CN105769643B - A kind of water outlet moisturiser and preparation method thereof - Google Patents
A kind of water outlet moisturiser and preparation method thereof Download PDFInfo
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- CN105769643B CN105769643B CN201610057370.8A CN201610057370A CN105769643B CN 105769643 B CN105769643 B CN 105769643B CN 201610057370 A CN201610057370 A CN 201610057370A CN 105769643 B CN105769643 B CN 105769643B
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Abstract
The invention provides a kind of water outlet moisturiser, which is composed of the following components：Ring five dimethyl silicone polymer, dimethyl silicone polymer, 10/1 dimethyl silicone polymers of cetyl PEG/PPG, ring five dimethyl silicone polymer/Dimethicone Crosspolymer, essence, glycerine, butanediol, propane diols, panthenol, glycine betaine, sodium chloride, acrylic acid (ester) class/25 methacrylate copolymer of docosyl alcohol polyethers, NaOH, Sodium Hyaluronate, daisy flower extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation product, glycyrrhiza glabra root extract, false portulaca oleracea extracts, biological carbohydrate gum, Phenoxyethanol/Sensiva SC50, deionized water.The moisturiser good stability of the present invention, closure is good, moisture retention is lasting, while smearing sense with softly smooth.
Description
Technical field
The present invention relates to technical field of skin care, more particularly to a kind of moisturiser of discharging type and preparation method thereof.
Background technology
Physiologic Studies shows that the 70% of body weight is moisture, and skin is the water-storage reservoir of human body, and water content accounts for body
The 18～20% of weight.The skin of health is smooth moist and whippy, if skin water shortage, gently then causes dry skin,
Follow the string, produce wrinkle and premature aging；Heavy then cause skin to be chapped from the cold.Thus it is guaranteed that skin have abundance moisture for
The health for maintaining body is very important.For making skin keep sufficient moisture, in addition to ensureing amount of drinking water enough daily,
Also need to the volatilization of moisture of skin is hindered by the skin care item with performance of keeping humidity and scatter and disappear.
With the raising of the level of consumption, consumer increasingly focuses on the performance of keeping humidity of moisturizer and the skin sense for using.Mesh
Before, commercially available moisture retention skin care item are all oil-in-water traditional creams mostly, do not possess water proofing property, and performance of keeping humidity is not lasting, with
Shi Yin contains more oil so that when smearing consumer feel relatively stick greasy, especially the consumer of oily skin or
When comparing hot summer；And commercially available Water-In-Oil moisturiser moisturizing persistence is relatively preferable, but skin sense is bad mostly, or
Stability is not good.Therefore, for above-mentioned prior art problem, urgent need is developed a kind of moisture retention and persistently, does not clearly stick greasy, skin sense
Soft moisturiser.
Content of the invention
The purpose of the present invention is for technical problem to be solved above, there is provided a kind of skin sense is smooth, salubrious glutinous greasy, guarantor
The good discharging type moisturiser of wet performance.
It is a further object to provide the preparation method of the moisturiser.
In order to realize object above, the invention provides a kind of water outlet moisturiser, it is characterised in that by weight percentage by
Following components is constituted：Ring five dimethyl silicone polymer 3-10%, dimethyl silicone polymer 2-6%, cetyl PEG/PPG-10/1
Dimethyl silicone polymer 0.5-1.2%, ring five dimethyl silicone polymer/Dimethicone Crosspolymer 0.5-1.5%,
Essence 0.02-0.04%, glycerine 6-10%, butanediol 4-8%, propane diols 8-12%, panthenol 0.1-0.3%, glycine betaine 1-
4%, sodium chloride 0.4-1%, -25 methacrylate copolymer 0.5-1.2% of acrylic acid (ester) class/docosyl alcohol polyethers, hydrogen-oxygen
Change sodium 0.018-0.043%, Sodium Hyaluronate 0.01-0.08%, daisy flower extract 0.5-2%, kappaphycus algae extract
0.1-0.5%, chlorella/Lupinus albus protein fermentation product 0.01-0.1%, glycyrrhiza glabra root extract 0.01-0.1%, false
Purslane extract 0.1-2%, biological carbohydrate gum 0.1-1%, Phenoxyethanol/Sensiva SC50 0.3-0.4%, more than deionized water
Amount.
The present invention also provides the preparation method of the water outlet moisturiser, and its step is as follows：
(1) deionized water is added in water phase pot, is heated to 85-90 DEG C, add the hyalomitome scattered with propane diols
Sour sodium, homogeneous add glycine betaine, panthenol, sodium chloride, glycerine, butanediol to after without particle, stir to being completely dissolved, lower the temperature
To 60 DEG C, acrylic acid (ester) class/- 25 methacrylate copolymer of docosyl alcohol polyethers is added, 45 DEG C is cooled to, is sequentially added young bird
Chrysanthemum extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation product, glycyrrhiza glabra root extract, false horse
Sativa extract and biological carbohydrate gum, stir, add NaOH, obtain the first mixture after stirring；
(2) by ring five dimethyl silicone polymer, cetyl PEG/PPG-10/1 dimethyl silicone polymers, five poly dimethyl of ring
Siloxanes/Dimethicone Crosspolymer stirring homogeneous is added to completely agranular uniform viscous pasty state is formed
Dimethyl silicone polymer and essence, obtain the second mixture after stirring；
(3) under stirring, first mixture is slowly added in second mixture, then with 500 turns/
The speed stirring of min, and the speed homogeneous 3min with 2000 turns/min, obtain the 3rd mixture；
(4) Phenoxyethanol/Sensiva SC50 is added in the 3rd mixture, stirred with the speed of 700 turns/min,
And the speed homogeneous 4min with 2500 turns/min, then the speed stirring 6-8min with 600 turns/min, when viscosity reaches 7-9 ten thousand
During mpa.s, discharging.
The moisturiser system of the present invention is the Water-In-Oil water outlet system that science matches various ingredients composition, only contains in its oil phase
There is the oil less than 15%, mainly include cyclic materials silicone oil and low viscous silicone oil so that skin sense is smooth and non-greasy, water outlet
Hurry up, produce the sensation of water profit.As silicone oil is the grease of the difficult emulsification of comparison, the unstable of system is easily caused, the present invention only makes
With a small amount of silicon water-in-oil emulsifier cetyl PEG/PPG-10/1 dimethyl silicone polymers, so that it may ensure stablizing for the formula
Property, its emulsifying capacity is strong, is highly suitable to be applied in oil phase the W/O emulsification systems containing silicone elastomer gel or silicone oil, while
Silkiness can also be embodied and slide sense, bright color outward appearance, have the performances such as moisturizing, conditioning and wetting concurrently.Additionally, also containing a small amount of silicon in oil phase
Body (ring five dimethyl silicone polymer/Dimethicone Crosspolymer), can give and soft and smooth smear sense.Water
Glycerine, propane diols and butanediol in phase can provide moisture retention, can improve the low-temperature stability of product again；Acrylic acid (ester)
Class/- 25 methacrylate copolymer of docosyl alcohol polyethers is water phase thickener, and which changes water soon, while can strengthen the steady of system again
Qualitative.Other active components in water phase such as glycine betaine, Sodium Hyaluronate, kappaphycus alvarezi (Kappaphycus
Alvarezii) extract, chlorella (Chlorella vulgaris)/Lupinus albus (Lupinus albus) protein fermentation are produced
The mutually Synergistic such as thing and glycyrrhiza glabra (Glycyrrhiza glabra) root extract, on the one hand can synergy moisturizing, while
Also can enhance immunity, maintain human body balance, promote skin metabolism, play a part of shining skin, anti-oxidant, anti-aging；And
Daisy (Bellis perennis) flower extract, bacopa monnieri (Bacopa monniera) extract and biological carbohydrate gum are in moisturizing
While, also can antiallergic anti-inflammatory, calmness releive, mitigate the excitant of outer bound pair skin.
Compared with prior art, water outlet moisturiser of the invention is water in oil system, with good stability, closure
The outstanding representation such as persistently of good, moisture retention, while smearing sense with softly smooth, and gradually changes aquatic products unboiled water pearl, and salubrious water moistens,
Give consumer the use feeling of pleasure, be especially suitable for oily skin or summer uses.
Description of the drawings
Fig. 1 is the performance of keeping humidity result of the water outlet moisturiser of the present invention.
Specific embodiment
Technical scheme is described in further detail with reference to specific embodiment, but the present invention be not limited to
Lower embodiment.
It should be noted that unless otherwise indicated, various components used in the present invention are this area current material, can
Obtained by commercial channel purchase.
Embodiment 1
Get the raw materials ready by following percentage by weight：
Ring five dimethyl silicone polymer 3%, dimethyl silicone polymer 6%, cetyl PEG/PPG-10/1 poly dimethyl silicon
Oxygen alkane 0.5%, ring five dimethyl silicone polymer/Dimethicone Crosspolymer 1.5%, essence 0.02%, glycerine
6%, butanediol 4%, propane diols 12%, panthenol 0.1%, glycine betaine 1%, sodium chloride 0.4%, acrylic acid (ester) class/docosyl alcohol
- 25 methacrylate copolymer 0.5% of polyethers, NaOH 0.018%, Sodium Hyaluronate 0.08%, daisy flower extract
0.5%, kappaphycus algae extract 0.1%, chlorella/Lupinus albus protein fermentation product 0.1%, glycyrrhiza glabra root extract
0.01%, false portulaca oleracea extracts 2%, biological carbohydrate gum 0.1%, Phenoxyethanol/Sensiva SC50 0.3%, more than deionized water
Amount.Wherein, the part by weight of Phenoxyethanol and Sensiva SC50 is 9:1.
The water outlet moisturiser of the present invention is prepared according to the following steps：
(1) deionized water is added in water phase pot, is heated to 85-90 DEG C, add the hyalomitome scattered with propane diols
Sour sodium, appropriate homogeneous add glycine betaine, panthenol, sodium chloride, glycerine, butanediol, propane diols to after without particle, stir to complete
Dissolving, is cooled to 60 DEG C, after acrylic acid (ester) class/- 25 methacrylate copolymer of docosyl alcohol polyethers is dissipated with a small amount of moisture
Add, be cooled to 45 DEG C, sequentially add daisy flower extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation
Product, glycyrrhiza glabra root extract, false portulaca oleracea extracts and biological carbohydrate gum, stir, and add NaOH, and stirring is
Standby after even；
(2) by ring five dimethyl silicone polymer, five poly- diformazan of cetyl PEG/PPG-10/1 dimethyl silicone polymers and ring
Radical siloxane/Dimethicone Crosspolymer is added in a clean vacuum emulsification pot, suitably stirring or homogeneous
To completely agranular uniform viscous pasty state is formed, dimethyl silicone polymer and essence is added, standby after stirring；
(3) under stirring, mixture that the mixture in (1) the step of handling well is slowly pumped into step (2)
In, stirred with the speed of 500 turns/min after exhausting, and the speed homogeneous 3min with 2000 turns/min；
(4) Phenoxyethanol/Sensiva SC50 is added, is stirred with the speed of 700 turns/min, and the speed with 2500 turns/min
Degree homogeneous 4min, then the speed stirring 6-8min with 600 turns/min, when viscosity reaches ten thousand mpa.s of 7-9, discharging.
After testing (by GB), the various performance parameters of the water outlet moisturiser of the embodiment of the present invention 1 are as follows：
Lotion outward appearance：The semi-transparent uniform and smooth lotion of white；
Smell：Consistent with essence standard specimen smell；
Heat-resisting：45 DEG C, 1 month stable testing；
Cold-resistant：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing；
Smear sense：Smear on skin, gradually change water, smear the soft and smooth exquisiteness of sense, salubrious water profit.
Embodiment 2
Press following percentage by weight dispensing：
Ring five dimethyl silicone polymer 6%, dimethyl silicone polymer 4%, cetyl PEG/PPG-10/1 poly dimethyl silicon
Oxygen alkane 0.8%, ring five dimethyl silicone polymer/Dimethicone Crosspolymer 1%, essence 0.03%, glycerine 8%,
Butanediol 6%, propane diols 10%, panthenol 0.2%, glycine betaine 2%, sodium chloride 0.7%, acrylic acid (ester) class/docosyl alcohol polyethers-
25 methacrylate copolymers 0.8%, NaOH 0.028%, Sodium Hyaluronate 0.04%, daisy flower extract 1% are long
Heart Kappa algae extract 0.2%, chlorella/Lupinus albus protein fermentation product 0.05%, glycyrrhiza glabra root extract 0.05%,
False portulaca oleracea extracts 0.5%, biological carbohydrate gum 0.5%, Phenoxyethanol/Sensiva SC50 0.3%, deionized water surplus.Its
In, the part by weight of Phenoxyethanol and Sensiva SC50 is 9:1.
The water outlet moisturiser of the present invention is prepared according to the following steps：
(1) deionized water is added in water phase pot, is heated to 85-90 DEG C, add the hyalomitome scattered with propane diols
Sour sodium, appropriate homogeneous add glycine betaine, panthenol, sodium chloride, glycerine, butanediol to after without particle, stir to being completely dissolved,
60 DEG C are cooled to, are added after acrylic acid (ester) class/- 25 methacrylate copolymer of docosyl alcohol polyethers is dissipated with a small amount of moisture,
Be cooled to 45 DEG C, sequentially add daisy flower extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation product,
Glycyrrhiza glabra root extract, false portulaca oleracea extracts and biological carbohydrate gum, stir, add NaOH, after stirring
Standby；
(2) by ring five dimethyl silicone polymer, cetyl PEG/PPG-10/1 dimethyl silicone polymers, five poly dimethyl of ring
Siloxanes/Dimethicone Crosspolymer is added in a clean vacuum emulsification pot, and appropriate stirring or homogeneous are extremely
Completely agranular uniform viscous pasty state is formed, dimethyl silicone polymer and essence is added, standby after stirring；
(3) under stirring, the mixture in the step of handling well 1 is slowly pumped in the mixture of step 2, is taken out
Stirred with the speed of 500 turns/min after complete, and the speed homogeneous 3min with 2000 turns/min；
(4) Phenoxyethanol/Sensiva SC50 is added, is stirred with the speed of 700 turns/min, and the speed with 2500 turns/min
Degree homogeneous 4min, then the speed stirring 6-8min with 600 turns/min, when viscosity reaches ten thousand mpa.s of 7-9, discharging.
After testing (by GB), the various performance parameters of the water outlet moisturiser of the embodiment of the present invention 2 are as follows：
Lotion outward appearance：The semi-transparent uniform and smooth lotion of white；
Smell：Consistent with essence standard specimen smell；
Heat-resisting：45 DEG C, 1 month stable testing；
Cold-resistant：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing；
Smear sense：Smear on skin, gradually change water, smear the soft and smooth exquisiteness of sense, salubrious water profit.
Embodiment 3
Press following percentage by weight dispensing：
Ring five dimethyl silicone polymer 10%, dimethyl silicone polymer 2%, cetyl PEG/PPG-10/1 poly dimethyl silicon
Oxygen alkane 1.2%, ring five dimethyl silicone polymer/Dimethicone Crosspolymer 0.5%, essence 0.04%, glycerine
10%, butanediol 8%, propane diols 8%, panthenol 0.3%, glycine betaine 4%, sodium chloride 1%, acrylic acid (ester) class/docosyl alcohol gather
- 25 methacrylate copolymer 1.2% of ether, NaOH 0.043%, Sodium Hyaluronate 0.01%, daisy flower extract
2%, kappaphycus algae extract 0.5%, chlorella/Lupinus albus protein fermentation product 0.01%, glycyrrhiza glabra root extract
0.1%, false portulaca oleracea extracts 0.1%, biological carbohydrate gum 1%, Phenoxyethanol/Sensiva SC50 0.4%, more than deionized water
Amount.Wherein, the part by weight of Phenoxyethanol and Sensiva SC50 is 9:1.
The water outlet moisturiser of the present invention is prepared according to the following steps：
(1) deionized water is added in water phase pot, is heated to 85-90 DEG C, add the hyalomitome scattered with propane diols
Sour sodium, appropriate homogeneous add glycine betaine, panthenol, sodium chloride, glycerine, butanediol to after without particle, stir to being completely dissolved,
60 DEG C are cooled to, are added after acrylic acid (ester) class/- 25 methacrylate copolymer of docosyl alcohol polyethers is dissipated with a small amount of moisture,
Be cooled to 45 DEG C, sequentially add daisy flower extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation product,
Glycyrrhiza glabra root extract, false portulaca oleracea extracts and biological carbohydrate gum, stir, add NaOH, after stirring
Standby；
(2) by ring five dimethyl silicone polymer, five poly- diformazan of cetyl PEG/PPG-10/1 dimethyl silicone polymers and ring
Radical siloxane/Dimethicone Crosspolymer is added in a clean vacuum emulsification pot, suitably stirring or homogeneous
To completely agranular uniform viscous pasty state is formed, dimethyl silicone polymer and essence is added, standby after stirring；
(3) under stirring, the mixture in the step of handling well 1 is slowly pumped in the mixture of step 2, is taken out
Stirred with the speed of 500 turns/min after complete, and the speed homogeneous 3min with 2000 turns/min；
(4) Phenoxyethanol/Sensiva SC50 is added, is stirred with the speed of 700 turns/min, and the speed with 2500 turns/min
Degree homogeneous 4min, then the speed stirring 6-8min with 600 turns/min, when viscosity reaches ten thousand mpa.s of 7-9, discharging.
After testing (by GB), the various performance parameters of the water outlet moisturiser of the embodiment of the present invention 3 are as follows：
Lotion outward appearance：The semi-transparent uniform and smooth lotion of white；
Smell：Consistent with essence standard specimen smell；
Heat-resisting：45 DEG C, 1 month stable testing；
Cold-resistant：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing；
Smear sense：Smear on skin, gradually change water, smear the soft and smooth exquisiteness of sense, salubrious water profit.
Test example 1
Evaluate the moisturiser of embodiments in accordance with the present invention 1,2,3 and the commonly skin sense of commercially available moisturiser, moisturizing degree, water outlet
Sense and salubrious sense.Tried out using user and opinion poll point system, the people of 40 20-45 year age brackets is chosen as on probation right
As every using effect total score is 5 points：5 points is best result, represents very well, very satisfied；4 points is preferable；3 points is good；3 points
It is below bad, can not receives.It is below every average, the results are shown in Table 1：
Table 1
The result of table 1 shows, compared with commercially available common moisturiser, the water outlet moisturiser of embodiment of the present invention 1-3 has more
Excellent skin sense, more preferable moisturizing degree and go out talent for swimming, it is the general expression that for user, when the water outlet for smearing embodiment of the present invention 1-3 is protected
When wet white, skin refreshing and non-greasy.
Test example 2
Method of testing：Healthy volunteer 20, the male sex 10, women 10, the age was at 20～45 years old.In isoperibol
(21 ± 1 DEG C), relative humidity 50 ± 5%, take respectively embodiment of the present invention 1-3 water outlet moisturiser be applied to experimenter's left hand before
On the inside of arm on the inside of (4cm × 4cm) and right forearm (4cm × 4cm).Blank (not applying) at the same test, using skinanalysis apparatus
MPA 6 after 30min, 60min, 120min, 240min and 360min of sample is painted with, determines tested region and blank is right respectively
According to the skin moisture content in region, survey 5 times, evaluation result is represented with mean value, as a result as shown in Figure 1.
As seen from Figure 1, after the moisturiser for having used the present invention, in 30min, moisture steeply rises, and in test
6 hours in, always all apparently higher than blank group, the moisture of skin illustrates that the moisturiser has good moistening effect.
Claims (2)
1. a kind of water outlet moisturiser, it is characterised in that composed of the following components by weight percentage：Ring five dimethyl silicone polymer
3-10%, dimethyl silicone polymer 2-6%, cetyl PEG/PPG-10/1 dimethyl silicone polymer 0.5-1.2%, five poly- diformazan of ring
Radical siloxane/Dimethicone Crosspolymer 0.5-1.5%, essence 0.02-0.04%, glycerine 6-10%, butanediol 4-
8%, propane diols 8-12%, panthenol 0.1-0.3%, glycine betaine 1-4%, sodium chloride 0.4-1%, acrylic acid（Ester）Class/docosyl alcohol polyethers-
25 methacrylate copolymer 0.5-1.2%, NaOH 0.018-0.043%, Sodium Hyaluronate 0.01-0.08%, Daisy
Extract 0.5-2%, kappaphycus algae extract 0.1-0.5%, chlorella/Lupinus albus protein fermentation product 0.01-0.1%, light
Fruit licorice root extract 0.01-0.1%, false portulaca oleracea extracts 0.1-2%, biological carbohydrate gum 0.1-1%, Phenoxyethanol/ethylhexyl
Glycerine 0.3-0.4%, deionized water surplus；Wherein, the part by weight of Phenoxyethanol and Sensiva SC50 is 9:1.
2. the preparation method of water outlet moisturiser according to claim 1, its step are as follows：
（1）Deionized water is added in water phase pot, 85-90 DEG C is heated to, the Sodium Hyaluronate scattered with propane diols is added,
Homogeneous to after without particle adds glycine betaine, panthenol, sodium chloride, glycerine, butanediol, stirs to being completely dissolved, be cooled to 60
DEG C, add acrylic acid（Ester）Class/- 25 methacrylate copolymer of docosyl alcohol polyethers, is cooled to 45 DEG C, sequentially adds Daisy
Extract, kappaphycus algae extract, chlorella/Lupinus albus protein fermentation product, glycyrrhiza glabra root extract, bacopa monnieri
Extract and biological carbohydrate gum, stir, add NaOH, obtain the first mixture after stirring；
（2）By ring five dimethyl silicone polymer, cetyl PEG/PPG-10/1 dimethyl silicone polymers, five polydimethylsiloxanes of ring
Alkane/Dimethicone Crosspolymer stirring homogeneous adds poly- two to completely agranular uniform viscous pasty state is formed
Methylsiloxane and essence, obtain the second mixture after stirring；
（3）Under stirring, first mixture is slowly added in second mixture, then with 500 turns/min
Speed stirring, and the speed homogeneous 3min with 2000 turns/min obtains the 3rd mixture；
（4）Phenoxyethanol/Sensiva SC50 is added in the 3rd mixture, is stirred with the speed of 700 turns/min, and with
The speed homogeneous 4min of 2500 turns/min, then the speed stirring 6-8min with 600 turns/min, when viscosity reaches ten thousand mpa.s of 7-9
When, discharging.
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| CN106420792A (en) * | 2016-09-21 | 2017-02-22 | 百奥迈科生物技术有限公司 | Micro-nucleic acid acne-removing compound |
| CN107753375A (en) * | 2017-10-31 | 2018-03-06 | 山东朱氏堂医疗器械有限公司 | A kind of dendrobium candidum globule sleep mask and preparation method thereof |
| CN108078854B (en) * | 2018-01-10 | 2019-01-08 | 壹田（广州）生活健康用品有限公司 | Hand frost and preparation method thereof is repaired in a kind of moisturizing |
| CN109431865B (en) * | 2018-11-01 | 2021-11-30 | 汕头市亚联药业有限公司 | Water-bursting cream for people staying up all night and preparation thereof |
| CN110101625A (en) * | 2019-06-14 | 2019-08-09 | 芳香世家化妆品(广州)有限公司 | A kind of nutrition restorative facial cream |
| CN112294732A (en) * | 2020-07-01 | 2021-02-02 | 西安博和医疗科技有限公司 | Moisturizing composition and preparation method thereof |
| CN113876642B (en) * | 2021-11-12 | 2023-10-20 | 湖北省麦诗特生物科技有限公司 | A facial cream composition containing lipid nanoparticle with moisturizing effect and its preparation method |
| CN115192478B (en) * | 2022-06-30 | 2023-10-17 | 广东柏俐臣生物科技有限公司 | Water-in-oil type physical sun protection emulsion with high stability and preparation method thereof |
| CN115737517A (en) * | 2022-11-28 | 2023-03-07 | 上海臻臣化妆品有限公司 | Moisturizing face cream |
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| CN103735444B (en) * | 2013-12-12 | 2015-11-25 | 诺斯贝尔(中山)无纺日化有限公司 | A kind of Multifunctional CC cream |
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