CN103655330A - Men skin refreshing and nourishing emulsion and preparation method thereof - Google Patents
Men skin refreshing and nourishing emulsion and preparation method thereof Download PDFInfo
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- CN103655330A CN103655330A CN201310667014.4A CN201310667014A CN103655330A CN 103655330 A CN103655330 A CN 103655330A CN 201310667014 A CN201310667014 A CN 201310667014A CN 103655330 A CN103655330 A CN 103655330A
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Abstract
The invention discloses a men skin refreshing and nourishing emulsion and a preparation method thereof. The emulsion comprises lactic menthol ester, menthol, tinocare GL, sodium hyaluronate, asparaginic acid aspartic acid, oat polypeptide, an oil-phase component, a water-phase component, triethanolamine, essence and preservative. The emulsion gives a comfortable tingling and refreshed feeling to people, can be used for activating skin cells and promoting skin circulation, has a remarkable skin refreshing effect, can be used for preventing occurrence of wrinkles, enables skin to be smooth, tender and soft. The emulsion is researched and developed according to the characteristics of men skin, and can effectively improve rough skin of men and prevent skin aging.
Description
[technical field]
The present invention relates to a kind of moisturizer and preparation method thereof, relate in particular to awake skin moisturizer of a kind of man and preparation method thereof, belong to daily cosmetics technical field.
[background technology]
Along with the progressively improvement of living standard, people also improve constantly beautiful pursuit, but most of cosmetics are all for women, and therefore, a lot of men at will select women's skin care item to use.
And in fact; male's skin and women's skin are discrepant; boy student's skin horny layer is conventionally thicker; skin corium elasticity is compared to women's skin flexible more; and sebaceous gland is relatively active flourishing, thus most of male belong to mixing partially oil to oiliness skin and be very easily subject to glossy and puzzlement small pox, but fortunately; just because this vigorous natural sebum makes the aging rate of male's skin be much more slowly than women as barrier protection, and start more late.
Along with social development, man's skin protection idea is also slowly changing, and increasing man starts to focus on instrument modification and the external makings of oneself, becomes the consumer of cosmetics.And the advertisement of " large treasured is shown in " has shown man's sense of loving to make up and wearing beautiful clothes especially everyday.Along with the expansion of the market demand, increasing men's cosmetics and cosmetic products arise at the historic moment.But domestic male cosmetic market can only be described with in the ascendant at present, and product manufacture, product function, location also have many deficiencies, seldom embody male's special use.But should say that this is a development trend, from now on, this may become the topic that increasing white collar man pays close attention to.Man is when carrying out skin of face health care; can select suitable cosmetics according to self skin conditions; generally select skin-care cosmetics and tonic cosmetics; with protection and skin nutrition; dosage form be take cream as good; oily skin is applicable without oily light water preparation cosmetics summer, in order to avoid cause pilosebaceous obstruction, produces pilosebaceous unit disease.But because male's skin and women's skin is different, men's cosmetics are different from lady's cosmetics after all, with regard to the cosmetics that need some to use for man specially, meet these demands.Though and quietly heat up in current male cosmetic market, also not by a long sight from " fire ".Especially skin protection for men only, must use, hair, the cosmetics such as sun-proof, product and market are still in breeding phase.
[summary of the invention]
The object of the invention is to make up the deficiencies in the prior art, provide a kind of and slow down pachylosis phenomenon and microgroove especially for the coarse skin of man, prevent that wrinkle from producing, and make that skin becomes smoothly, delicate, the soft awake skin moisturizer of man.
Another object of the present invention is to provide a kind of preparation method of above-mentioned moisturizer.
The present invention to achieve these goals, by the following technical solutions:
Man's skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.03～0.3%
Mentholum 0.05～0.5%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.3～1.0%.
A kind of man of the present invention skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.03～0.1%
Mentholum 0.05～0.2%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.5～0.8%.
A kind of man of the present invention skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.2～0.3%
Mentholum 0.3～0.5%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.5～0.8%.
Below component compatibility mechanism of the present invention is elaborated:
1, Mentholum is with menthyl lactate together adapted
Mentholum molecule has four kinds of structure bodies, i.e. Mentholum, carvomenthol, strange Herba Menthae and neomenthol.And each isomer has respectively dextrorotation and two kinds of chirality enantiomer of derotation, so the molecular change of Mentholum obtains complicated.Our daily said Natural menthol and commodity Mentholum refer to left-handed Mentholum chiral isomer (L-Mentholum).
Because can making skin and mucosa, L-Mentholum produces cool feeling, so it takes the course of its own in aromachemicals.The cool feeling that Mentholum produces skin is far longer than ethanol or hexane equal solvent is coated in the cool feeling causing on skin.Although we know that some other compound also can produce such cool feeling,, nearly all these compounds are all the derivants of L-Mentholum.
Mentholum has Herba Menthae icy and light and salubrious fragrance.Because variable concentrations L-Mentholum can produce different picotements and cool feeling, so that its fragrance just becomes is very complicated.The Mentholum of extremely low concentration has micro-peppery sense and pure and fresh Herba Menthae icy; The Mentholum of intermediate concentration starts to have cool feeling; Along with the raising of concentration, it is more and more stronger that cool feeling becomes, and starts to have desensitization, and produce cool and numb reaction.
This neural picotement has the desired throat analgesic effect of Pectoral medicine.With rambling about in Mentholum factory, illustrate that its desensitization has been again good example only, when a people steps into the Existential Space of Mentholum completely, first its abnormal smells from the patient drills in his mouth, nose and eye.When Mentholum gas permeation enters after his clothes, his whole body is felt fiber crops thorn, and then produces feeling of numbness.
Menthyl lactate is a kind of micro-yellow thick liquid of being made by natural material, has strong sweet taste and refrigerant fragrance.Volatilization temperature, up to 38 ℃, can make the products such as medicated cigarette, toothpaste, confection add fresh and sweet characteristic, and extend the shelf life.
Menthyl lactate is a kind of Herba Menthae derivant, and teacher of the formula designed cold-type yellow (clear) product and can only adopt Herba Menthae in the past, there is no other selections.But the volatility of Herba Menthae and zest are very large, cause cooling effect strong and very brief, because thering is special mint flavored, deduct a percentage and cover the abnormal smells from the patient of essence.
This product is not chafe of long-acting tasteless freshener, and mucosa is not had to zest, is therefore applicable to sensitive-skinned product.Do not cover odor type: because only having faint abnormal smells from the patient, can freely select essence to be applicable to your market concept, a refrigerant product that there is no mint flavored.There is lasting cooling effect, can make salubrious pleasant refrigerant product.
Menthyl lactate has good compatibility, and menthyl lactate and Mentholum one are reinstated other character that not only can improve previous product taste effect and can not affect product.
2, can GL over sky
Can GL over pure natural macromolecule polysaccharide compounds-sky of being prepared by vapour bar (Ciba) company high-tech biotechnology; it has moisture retention, improves skin coarseness, also has anti-inflammatory effect; there is excellent cellular immunization activation; can effectively protect and photoaging that pre-resisting ultraviolet radiation causes; chafe cytoactive; efficient repairing sheath skin, the autoimmune protective capability of reinforcement skin.
Moisture retention contrast test
Can GL and commercially available moisturizing gel over-10% day,
On 10 volunteers' skin of forearm, test 2 weeks (one day twice), every person's 4 place's test points, two points were smeared over 10% day can GL, two points are smeared commercially available moisturizing gel, and Cornemeter(cutin instrument is used in research) test front and back humidity of skin variations (used test should carry out after 12 hours)
Application can improve 30% by mono-week skin moisture-keeping degree of GL over sky, and the skin of ending to stop using can be adhered to moisturizing again 7 days, and apply one week skin moisture-keeping degree of commercially available moisturizing gel, only improves 15%, and the skin of ending to stop using can adhere to being incubated 3 days again.
The contrast test of skin coarseness:
Roughness with radiating surface photometer research volunteer skin of forearm
10 volunteers
Test products
-contain over 5% day can GL emulsion
-blank emulsion
Before test is used and single use the roughness of latter 8 hours skin, can find, with skin coarseness that can GL over sky, with respect to untapped skin coarseness, reduced by 32%, and blank emulsion has only reduced by 20%.
Test antiinflammatory contrast test
Test volunteer back is because of the UV-induced erythema of UV
Test products:
Can GL over-10% day
-2%D-pantothenylol
-10% Aloe
Use Minolta Chromameter to test respectively the reduction of using skin erythema after 24 hours and 72 hours, result is:
After 24 hours with respect to untreated skin erythema place, with day over can GL skin erythema reduced 18%, use D-panthenol minimizing 12%, use Aloe minimizing 17%.
After 72 hours with respect to untreated skin erythema place, with day over can GL skin erythema reduced 23%, use D-panthenol minimizing 24%, use Aloe minimizing 19%.
Hence one can see that, can GL over having added day, and significantly booster injection is to the red effect of skin lower limb, and after 24-72 hour, still has obvious excellent results.
3, oat polypeptide
Oat polypeptide is a kind of plant complex that is derived from Herba bromi japonici, comprises avenin and avenabeta glucosan.It has very outstanding moistening effect, and the instant effect of tightening up and softening tiny wrinkle, strengthens skin care, improves the ability of skin opposing environmental stimuli, also has antiageing effect texts
The advanced technologies of oat polypeptide based on unique produced, with protein and the beta glucan of water extraction avenia part.The avenin extracting comprises: albumin and globulin; The avenabeta glucosan extracting is in the field of activity of polysaccharide
The cosmetics function of oat polypeptide:
(1) the softening skin of moisturizing &
The albumen of high molecular and avenabeta glucosan can guarantee its performance of keeping humidity and the film forming ability of protectiveness, the outward appearance of can also film forming giving skin smooth.
(2) wrinkle removal function
20 people have been carried out to organoleptic test, and product acts on eye.In test, in formula, contain 20% oat polypeptide, compare with the formula of placebo respectively.
Result: have 80.5% people to have wrinkle improvement effect in the group that oat polypeptide content is 20%, have 23.5% people to have wrinkle improvement effect and use in the group of placebo, recording 90% volunteer has positive effect using in 5 minutes.
(3) excellent film forming function.
Oat polypeptide contains avenin and avenabeta glucosan, can, in film forming under low concentration, play the effect of embedding or isolation small-molecule substance, fast Transport Activities composition or time controlled released.
(4) aging resistance
Oat polypeptide is proved to be to have and improves the effect of skin coarseness and free radical resisting and can suppress and prevent skin aging, improves skin surface situation.
A, minimizing skin coarseness
After using oat polypeptide, skin texture improves
B, free radical resisting
Skin is the natural cover for defense of resisting external environment infringement.Yet its long term exposure, in external environment, unavoidably can sustain damage, wherein the nocuous factor of tool is ultraviolet, infrared ray, pollution and flue dust.Dermal exposure is when external environment, and cell can constantly produce free radical, and these free radicals can injure epidermis and corium (damage of oxidisability comprises oil peroxidation and weakens skin defense function).This can cause skin premature aging (skin occurs wrinkle and becomes lax), especially long term exposure in the position of sunlight and reaction minimizing.
According to the experimental data of some researcher's issues, be presented at the protective effect of local use free radical scavenger (compound that can suppress radical reaction) to skin in the infringement that reduces skin vigorous oxidation.Long-term benefit is significantly to suppress thinning of skin and flexibility decrease.The formation of wrinkle is slowed down, and also has some damages to be repaired.
It is different that variable concentrations oat polypeptide is removed ability to hydroxy radical, and concentration increases removes strong free radical ability enhancing.10% oat polypeptide reaches 60% to hydroxy radical suppression ratio
Essence in the present invention and the mass percent of antiseptic are respectively: essence 0.1～0.5%; Antiseptic 0.2～0.5%.
A preparation method for the above-mentioned awake skin moisturizer of man, is characterized in that comprising the following steps:
(1) D is warmed up to 85 ℃ mutually, insulation is to 80 ℃, and stirring and dissolving is complete, cooling;
(2) C is warmed up to 70 ℃ mutually, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, then suction C phase slowly, homogenizing 10min, insulated and stirred 10min, evacuation cooling;
(4) while being cooled to 60 ℃, add B phase, then add E to neutralize mutually, homogenizing 2～3min, stirs;
(5) while being cooled to 40 ℃, add A phase, F phase, stirs, physical and chemical index after the assay was approved, discharging.
When prepared by the present invention, with triethanolamine, regulate pH value between 4.0～7.0.
The viscosity of the moisturizer that the present invention makes is 1000～10000mpa.s.
Outward appearance of the present invention is white emulsion, and heat-resistant stability is investigated (48 ℃ * 24H): qualified, and cold-resistant study on the stability (15 ℃ * 24H): qualified.
Using method of the present invention:
After clean face, get and be evenly applied in right amount face, be massaged into gently absorption.
Moisturizer of the present invention has the following advantages:
1, the cooperation of menthyl lactate and Mentholum can be given the most comfortable picotement, the refrigerant sense of people.Activate Skin Cell, promote skin circulation, there is the skin effect of significantly waking up.
2, with TG-L, in formula, coordinate hyaluronate sodium.There is moisture retention, improve skin coarseness, also have anti-inflammatory effect; there is excellent cellular immunization activation, can effectively protect and photoaging that pre-resisting ultraviolet radiation causes chafe cytoactive; efficient repairing sheath skin, the autoimmune protective capability of reinforcement skin.The skin that man is coarse, can find out significantly that coarse phenomenon slows down, and the microgroove of skin surface also reduces after use.Prevent that wrinkle from producing, and make that skin seems smoothly, delicacy, soft.
3, oat polypeptide and hydrolecithin can form a meticulous thin film in cortical surface, can make to damage skin becomes at short notice and more smoothly makes it have obvious skin moistening effect, compared with other products, its effect is more rapid, has obvious effect about 15-30 minute.
The present invention, especially for the feature of man's skin and research and develop, more can effectively improve the coarse skin of man and prevent aging.
[accompanying drawing explanation]
Fig. 1 is the skin texture figure before trial edition invention product;
Fig. 2 is the skin texture figure of trial edition invention product after three months.
[specific embodiment]
Below in conjunction with specific embodiment, the invention will be further described, refers to table 1:
Table 1: the formula of each embodiment forms, and represents with weight percentage.
The preparation technology of above embodiment is as follows:
(1) D is warmed up to 85 ℃ mutually, insulation is to 80 ℃, and stirring and dissolving is complete, cooling;
(2) C is warmed up to 70 ℃ mutually, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, then suction C phase slowly, homogenizing 10min, insulated and stirred 10min, evacuation cooling;
(4) while being cooled to 60 ℃, add B phase, then add E to be neutralized to mutually ph value of emulsion between 4.0～7.0, homogenizing 2～3min, stirs;
(5) while being cooled to 40 ℃, add A phase, F phase, stirs, physical and chemical index after the assay was approved, discharging.
The effect checking of embodiment of the present invention 1-6:
Choose 6 groups of man volunteers embodiment 1-6 product on probation, 10 every group, skin coarseness is approximate, smears every day three times, and result on trial is as shown in table 2:
Table 2:
As shown in Table 2, the present invention has more than 70% obvious improvement to man's rough grain, can be with reference to the contrast of accompanying drawing 1 and accompanying drawing 2, and the obvious degree of improvement of embodiment 1-6 is approximate, all has the sensation of the salubrious skin of waking up during use.
Claims (7)
1. man's skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.03～0.3%
Mentholum 0.05～0.5%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.3～1.0%.
2. a kind of man according to claim 1 skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.03～0.1%
Mentholum 0.05～0.2%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.5～0.8%.
3. a kind of man according to claim 1 skin moisturizer of waking up, is characterized in that being comprised of following percentage by weight component:
A phase: the skin component of waking up
Menthyl lactate 0.2～0.3%
Mentholum 0.3～0.5%
B phase: skin moistening component
C phase: oil phase component
D phase: water component
E phase: triethanolamine 0.1～0.5%
F phase: essence and antiseptic 0.5～0.8%.
4. according to the awake skin moisturizer of a kind of man described in any one in claim 1-3, it is characterized in that described essence and the mass percent of antiseptic are respectively:
Essence 0.1～0.5%
Antiseptic 0.2～0.5%.
5. the wake up preparation method of skin moisturizer of the man described in any one in claim 1-3, is characterized in that comprising the following steps:
(1) D is warmed up to 85 ℃ mutually, insulation is to 80 ℃, and stirring and dissolving is complete, cooling;
(2) C is warmed up to 70 ℃ mutually, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, then suction C phase slowly, homogenizing 10min, insulated and stirred 10min, evacuation cooling;
(4) while being cooled to 60 ℃, add B phase, then add E to neutralize mutually, homogenizing 2～3min, stirs;
(5) while being cooled to 40 ℃, add A phase, F phase, stirs, physical and chemical index after the assay was approved, discharging.
6. the preparation method of the awake skin moisturizer of a kind of man according to claim 5, is characterized in that described triethanolamine regulates pH value between 4.0～7.0.
7. a kind of man according to claim 5 preparation method of skin moisturizer of waking up, the viscosity that it is characterized in that described moisturizer is 1000～10000mpa.s.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104739724A (en) * | 2015-03-19 | 2015-07-01 | 百芮生物科技（上海）有限公司 | Preparation process of natural skincare hydrating micro-emulsified essence composition |
| CN109464302A (en) * | 2018-12-29 | 2019-03-15 | 上海家化联合股份有限公司 | Composition containing dipotassium glycyrrhizinate |
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| CN104739724A (en) * | 2015-03-19 | 2015-07-01 | 百芮生物科技（上海）有限公司 | Preparation process of natural skincare hydrating micro-emulsified essence composition |
| CN109464302A (en) * | 2018-12-29 | 2019-03-15 | 上海家化联合股份有限公司 | Composition containing dipotassium glycyrrhizinate |
| CN109464302B (en) * | 2018-12-29 | 2021-11-23 | 上海家化联合股份有限公司 | Composition containing dipotassium glycyrrhizinate |
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| CN103655330B (en) | 2015-08-05 |
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Effective date of registration: 20170602 Address after: 510000, No. 2, A zone, industrial road, Taihe village, Zhenlong, Baiyun District, Guangzhou, Guangdong Patentee after: Guangzhou sunshine Cosmetics Co., Ltd. Address before: 510000, A, No. 2, Xia Cheng Industrial Park, long Cheng garden, Baiyun District, Guangdong, Guangzhou Patentee before: Peng Zaihui |
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