CN109431865B - Water-bursting cream for people staying up all night and preparation thereof - Google Patents

Water-bursting cream for people staying up all night and preparation thereof Download PDF

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CN109431865B
CN109431865B CN201811292721.9A CN201811292721A CN109431865B CN 109431865 B CN109431865 B CN 109431865B CN 201811292721 A CN201811292721 A CN 201811292721A CN 109431865 B CN109431865 B CN 109431865B
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water
cream
polydimethylsiloxane
boron nitride
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CN109431865A (en
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杨培喜
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Shantou City Yalian Pharmaceutical Co ltd
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Shantou City Yalian Pharmaceutical Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/895Polysiloxanes containing silicon bound to unsaturated aliphatic groups, e.g. vinyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/06Emulsions
    • A61K8/064Water-in-oil emulsions, e.g. Water-in-silicone emulsions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/23Sulfur; Selenium; Tellurium; Compounds thereof
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    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/673Vitamin B group
    • A61K8/675Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A61K8/894Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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Abstract

The invention relates to a water-bursting cream for people staying up at night and a preparation method thereof, which comprises 10-15% of cyclopentadimethylsiloxane, 1-4% of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer, 1-2% of organic silicon emulsifier, 1-3% of modified organic silicon conditioner, 1-2% of polydimethylsiloxane/hydrogenated polyisobutene, 0.5% of tocopherol, 0.05% of essence, 6-12% of glycerol, 3-6% of propylene glycol, 0.05% of hyaluronic acid, 4-7% of aloe extract, 0.8% of magnesium sulfate, 0.2% of phenoxyethanol, 0.1% of ethylhexylglycerol, 3-8% of cyclopentadimethylsiloxane/trimethylalkoxy silicate, 2-5% of cyclopentadimethylsiloxane/boron nitride/octylmethylsiloxane/C30-45 alkyl cetylstearyl polydimethylsiloxane cross-linked copolymer, water is added to 100%. The water-bursting cream disclosed by the invention is large in emulsified particle size, quick in water bursting, silky in skin feel, moist and easy to absorb, and optimal in moisturizing effect, and the skin can be kept moist for a long time and is not greasy, so that loose, dry and greasy skin can be quickly repaired, and the water-bursting cream is bright and colorful and is suitable for people staying up at night.

Description

Water-bursting cream for people staying up all night and preparation thereof
Technical Field
The invention relates to a water-bursting cream, in particular to a water-bursting cream for people staying up all night and a preparation method thereof.
Background
Due to increasingly intense social competition and accelerated pace of life and work, staying up all night is a frequent occurrence for modern people. The skin of a person staying overnight is seriously damaged, and the best time for the skin to rest is in the evening. The long-term staying up all night can cause endocrine dyscrasia and unbalance water and oil of the skin, so that the oil secretion is increased, the water retention is poor, and the skin is loose and dry; it also causes the skin to become rough and not glossy, and pores to become larger and larger. Often staying up to midnight, the skin's epidermal blood circulation will slow down, causing the skin to become dark yellow, dark, lacking luster. The secretion of adrenaline is increased after staying up, so that sebum is increased to block pores, thereby causing the growth of blackheads and acnes.
The main principle of the water-bursting cream is the water-in-oil structure, when the water-bursting cream is applied, emulsion particles bearing high water content instantly release small water drops, a plurality of small water drops are combined into large water drops which can be seen by naked eyes, the skin is fully moistened, and the water moistening feeling is endless all day long. The larger the particle diameter of the water-bursting cream is, the higher the water content of the water-bursting cream is, but the technical difficulty of the water-bursting cream is increased correspondingly. The current water-bursting creams on the market have the average diameter of water-in-oil emulsified particles of 1-2 microns, have relatively limited water content, cannot supplement water for a long time and have greasy feeling when in use.
Disclosure of Invention
The invention aims to provide water-bursting cream for people staying up at night and a preparation method thereof, so as to solve the problems in the prior art.
The water-bursting cream for people staying up at night mainly comprises the following components in percentage by weight:
10-15% of cyclopenta dimethyl silicone polymer
Polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 1-4%
1 to 2 percent of organic silicon emulsifier
1 to 3 percent of modified organic silicon conditioner
Polydimethylsiloxane/hydrogenated polyisobutene 1-2%
Tocopherol of 0.5%
0.05 percent of essence
6-12% of glycerin
3-6% of propylene glycol
Hyaluronic acid 0.05%
4 to 7 percent of aloe extract
Magnesium sulfate 0.8%
0.2 percent of phenoxyethanol
Ethylhexyl glycerin 0.1%
Cyclopenta dimethyl siloxane/trimethyl alkoxy silicate 3-8%
Cyclopenta-dimethicone/boron nitride/octyl methicone/C30-45 alkyl cetearyl dimethicone crosspolymer 2-5%
Water is added to 100%.
Cyclopenta-dimethicone is a base oil ester that functions as an emollient and to modify body consistency. The magnesium sulfate enhances the stability of the material body when the material body is frost-resistant.
The cyclopentasiloxane/trimethylalkoxy silicate ester has the functions of improving the spreadability and forming a water locking film to prevent the loss of skin moisture; the effects of soft focal length, matte and wrinkle removal can be achieved, and an unexpected silky touch feeling is provided. Cyclopenta-polydimethylsiloxane/trimethylalkoxy silicate is a spherical silicone resin with micro-particles of 4-6 microns in diameter.
Cyclopenta-dimethyl silicone/boron nitride/octyl methyl silicone/C30-45 alkyl cetearyl dimethyl silicone crosslinked copolymer is composed of semitransparent boron nitride and multifunctional skin feel reinforcing structure, wherein the boron nitride has good effect of softening focal length, and the octyl methyl silicone is added to help the boron nitride to disperse in the structure, so that a matrix type condensation structure is formed, the skin feel is more natural and smooth, and the SPF improvement effect is remarkable. The boron nitride powder has a brilliant effect, provides tactile and visual enjoyment, and has a unique silky feeling. The unique crystal structure characteristics of the boron nitride layer and the hexagon can endow the product with soft focal length effect to a great extent, and can improve skin-friendly property and keep makeup lasting.
Further, the paint mainly comprises the following components in percentage by weight:
cyclopenta dimethyl siloxane 12%
Polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 2%
1.5 percent of organic silicon emulsifier
2 percent of modified organic silicon conditioner
Polydimethylsiloxane/hydrogenated polyisobutene 1.5%
Tocopherol of 0.5%
0.05 percent of essence
8 percent of glycerin
Propylene glycol 5%
Hyaluronic acid 0.05%
Aloe extract 6%
Magnesium sulfate 0.8%
0.2 percent of phenoxyethanol
Ethylhexyl glycerin 0.1%
Cyclopenta-polydimethylsiloxane/trimethylalkoxy silicate 4%
Cyclopentadimethicone/boron nitride/octyl methicone/C30-45 alkyl cetearyl dimethicone crosspolymer 4%
Water is added to 100%.
Further, the organic silicon emulsifier is PEG/PPG-20/15 polydimethylsiloxane. PEG/PPG-20/15 Dimethicone is a 40% solution of silicone polyether copolymer dispersed in cyclopentasiloxane. The ratio of polyether to polysiloxane is such that the hydrophilic (polyether moiety)/hydrophobic (polysiloxane moiety) structure formed is useful in formulating highly stable water-in-oil emulsions. PEG/PPG-20/15 polydimethylsiloxane not only has emulsifying ability, but also imparts silky soft skin feel, and improves water resistance and durability. It is generally recommended to use 2.5-5%. But is slightly irritating to the skin and eyes. The invention reduces the content of PEG/PPG-20/15 dimethyl silicone polymer to 1.5% by reasonably regulating and controlling the components and the content thereof.
Further, the modified silicone conditioning agent octyl polymethylsiloxane. Octyl polymethylsiloxane is low in molecular weight and viscosity, can provide soft silk feeling for skin care products, and can improve the spreadability and the covering surface of various components such as oil, fat, petrolatum and mineral oil by reducing the surface tension of the oil, so that cream can be coated on the skin more easily and uniformly; reduce greasy feeling.
Further, the boron nitride in the cross-linked copolymer of the cyclopentasiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone is a hexagonal boron nitride nanosheet of 300-500nm, and the mass of the boron nitride accounts for 20% of that of the cross-linked copolymer of the cyclopentasiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone. When the boron nitride is a nano-sheet, the nano-sheet has larger comparative area and dispersing ability, and can be better dispersed in a system.
Further, the mass ratio of the polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer to the polydimethylsiloxane/hydrogenated polyisobutene is 2: 1.5. the polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer is a skin feel improver and provides a silky, soft skin feel. The dimethyl siloxane crosslinked copolymer modified by C16-C18 alkyl is dispersed in low-viscosity 5cst dimethyl silicone oil. Because the product does not contain volatile silicone oil, the product has long-lasting silky skin feel. The polydimethylsiloxane/hydrogenated polyisobutene function is to moisturize the smooth skin feel. The polydimethylsiloxane/hydrogenated polyisobutene and the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer are compounded, so that mutual promotion can be realized, and the skin feeling can be improved. When the mass ratio of polydimethylsiloxane to hydrogenated polyisobutene is 2: 1.5 when mixed, the composition has optimal moistening and silky feeling.
Further, the mass ratio of the cyclopentadimethylsiloxane/trimethylalkoxysilicate to the cyclopentadimethylsiloxane/boron nitride/octylmethylsiloxane/C30-45 alkyl cetearyl dimethicone crosspolymer is 1: 1. when the skin moisturizing cream is mixed according to the proportion, the emulsified particle size is large, the water burst is fast, the skin feels silky, the moisturizing effect is easy to absorb, the moisturizing effect is optimal, the skin can be kept moist for a long time, and is not greasy, so that loose, dry and greasy skin can be quickly repaired, and the skin moisturizing cream is bright and is especially suitable for people staying up to night.
Further, the collagen peptide also comprises 1% of glucan, 1% of collagen peptide and 1% of water-soluble vitamin. The water soluble vitamin is B3, B5, B6 or VC. When the glucan, the collagen peptide and the water-soluble vitamin are mixed in the system of the invention according to the proportion, the glucan, the collagen peptide and the water-soluble vitamin act together with hyaluronic acid, and the effect of immediate whitening can be achieved.
The preparation of the water-bursting cream for people staying up all night mainly comprises the following steps:
(1) preparing an aqueous phase: adding deionized water into a water kettle, opening and stirring, adding propylene glycol, glycerol and hyaluronic acid into the deionized water, then adding magnesium sulfate, and stirring until the materials are completely dissolved; adding Aloe extractive solution, antiseptic, and antibacterial agent before sucking;
(2) preparing an oil phase: adding the rest components into oil pan, stirring for 20-30min to disperse uniformly;
(3) extracting the oil phase into an emulsifying pot under the conditions that the rotating speed is 600 revolutions per minute and the vacuum degree is 0.05; after the oil phase is extracted, heating the water phase to 70 ℃, and then extracting the water phase to an emulsifying pot according to the speed of 300Kg/30 min;
(4) emulsifying for 15min under the conditions of the rotating speed of 600 revolutions per minute and the vacuum degree of 0.05, emulsifying for 15min under the conditions of the rotating speed of 100 revolutions per minute and the vacuum degree of 0.05, cooling to below 30 ℃, and discharging.
Compared with the prior art, the emulsified water cream has large emulsified particle size of 5-8 microns through reasonable regulation and control of various raw material components, contents and processes. The skin-care product has the advantages of quick water burst, silky and smooth skin feeling, moisture and easiness in absorption, and optimal water replenishing effect, can keep the moisture of the skin for a long time, is not greasy, can quickly restore the loose, dry and greasy skin, is bright and is especially suitable for people staying up all night. The skin feeling of the body is adjusted by compounding the raw materials, so that the skin-care cream has better moistening and silky feeling and gives a pleasant use feeling to consumers. The massage water bursts to form a thin water film on the surface layer of the skin, moisture is released for a long time, water is replenished circularly, the skin is kept tender and tender, and the functions of water replenishing, moisture retention and tightening are achieved.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention will be described in further detail below.
Example 1
The water-bursting cream for people staying up at night mainly comprises the following components in percentage by weight:
12% of cyclopentasiloxane, 2% of dimethicone/vinyl dimethicone crosspolymer, 1.5% of PEG/PPG-20/15 dimethicone, 2% of octyl methicone, 1.5% of dimethicone/hydrogenated polyisobutene, 0.5% of tocopherol, 0.05% of perfume, 8% of glycerol, 5% of propylene glycol, 0.05% of hyaluronic acid, 6% of aloe vera extract, 0.8% of magnesium sulphate, 0.2% of phenoxyethanol, 0.1% of ethylhexylglycerol, 4% of cyclopentasiloxane/trimethylalkoxysilicate, 4% of cyclopentasiloxane/boron nitride/octylmethicone/C30-45% of alkyl cetearyl dimethicone crosspolymer, water added to 100%.
The boron nitride in the cross-linked copolymer of the cyclopentasiloxane/the boron nitride/the octyl methicone/the C30-45 alkyl cetearyl dimethicone is a hexagonal boron nitride nanosheet with the particle size of 300-500nm, and the mass of the boron nitride accounts for 20% of that of the cross-linked copolymer of the cyclopentasiloxane/the boron nitride/the octyl methicone/the C30-45 alkyl cetearyl dimethicone.
Example 2
The water-bursting cream for people staying up at night mainly comprises the following components in percentage by weight:
10% of cyclopentasiloxane, 4% of dimethicone/vinyl dimethicone crosspolymer, 2% of PEG/PPG-20/15 dimethicone, 3% of octyl methicone, 2% of dimethicone/hydrogenated polyisobutene, 0.5% of tocopherol, 0.05% of perfume, 12% of glycerol, 3% of propylene glycol, 0.05% of hyaluronic acid, 4% of aloe vera extract, 0.8% of magnesium sulphate, 0.2% of phenoxyethanol, 0.1% of ethylhexylglycerol, 3% of cyclopentasiloxane/trimethylalkoxy silicate, 5% of cyclopentasiloxane/boron nitride/octylmethicone/C30-45% of alkyl cetostearyl dimethicone crosspolymer, water added to 100%.
Example 3
The water-bursting cream for people staying up at night mainly comprises the following components in percentage by weight:
15% of cyclopentasiloxane, 1% of dimethicone/vinyl dimethicone crosspolymer, 1% of PEG/PPG-20/15 dimethicone, 1% of octyl methicone, 1% of dimethicone/hydrogenated polyisobutene, 0.5% of tocopherol, 0.05% of perfume, 6% of glycerol, 6% of propylene glycol, 0.05% of hyaluronic acid, 7% of aloe vera extract, 0.8% of magnesium sulphate, 0.2% of phenoxyethanol, 0.1% of ethylhexylglycerol, 8% of cyclopentasiloxane/trimethylalkoxy silicate, 2% of cyclopentasiloxane/boron nitride/octylmethicone/C30-45% of alkyl cetearyl dimethicone crosspolymer, water added to 100%.
The preparation process of examples 1-3 essentially comprises the following steps:
(1) preparing an aqueous phase: adding deionized water into a water kettle, opening and stirring, adding propylene glycol, glycerol and hyaluronic acid into the deionized water, then adding magnesium sulfate, and stirring until the materials are completely dissolved; adding Aloe extractive solution, antiseptic, and antibacterial agent before sucking;
(2) preparing an oil phase: adding the rest components into oil pan, stirring for 20-30min to disperse uniformly;
(3) extracting the oil phase into an emulsifying pot under the conditions that the rotating speed is 600 revolutions per minute and the vacuum degree is 0.05; after the oil phase is extracted, heating the water phase to 70 ℃, and then extracting the water phase to an emulsifying pot according to the speed of 300Kg/30 min;
(4) emulsifying for 15min at rotation speed of 600 r/min and vacuum degree of 0.05, emulsifying for 15min at rotation speed of 100 r/min and vacuum degree of 0.05, cooling to below 30 deg.C, and discharging
The test reports obtained for the burst water creams for the overnight population in examples 1-3 are as follows:
appearance: the paste is fine and uniform;
pH value: the pH value is 6.6;
emulsified particle size of the water-bursting cream: up to 5-8 microns;
the heat resistance is tested at 45 +/-1 ℃ for 24 hours, and the paste body is free of oil-water separation after being restored to the room temperature;
and (3) cold resistance testing is carried out at a temperature of between 5 ℃ below zero and 10 ℃ below zero for 24 hours, and no obvious character difference exists after the temperature is restored to room temperature.
And (3) performance testing:
the skin feel, moisturizing degree, water-out feel and refreshing feel of the burst water cream for the overnight population according to examples 1 to 3 and the ordinary commercially available moisturizing cream (natura water cream comparative example 1) and the ordinary commercially available burst water cream (yabang burst water cream comparative example 2) were compared. By adopting a user trial and opinion investigation grading method, 100 people in the age range of 25-40 years are selected as trial objects, and each using effect is divided into 5 in total: the score of 5 is the highest score, which represents good and very satisfactory; 4, the division is better; 3, dividing into good; a score of 3 or less is not good and is not acceptable. The average scores for each are as follows, and the results are shown in table 1:
TABLE 1 comparison of skin feel, moisturization, water out feel and freshness
Test items Example 1 Example 2 Example 3 Comparative example 1 Comparative example 2
Skin feel 4.8 4.6 4.5 4.0 4.1
Moisture retention 4.7 4.5 4.6 3.8 3.5
Sense of water discharge 4.5 4.5 4.4 3.4 4.0
Refreshing feeling 4.2 4.1 4.0 3.3 3.0
The results in table 1 show that the outlet moisturizing cream of the embodiments 1 to 3 has more excellent skin feel, better moisturizing property and outlet feel compared with the commercially available common moisturizing cream and the commercially available water-bursting cream, and users generally show that when the outlet moisturizing cream of the embodiments 1 to 3 of the present invention is applied, the skin is fresh and not greasy, the skin feel is silky, the skin is moist and easy to absorb, the moisturizing effect is optimal, and the skin can be kept moist for a long time.
Selecting 100 persons staying up at the age of 25-40 years as trial objects, smearing the water-bursting cream aiming at the persons staying up at night according to the examples 1-3, common commercial moisturizing cream (a natural hall water-moistening cream comparative example 1) and common commercial water-bursting cream (a Yabang water-bursting cream comparative example 2) on the left face and the right face of a subject, using a skin tester to respectively coat 1h, 2h, 3h, 6h and 12h of a sample, measuring the skin moisture content of the left face and the right face for 5 times, and expressing the evaluation result by an average value, wherein the result is shown in Table 2. Meanwhile, oil bleeding began after recording how long the face was smeared, and the evaluation results were expressed as an average value, as shown in table 3.
TABLE 2 comparison of moisture content after 1h, 2h, 3h, 6h, 12h of painted samples
Time of measurement Blank comparison Example 1 Example 2 Example 3 Comparative example 1 Comparative example 2
1h 28% 75% 73% 74% 70% 69%
2h 28% 72% 70% 69% 57% 60%
3h 27% 66% 62% 63% 43% 45%
6h 24% 58% 54% 52% 35% 34%
12h 24% 50% 45% 45% 33% 30%
TABLE 3 comparison of oil production for the painted samples
Figure BDA0001850332090000071
Figure BDA0001850332090000081
As can be seen from tables 2 and 3, the water-bursting creams for people staying up at night in examples 1 to 3 are quick in water bursting, optimal in water replenishing effect, capable of keeping skin moist and not greasy for a long time, capable of keeping skin moist and not oily for a long time, and particularly suitable for people staying up at night.
30 persons staying up at 25-40 years old were selected respectively as the blasting cream and the common commercial moisturizing cream (natural hall moisturizing cream comparative example 1) and the common commercial blasting cream (yabang blasting cream comparative example 2) aiming at the persons staying up at night in the morning and evening of each day in examples 1-3, and the number of persons with comprehensive skin improvement degree (including comprehensive evaluation of skin oil secretion, skin laxity, dryness, roughness, dark yellow, luster, pores, blackhead acne, pox and the like) was recorded, as shown in table 4.
TABLE 4 improvement of skin after sample application
Test time (week) Example 1 Example 2 Example 3 Comparative example 1 Comparative example 2
1 2 1 1 0 0
4 8 7 7 5 5
8 13 12 13 8 8
12 17 16 16 10 11
16 23 22 21 14 14
As can be seen from table 4, the skin improvement after 16 weeks of use was good after the burst cream for the overnight population of examples 1-3 was used.
Example 4
The water-bursting cream for people staying up at night mainly comprises the following components in percentage by weight:
12% of cyclopentasiloxane, 2% of dimethicone/vinyl dimethicone crosspolymer, 1.5% of PEG/PPG-20/15 dimethicone, 2% of octyl methicone, 1.5% of dimethicone/hydrogenated polyisobutene, 0.5% of tocopherol, 0.05% of essence, 8% of glycerol, 5% of propylene glycol, 0.05% of hyaluronic acid, 6% of aloe vera extract, 0.8% of magnesium sulfate, 0.2% of phenoxyethanol, 0.1% of ethylhexylglycerol, 4% of cyclopentasiloxane/trimethylalkoxy silicate, 4% of cyclopentasiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone crosspolymer, 4% of dextran, 1% of collagen peptide, 1% of water-soluble vitamins (B3, B5, B6 or VC) 1%, water is added to 100%.
The boron nitride in the cross-linked copolymer of the cyclopentasiloxane/the boron nitride/the octyl methicone/the C30-45 alkyl cetearyl dimethicone is a hexagonal boron nitride nanosheet with the particle size of 300-500nm, and the mass of the boron nitride accounts for 20% of that of the cross-linked copolymer of the cyclopentasiloxane/the boron nitride/the octyl methicone/the C30-45 alkyl cetearyl dimethicone.
After the water-bursting cream for the people staying up at night in the embodiment 4 is used, the performances of water replenishing, moisture keeping and the like are similar to those of the embodiment 1, the instant whitening effect is also realized, and the skin color is obviously whitened after 1 week of use.
Example 5
And (2) respectively mixing polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polydimethylsiloxane/hydrogenated polyisobutene according to the mass ratio of 3: 1. 2: 1. 2: 2. 2: 3, the total content is kept at 3.5 percent, other components, contents and preparation thereof are the same as those of the example 1, and the water-bursting cream is prepared, and the moisturizing, silky feeling and refreshing effects are found to be inferior to those of the example 1.
Example 6
And the cross-linked copolymer of cyclopentadimethylsiloxane/trimethylalkoxy silicate and cyclopentadimethylsiloxane/boron nitride/octyl methylsiloxane/C30-45 alkyl cetearyl polydimethylsiloxane is prepared according to the mass ratio of 3: 1. 2: 1. 1: 2. 1: 3, the total content is kept at 8 percent, other components, contents and preparation thereof are the same as those of the example 1, and the water-bursting cream is prepared, and the emulsion particle size, the water-bursting speed, the water replenishing effect, the absorption effect and the refreshing effect are all inferior to those of the example 1.

Claims (9)

1. The water-bursting cream for people staying up at night is characterized by mainly comprising the following components in percentage by weight:
10-15% of cyclopenta dimethyl silicone polymer
Polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 1-4%
1 to 2 percent of organic silicon emulsifier
1 to 3 percent of modified organic silicon conditioner
Polydimethylsiloxane/hydrogenated polyisobutene 1-2%
Tocopherol of 0.5%
0.05 percent of essence
6-12% of glycerin
3-6% of propylene glycol
Hyaluronic acid 0.05%
4 to 7 percent of aloe extract
Magnesium sulfate 0.8%
0.2 percent of phenoxyethanol
Ethylhexyl glycerin 0.1%
Cyclopenta dimethyl siloxane/trimethyl alkoxy silicate 3-8%
Cyclopenta-dimethicone/boron nitride/octyl methicone/C30-45 alkyl cetearyl dimethicone crosspolymer 2-5%
Deionized water was added to 100%.
2. The explosive water cream for the people staying up at night according to claim 1, which is characterized by mainly comprising the following components in percentage by weight:
cyclopenta dimethyl siloxane 12%
Polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer 2%
1.5 percent of organic silicon emulsifier
2 percent of modified organic silicon conditioner
Polydimethylsiloxane/hydrogenated polyisobutene 1.5%
Tocopherol of 0.5%
0.05 percent of essence
8 percent of glycerin
Propylene glycol 5%
Hyaluronic acid 0.05%
Aloe extract 6%
Magnesium sulfate 0.8%
0.2 percent of phenoxyethanol
Ethylhexyl glycerin 0.1%
Cyclopenta-polydimethylsiloxane/trimethylalkoxy silicate 4%
Cyclopentadimethicone/boron nitride/octyl methicone/C30-45 alkyl cetearyl dimethicone crosspolymer 4%
Deionized water was added to 100%.
3. The pop water cream for the overnight population according to claim 1, wherein the silicone emulsifier is PEG/PPG-20/15 dimethicone.
4. The pop water cream for the overnight population of claim 1, wherein the modified silicone conditioning agent is octyl methicone.
5. The pop water cream for the overnight population as recited in claim 1, wherein the boron nitride in the cyclopentasiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone crosspolymer is hexagonal boron nitride nanosheets and is 300-500nm, and the mass of the boron nitride accounts for 20% of that of the cyclopentasiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone crosspolymer.
6. The pop water cream for the overnight population according to claim 1, wherein the mass ratio of the dimethicone/vinyl dimethicone crosspolymer to the dimethicone/hydrogenated polyisobutene is 2: 1.5.
7. the pop water cream for the overnight population according to claim 1, wherein the weight ratio of cyclopentadimethylsiloxane/trimethylalkoxysilicate to cyclopentadimethylsiloxane/boron nitride/octylmethicone/C30-45 alkyl cetearyl dimethicone crosspolymer is 1: 1.
8. the pop water cream for the overnight population according to claim 1, further comprising 1% dextran, 1% collagen peptide, and 1% water-soluble vitamin.
9. The preparation of the burst water cream for the people staying up at night according to claim 1 is characterized by mainly comprising the following steps:
(1) preparing an aqueous phase: adding deionized water into a water kettle, opening and stirring, adding propylene glycol, glycerol and hyaluronic acid into the deionized water, then adding magnesium sulfate, and stirring until the materials are completely dissolved; adding Aloe extractive solution, phenoxyethanol, and ethylhexyl glycerol before sucking;
(2) preparing an oil phase: adding the rest components into oil pan, stirring for 20-30min to disperse uniformly;
(3) extracting the oil phase into an emulsifying pot under the conditions that the rotating speed is 600 revolutions per minute and the vacuum degree is 0.05; after the oil phase is extracted, heating the water phase to 70 ℃, and then extracting the water phase to an emulsifying pot according to the speed of 300Kg/30 min;
(4) emulsifying for 15min under the conditions of the rotating speed of 600 revolutions per minute and the vacuum degree of 0.05, then emulsifying for 15min under the conditions of the rotating speed of 100 revolutions per minute and the vacuum degree of 0.05, cooling to below 30 ℃, and discharging.
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