CN103655330B - A kind of man wakes up skin moisturizer and preparation method thereof - Google Patents

A kind of man wakes up skin moisturizer and preparation method thereof Download PDF

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CN103655330B
CN103655330B CN201310667014.4A CN201310667014A CN103655330B CN 103655330 B CN103655330 B CN 103655330B CN 201310667014 A CN201310667014 A CN 201310667014A CN 103655330 B CN103655330 B CN 103655330B
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phase
skin
man
wakes
mentholum
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CN103655330A (en
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彭再辉
彭晓丹
邓晓群
严涛
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Guangzhou Sunshine Cosmetics Co Ltd
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Abstract

The invention discloses a kind of man to wake up skin moisturizer and preparation method thereof, this emulsion comprises menthyl lactate, Mentholum, can GL over sky, hyaluronate sodium, aspartic acid oat polypeptide, oil phase component, water phase components, triethanolamine and essence and antiseptic.The present invention can give the picotement that people is the most comfortable, refrigerant sense.Activate Skin Cell, promote skin circulation, there is skin effect of significantly waking up, prevent wrinkle from producing, and skin is seemed smoothly, delicacy, soft.The present invention especially for man's skin feature and research and develop, more effectively can improve the coarse skin of man and prevent aging.

Description

A kind of man wakes up skin moisturizer and preparation method thereof
[technical field]
The present invention relates to a kind of moisturizer and preparation method thereof, particularly relate to a kind of man and to wake up skin moisturizer and preparation method thereof, belong to daily cosmetics technical field.
[background technology]
Along with the progressively improvement of living standard, the pursuit of people to U.S. also improves constantly, but most of cosmetics are all for women, and therefore, a lot of man at will selects women's skin care item to use.
And in fact; male's skin and women's skin are discrepant; the skin horny layer of boy student is usually thicker; skin corium elasticity is compared to women's skin flexible more; and sebaceous gland is relatively active flourishing, thus most of male belong to mixing partially oil be very easily subject to glossy and puzzlement that is small pox to oiliness skin, but fortunately; just because this vigorous natural sebum makes the aging rate of male's skin be much more slowly than women as barrier protection, and beginning is more late.
Along with the development of society, the skin protection idea of man is also slowly changing, and the instrument that increasing man starts to focus on oneself is modified and external makings, becomes the consumer of cosmetics.And the advertisement of " large treasured is shown in everyday ", show man's sense of loving to make up and wearing beautiful clothes especially.Along with the expansion of the market demand, increasing men's cosmetics and cosmetic products arise at the historic moment.But male cosmetic market domestic at present can only be described with in the ascendant, product manufacturing, product function, location also have many deficiencies, seldom embody male special.But should say that this is a development trend, from now on, this may become the topic that increasing white collar man pays close attention to.Man is when carrying out skin of face health care; suitable cosmetics can be selected according to autologous skin situation; generally select skin-care cosmetics and tonic cosmetics; with protection and skin nutrition; dosage form is good with cream; oily skin is suitable for without oily light water preparation cosmetics summer, in order to avoid cause pilosebaceous obstruction, produces hair follicle sebum gland disease.But because male's skin and women's skin is different, men's cosmetics are different from lady's cosmetics after all, with regard to need some specially for the cosmetics of man to meet these demands.Though and quietly heat up in current male cosmetic market, also not by a long sight from " fire ".Especially skin protection for men only, must use, hair, the cosmetics such as sun-proof, product and market are still in breeding phase.
[summary of the invention]
The object of the invention is to make up the deficiencies in the prior art, provide a kind of special for the coarse skin of man, slow down pachylosis phenomenon and microgroove, prevent wrinkle from producing, and skin is become smoothly, delicacy, soft man wake up skin moisturizer.
Another object of the present invention is to provide a kind of preparation method of above-mentioned moisturizer.
The present invention to achieve these goals, by the following technical solutions:
A kind of man wakes up skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.03 ~ 0.3%
Mentholum 0.05 ~ 0.5%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.3 ~ 1.0%.
A kind of man of the present invention wakes up skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.03 ~ 0.1%
Mentholum 0.05 ~ 0.2%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.5 ~ 0.8%.
A kind of man of the present invention wakes up skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.2 ~ 0.3%
Mentholum 0.3 ~ 0.5%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.5 ~ 0.8%.
Below component compatibility mechanism of the present invention is described in detail:
1, Mentholum is with menthyl lactate adapted together
Mentholum molecule has four kinds of structure bodies, i.e. Mentholum, carvomenthol, strange Herba Menthae and neomenthol.And each isomer has dextrorotation and derotation two kinds of chiral enantiomer respectively, therefore the molecular change of Mentholum obtains complicated.Our daily said Natural menthol and commodity Mentholum refer to levomenthol chiral isomer (L-Mentholum).
Because L-Mentholum can make skin and mucosa produce cool feeling, so it takes the course of its own in aromachemicals.The cool feeling that Mentholum makes skin produce is far longer than ethanol or hexane equal solvent is coated in the cool feeling that skin causes.Although we know that some other compound also can produce such cool feeling, these compounds nearly all are all the derivants of L-Mentholum.
Mentholum has Herba Menthae icy and light and salubrious fragrance.Because variable concentrations L-Mentholum can produce different picotements and cool feeling, so its fragrance just becomes very complicated.The Mentholum of extremely low concentration has micro-peppery sense and pure and fresh Herba Menthae icy; The Mentholum of intermediate concentration starts to have cool feeling; Along with the raising of concentration, cool feeling becomes more and more stronger, starts to have desensitization, and produces cool and numb reaction.
This neural picotement has the throat analgesic effect required by Pectoral medicine.Illustrate that its desensitization has been again good example only with rambling about in Mentholum factory, when a people steps into the Existential Space of Mentholum completely, first its abnormal smells from the patient drills in his mouth, nose and eye.After Mentholum gas penetrates into his clothes, his whole body feels fiber crops thorn, and then produces feeling of numbness.
Menthyl lactate is a kind of micro-yellow viscous liquid be made up of natural material, has strong sweet taste and refrigerant fragrance.Volatilization temperature, up to 38 DEG C, can make the products such as medicated cigarette, toothpaste, confection add fresh and sweet characteristic, and extend the shelf life.
Menthyl lactate is a kind of Herba Menthae derivant, and formula teacher designed cold-type yellow (clear) product and can only adopt Herba Menthae in the past, did not have other to select.But the volatility of Herba Menthae and zest are very large, cause cooling effect strong and very brief, the abnormal smells from the patient of lid essence of deducting a percentage because having special mint flavored.
This product is long-acting tasteless freshener not chafe, does not have zest, be therefore applicable to sensitive-skinned product to mucosa.Not covering odor type: because only having faint abnormal smells from the patient, your market concept applicable can be carried out by unrestricted choice essence, a refrigerant product not having a mint flavored.There is lasting cooling effect, clearly pleasant refrigerant product can be made.
Menthyl lactate has good compatibility, and menthyl lactate and Mentholum one are reinstated the product taste effect before not only can improveing and can not be affected other character of product.
2, can GL over sky
Being clung to over pure natural macromolecule polysaccharide compounds-sky prepared by (Ciba) company high-tech biotechnology by vapour can GL; it has moisture retention, improves skin coarseness, also has anti-inflammatory effect; there is excellent cellular immunization activation; can the photoaging that causes of available protecting pre-resisting ultraviolet radiation; chafe cytoactive; efficient repairing sheath skin, strengthens the autoimmune protective capability of skin.
Moisture retention contrast test
Can GL and commercially available moisturizing gel over-10% day,
The skin of forearm of 10 volunteers is tested 2 weeks (one day twice), every person 4 place test point, two points were smeared over 10% day can GL, two points smear commercially available moisturizing gel, and research uses Cornemeter(cutin instrument) test front and back humidity of skin change (used test should carry out after 12h)
Application can improve 30% by GL mono-week skin moisture-keeping degree over sky, and the skin that stops to stop using can adhere to moisturizing again 7 days, and applies commercially available moisturizing gel one week skin moisture-keeping degree and only improve 15%, and the skin that stops to stop using can adhere to being incubated 3 days again.
The contrast test of skin coarseness:
By the roughness of radiating surface photometer research volunteer skin of forearm
10 volunteers
Test products
-containing can the emulsion of GL over 5% day
-blank emulsion
Before test uses and single use the roughness of latter 8 hours skin, can find, to use over sky and the skin coarseness of GL can reduce 32% relative to untapped skin coarseness, and blank emulsion only reduce 20%.
Test anti-inflammatory contrast test
Test volunteer back is because of the UV-induced erythema of UV
Test products:
Can GL over-10% day
-2%D-pantothenylol
-10% Aloe
Use Minolta Chromameter to test the reduction of use skin erythema after 24 hours and 72 hours respectively, result is:
Relative to untreated skin erythema place after 24 hours, to use over sky and the skin erythema of GL can decrease 18%, what use D-panthenol decreases 12%, and what use Aloe decreases 17%.
Relative to untreated skin erythema place after 72 hours, to use over sky and the skin erythema of GL can decrease 23%, what use D-panthenol decreases 24%, and what use Aloe decreases 19%.
It can thus be appreciated that with the addition of over sky can GL, significantly to the red effect of skin lower limb, and can still there is obvious excellent results after 24-72 hour by booster injection.
3, oat polypeptide
Oat polypeptide is a kind of plant complex being derived from Herba bromi japonici, comprises avenin and avenabeta glucosan.It has very outstanding moistening effect, instant tightens up and the effect of softening fine wrinkles, strengthens skin care, improves the ability of skin opposing environmental stimuli, also have the effects such as antiageing effect
Oat polypeptide is produced based on the advanced technologies of uniqueness, with the protein of water extraction avenia part and beta glucan.The avenin extracted comprises: albumin and globulin; The avenabeta glucosan extracted is in the field of activity of polysaccharide
The cosmetics function of oat polypeptide:
(1) moisturizing & softens skin
The albumen of high molecular and avenabeta glucosan can ensure its performance of keeping humidity and the film forming ability of protectiveness, film forming can also give the outward appearance of skin smooth.
(2) wrinkle removal function
Carried out organoleptic test to 20 people, product acts on eye.In testing, containing the oat polypeptide of 20% in formula, compare with the formula of placebo respectively.
Result: oat polypeptide content is have the people of 80.5% to have wrinkle improvement effect in the group of 20%, and use in the group of placebo and have the people of 23.5% to have wrinkle improvement effect, the volunteer recording 90% has positive effect in use in 5 minutes.
(3) excellent film forming function.
Oat polypeptide contains avenin and avenabeta glucosan, can in film forming under low concentration, play the effect of embedding or isolation small-molecule substance, can Transport Activities composition or time controlled released fast.
(4) aging resistance
Oat polypeptide is proved to be the effect that has and improve skin coarseness and free radical resisting and can suppresses and prevent skin aging, improves skin surface situation.
A, minimizing skin coarseness
After using oat polypeptide, skin texture improves
B, free radical resisting
Skin is the natural cover for defense resisting external environment infringement.But it is exposed in external environment for a long time, inevitably sustains damage, wherein the nocuous factor of most is ultraviolet, infrared ray, pollution and flue dust.Dermal exposure is when external environment, and cell constantly can produce free radical, and these free radicals can injure epidermis and corium (damage of oxidisability comprises oil peroxidation and weakens skin defense function).This can cause premature skin ageing (skin occurs wrinkle and becomes lax), is exposed to the position of sunlight and reaction minimizing especially for a long time.
The experimental data issued according to some researchers is presented at local in the infringement reducing skin vigorous oxidation and uses free radical scavenger (can suppress the compound of the radical reaction) protective effect to skin.Long-term benefit significantly suppresses thinning of skin and flexibility decrease.The formation of wrinkle is slowed down, and also has some damages to be repaired.
Variable concentrations oat polypeptide is different to Hydroxyl radical-scavenging ability, and concentration increases removes the enhancing of strong free radical ability.10% oat polypeptide reaches 60% to hydroxy radical suppression ratio
Essence in the present invention and the mass percent of antiseptic are respectively: essence 0.1 ~ 0.5%; Antiseptic 0.2 ~ 0.5%.
Above-mentioned man wakes up the preparation method of skin moisturizer, it is characterized in that comprising the following steps:
(1) D phase is warmed up to 85 DEG C, is incubated 80 DEG C, stirring and dissolving is complete, cooling;
(2) C phase is warmed up to 70 DEG C, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, more slowly suction C phase, homogenizing 10min, insulated and stirred 10min, evacuation is lowered the temperature;
(4) add B phase when being cooled to 60 DEG C, then add E phase and neutralize, homogenizing 2 ~ 3min, stirs;
(5) add A phase when being cooled to 40 DEG C, F phase, stirs, physical and chemical index after the assay was approved, discharging.
Time prepared by the present invention by triethanolamine adjust ph between 4.0 ~ 7.0.
The viscosity of the moisturizer that the present invention obtains is 1000 ~ 10000mpa.s.
Outward appearance of the present invention is white emulsion, and heat-resistant stability investigates (48 DEG C × 24H): qualified, cold-resistant study on the stability (-15 DEG C × 24H): qualified.
Using method of the present invention:
After clean face, get appropriate uniform application in face, be massaged into absorption gently.
Moisturizer of the present invention has the following advantages:
1, the cooperation of menthyl lactate and Mentholum can give the picotement that people is the most comfortable, refrigerant sense.Activate Skin Cell, promote skin circulation, there is skin effect of significantly waking up.
2, in formula, hyaluronate sodium is coordinated with TG-L.There is moisture retention, improve skin coarseness, also have anti-inflammatory effect; there is excellent cellular immunization activation, can the photoaging that causes of available protecting pre-resisting ultraviolet radiation, chafe cytoactive; efficient repairing sheath skin, strengthens the autoimmune protective capability of skin.The skin that man is coarse, can find out that coarse phenomenon slows down significantly, and the microgroove of skin surface also reduces after using.Prevent wrinkle from producing, and skin is seemed smoothly, delicate, soft.
3, oat polypeptide and hydrolecithin can form a meticulous thin film in cortical surface, damage skin can be made to become at short notice and more smoothly to make it have obvious skin moistening effect, comparatively other products, its effect is more rapid, namely has obvious effect about 15-30 minute.
The present invention especially for man's skin feature and research and develop, more effectively can improve the coarse skin of man and prevent aging.
[accompanying drawing explanation]
Fig. 1 is the skin texture figure before trial edition invention product;
Fig. 2 is the skin texture figure of trial edition invention product after three months.
[detailed description of the invention]
Below in conjunction with specific embodiment, the invention will be further described, refers to table 1:
Table 1: the formula composition of each embodiment, represents with weight percentage.
The preparation technology of above embodiment is as follows:
(1) D phase is warmed up to 85 DEG C, is incubated 80 DEG C, stirring and dissolving is complete, cooling;
(2) C phase is warmed up to 70 DEG C, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, more slowly suction C phase, homogenizing 10min, insulated and stirred 10min, evacuation is lowered the temperature;
(4) add B phase when being cooled to 60 DEG C, then add E phase and be neutralized to ph value of emulsion between 4.0 ~ 7.0, homogenizing 2 ~ 3min, stirs;
(5) add A phase when being cooled to 40 DEG C, F phase, stirs, physical and chemical index after the assay was approved, discharging.
The both effectiveness checking of embodiment of the present invention 1-6:
Choose 6 groups of man volunteers and try out embodiment 1-6 product, often organize 10, skin coarseness is similar to, and smear three every day, result on trial is as shown in table 2:
Table 2:
As shown in Table 2, the present invention has the obvious improvement of more than 70% to man's rough grain, can with reference to the contrast of accompanying drawing 1 with accompanying drawing 2, and the obvious degree of improvement of embodiment 1-6 is similar to, and all has the sensation of salubrious skin of waking up during use.

Claims (7)

1. man wakes up a skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.03 ~ 0.3%
Mentholum 0.05 ~ 0.5%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.3 ~ 1.0%.
2. a kind of man according to claim 1 wakes up skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.03 ~ 0.1%
Mentholum 0.05 ~ 0.2%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.5 ~ 0.8%.
3. a kind of man according to claim 1 wakes up skin moisturizer, it is characterized in that being made up of following weight percent composition:
A phase: skin component of waking up
Menthyl lactate 0.2 ~ 0.3%
Mentholum 0.3 ~ 0.5%
B phase: emollient ingredient
C phase: oil phase component
D phase: water phase components
E phase: triethanolamine 0.1 ~ 0.5%
F phase: essence and antiseptic 0.5 ~ 0.8%.
4. a kind of man according to any one of claim 1-3 wakes up skin moisturizer, it is characterized in that the mass percent of described essence and antiseptic is respectively:
Essence 0.1 ~ 0.5%
Antiseptic 0.2 ~ 0.5%.
5. the man according to any one of claim 1-3 wakes up the preparation method of skin moisturizer, it is characterized in that comprising the following steps:
(1) D phase is warmed up to 85 DEG C, is incubated 80 DEG C, stirring and dissolving is complete, cooling;
(2) C phase is warmed up to 70 DEG C, stirring and dissolving is complete;
(3) first by D phase suction emulsifying pot, more slowly suction C phase, homogenizing 10min, insulated and stirred 10min, evacuation is lowered the temperature;
(4) add B phase when being cooled to 60 DEG C, then add E phase and neutralize, homogenizing 2 ~ 3min, stirs;
(5) add A phase when being cooled to 40 DEG C, F phase, stirs, physical and chemical index after the assay was approved, discharging.
6. a kind of man according to claim 5 wakes up the preparation method of skin moisturizer, it is characterized in that described triethanolamine adjust ph is between 4.0 ~ 7.0.
7. a kind of man according to claim 5 wakes up the preparation method of skin moisturizer, it is characterized in that the viscosity of described moisturizer is 1000 ~ 10000mpa.s.
CN201310667014.4A 2014-01-23 2014-01-23 A kind of man wakes up skin moisturizer and preparation method thereof Active CN103655330B (en)

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Publication number Priority date Publication date Assignee Title
CN104739724B (en) * 2015-03-19 2017-12-15 百芮生物科技(上海)有限公司 A kind of preparation technology of natural beautiful skin moisturizing microemulsified Essence composition
CN109464302B (en) * 2018-12-29 2021-11-23 上海家化联合股份有限公司 Composition containing dipotassium glycyrrhizinate

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Address after: 510000, No. 2, A zone, industrial road, Taihe village, Zhenlong, Baiyun District, Guangzhou, Guangdong

Patentee after: Guangzhou sunshine Cosmetics Co., Ltd.

Address before: 510000, A, No. 2, Xia Cheng Industrial Park, long Cheng garden, Baiyun District, Guangdong, Guangzhou

Patentee before: Peng Zaihui

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