seed oil, 6 parts of phytosterol isostearate, 12 parts of diisostearyl malate, 16 parts of jojoba seed oil, 15 parts of sunflower seed oil, 12 parts of hydrogenated vegetable oil, 10 parts of oleic acid/linoleic acid/linolenic acid polyglycerol ester, 6 parts of PEG-12 carnauba wax, 6 parts of candelilla wax, 6 parts of jatropha wax, 3.9 parts of ozokerite, 1 part of Rosa canina fruit oil and 0.1 part of propylhydroxybenzoate.
4. The nourishing lip balm according to claim 1, wherein the weight ratio of the Boerhugu seed oil to the phytosterol isostearate is 1: (0.5-5).
5. A nourishing lip balm according to claim 4, wherein the weight ratio of Boerhans walnut seed oil to phytosterol isostearate is 1:1.
6. the method of preparing the nourishing lip gloss according to any one of claims 1 to 5, comprising the steps of:
(1) Uniformly mixing diisostearyl malate, jojoba seed oil, sunflower seed oil, hydrogenated vegetable oil, oleic acid/linoleic acid/linolenic acid polyglycerol ester, PEG-12 carnauba wax, candelilla wax, elaeagnus mollis fruit wax and ozokerite, adding Boerhu walnut seed oil and phytosterol isostearate, and uniformly mixing to obtain a premix;
(2) Adding Rosa canina fruit oil and propyl hydroxybenzoate into the premix, mixing, discharging, and cooling to room temperature to obtain the nourishing lip balm.
7. The method of claim 6, wherein the mixing temperature in the step (1) is 80-100 ℃.
8. The method of claim 6, wherein the mixing temperature in step (2) is 75-85 ℃.
9. The method of claim 6, wherein the discharge temperature in step (2) is 65-75 ℃.
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| CN114028268A (en) * | 2021-10-21 | 2022-02-11 | 曼秀雷敦(中国)药业有限公司 | Natural plant component lip balm and preparation method thereof |
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| NZ575991A (en) * | 2006-10-11 | 2012-02-24 | Wyeth Corp | Stick lip balm comprising carnauba wax, candelilla wax, jojoba esters and botanical butters |
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