CN106176567B - A kind of double-deck facial treatment milk and preparation method thereof - Google Patents
A kind of double-deck facial treatment milk and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of double-deck facial treatment milk and preparation method thereof, it is desirable to provide one kind can promote cell metabolism, the good emulsion of moisturizing effect；The emulsion is mainly prepared from the following materials：EDETATE SODIUM, polyglutamic acid, glycerine, polyethylene glycol 400, dipropylene glycol, the rilanit specials of PEG 40, myristoyl glutamate sodium, the laureths 25 of PPG 25, ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, phytosterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat, radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/Sensiva SC50, essence, surplus is deionized water；Belong to cosmetic technical field.
Description
Technical field
The present invention provides a kind of emulsion, is a kind of double-deck facial treatment milk, the invention further relates to the double-deck skin care specifically
The preparation method of emulsion；Belong to cosmetic technical field.
Background technology
Toner and facial treatment milk are in our daily lifes essential to skin care.And generally for seeking product formulation
Stability, existing toner and emulsion nearly all are individually separated using on the market.
But in recent years, consider from viewpoints such as the conveniences used, consumer it is expected that a kind of while having can be obtained
The novel cosmetic of the use feeling of adornment water and emulsion.In these novel cosmetics, it is desirable to which moisture is more, has during use
There is the low viscous water moisture feeling of toner, while also there is the lasting moisture feeling of emulsion.At present, in the market this kind of product is also fewer,
Similar products existing for minority typically all have certain viscosity, and use skin sense not in order to ensure the stability of its shelf life
It is good, therefore in order to meet the use demand of consumer, it is necessary to develop that a kind of viscosity is low, emulsion stability is high, skin sense is good and
Easy-to-use cosmetics.
The content of the invention
In view of the above-mentioned problems, it is an object of the invention to provide a kind of double-deck facial treatment milk, when the emulsion is stood emulsion layer and
Water layer separate, upper strata moisten elite breast, lower floor's moisture retention water, when in use by gently vibrate be easy for it is dispersed, and
The emulsion layer and water layer for being separated into script again are stood after use, so as to form the low and stable Separated two-layer skin care milk of viscosity
Liquid, have moisturizing effect concurrently, cell metabolism can be promoted, strengthen cell, make skin recover water profit elasticity；The present invention's is another
One purpose there is provided the preparation method of above-mentioned double-deck facial treatment milk.
To achieve these goals, first technical scheme of use is such to the present invention：
A kind of double-deck facial treatment milk, mainly it is prepared by following raw material by mass percentage：EDETATE SODIUM 0.05-
0.1%, polyglutamic acid 0.01-0.1%, glycerine 2-6%, PEG-4000 4-12%, dipropylene glycol 3-8%, PEG-40 hydrogen
Change castor oil 0.5-2%, the 0.2-0.6% of myristoyl glutamate sodium 0.02-0.15%, PPG-25- laureth -25, ring
Five dimethyl silicone polymer 1-4%, Nexbase 2004 2-8%, tocopherol acetate 0.2-1%, caprylic/capric triglyceride 2-
6%, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-1.0%, Parleam 2-6%, Butyrospermum parkii fruit fat
0.5-2%, radix scutellariae root extract 0.22%-0.76%, kuh-seng root extract 0.14%-0.62%, swollen fruit Radix root extract
0.14%-0.62%, Herba Verbenae 0.2-1%, Bacillus acidi lactici/bear's weed tunning extract 0.5-2%, benzene oxygen
Ethanol/Sensiva SC50 0.8-1%, essence 0.05-0.15%, surplus are deionized water.
Further, above-mentioned a kind of double-deck facial treatment milk, in addition to banana leaf extract 0.1-1.2%.
Further, above-mentioned a kind of double-deck facial treatment milk, in addition to Juniperus communis berry extract 0.2-0.8%.
Further, above-mentioned a kind of double-deck facial treatment milk, in addition to Lens culinaris berry extract 0.2-0.6%.
Further, above-mentioned a kind of double-deck facial treatment milk, described double-deck facial treatment milk, upper strata is white breast after standing
Liquid, lower floor are translucent liquid, and bilevel ratio is 1:1, it is white uniformity emulsion after shaking up, pH 5.3-6.0, without viscous
Degree.
To prepare above-mentioned double-deck facial treatment milk, another technical scheme of the invention is such：
1) each component is weighed；
2) ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, the caprylic/capric weighed step 1)
Triglycerides, phytosterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase
In pot, stirring is warming up to 75-85 DEG C, and insulation is standby after dissolving completely, obtains oil phase；
3) EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, the PEG-40 hydrogen weighed step 1)
Change castor oil, myristoyl glutamate sodium, PPG-25- laureths -25 and water to be placed in emulsification pot, be heated with stirring to 80-
90 DEG C, insulated and stirred is complete to all dissolution of raw material, obtains aqueous phase；
4) under stirring, oil phase prepared by step 2) is slowly pumped into the aqueous phase in emulsification pot, homogeneous 2-
After 4min, insulated and stirred 10-20min is complete to defoaming, and is cooled to 40-45 DEG C, adds radix scutellariae root extract, radix sophorae extraction
Thing, swollen fruit Radix root extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/second
Base hexyl glycerine, essence, discharge after stirring, and produce double-deck facial treatment milk.
In addition, step 4) also include addition banana leaf extract, Juniperus communis berry extract, Lens culinaris berry extract wherein it
One or any combination.
Compared with prior art, the beneficial effect of technical scheme provided by the invention：
1st, the polyglutamic acid added in technical scheme provided by the invention can increase skin hyaluronic acid and natural moisture preserving because
The content of son, promote skin to be better than hyaluronic acid and collagen to maintaining the absorption of composition, moistening effect, at the same can be long when
Between keep skin moisten, strengthen skin elasticity, reduce skin wrinkle.
2nd, contain in the Herba Verbenae added in technical scheme provided by the invention has similar ammonia to keratoprotein
Base acid structure, skin-friendly is good, can penetrate into skin bottom, and deep layer imports moisture, and skin deep layer is effectively goed deep into long-acting moisturizing in 24 hours,
Reach skin water and oil balance, be the efficient skin moisture-keeping factor, the balance skin cell control under conditions of over-drying and damp and hot
Outlet capacity, resist environmental contaminants and injured to caused by skin, promote original Skin Cell vigor, safeguard normal new old generation
Thank.
3rd, the Bacillus acidi lactici added in technical scheme provided by the invention/bear's weed tunning extract, purchased from wide
Zhou Nuoran bio tech ltd, containing abundant natural polysaccharide body and glycoprotein, the glycoprotein structure of similar human skin,
Wettability and Nutrient Absorption can be promoted by providing high skin-friendly, have the function that moisturizing, moist, have more preferable moisture retention than aloe
Can, and have the function that to maintain long-acting moisturizing degree, make skin feel younger immediately, it is more soft and smooth, also with calm flesh
The effect of skin, stimulation can be reduced, such as the inflammation as caused by dry skin, erythema etc..
4th, in technical scheme provided by the invention, oil phase raw material is by selected rational collocation so that skin care of the invention
Emulsion can make skin become soft when keeping preferable spreadability, while also have preferable moisture-keeping efficacy.Nexbase 2004,
Parleam, tocopherol acetate collaboration provide uniqueness, clearly non-greasy, abundant moist skin sense, tocopheryl acetate
Ester also has oxidation resistant effect；Butyrospermum parkii fruit fat (shea butter) is a kind of pure natural vegetable fat, is had superpower
Antioxidant effect, it is gentle non-stimulated, contain the abundant non-saponified composition being easily absorbed by the body, can be formed and protected in skin surface
Cuticula, have the function that moisturizing, deep layer moisten, prevent scaly dry skin from ftractureing；Phytosterol/octyl dodecanol lauroyl glutamate
Ester, is a kind of emollient from glutamic acid, natural acid, higher alcohol and phytosterol, and research has shown that it can be as god
Liquid crystal film is equally formed through acid amides, therefore, its emollient can compare favourably with ceramide, help skin stabilized liposome wall
Barrier prevents moisture loss, increases skin water content, prevention external stimulus infringement, lifting skin moisturizing and tender degree.
5th, double-deck facial treatment milk provided by the invention is on the basis of oil phase and aqueous phase are each provided with moisturizing, with polyglutamic
It is acid, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, radix scutellariae root extract, kuh-seng root extract, swollen
Fruit licorice root extract, banana leaf extract, Juniperus communis berry extract, Lens culinaris berry extract etc. cooperate with, and have moisturizing reparation work concurrently
With keeping skin moisturizing, promote cell metabolism, strengthen cell, make skin recover elasticity, lift the tender degree of skin.
6th, double-deck facial treatment milk provided by the invention is a kind of no viscosity, emulsifies the excellent cosmetics of ageing stability,
Emulsion layer and water layer separation, upper strata moisten elite breast, lower floor's moisture retention water, are easy for ground by gently vibrating when in use during standing
It is dispersed, and using rear standing and the emulsion layer and water layer of script are separated into, so as to form stable Separated two-layer shield
Skin emulsion, novel appearance are beautiful, have both had the low viscous water moisture feeling of toner during use, and have been provided simultaneously with the excellent of emulsion and have moistened
Sense, has very excellent use feeling and sense of touch.
Embodiment
Technical scheme is described in further detail with reference to specific embodiment, but the invention is not restricted to following
Embodiment.It is worth noting that, unless otherwise indicated, various components used in the present invention are this area current material, can
Bought by commercial channel and obtain or be made by existing method.
Radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root extract are purchased in Shanghai Jia Ye Industrial Co., Ltd.s,
Banana leaf extract is purchased in Shaanxi Yong Yuan Bioisystech Co., Ltd；Juniperus communis berry extract is purchased in beautiful a surname's trade (Shanghai)
Co., Ltd；Lens culinaris fruit (Lentil) extract is purchased in Changsha Rui Ding bio tech ltd；Herba Verbenae is purchased
In Guangzhou Hui Lang bio tech ltd；Bacillus acidi lactici/bear's weed tunning extract is purchased so biological in Guangzhou promise
Science and Technology Ltd..
Embodiment 1
A kind of double-deck facial treatment milk provided by the invention, based on gross weight 100g, by the raw material preparation of following mass number
Into：EDETATE SODIUM 0.1g, polyglutamic acid 0.05g, glycerine 5g, PEG-4000 8g, dipropylene glycol 5g, PEG-40 hydrogenation castor
Sesame oil 1g, myristoyl glutamate sodium 0.05g, PPG-25- laureth -25 0.3g, ring five dimethyl silicone polymer 2g,
Nexbase 2004 6g, tocopherol acetate 0.3g, caprylic/capric triglyceride 4g, phytosterol/octyl dodecanol lauroyl paddy
Propylhomoserin ester 0.5g, Parleam 4.5g, Butyrospermum parkii fruit fat 1.2g, radix scutellariae root extract 0.22g, kuh-seng root extract
0.14g, swollen fruit Radix root extract 0.14g, Herba Verbenae 0.8g, Bacillus acidi lactici/bear's weed tunning extract
2g, Phenoxyethanol/Sensiva SC50 0.9g, essence 0.05g, surplus is water.
Above-mentioned double-deck facial treatment milk preparation method is as follows：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 85 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80 DEG C, insulated and stirred is extremely
All dissolution of raw material are complete, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 4min, insulated and stirred
10min is complete to defoaming, and is cooled to 45 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root extract, horse
Whip grass extract, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/Sensiva SC50, essence, stirring are equal
Discharged after even, produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 1 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 5.3, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Embodiment 2
The double-deck facial treatment milk of another kind provided by the invention, based on gross weight 100g, by it is following by mass percentage
Raw material is prepared：EDETATE SODIUM 0.05g, polyglutamic acid 0.01g, glycerine 6g, PEG-4000 4g, dipropylene glycol 7g,
The 0.2g of Cremophor RH40 0.5g, myristoyl glutamate sodium 0.02g, PPG-25- laureth -25, ring five poly- two
Methylsiloxane 1g, Nexbase 2004 8g, tocopherol acetate 0.2g, caprylic/capric triglyceride 3.5g, phytosterol/pungent
Base lauryl alcohol lauroyl glutamate ester 0.7g, Parleam 6g, Butyrospermum parkii fruit fat 0.5g, radix scutellariae root extract 0.3g,
Kuh-seng root extract 0.2g, swollen fruit Radix root extract 0.2g, banana leaf extract 1.2g, Herba Verbenae 1g, lactic acid bar
Bacterium/bear's weed tunning extract 1.8g, Phenoxyethanol/Sensiva SC50 1g, essence 0.06g, surplus is water.
Above-mentioned double-deck facial treatment milk preparation method is as follows：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 75 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 90 DEG C, insulated and stirred is extremely
All dissolution of raw material are complete, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2min, insulated and stirred
20min is complete to defoaming, and is cooled to 40 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root extract, perfume (or spice)
Any of several broadleaf plants leaf extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/ethylhexyl are sweet
Oil, essence, discharge after stirring, produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 2 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 5.6, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Embodiment 3
The double-deck facial treatment milk of another kind provided by the invention, based on gross weight 100g, by it is following by mass percentage
Raw material is prepared：EDETATE SODIUM 0.06g, polyglutamic acid 0.03g, glycerine 4g, PEG-4000 9g, dipropylene glycol 4g,
The 0.4g of Cremophor RH40 0.8g, myristoyl glutamate sodium 0.08g, PPG-25- laureth -25, ring five poly- two
Methylsiloxane 3g, Nexbase 2004 3g, tocopherol acetate 1g, caprylic/capric triglyceride 6g, phytosterol/octyl group ten
Glycol lauroyl glutamate ester 0.3g, Parleam 5g, Butyrospermum parkii fruit fat 1g, radix scutellariae root extract 0.6g, radix sophorae
Extract 0.4g, swollen fruit Radix root extract 0.4g, Juniperus communis berry extract 0.8g, Herba Verbenae 0.6g, Bacillus acidi lactici/
Bear's weed tunning extract 0.8g, Phenoxyethanol/Sensiva SC50 0.9g, essence 0.08g, surplus is water.
The preparation method of the double-deck facial treatment milk, comprises the following steps：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 75-85 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80-90 DEG C, insulation is stirred
Mix complete to all dissolution of raw material, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2-4min, insulation is stirred
It is complete to defoaming to mix 10-20min, is cooled to 40-45 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root and carries
Take thing, Juniperus communis berry extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/second
Base hexyl glycerine, essence, discharge after stirring, and produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 3 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 5.46, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Embodiment 4
The double-deck facial treatment milk of another kind provided by the invention, based on gross weight 100g, by it is following by mass percentage
Raw material is prepared：EDETATE SODIUM 0.07g, polyglutamic acid 0.07g, glycerine 3g, PEG-4000 10g, dipropylene glycol 6g,
The 0.5g of Cremophor RH40 1.2g, myristoyl glutamate sodium 0.1g, PPG-25- laureth -25, ring five poly- two
Methylsiloxane 4g, Nexbase 2004 2g, tocopherol acetate 0.8g, caprylic/capric triglyceride 3g, phytosterol/octyl group
Lauryl alcohol lauroyl glutamate ester 0.1g, Parleam 3g, Butyrospermum parkii fruit fat 1.5g, radix scutellariae root extract 0.5g, hardship
Join root extract 0.3g, swollen fruit Radix root extract 0.3g, Lens culinaris berry extract 0.6g, Herba Verbenae 0.5g, lactic acid bar
Bacterium/bear's weed tunning extract 1.5g, Phenoxyethanol/Sensiva SC50 0.8g, essence 0.1g, surplus is water.
The preparation method of the double-deck facial treatment milk, comprises the following steps：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 75-85 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80-90 DEG C, insulation is stirred
Mix complete to all dissolution of raw material, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2-4min, insulation is stirred
It is complete to defoaming to mix 10-20min, is cooled to 40-45 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root and carries
Take thing, Lens culinaris berry extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/ethyl
Hexyl glycerine, essence, discharged after stirring, produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 4 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 5.8, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Embodiment 5
The double-deck facial treatment milk of another kind provided by the invention, based on gross weight 100g, by it is following by mass percentage
Raw material is prepared：EDETATE SODIUM 0.08g, polyglutamic acid 0.09g, glycerine 2g, PEG-4000 12g, dipropylene glycol 3g,
The 0.6g of Cremophor RH40 1.5g, myristoyl glutamate sodium 0.12g, PPG-25- laureth -25, ring five poly- two
Methylsiloxane 3.5g, Nexbase 2004 4g, tocopherol acetate 0.7g, caprylic/capric triglyceride 2g, phytosterol/pungent
Base lauryl alcohol lauroyl glutamate ester 0.9g, Parleam 2g, Butyrospermum parkii fruit fat 0.8g, radix scutellariae root extract 0.7g,
Kuh-seng root extract 0.5g, swollen fruit Radix root extract 0.5g, banana leaf extract 0.1g, Lens culinaris berry extract 0.2g, horsewhip
Careless extract 0.4g, Bacillus acidi lactici/bear's weed tunning extract 0.5g, Phenoxyethanol/Sensiva SC50 1g, essence
0.12g, surplus are water.
The preparation method of above-mentioned double-deck facial treatment milk, comprises the following steps：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 75-85 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80-90 DEG C, insulation is stirred
Mix complete to all dissolution of raw material, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2-4min, insulation is stirred
It is complete to defoaming to mix 10-20min, is cooled to 40-45 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root and carries
Take thing, banana leaf extract, Lens culinaris berry extract 0.2g, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extraction
Thing, Phenoxyethanol/Sensiva SC50, essence, discharge after stirring, and produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 5 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 6.0, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Embodiment 6
The double-deck facial treatment milk of another kind provided by the invention, based on gross weight 100g, by it is following by mass percentage
Raw material is prepared：EDETATE SODIUM 0.09g, polyglutamic acid 0.1g, glycerine 3g, PEG-4000 6g, dipropylene glycol 8g,
The 0.4g of Cremophor RH40 2g, myristoyl glutamate sodium 0.15g, PPG-25- laureth -25, five poly- diformazan of ring
Radical siloxane 2.5g, Nexbase 2004 5.5g, tocopherol acetate 0.5g, caprylic/capric triglyceride 5g, phytosterol/pungent
Base lauryl alcohol lauroyl glutamate ester 1g, Parleam 4g, Butyrospermum parkii fruit fat 2g, radix scutellariae root extract 0.76g, kuh-seng
Root extract 0.62g, swollen fruit Radix root extract 0.62g, banana leaf extract 0.5g, Juniperus communis berry extract 0.2g, Lens culinaris
Berry extract 0.3g, Herba Verbenae 0.2g, Bacillus acidi lactici/bear's weed tunning extract 1g, Phenoxyethanol/ethyl
Hexyl glycerine 0.8g, essence 0.15g, surplus is water.
The preparation method of the double-deck facial treatment milk, comprises the following steps：
(1) by ring five dimethyl silicone polymer, Nexbase 2004, tocopherol acetate, caprylic/capric triglyceride, plant
Thing sterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot, and stirring rises
For temperature to 75-85 DEG C, insulation is standby after dissolving completely, obtains oil phase；
(2) by EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, Cremophor RH40, meat
Myristoyl sodium glutamate, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80-90 DEG C, insulation is stirred
Mix complete to all dissolution of raw material, obtain aqueous phase；
(3) under stirring, oil phase is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2-4min, insulation is stirred
It is complete to defoaming to mix 10-20min, is cooled to 40-45 DEG C, adds radix scutellariae root extract, kuh-seng root extract, swollen fruit Radix root and carries
Take thing, banana leaf extract, Juniperus communis berry extract, Lens culinaris berry extract, Herba Verbenae, Bacillus acidi lactici/bear's weed
Tunning extract, Phenoxyethanol/Sensiva SC50, essence, discharge after stirring, and produce double-deck facial treatment milk.
After testing, the properties of the double-deck facial treatment milk of the embodiment of the present invention 6 are as follows：
Outward appearance：Bilayer, upper strata are white emulsion, and lower floor is half transflective liquid, and bilevel ratio is 1:1, be after shaking up
White uniformity emulsion, pH 5.86, no viscosity.
Smell：It is consistent with essence standard specimen smell；
Heat resistance：45 DEG C, 1 month stable testing；
Cold tolerance：- 18 DEG C, 1 month low-temperature stabilization；
Alternation of chills and fever：1 month stable testing.
Experiment effect
1st, human trial
Double-deck facial treatment milk and common commercially available surfactant and facial treatment milk prepared by the embodiment of the present invention 1,3,5 is compared
Compared with their moisture retention, moistness, sticky sense and excitant of grading.Using user is on probation and opinion poll point system, choose
The people of 100 20-45 year age brackets is as object on probation, usage time one month.It is below every average, the results are shown in Table
1：
Table 1
| Test event | Embodiment 1 | Embodiment 3 | Embodiment 5 | Common commercially available surfactant | Common commercially available facial treatment milk |
| Moisture retention | 4.7 | 4.8 | 4.9 | 3.5 | 4.2 |
| Moistness | 4.8 | 4.9 | 5.0 | 3.2 | 4.5 |
| Sticky sense | 4.5 | 4.6 | 4.9 | 4.5 | 3.0 |
Explanation：
5 points represent that product moisture retention, moistness are fine；Clearly, it is completely not glutinous greasy；
4 points represent that product moisture retention, moistness are good；Clearly, it is somewhat glutinous greasy；
3 points represent that product moisture retention, moistness are preferable；It is a little glutinous greasy；
2 points represent that product moisture retention, moistness are general；Compare glutinous greasy；
1 point represents that product moisture retention, moistness are bad；It is very glutinous greasy.
The result of table 1 shows that double-deck facial treatment milk skin sense prepared by the embodiment of the present invention 1,3,5 is salubrious, moisture retention, moistens
Property be superior to commercially available common surfactant and facial treatment milk, sticky sense are significantly lower than certain commercially available common facial treatment milk.User is universal
Represent, smear the double-deck facial treatment milk of the embodiment of the present invention 1,3,5, skin sense is good, completely non-stimulated, is provided simultaneously with surfactant and shield
The moisture retention and moistness of skin emulsion, easy to use, after using one month, skin water moisture feeling is obviously improved, and skin is gradually extensive
Complex elasticity, become tender, fine and smooth..
2nd, moisture-keeping efficacy evaluation experimental
According to light industry standard QB/T 4256-2011 cosmetics moisture-keeping efficacy evaluation guides, Example 2,4,6 is made
Standby double-deck facial treatment milk determines moistening effect as test specimen.
Method of testing：Healthy volunteer 40, the age was at 20~50 years old.In isoperibol (22 ± 1 DEG C), relative humidity 50
± 5%, rest 1 hour after.By (2.0 ± 0.1) mg/cm2 dosage samples be coated in subject's left hand inner forearm (4cm ×
4cm) and on the inside of right forearm (4cm × 4cm).Blank control (not applying) while test.Respectively be painted with 0.5h, 1h of sample, 2h,
4h, 6h test the moisture of Corneometer CM825 test skins with moisture content of skin, calculate moisture difference and water
Conjunction rate.Evaluation result is as follows：
The moisture test result of table 1
The moisture difference test result of table 2
The hydration rate testing result of table 3
It can be seen from table 1,2 after the double-deck facial treatment milk using embodiments of the invention 2,4,6, with respect to initial value,
Compared with blank control group, there is significant difference (p ＜ in moisture result with the double-deck facial treatment milk sample of the present invention
0.05)；The double-deck facial treatment milk sample of the present invention started significant difference be present with blank group after 0.5 hour；And in 1h extremely
In moisture content change in a period of 6h, double-deck facial treatment milk sample moisture of the invention is substantially always above blank
Group.
As can be seen from Table 3, the hydration rate of double-deck facial treatment milk sample of the invention is significantly higher than blank control always, with
Blank, which compares, keeps moisture positive effect, and after using 6 hours, hydration rate remains at 30% or so, illustrates the present invention
Double-deck facial treatment milk there is preferable moistening effect.
Claims (6)
1. a kind of double-deck facial treatment milk, it is characterised in that be prepared by following raw material by mass percentage：EDETATE SODIUM
0.05-0.1%, polyglutamic acid 0.01-0.1%, glycerine 2-6%, PEG-4000 4-12%, dipropylene glycol 3-8%,
The 0.2- of Cremophor RH40 0.5-2%, myristoyl glutamate sodium 0.02-0.15%, PPG-25- laureth -25
0.6%, ring five dimethyl silicone polymer 1-4%, Nexbase 2004 2-8%, tocopherol acetate 0.2-1%, caprylic/capric are sweet
Three ester 2-6% of oil, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-1.0%, Parleam 2-6%, butter
Fruit tree fruit fat 0.5-2%, radix scutellariae root extract 0.22%-0.76%, kuh-seng root extract 0.14%-0.62%, swollen fruit Radix
Root extract 0.14%-0.62%, Herba Verbenae 0.2-1%, Bacillus acidi lactici/bear's weed tunning extract 0.5-
2%, Phenoxyethanol/Sensiva SC50 0.8-1%, essence 0.05-0.15%, surplus is deionized water.
2. a kind of double-deck facial treatment milk, it is characterised in that be prepared by following raw material by mass percentage：EDETATE SODIUM
0.05-0.1%, polyglutamic acid 0.01-0.1%, glycerine 2-6%, PEG-4000 4-12%, dipropylene glycol 3-8%,
The 0.2- of Cremophor RH40 0.5-2%, myristoyl glutamate sodium 0.02-0.15%, PPG-25- laureth -25
0.6%, ring five dimethyl silicone polymer 1-4%, Nexbase 2004 2-8%, tocopherol acetate 0.2-1%, caprylic/capric are sweet
Three ester 2-6% of oil, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-1.0%, Parleam 2-6%, butter
Fruit tree fruit fat 0.5-2%, radix scutellariae root extract 0.22%-0.76%, kuh-seng root extract 0.14%-0.62%, swollen fruit Radix
Root extract 0.14%-0.62%, Herba Verbenae 0.2-1%, Bacillus acidi lactici/bear's weed tunning extract 0.5-
2%, Phenoxyethanol/Sensiva SC50 0.8-1%, essence 0.05-0.15%, banana leaf extract 0.1-1.2%, surplus is
Deionized water.
3. a kind of double-deck facial treatment milk, it is characterised in that be prepared by following raw material by mass percentage：EDETATE SODIUM
0.05-0.1%, polyglutamic acid 0.01-0.1%, glycerine 2-6%, PEG-4000 4-12%, dipropylene glycol 3-8%,
The 0.2- of Cremophor RH40 0.5-2%, myristoyl glutamate sodium 0.02-0.15%, PPG-25- laureth -25
0.6%, ring five dimethyl silicone polymer 1-4%, Nexbase 2004 2-8%, tocopherol acetate 0.2-1%, caprylic/capric are sweet
Three ester 2-6% of oil, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-1.0%, Parleam 2-6%, butter
Fruit tree fruit fat 0.5-2%, radix scutellariae root extract 0.22%-0.76%, kuh-seng root extract 0.14%-0.62%, swollen fruit Radix
Root extract 0.14%-0.62%, Herba Verbenae 0.2-1%, Bacillus acidi lactici/bear's weed tunning extract 0.5-
2%, Phenoxyethanol/Sensiva SC50 0.8-1%, essence 0.05-0.15%, Juniperus communis berry extract 0.2-0.8%, surplus
For deionized water.
4. a kind of double-deck facial treatment milk, it is characterised in that be prepared by following raw material by mass percentage：EDETATE SODIUM
0.05-0.1%, polyglutamic acid 0.01-0.1%, glycerine 2-6%, PEG-4000 4-12%, dipropylene glycol 3-8%,
The 0.2- of Cremophor RH40 0.5-2%, myristoyl glutamate sodium 0.02-0.15%, PPG-25- laureth -25
0.6%, ring five dimethyl silicone polymer 1-4%, Nexbase 2004 2-8%, tocopherol acetate 0.2-1%, caprylic/capric are sweet
Three ester 2-6% of oil, phytosterol/octyl dodecanol lauroyl glutamate ester 0.1-1.0%, Parleam 2-6%, butter
Fruit tree fruit fat 0.5-2%, radix scutellariae root extract 0.22%-0.76%, kuh-seng root extract 0.14%-0.62%, swollen fruit Radix
Root extract 0.14%-0.62%, Herba Verbenae 0.2-1%, Bacillus acidi lactici/bear's weed tunning extract 0.5-
2%, Phenoxyethanol/Sensiva SC50 0.8-1%, essence 0.05-0.15%, Lens culinaris berry extract 0.2-0.6%, surplus is
Deionized water.
5. a kind of double-deck facial treatment milk according to claim 1, it is characterised in that described double-deck facial treatment milk, stand
Upper strata is white emulsion afterwards, and lower floor is translucent liquid, and bilevel ratio is 1:1, it is white uniformity emulsion after shaking up, pH
For 5.3-6.0, no viscosity.
6. the preparation method of the double-deck facial treatment milk described in claim 1, it is characterised in that comprise the following steps successively：
1) mass number as described in claim 1 weighs each component；
2) ring five dimethyl silicone polymer that weighs step 1), Nexbase 2004, tocopherol acetate, caprylic/capric glycerine
Three esters, phytosterol/octyl dodecanol lauroyl glutamate ester, Parleam, Butyrospermum parkii fruit fat are placed in oil phase pot,
Stirring is warming up to 75-85 DEG C, and insulation is standby after dissolving completely, obtains oil phase；
3) EDETATE SODIUM, polyglutamic acid, glycerine, PEG-4000, dipropylene glycol, the PEG-40 hydrogenation castors weighed step 1)
Sesame oil, myristoyl glutamate sodium, PPG-25- laureths -25 and water are placed in emulsification pot, are heated with stirring to 80-90 DEG C,
Insulated and stirred is complete to all dissolution of raw material, obtains aqueous phase；
4) under stirring, oil phase prepared by step 2) is slowly pumped into the aqueous phase in emulsification pot, after homogeneous 2-4min,
Insulated and stirred 10-20min is complete to defoaming, and is cooled to 40-45 DEG C, and it is sweet to add radix scutellariae root extract, kuh-seng root extract, swollen fruit
Grass roots extract, Herba Verbenae, Bacillus acidi lactici/bear's weed tunning extract, Phenoxyethanol/ethylhexyl are sweet
Oil, essence, discharge after stirring, produce double-deck facial treatment milk.
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| CN106860233A (en) * | 2017-01-18 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment antiallergy emulsion |
| CN106983691B (en) * | 2017-05-18 | 2020-03-27 | 广州娇漾生物科技有限公司 | Lotus polyphenol-containing anti-oxidation pore-shrinking sleeping mask and preparation method thereof |
| CN110269822B (en) * | 2019-06-17 | 2021-12-31 | 临沂大学 | Salmon proteoglycan moisturizing skin care emulsion and preparation method and application thereof |
| CN110339131B (en) * | 2019-08-15 | 2021-11-16 | 广东芭薇生物科技股份有限公司 | Repairing emulsion and preparation method thereof |
| CN111214421B (en) * | 2020-03-17 | 2022-03-11 | 广东芭薇生物科技股份有限公司 | Double-layer moisturizing essence and preparation method thereof |
| CN113520944A (en) * | 2021-07-28 | 2021-10-22 | 上海梦希生物科技有限公司 | Gel composition for quickly eliminating acne and preparation method and application thereof |
| CN114983901A (en) * | 2022-07-20 | 2022-09-02 | 蓝科医美科学技术(吉林)有限公司 | Skin care emulsion and preparation method thereof |
| CN115501123A (en) * | 2022-10-20 | 2022-12-23 | 上海家化联合股份有限公司 | Stable double-layer toning lotion and preparation method thereof |
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| CN104814917A (en) * | 2015-04-24 | 2015-08-05 | 新疆西域果宝生物科技有限公司 | Cosmetic composition |
| CN105362112A (en) * | 2014-08-27 | 2016-03-02 | 王萍 | Moisturizing cosmetic |
| CN105395393A (en) * | 2015-11-25 | 2016-03-16 | 广州丹奇日用化工厂有限公司 | Skin care product composition with acne mark removing function and acne treatment cream |
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| CN105362112A (en) * | 2014-08-27 | 2016-03-02 | 王萍 | Moisturizing cosmetic |
| CN104814917A (en) * | 2015-04-24 | 2015-08-05 | 新疆西域果宝生物科技有限公司 | Cosmetic composition |
| CN105395393A (en) * | 2015-11-25 | 2016-03-16 | 广州丹奇日用化工厂有限公司 | Skin care product composition with acne mark removing function and acne treatment cream |
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