CN103989614B - A kind of whitening face cleaning facial treatment mask and preparation method thereof - Google Patents

A kind of whitening face cleaning facial treatment mask and preparation method thereof Download PDF

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CN103989614B
CN103989614B CN201410229015.5A CN201410229015A CN103989614B CN 103989614 B CN103989614 B CN 103989614B CN 201410229015 A CN201410229015 A CN 201410229015A CN 103989614 B CN103989614 B CN 103989614B
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powder
skin
essence
face cleaning
distilled water
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CN103989614A (en
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孙淑萍
李国柱
吴泽华
赵飒娜
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Guangdong Gaohang Intellectual Property Operation Co ltd
Guangzhou Xiao Cosmetics Co ltd
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Wannan Medical College
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Abstract

The invention discloses a kind of whitening face cleaning facial treatment mask and preparation method thereof, containing following material and weight portion in facial film: fibroin, Margarita powder, Bombyx Batryticatus powder, green stone mud, spaonin powder, pearl essence, carbomer, 30% triethanolamine solution, sodium alginate, 5% ethyl hydroxybenzoate propylene glycol solution, safflower oil, Rice oil, tragacanth, arabic gum, distilled water, essence.Facial film prescription prepared by the present invention with the addition of substantial amounts of natural component.Fibroin can go deep into skin bottom, fundamentally skin whitening and have no side effect;Margarita powder Titanium Dioxide, adsorbs oils and fats.The nutritious skin of Bombyx Batryticatus and beautification function.In formula, each composition complements each other, comprehensive nourishes rough skin, repairs skin, supplements its various nutrient substance needed, and makes skin obtain comprehensive conditioning from inside to outside, gradually recovers whitening honorable.

Description

A kind of whitening face cleaning facial treatment mask and preparation method thereof
Technical field
The present invention relates to a kind of facial film and preparation method thereof, particularly to a kind of whitening face cleaning facial treatment mask and preparation side thereof Method.
Background technology
In actual life, everyone wants to have healthy delicate skin.Skin is one of organ of wanting of our body weight for humans, It protects our health.
The work that grows with each passing day, life stress, environmental pollution, make the skin of many people face the threat of subhealth state.Various Dermatosis occurs again and again, and it is relevant that this lacks various nutrient substance with skin.Modern does not moves all day, is not careful in one's diet, Some people there will be the symptom that facial muscle is sagging very early, and this is just because of there being two kinds of protein in the skin corium of skin: glue Former albumen and elastic fibers albumen, they have supported skin makes it full compact.After 25 years old, both albumen is due to people's asthenia Old process and naturally reduce, the support force of skin declines the most therewith, and elastic force reduces, and lax and wrinkle then occurs.
The radiation sources such as keyboard, computer screen, mobile phone directly influence whether the steady random of the hormonal system of our health, so that Skin metabolism is irregular, and adding computer is magnetic, and can build up some dusts and unclean air etc., and these all can have influence on me Skin, aggravation skin degree of aging.
Variations in temperature that air-conditioning, environmental pollution, Seasonal conversion bring and pressure, and skin aging, metabolism slow down etc. because of Element all can cause skin water loss, make skin coarse, dim mute, form dry stricture of vagina, cause many skin problems.
Protection skin is accomplished by supplementing the various nutrient substance that it needs, and it could be allowed to be in the state of health.Chinese medicine Elite is dissolved in the middle of skin care item, is the Development Trend of modern skin protection science and technology.For busy modern, use containing natural The whitening face cleaning skin care item of component extract are excellent selections.
Summary of the invention
For solving above-mentioned technical problem, the present invention provides a kind of whitening face cleaning skin protection face containing natural component extract Film.
Present invention also offers the preparation method of a kind of whitening face cleaning facial treatment mask.
A kind of whitening face cleaning facial treatment mask that the present invention provides, containing following material in 76.4g facial film:
Described essence be Fructus Citri Limoniae essence, rose essence, osmanthus flower fragrance, peach flavor, flavoring pineapple essence, green cucumber essence, Jasmin essence.
Described Bombyx Batryticatus powder is prepared by the following method:
Weigh Bombyx Batryticatus appropriate, pulverize with pulverizer, cross 100-150 mesh sieve, standby.
The preparation method of a kind of whitening face cleaning facial treatment mask that the present invention provides, comprises the following steps:
A) weigh sodium alginate 0.1-2g with beaker, add 20-40ml distilled water, the transparent sparkling and crystal-clear shape of the most swelling formation State, for substrate 1;
B) weigh carbomer 0.01-2g with beaker, add 1-15ml distilled water, the transparent sparkling and crystal-clear shape of the most swelling formation State, drips 30% triethanolamine solution 0.04-0.4ml, is uniformly mixed, for substrate 2;
C) weigh arabic gum 0-2g, tragacanth 0-2g, safflower oil 0-5g, Rice oil 1-4g, add edge in mortar Same direction is fully ground, and adds 2-10ml distilled water inward, after hearing that crack forms colostrum, is gradually added into 0-10ml and steams Distilled water, is fully ground;
D) adding silk fibroin powder 0-4g, Margarita powder 0-6g in mortar, Bombyx Batryticatus powder 0-5g, ground and mixed is uniform;
E) adding green stone mud 0-5g, spaonin powder 0-6g, pearl essence 0-4g in mortar, ground and mixed is uniform;
F) adding substrate 1, substrate 2 in mortar, ground and mixed is uniform, adds 5% ethyl hydroxybenzoate propylene glycol solution 0-4ml, adds essence 0-0.4ml, is fully ground mix homogeneously, obtains whitening face cleaning facial treatment mask.
Various compositions in the present invention are as follows:
Fibroin has another name called fibroin albumen, is the natural polymer fibrin extracted from silkworm silk, containing 18 kinds of amino Acid, wherein glycine, alanine and serine account for more than 80% always formed.Aminoacid therein and small protein, It it is easily percutaneous absorption, it is provided that the nutritional labeling needed for skin whitening.
Active ingredient layering release in native fibroin hydrolyzed solution, 10 seconds infiltration skin skin coriums, effectively suppress Melanin generates, and controls pigment, promotes collagen protein synthesis, activating cell, improves the immunity of cell, promotes the oldest of skin Metabolic rate, helps to repair impaired skin histology, makes low and deep tired skin add life again, thus reduction is beautiful in very short time In vain, the skin of gloss.The Tang Dynasty Sun Simiao Thousand Golden Prescriptions, Ming Dynasty's Li Shizhen (1518-1593 A.D.) Compendium of Material Medica etc. are cured in nationality the most on the books, silkworm silk Natural skin-friendly ability fairly obvious.So fibroin can go deep into skin bottom, fundamentally skin whitening and have no side effect.
Margarita spreads white-skinned face function from ancient times, and in Margarita, trace element can promote that the quantity of SOD increases, increased activity.Margarita Contained selenium is the main matter manufacturing glutathion peroxidase, and this enzyme can be removed free radical as SOD, improve skin Color.Margarita powder particle diameter is superfine, so surface area is very big, has fabulous absorbability, can be adsorbed thereon by excess oil, can So that dead bark and pore deep layer dirt " are inhaled ", can effectively remove blackhead.It also has astriction simultaneously, can control oil Fat secretion allows the dry and comfortable cleaning of skin.Margarita powder can be with heat-clearing and toxic substances removing, cleaning skin, controls oil point, may additionally facilitate damaged tissues again Raw recovery.For oral administration can heat-clearing and toxic substances removing, oral administration and externally combines, and tackles small pox largely effective.Compendium of Material Medica already explicitly points out: " Margarita, except black dim ", Macro and microelements contained in Margarita powder can effectively be contained the increase of lipid peroxidation, thus effectively be gone Except mottle.
Margarita powder has preferable repair to the wound of skin (knife injury, burn, scald etc.).Margarita powder can promote Collagenocyte growth in human body, and collagenocyte is the main person who has rendered outstanding service promoting skin to regenerate, Margarita powder also has comparison to show simultaneously The antiinflammation write, it is possible to suppression inflammatory cell regeneration, prevents wound from deteriorating further.Group can be filled for wound outside Margarita powder Knit gap, adhesion vascular tissue, play its antiinflammatory, the effect promoting collagenocyte to grow, promote body cell to regenerate.
Recording on Shennong's Herbal, Bombyx Batryticatus has the effect of " go out black speck, makes us complexion good ".Bombyx Batryticatus contains aminoacid With activity mercerising element material ammonium oxalate, nutritious skin and beautification function.Protein contained by Bombyx Batryticatus has stimulation epithelium adipose gland, adjusts The effect of joint sex hormones secretion, thus the chloasma causing female sex hormone secretion imbalance has certain curative effect.Bombyx Batryticatus vitamin E Content be 9.89%, vitamin E can remove free radical, the senile plaque that lipid peroxidation inhibition is formed.Its contained active mercerising element Skin Cell can be promoted newborn, regulate sebum, improve skin microcirculation, can brighten sun-proof, eliminate pigmentation, keep skin bullet Property.Bombyx Batryticatus contains oxamide, and also the hydrolytic enzyme such as protease, chitinase, lipase can digest cutin, decomposes the anti-cicatrix of pigment and goes Acne control the effect of ecchymosis.
Green stone mud contains abundant mineral, containing materials such as calcium, magnesium, potassium, sodium, can strengthen connective tissue, for human body Skin institute is necessary.The green distinctive cavernous structure of stone mud, has absorbability free from worldly cares, can thoroughly remove skin deep layer dirt and oil Fat, makes skin keep clean state, to absorb other nutrition skin-protection compositions further.Peculiar negative charge and PH phase natural with skin The vigor of same pH-value energy activated cell, promotes skin metabolism.Green stone mud has sterilization, heals, prevents aging effect, Make that skin becomes is smooth, glossy, can supplement the nutrient needed for dry skin.
Spaonin powder can feel very salubrious fine and smooth on the face after washing one's face, has layer protecting film, the most smooth.The flesh that spaonin powder is washed Gloss soft as superficial shusu, is the health distributed from inside to outside, adheres to getting off, it is found that originally skin is coarse, pruritus, The situation of the long small pox of shirtfront back all can make moderate progress, and skin can be more and more healthy.
Rich in vitamin E in safflower oil, as a kind of Natural antioxidant, human body cell is divided by it, slow down aging has Important function, have in terms of beauty treatment and well act on: energy pore refining, alleviate xerosis cutis, delay skin aging, whitening flesh Skin, can repair the skin of sunburn, moreover it is possible to the generation of prevention skin carcinoma, is suitable for various skin quality.
Rice oil has moisturizing, antioxidative effect, and melanin can be suppressed to generate, and allows skin become fair and clear.And because of Fine for moisturizing effect, it is not suitable for ripe age or scaly dry skin person, skin care, prevents aging.
Pearlescent cosmetic is the ideal product that modern pursues, and it can make beauty lovers so beautiful that it excites men and the most any to skin Toxic and side effects.Pearlescent pigment has nontoxic, gorgeous natural pearly luster, applies quite varied in Cosmetic Manufacture.
In Cosmetic Manufacture kind, pearlescent pigment installs to content from outsourcing, can give full play to its hyperchromic effect.Muffin, Lip pomade, eye shadow, nial polish, aerosol hair spray all can make an addition in base material with the ratio of 3%, and produced gloss is the most charming. Pearlescent pigment can also be stearic with ethylene glycol etc. organic pearling agent share, make color and gloss more preferable.
This facial film prescription with the addition of substantial amounts of natural component.Fibroin can go deep into skin bottom, fundamentally beautiful White muscle skin and have no side effect;Margarita powder Titanium Dioxide, adsorbs oils and fats.The nutritious skin of Bombyx Batryticatus and beautification function.All things close With, supply skin-nourishing material, make deep skin nourish, thus skin more high resilience, more whitening.Each composition in prescription Complement each other, comprehensive nourishes rough skin, repair skin, supplement its various nutrient substance needed, make skin obtain from inside to outside Conditioning comprehensively, gradually recovers whitening honorable.
Facial film made by the present invention is light green, and viscosity is suitable, and fine and smooth uniform, stretchability is good, cool and comfortable, surely Qualitative good, fragrant.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Safflower oil in the present invention, arabic gum, ethyl hydroxybenzoate are commercially available.
Embodiment 1
The preparation of 1.1 Bombyx Batryticatus powder
Weigh Bombyx Batryticatus 50g, pulverize with pulverizer, cross 150 mesh sieves, standby.
The preparation of 1.2 whitening face cleaning facial treatment mask
A) weigh sodium alginate 0.3g with beaker, add 25ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, for Substrate 1;
B) weigh Acritamer 940 0.3g with beaker, add 10ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, Drip 30% triethanolamine solution 0.12ml, be uniformly mixed, for substrate 2;
C) weigh arabic gum 0.75g, tragacanth 0.2g, safflower oil 2.5g, Rice oil 2.0g, add edge in mortar Same direction is fully ground, and adds 8ml distilled water inward, after hearing that crack forms colostrum, is gradually added into 6ml distilled water, It is fully ground;
D) adding silk fibroin powder 0.8g, Margarita powder 0.6g in mortar, Bombyx Batryticatus powder 0.8g, ground and mixed is uniform;
E) adding green stone mud 0.5g, spaonin powder 0.3g, pearl essence 0.2g in mortar, ground and mixed is uniform;
F) adding substrate 1, substrate 2 in mortar, ground and mixed is uniform, adds 5% ethyl hydroxybenzoate propylene glycol solution 2ml, adds essence 0.16ml, is fully ground mix homogeneously, obtains whitening face cleaning facial treatment mask.
Embodiment 2
The preparation of 2.1 Bombyx Batryticatus powder
Weigh Bombyx Batryticatus 50g, pulverize with pulverizer, cross 100 mesh sieves, standby.
The preparation of 2.2 whitening face cleaning facial treatment mask
A) weighing sodium alginate 1g with beaker, add 38ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, for base Matter 1;
B) weigh carbomer 0.5g with beaker, add 15ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, dropping 30% triethanolamine solution 0.16ml, is uniformly mixed, for substrate 2;
C) weigh arabic gum 1g, tragacanth 0.5g, safflower oil 2g, Rice oil 2g, add in mortar along same side To being fully ground, add 8ml distilled water inward, after hearing that crack forms colostrum, be gradually added into 8ml distilled water, fully grind Mill;
D) adding silk fibroin powder 1g, Margarita powder 1g, Bombyx Batryticatus 1g in mortar, ground and mixed is uniform;
E) adding green stone mud 2g, spaonin powder 2g, pearl essence 0.5g in mortar, ground and mixed is uniform;
F) adding substrate 1, substrate 2 in mortar, ground and mixed is uniform, adds 5% ethyl hydroxybenzoate propylene glycol solution 3ml, adds essence 7d, is fully ground mix homogeneously, obtains whitening face cleaning facial treatment mask.
Embodiment 3:
The physical and chemical index of embodiment 1 is as follows:
3.1 character
This product is light green, and viscosity is suitable, and fine and smooth uniformly stretchability is good, cool and comfortable, good stability, and abnormal smells from the patient is fragrant The facial film of virtue.
3.2PH value checks
Dipping a small amount of facial film with the PH reagent paper of moistening, PH is 6-7.
3.3 caloric test
Facial film is packaged in transparence cosmetic bottle, observes without lamination in the refrigerator cold-storages about a week of 4 DEG C.In 55 DEG C calorstat in 24h, facial film is without layering, the phenomenon such as spoiled.
3.4 centrifugal test
Being packaged in by facial film in tool plug test tube, 3000r/min is centrifuged 20min, without lamination.
3.5 irritation tests, anaphylaxis are tested
White mice back cuts off hair, smears the facial film by embodiment 1,2 preparation respectively in cutting plucked position, and no painting portion Position compares, and result does not has zest and anaphylaxis.
Example 1 gram is applied in volunteer (15-65 year, 100 people) gesture and facial expression, observes after spending 30 minutes, does not all occur sending out Red, dermexanthesis, foaming phenomena.
3.6 room temperatures place experiment
Being placed in bottle for cosmetics by the made facial film of embodiment 1,2, room temperature stands to be investigated 6 months, without lamination, after using Feeling unchanged, abnormal smells from the patient is unchanged.
3.7 whitening and softening skin effects
Choose volunteer (15-65 year, 100 people), be applied to volunteer on the face with obtained facial film, after crossing 15min, use water Rinse out.Generally feeling that with rear volunteers skin slip is comfortable, feel is preferable, without greasy feeling.Skin moisturization is preferable, washes Afterwards without pruritus phenomenon.Through the continuous use of month, skin was substantially had rosy cheeks, pale can people.
Embodiment 4:
Skin whitening effect experimental
Choose the people of 100 15-65 year age brackets as object on probation, be arbitrarily divided into two groups, use embodiment system respectively Standby whitening face cleaning facial treatment mask washes one's face, and every day is the most each once, and the use time is one month.Wherein embodiment 1, in 50 examples, Man's 22 examples, female 28 example.Embodiment 2, in 50 examples, male 26 examples, female 24 example.Selected masculinity femininity skin complexion black and white degree is different.
Effect standard: effective, dark skin bleaches color, and dark skin improves significantly;Effectively, dark skin slowly becomes In vain, dark skin is improved.Invalid, dark skin does not bleach.The results are shown in Table 1:
Table 1 whitening experimental result
Effective (people) Effectively (people) Invalid (people) Total effective rate (%)
Embodiment 1 40 5 5 90
Embodiment 2 41 5 4 92
Embodiment 4
Whitening face cleaning facial treatment mask resultant effect is investigated
Feel to evaluate the effect of the whitening face cleaning facial treatment mask that embodiment produces following with on probation.The employing will of the people is adjusted Look into point system, choose the people of 100 15-65 year age brackets as object on probation, be arbitrarily divided into two groups, use embodiment system respectively Standby whitening face cleaning facial treatment mask is applied on the face, washes off with clear water after 15min.Every day is early, evening, the most once the use time was 1 Month.Every using effect total score is 5 points: 5 to be divided into best result, represents preferably, the most satisfied;4 are divided into very well;3 are divided into and can connect It is subject to;Less than 3 points is bad, it is impossible to accept.It is below every average, the results are shown in Table 2:
Table 2 resultant effect is investigated
Using effect The every average of embodiment 1 The every average of embodiment 2
Whitening 4.8 4.8
Alimentary 4.9 4.8
Moisture retention 4.8 4.9
Soil release performance 5 5
In sum, this whitening face cleaning facial treatment mask soil release performance is good, moisture retention, alimentary good, has certain whitening effect.

Claims (6)

1. a whitening face cleaning facial treatment mask, it is characterised in that described whitening face cleaning facial treatment mask is made up of following material:
Silk fibroin powder 0.8g
Margarita powder 0.6g
Bombyx Batryticatus powder 0.8g
Green stone mud 0.5g
Spaonin powder 0.3g
Pearl essence 0.2g
Safflower oil 2.5g
Rice oil 2.0g
Arabic gum 0.75g
Tragacanth 0.2g
30% triethanolamine solution 0.12ml
Acritamer 940 0.3g
Sodium alginate 0.3g
5% ethyl hydroxybenzoate propylene glycol solution 2ml
Distilled water 49ml
Essence 0.16ml.
2. a whitening face cleaning facial treatment mask, it is characterised in that described whitening face cleaning facial treatment mask is made up of following material:
Silk fibroin powder 1g
Margarita powder 1g
Bombyx Batryticatus powder 1g
Green stone mud 2g
Spaonin powder 2g
Pearl essence 0.5g
Safflower oil 2g
Rice oil 2g
Arabic gum 1g
Tragacanth 0.5g
30% triethanolamine solution 0.16ml
Carbomer 0.5g
Sodium alginate 1g
5% ethyl hydroxybenzoate propylene glycol solution 3ml
Distilled water 69ml
7, essence.
Whitening face cleaning facial treatment mask the most according to claim 1 and 2, it is characterised in that described essence be Fructus Citri Limoniae essence, Rose essence, osmanthus flower fragrance, peach flavor, flavoring pineapple essence, green cucumber essence, jasmin essence.
Whitening face cleaning facial treatment mask the most according to claim 1 and 2, it is characterised in that described Bombyx Batryticatus powder by with Prepared by lower section method:
Weigh Bombyx Batryticatus appropriate, pulverize with pulverizer, cross 100-150 mesh sieve, standby.
5. the preparation method of the whitening face cleaning facial treatment mask described in claim 1, it is characterised in that comprise the following steps:
A) weighing sodium alginate 0.3g with beaker, add 25ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, for substrate 1;
B) weigh Acritamer 940 0.3g with beaker, add 10ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, dropping 30% triethanolamine solution 0.12ml, is uniformly mixed, for substrate 2;
C) weigh arabic gum 0.75g, tragacanth 0.2g, safflower oil 2.5g, Rice oil 2.0g, add in mortar along same Direction is fully ground, and adds 8ml distilled water inward, after hearing that crack forms colostrum, is gradually added into 6ml distilled water, fully Grind;
D) adding silk fibroin powder 0.8g, Margarita powder 0.6g in mortar, Bombyx Batryticatus powder 0.8g, ground and mixed is uniform;
E) adding green stone mud 0.5g, spaonin powder 0.3g, pearl essence 0.2g in mortar, ground and mixed is uniform;
F) adding substrate 1, substrate 2 in mortar, ground and mixed is uniform, adds 5% ethyl hydroxybenzoate propylene glycol solution 2ml, adds Enter essence 0.16ml, be fully ground mix homogeneously, obtain whitening face cleaning facial treatment mask.
6. the preparation method of the whitening face cleaning facial treatment mask described in claim 2, it is characterised in that comprise the following steps:
A) weighing sodium alginate 1g with beaker, add 38ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, for substrate 1;
B) weigh carbomer 0.5g with beaker, add 15ml distilled water, the transparent sparkling and crystal-clear state of the most swelling formation, drip 30% Triethanolamine solution 0.16ml, is uniformly mixed, for substrate 2;
C) weigh arabic gum 1g, tragacanth 0.5g, safflower oil 2g, Rice oil 2g, add in mortar and fill in the same direction Divide and grind, add 8ml distilled water inward, after hearing that crack forms colostrum, be gradually added into 8ml distilled water, be fully ground;
D) adding silk fibroin powder 1g, Margarita powder 1g in mortar, Bombyx Batryticatus powder 1g, ground and mixed is uniform;
E) adding green stone mud 2g, spaonin powder 2g, pearl essence 0.5g in mortar, ground and mixed is uniform;
F) adding substrate 1, substrate 2 in mortar, ground and mixed is uniform, adds 5% ethyl hydroxybenzoate propylene glycol solution 3ml, adds Enter 7, essence, be fully ground mix homogeneously, obtain whitening face cleaning facial treatment mask.
CN201410229015.5A 2014-05-27 2014-05-27 A kind of whitening face cleaning facial treatment mask and preparation method thereof Active CN103989614B (en)

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CN104323969B (en) * 2014-11-14 2017-07-04 皖南医学院 A kind of nti-freckle antiphlogistic suncream and preparation method thereof
CN104840679B (en) * 2015-05-12 2019-12-24 廖万清 Pharmaceutical composition for treating pigmentation, external pharmaceutical preparation and preparation method
CN105267120B (en) * 2015-10-28 2018-06-22 皖南医学院 A kind of nourishing chest enlarge lotion containing natural plant extracts and preparation method thereof
CN106176556A (en) * 2016-08-31 2016-12-07 张进 A kind of removing acnes and controlling oil whitening cream
CN108542853A (en) * 2018-07-13 2018-09-18 哈尔滨伟平科技开发有限公司 A kind of production method of natural moisture preserving blush

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Inventor after: Zhao Ming

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