CN113018199A

CN113018199A - Multipurpose ice film for repairing epidermis and preparation method thereof

Info

Publication number: CN113018199A
Application number: CN202011487703.3A
Authority: CN
Inventors: 杨文贤
Original assignee: Shenzhen Jingguang Biological Technology Co ltd
Current assignee: Shenzhen Jingguang Biological Technology Co ltd
Priority date: 2020-12-16
Filing date: 2020-12-16
Publication date: 2021-06-25

Abstract

The invention discloses a multipurpose ice membrane for repairing epidermis, which comprises a silk membrane and a mask liquid soaked and attached to the silk membrane, wherein the mask liquid comprises the following components in percentage by mass: 1 to 25 percent of humectant, 0.2 to 9 percent of skin conditioner, 0.1 to 2.0 percent of thickening agent, 0.5 to 5 percent of anti-allergy agent, 0.1 to 0.8 percent of preservative, 0.01 to 0.5 percent of freshener and the balance of purified water. The invention also discloses a preparation method of the multipurpose ice film for repairing epidermis, which is characterized in that an anti-allergy agent, a freshener, a skin conditioner, three components and silk film cloth are added to the components of the original facial mask liquid as carriers, the anti-allergy agent relieves allergic symptoms of skin injury after medical and artistic work, the freshener reduces burning sensation, stabbing pain and itching, the skin conditioner is perfectly combined with the silk film cloth, and the wound protection and healing speed after medical and cosmetic operation is accelerated. Thereby obtaining more effective postoperative repair function.

Description

Multipurpose ice film for repairing epidermis and preparation method thereof

Technical Field

The invention relates to the technical field of skin care, in particular to a multipurpose ice film for repairing and protecting epidermis and a preparation method thereof.

Background

With the continuous improvement of living standard of people and the continuous increase of beautiful demand of the masses of people, the medical plastic beauty industry is continuously developed, hundreds of thousands of people receive various medical plastic beauty operations every year, the current medical beauty operations are very popular, the market quantity is huge, the medical beauty operations can cause skin, mainly face wound, consumers are very interested in repairing the face wound surface, and after the medical beauty operations are completed, consumers generally select a repairing facial mask to repair in time, so that the problems of inflammation, burning sensation, stabbing pain, long-term no healing of pruritus or healing scar and the like of the wound surface in the later period are avoided.

The existing ice film in the market obviously stimulates eyes after being coated with the algefacient due to improper selection of raw materials of the algefacient; the addition of the preservative is improper, and the skin of the wound surface is more sensitive than normal skin, so that the wound surface has an irritation response; the problems of improper compress material selection and poor biocompatibility are solved, and therefore, a multipurpose ice film for repairing epidermis and a preparation method thereof are provided.

Disclosure of Invention

The invention aims to provide a multipurpose ice film for repairing the epidermis and a preparation method thereof, so as to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme: a multipurpose ice membrane for repairing epidermis comprises a silk membrane and a mask liquid soaked and attached on the silk membrane, wherein the carrier of the mask liquid is the silk membrane;

the mask liquid comprises the following components in percentage by mass: 1 to 25 percent of humectant, 0.2 to 9 percent of skin conditioner, 0.1 to 2 percent of thickening agent, 0.5 to 5 percent of anti-allergy agent, 0.1 to 0.8 percent of preservative, 0.05 to 0.5 percent of freshener and the balance of purified water;

the anti-allergy agent is a desensitization repairing essence; the desensitizing and repairing essence comprises lactobacillus/semen Phaseoli Radiati (Phaseolus RADIATUS) seed extract fermentation product filtrate. The addition amount is 0.5-5%.

Further, the humectant is characterized in that the humectant is one or more of glycerol, butanediol, trehalose, sodium hyaluronate, squalane and betaine; the humectant contains glycerol 1-10%, butanediol 2-8%, trehalose 0.5-3%, sodium hyaluronate 0.01-0.5%, squalane 0.5-2%, and betaine 1-6%.

Further, the skin conditioner is one or more of Hamamelis virginiana (HAMAMELIS VIRGINIANA) bark/leaf/stem extract, allantoin, dipotassium glycyrrhizinate, radix et rhizoma Rhei extract, Tremella FUCIFORMIS (Tremella FUCIFORMIS) polysaccharide, and bisabolol; the skin conditioner contains Hamamelis virginiana (HAMAMELIS VIRGINIANA) bark/leaf/stem extract 1-5%, allantoin 0.01-0.2%, dipotassium glycyrrhizinate 0.1-2%, radix et rhizoma Rhei extract 0.1-2%, Tremella (Tremella FUCIFORMIS) polysaccharide 0.1-2%, and bisabolol 0.1-3%.

Further, the thickening agent is carbomer, and the addition amount is 0.1% -0.5%.

Furthermore, the addition amount of the menthane formylethylamine in the freshener is 0.01-0.5%.

Further, the preservative is p-hydroxyacetophenone, hexanediol and methyl hydroxybenzoate;

the p-hydroxyacetophenone has an antioxidant effect, the hexanediol has a certain moisturizing effect, and both are mild and non-irritant preservative components, and the p-hydroxyacetophenone and the hexanediol are combined together to form a preservative synergistic effect and reduce the usage amount of the p-hydroxyacetophenone and the hexanediol. The addition amount of p-hydroxyacetophenone in the antiseptic is 0.1-0.8%, the addition amount of hexanediol is 0.1-0.8%, and the addition amount of methylparaben is 0.1%.

The invention also provides a preparation method of the multi-effect repairing ice film, which comprises the following steps:

step S1: pouring the purified water into a water kettle, heating to 85 ℃, mixing the humectant, the thickening agent and the water, and stirring until the purified water is completely dissolved. Keeping the temperature and stirring for 20 min;

step S2: sequentially adding skin conditioner when the temperature of the water kettle is reduced to 60 ℃, and fully stirring;

step S3: continuously cooling the water pot in the step S2 to 40 ℃, sequentially adding the anti-allergic agent, the preservative and the freshener, and stirring for 30min to obtain essence;

step S4: and (5) filling the essence prepared in the step (S3) into an aluminum foil bag containing silk mask cloth by using a high-speed mask filling machine or a full-automatic mask filling machine in a clean environment to obtain the multipurpose ice film for repairing the epidermis.

The essence prepared in the step S3 is transparent viscous liquid, and the pH value range is 5.0-6.5. The pH value of the prepared ice film essence is weakly acidic, meets the dermatological requirement that the pH value of the skin is 5.0-6.5, namely the weak acidity, and provides an optimum repairing environment for the skin.

Compared with the prior art, the invention has the following beneficial effects: the multipurpose ice film for repairing the epidermis and the preparation method thereof are characterized in that an anti-allergic agent, a freshener and a skin conditioner are added to the components of the original facial mask liquid, silk membrane cloth is combined as a carrier, the anti-allergic agent is used for relieving allergic symptoms of postoperative injured skin, the freshener is used for reducing burning sensation, stabbing pain and itching, and the wound protection and healing speed after medical cosmetology operation is accelerated. Thereby obtaining more effective postoperative repair function. The skin can be more moist, healthy and beautiful after being frequently used, and the mask containing the menthane formylethylamine can bring fresh feeling to the skin in summer; the absorption is fast, and the red skin of the back part after the sun is fast faded and calmed, and the allergy is relieved; the facial mask is required by facial skin in summer and has strong effect on repairing the skin after sunburn. The ice film is a repairing facial mask which is used for ice and cool on the face, is a very good repairing facial mask after being dried in the sun in summer, is developed aiming at sensitive skin, and has good relieving effect on skin injury caused by sun ultraviolet rays, erosion of wind and sand, external pollution, skin dryness, water shortage and the like due to dry weather and various sensitive symptoms caused by poor immunity of the skin.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely in conjunction with the implementation of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention provides a technical scheme that: a multipurpose ice film for repairing epidermis and a preparation method thereof,

the first embodiment is as follows: a multi-effect ice film for repairing epidermis comprises the following components in percentage by mass:

25% of a humectant, wherein the addition amount of glycerol is 10%, the addition amount of butanediol is 6%, the addition amount of trehalose is 2%, the addition amount of sodium hyaluronate (10-120 kilodaltons) is 0.2%, the addition amount of bioglycan is 2%, the addition amount of betaine is 2.8%, and the addition amount of squalane is 2%.

8% of skin conditioner, 4.3% of the extract of bark, leaf and stem of Hamamelis virginiana (HAMAMELIS VIRGINIANA), 0.2% of allantoin, 1% of dipotassium glycyrrhizinate, 1% of medicinal rhubarb extract, 1% of oat beta-glucan and 0.5% of bisabolol.

The thickener is carbomer, and the addition amount is 0.15%.

The antiallergic agent can be used for relieving allergy, and the filtrate of fermented product of refined lactobacillus/semen Phaseoli Radiati (Phaseolus RADIATUS) seed extract is added in an amount of 2.0%.

The menthane formylethylamine content in the algefacient is 0.1%

The addition amount of p-hydroxyacetophenone in the antiseptic was 0.4%, the addition amount of 1, 2 hexanediol was 0.4%, and the addition amount of methylparaben was 0.1%.

The balance being purified water.

The production process comprises the following steps:

1. pouring purified water into a water kettle, heating to 85-90 ℃, mixing the humectant, the thickening agent and the water, and stirring until the purified water is completely dissolved. Keeping the temperature and stirring for 20 min;

2. sequentially adding skin conditioner when the temperature of the water kettle is reduced to 60 ℃, and uniformly stirring;

3. continuously cooling to 40 deg.C, sequentially adding anti-allergic agent, antiseptic and algefacient, and stirring for 30 min;

4. and filling the essence prepared by the process into an aluminum foil bag containing silk mask cloth to obtain the multipurpose ice film for repairing the epidermis.

Example two: a multipurpose ice film for repairing epidermis comprises the following components in percentage by mass:

15% of humectant, wherein the addition amount of glycerin is 15%.

0.3% of skin conditioner, 4% of Hamamelis virginiana (HAMAMELIS VIRGINIANA) bark/leaf/stem extract, 0.2% of allantoin and 0.2% of bisabolol.

The thickener is carbomer, and the addition amount is 0.15%.

The antiallergic agent can be used for relieving allergy, and the filtrate of fermented product of refined lactobacillus/semen Phaseoli Radiati (Phaseolus RADIATUS) seed extract has an addition amount of 1%.

The menthane formylethylamine content in the algefacient is 0.03%

The addition amount of p-hydroxyacetophenone in the preservative was 0.4%, and the addition amount of propylene glycol was 0.4% and the addition amount of methylparaben was 0.1%. .

The balance being purified water.

The production process comprises the following steps:

1. pouring the purified water into a water kettle, heating to 85 ℃, mixing the humectant, the thickening agent and the water, and stirring until the purified water is completely dissolved. Keeping the temperature and stirring for 20 min;

Example three: a multipurpose ice film for repairing epidermis comprises the following components in percentage by mass:

10% of a humectant, wherein the addition amount of glycerol is 4.48%, the addition amount of butanediol is 2%, the addition amount of trehalose is 1%, the addition amount of sodium hyaluronate (10-120 ten thousand daltons) is 0.02%, the addition amount of bioglycan is 0.5%, the addition amount of betaine is 1%, and the addition amount of squalane is 1%.

4% of skin conditioner, wherein the addition amount of the extract of bark/leaf/stem of Hamamelis virginiana (HAMAMELIS VIRGINIANA) is 2.6%, the addition amount of allantoin is 0.2%, the addition amount of dipotassium glycyrrhizinate is 0.2%, the addition amount of medicinal rhubarb extract is 0.3%, the addition amount of oat beta-glucan is 0.5%, and the addition amount of bisabolol is 0.2%.

The thickener is carbomer, and the addition amount is 0.1%.

The antiallergic agent can be added into fermented product filtrate of semen Phaseoli Radiati (Phaseolus RADIATUS) seed extract at an amount of 1.0%.

The menthane formylethylamine content in the algefacient is 0.1%

The addition amount of p-hydroxyacetophenone propylene glycol, propylene glycol and methyl hydroxybenzoate in the antiseptic is 0.4%, 0.4% and 0.1%.

The balance being purified water.

The production process comprises the following steps:

4. filling the essence prepared by the process into an aluminum foil bag containing silk mask cloth to obtain a multipurpose ice film for repairing epidermis;

example 4: based on example 3, the anti-allergic agent is changed into radix stephaniae tetrandrae extract, the addition amount is 0.5%, and the freshener is changed into borneol, the addition amount is 0.1%. The production process was the same as in example 3.

Comparative example 1: on the basis of example 3, no anti-sensitivity agent was added.

Comparative example 2: on the basis of example 3, no cooling agent was added.

Comparative example 3: on the basis of the example 3, no skin conditioner is added, and the compress is changed into a common non-woven fabric film cloth.

Skin moisture retention test:

testing the moisture retention of skin by using a skin moisture tester, wherein the testing steps are as follows:

the test is carried out under normal room temperature conditions (the temperature is about 25 ℃, and the relative humidity is 40-60%), and the scoring standards of the test are shown in table 1:

status of state	Face part
		Dry skin	＜50
The skin is drier	50-60
		The skin has sufficient moisture	＞60

Selecting 10 women with age below 30 as testers, the tester is skin moisture tester, the test part is face mark test area, and each test area is 5

5cm2, the test sample amount is 0.5 g. The subjects were measured in a constant environment at 0.5h, 1h, 4h sitting still.

The test procedure was as follows:

1. before the test, the testee needs to uniformly clean the face with clear water;

2. pulling out the head cover of the skin moisture tester;

3. pressing a power switch of the skin moisture tester;

4. after a two-click prompt, the display stabilizes "00.0";

5. the probe of the skin moisture tester is vertical to the tested part, is stuck on the skin (remembering that the test probe is pressed into the shell completely), and can read the data after hearing the beep sound;

6. pressing a zero clearing key of '0' during continuous testing;

7. coating facial mask liquid on the designated position, and measuring for 0.5h, 1h and 4h respectively, wherein the testing method is the same as the steps 4 and 5;

8. after the test, the test probe is wiped clean with soft cloth or tissue paper soaked in alcohol, and the head cover is covered.

The test results are shown in table 2:

it can be seen from table 2 that the addition of the moisturizing component has a good moisturizing effect, and the moisturizing requirement cannot be met only by adding glycerin.

And (3) red fading and swelling subsiding test:

20 women who just finished medical cosmetic surgery, such as water treatment surgery, were selected as test persons and had obvious wound surfaces after the surgery, and were randomly divided into 2 groups, one of which was applied with the mask prepared in example 3 and the other was applied with the mask prepared in comparative example 1, and the effects of the test were observed after the surgery for 1 time, and the results are shown in table 3.

Testing indexes are as follows: the red and swollen phenomenon is avoided; slight red and swollen; obvious red swelling;

the test environment is an indoor environment; no strong sunlight or direct light; the environmental temperature is 20-25 ℃; the relative humidity is 40-60%;

TABLE 3 test results

As can be seen from Table 3, the addition of the cooling effect component has a better effect of eliminating swelling and diminishing redness. Is more beneficial to sensory experience of sensitive skin after operation and avoids stabbing pain and burning sensation.

Therefore, the effect of the product is compared with that of a product which uses common non-woven fabric and does not contain the three components, and a post-operation repair test is carried out on 20 patients after the micro-needle operation. Wherein 10 cases of postoperative use of multi-effect repair ice films as sample groups; after 10 cases of operation, the non-woven fabric mask with the conventional formula was used as a control group, and finally the blushing property, the hypersensitivity, the irritation, the repairing time and the skin improvement degree after healing were compared, and the results are shown in table 4:

the results show that the sample group is obviously superior to the control group in the aspects of red fading property, anaphylaxis, irritation, repairing time and skin improvement degree after healing.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. The utility model provides a multipurpose ice membrane is repaiied to epidermis, its characterized in that includes silk membrane cloth and soaks the facial mask liquid of adhering to on silk membrane cloth, the facial mask liquid comprises following mass percent component: 1 to 25 percent of humectant, 0.2 to 9 percent of skin conditioner, 0.1 to 2.0 percent of thickening agent, 0.5 to 5.0 percent of anti-allergy agent, 0.1 to 0.8 percent of preservative, 0.01 to 0.5 percent of freshener and the balance of purified water.

2. The multipurpose ice film for repairing epidermis of claim 1, wherein the humectant is one or more of glycerin, butylene glycol, trehalose, sodium hyaluronate, squalane and betaine; the humectant contains 1-10% of glycerol, 2-8% of butanediol, 0.5-3% of trehalose, 0.01-0.5% of sodium hyaluronate, 0.5-2% of squalane and 1-6% of betaine.

3. The multipurpose ice film for epidermis repair according to claim 1, wherein the skin conditioner is one or more of witch hazel bark/leaf/stem extract, allantoin, dipotassium glycyrrhizinate, rhubarb horsetails extract, tremella polysaccharide, and bisabolol; the skin conditioner contains Hamamelis virginiana bark/leaf/stem extract 1-5%, allantoin 0.01-0.2%, dipotassium glycyrrhizinate 0.1-2%, medicinal radix et rhizoma Rhei extract 0.1-2%, Tremella polysaccharide 0.1-3%, and bisabolol 0.1-3%.

4. The epidermal repair multi-purpose ice film of claim 1, wherein the thickener is carbomer and is present in an amount from 0.1% to 0.5%.

5. The multi-purpose ice film for repairing epidermis of claim 1, wherein the soothing repairing essence consists of a lactobacillus/mung bean (PHASEOLUS RADIATUS) seed extract fermentation product filtrate. The addition amount is 0.5 to 5 percent.

6. The skin-repairing multi-purpose ice film as claimed in claim 1, wherein said preservative is p-hydroxyacetophenone and hexylene glycol; the addition amount of p-hydroxyacetophenone in the antiseptic is 0.1-0.8%, the addition amount of hexanediol is 0.1-0.8%, and the addition amount of methyl hydroxybenzoate is 0.1%.

7. The multipurpose ice film for repairing epidermis of claim 1, wherein the cooling agent is menthane formylethylamine in an amount of 0.01% to 0.5%.

8. A method for preparing the skin-repairing multipurpose ice sheet as claimed in any one of claims 1 to 7, comprising:

step S3: and (4) continuously cooling the water kettle in the step S2 to 40 ℃, sequentially adding the anti-allergic agent, the preservative and the freshener, stirring for 30min to obtain the essence with the pH value ranging from 5.0 to 6.5 (direct measurement method), and discharging after the essence is qualified.

Step S4: and (5) filling the essence prepared in the step (S3) into an aluminum foil bag containing silk mask cloth in a clean environment to obtain the multipurpose ice film for repairing the epidermis.