CN104997653B - Skin cream that a kind of suitable Oily uses and preparation method thereof - Google Patents
Skin cream that a kind of suitable Oily uses and preparation method thereof Download PDFInfo
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- CN104997653B CN104997653B CN201510463877.9A CN201510463877A CN104997653B CN 104997653 B CN104997653 B CN 104997653B CN 201510463877 A CN201510463877 A CN 201510463877A CN 104997653 B CN104997653 B CN 104997653B
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Abstract
The invention provides the skin cream that a kind of suitable Oily uses, the skin cream includes emollient 10 35%, emulsion stabilizer 3 10%, NMF 1 3%, thickener 0.1 2%, the natural wooden fiber's element powder 0.5 5% and deionized water surplus that mesh number is 115 1340 mesh by weight percentage；Emollient is the one or more in isobutyl palmitate, caprylic/capric triglyceride, isopropyl stearate, isopropyl isostearate, laurate ethylhexyl, cetearyl caprylate, isononyl isononanoate, saualane, dimethyl silicone polymer, phenyl trimethicone polysiloxanes or cyclopentasiloxane；Emulsion stabilizer is the one or more in AEO, methyl glucoside sesquistearate, polyoxyethylene stearic acid ester, glycerin monostearate, polysorbate, cetostearyl alcohol or cetanol.The skin cream of the present invention can make Oily obtain moistening for deep layer, and user can be allowed to have salubrious, lubrication, the sensation of pro-skin.The present invention also provides a kind of preparation method of above-mentioned skin cream.
Description
Technical field
The present invention relates to a kind of skin care item, more particularly to a kind of skin cream, specifically relate to a kind of suitable Oily
The skin cream used.The invention further relates to a kind of preparation method of above-mentioned skin cream.
Background technology
Skin cream is a kind of cosmetics that people are commonly used in daily life, has skin nutrition, supplement skin
Required moisture, make the tender smooth effect of skin.The formula of common skin cream is similar, be substantially by water-soluble component and
Oil-soluble constitents act on the emulsification paste to form oil-in-water or water-in-oil type, wherein oil-soluble constitents content one by emulsifying agent
As be 10%-70%, its product is between weak oiliness and oiliness.The journey of the crowd of different skin quality, skin secretion grease and water lock
Degree is had nothing in common with each other, thus the requirement to skin cream formulation is also different, oil-in-water lotion, salubrious non-greasy, is suitable for Oily
Use, Water-In-Oil lotion is more containing grease, wax class composition, has preferable moisten effect to skin, is suitable for Dry, existing
Some skin cream use generally by the ratio of adjustment oil-soluble constitents and water-soluble component suitable all kinds of skins are made
Product.Oil-soluble constitents can provide the nourishing of deep layer for skin, balance the water tariff collection in skin, reach the effect of moisturizing
Fruit, but for the crowd of oily skin, because fat secretion is more vigorous, in order to avoid pore is blocked, often selection is oily
Property the few skin cream of Component comparison, it is so long-term use of, deep layer flesh can be caused to lack and nourished, the phenomenon done in outer oil occur.For
Solves this problem, those skilled in the art is proposed using plant extract, fat-soluble salicylic acid, inorganic mineral class
Grain etc. is added in skin cream as oil-control composition, reaches the purpose for reducing greasy feeling, such as Application No.
CN201310625349.X, entitled " a kind of 5α-reductase inhibitor and application thereof " Chinese patent application, disclose one kind
Fructus Litchi extract is as the additive with 5α-reductase inhibitory action in the personal care product with oil-control effect is prepared
Application；Application No. CN201410563809.5, entitled " a kind of salicylic acid microcapsules and preparation method thereof and cold cream
The patent application of frost ", disclose one kind and reached using salicylic acid dissolving facial pores excess oil and old dead impaired horn cell
To the method for oil-control；Application No. 201210422637.0, entitled " a kind of zinc oxide and salicylic toner and its preparation
The patent of method ", disclose the effect for reaching oil-control by adding zinc oxide in toner.Due to botanical extract, nothing
Machine mineral substance particle can influence its security because impurity in product preparation process be present, and fat-soluble salicylic acid is insoluble in water and tool
There is stronger excitant, these defects can be very restricted in application.
The content of the invention
To solve the problem present on, it is an object of the invention to provide the skin cream that a kind of suitable Oily uses,
The skin cream has pro-skin, the effect of oil-control.
It is a further object of the present invention to provide a kind of preparation method of above-mentioned skin cream.
To realize object above, the skin cream that suitable Oily of the invention uses, including by weight percentage
Emollient 10-35%, emulsion stabilizer 3-10%, NMF 1-3%, thickener 0.1-2%, the natural wood that mesh number is 115-1340 mesh
Matter cellulose powder 0.5- 5% and deionized water surplus；Emollient is isobutyl palmitate, caprylic/capric triglyceride, tristearin
Isopropyl propionate, isopropyl isostearate, laurate ethylhexyl, cetearyl caprylate, isononyl isononanoate, saualane,
One or more in dimethyl silicone polymer, phenyl trimethicone polysiloxanes or cyclopentasiloxane；Emulsion stabilizer is fat
Alcohol APEO, methyl glucoside sesquistearate, polyoxyethylene stearic acid ester, glycerin monostearate, poly- sorb
One or more in alcohol ester, cetostearyl alcohol or cetanol.
The preferred Germany of above-mentioned natural wooden fiber's element powder is auspicious to step on Mel father and son company（Abbreviation JRS）The model of production
Vivapur CS 9 FM, Vitacel CS 20 FC, the FM of 70 FM or Vivapur CS of Vivapur CS 130 natural wood
Matter cellulose powder.
One or more in above-mentioned NMF preferably glycerine, butanediol, propane diols or polyethylene glycol.
One or more in the preferred sodium carboxymethyl starch of above-mentioned thickener, carbomer or xanthans.
In order that skin cream has more preferable antibacterial, anti-corrosion, anti-mold effect, while make skin cream that there is pleasant smell,
Above-mentioned skin cream also includes preservative and essence, and the percentage by weight of preservative and essence in skin cream is preservative
0.25-0.45%, essence 0.1-0.2%.
One or more in the preferred Phenoxyethanol of foregoing preservatives, parabens, methylisothiazolinone；Essence is excellent
Select flavoring rose essence or lily essence.
In order that skin cream has the application effect of preferably thickening moisturizing, above-mentioned skin cream also includes nertralizer, should
One or more in the preferred triethanolamine of nertralizer, sodium hydroxide or potassium hydroxide, weight hundred of the nertralizer in skin cream
It is 0.2-0.3% to divide ratio.
The present invention also provides a kind of preparation method for the skin cream that above-mentioned suitable Oily uses, and this method is by moisturizing
70-80 DEG C is heated to after agent, emulsion stabilizer are well mixed, oil phase is made；By NMF, thickener, natural wooden fiber's element
70-80 DEG C is heated to after powder, deionized water are well mixed, aqueous phase is made；Oil phase and aqueous phase are added in vacuum homogenizer again
Emulsifying 3-5 minutes, degassing, less than 45 DEG C are cooled to, discharging, obtains skin cream.
In above-mentioned preparation method, preservative is added after oil phase and aqueous phase emulsifying, 10-30 minutes is stirred, is cooled to
At 50-60 DEG C, essence is added, is stirred 5-10 minutes, degassing, continues cool to less than 45 DEG C, discharging.
In above-mentioned preparation method, nertralizer is added with the aqueous phase.
The skin cream that the suitable Oily of the present invention uses, using natural wooden fiber's element powder of specified particle diameter as powder
Material, the suitable emollient of simultaneous selection and emulsion stabilizer, then coordinate the compositions such as NMF and thickener to be emulsified and be made；
Due to natural wooden fiber's powder good dispersion, microstructure is band sigmoid, uneven, porous surface hole, thus with big
Specific surface area, this big specific surface area adds because its capillary effect has very strong absorption affinity to grease in oily components
In the case that dosage is bigger, still with good oil-control effect, in addition, natural wooden fiber's element powder it is nontoxic, it is tasteless, without dirt
Contaminate, be "dead", and being chemically highly stable material at typical condition, being highly suitable as powder and be added to skin cream
In.Skin cream preparation method of the invention is simple, the fine and smooth stabilization of lotion, and Oily can be made to obtain moistening for deep layer, and
It can allow user that there is salubrious, lubrication, the sensation of pro-skin, be particularly suitable for Oily use.
Embodiment
Technical scheme is described further below by specific embodiment, but these embodiments are not used
In limiting the scope of the invention, on the premise of theory of the present invention is not departed from, to the equivalent replacement of each component or each component
The adjustment of proportioning, protection scope of the present invention all should be belonged to.
1st, product example
Embodiment 1
（1）Product formula（In terms of 100 parts of gross weight component）
5 parts of isobutyl palmitate, 2 parts of dimethyl silicone polymer, 5 parts of saualane, 1 part of cetostearyl alcohol, fatty alcohol polyoxy
2 parts of vinethene, 1.5 parts of glycerin monostearate, 3 parts of glycerine, 1 part of sodium carboxymethyl starch, the FM natural woods of Vivapur CS 9
2 parts of matter cellulose powder, 0.2 part of methyl hydroxybenzoate, 0.1 part of Nipasol, 0.15 part of flavoring rose essence, deionized water surplus.
（2）Preparation technology
Isobutyl palmitate, dimethyl silicone polymer, saualane, cetostearyl alcohol, AEO, list is hard
Glycerol is well mixed, and is heated to 75 DEG C and oil phase is made；Glycerine, sodium carboxymethyl starch, the FM of Vivapur CS 9 is natural
Lignocellulose, deionized water are well mixed, and are heated to 75 DEG C and aqueous phase is made；Oil phase, aqueous phase are all added into vacuum homogenizer
Middle emulsifying 5 minutes, methyl hydroxybenzoate, Nipasol are added, stirred 20 minutes；Raw material is cooled to 50 ~ 60 DEG C after emulsification, adds
Flavoring rose essence, it is stirred for 5 minutes, deaerates, continue to cool to 35 ~ 40 DEG C of dischargings, obtains fine and smooth pure white beautiful, pH value 6, viscosity
For 42550 mPas lotion.
Embodiment 2
（1）Product formula（In terms of 100 parts of gross weight component）
10 parts of isobutyl palmitate, 5 parts of dimethyl silicone polymer, 15 parts of saualane, 3 parts of cetostearyl alcohol, poly alkyl alcohol
4 parts of oxygen vinethene, 3 parts of glycerin monostearate, 2 parts of glycerine, 2 parts of sodium carboxymethyl starch, the FC natural woods of Vitacel CS 20
2 parts of matter cellulose powder, 0.2 part of methylisothiazolinone, 0.1 part of Nipasol, 0.15 part of lily essence, deionized water surplus.
（2）Preparation technology
Isobutyl palmitate, dimethyl silicone polymer, saualane, cetostearyl alcohol, AEO, list is hard
Glycerol is well mixed, and is heated to 75 DEG C and oil phase is made；By glycerine, sodium carboxymethyl starch, Vitacel CS 20 FC days
Right lignocellulose, deionized water are well mixed, and are heated to 75 DEG C and aqueous phase is made；It is equal that oil phase, aqueous phase are all added to vacuum
Emulsifying in matter device, adds methylisothiazolinone, Nipasol, and stirring 25 is uniform；Raw material is cooled to 50 ~ 60 after emulsification
DEG C, lily essence is added, is stirred for 5 minutes, is deaerated, is continued to cool to 35 ~ 40 DEG C of dischargings, obtain 42550 mPas, pH value
For the lotion that 6, viscosity is 42800 mPas.
Embodiment 3
（1）Product formula（In terms of 100 parts of gross weight component）
4 parts of isobutyl palmitate, 1 part of dimethyl silicone polymer, 5 parts of saualane, 2 parts of cetostearyl alcohol, fatty alcohol polyoxy
2 parts of vinethene, 1 part of glycerin monostearate, 3 parts of glycerine, 0.2 part of carbomer, the FM natural wooden fibers of Vivapur CS 70
Plain 1 part of powder, 0.3 part of triethanolamine, 0.2 part of methylisothiazolinone, 0.2 part of methyl hydroxybenzoate, 0.15 part of flavoring rose essence, go from
Sub- water surplus.
（2）Preparation technology
Isobutyl palmitate, dimethyl silicone polymer, saualane, cetostearyl alcohol, AEO, list is hard
Glycerol is well mixed, and is heated to 75 DEG C and oil phase is made；By glycerine, carbomer, the FM natural woods of Vivapur CS 70
Cellulose powder, triethanolamine, deionized water are well mixed, and are heated to 80 DEG C and aqueous phase is made；Oil phase, aqueous phase are all added to vacuum
Emulsifying in homogenizer, methylisothiazolinone, methyl hydroxybenzoate are added, stirred 25 minutes；Raw material is cooled to 50-60 after emulsification
DEG C, flavoring rose essence is added, is stirred for 5 minutes, deaerates, continues to cool to 35 ~ 40 DEG C of dischargings, obtains fine and smooth pure white beautiful, pH value
For the lotion that 5.8, viscosity is 41300 mPas.
Embodiment 4
（1）Product formula（In terms of 100 parts of gross weight component）
5 parts of caprylic/capric triglyceride, 8 parts of isobutyl palmitate, 1 part of dimethyl silicone polymer, isopropyl stearate
8 parts, 2 parts of cetanol, 0.5 part of methyl glucoside sesquistearate, 1 part of AEO, glycerol monostearate
1 part of ester, 3 parts of glycerine, 1.5 parts of sodium carboxymethyl starch, 1 part of the FM natural wooden fibers element powder of Vivapur CS 130, methyl is different
0.2 part of thiazolinone, 0.2 part of methyl hydroxybenzoate, 0.15 part of lily essence, deionized water surplus.
（2）Preparation technology
By caprylic/capric triglyceride, isobutyl palmitate, dimethyl silicone polymer, isopropyl stearate, spermaceti
Alcohol, methyl glucoside sesquistearate, AEO, glycerin monostearate are well mixed, and are heated to 80
DEG C oil phase is made；Glycerine, xanthans, the FM natural wooden fibers element powder of Vivapur CS 130, deionized water are well mixed,
It is heated to 80 DEG C and aqueous phase is made；Oil phase, aqueous phase are all added into emulsifying in vacuum homogenizer, add methylisothiazolinone,
Methyl hydroxybenzoate, stir 20 minutes；Raw material is cooled to 50 ~ 60 DEG C after emulsification, adds lily essence, is stirred for 5 minutes, deaerates, after
It is continuous to cool to 35 ~ 40 DEG C of dischargings, obtain fine and smooth pure white beautiful, pH value 6, the lotion that viscosity is 36900 mPas.
2nd, product stability detects
According to cosmetics QB/T 1857-2013 standards, the product that embodiment 1-4 is obtained is carried out under the conditions of 48 ± 1 DEG C
Resistance to Thermal test, cold-resistant test is carried out under the conditions of -15 ± 1 DEG C, be centrifuged under the conditions of 3000 r/min, as a result such as
Under：
As can be seen from the above table, skin cream of the invention in high temperature, low temperature, be centrifuged at a high speed under conditions of it is all quite steady
Fixed, its every organoleptic indicator, physical and chemical index, sanitary index also comply fully with cosmetics QB/T 1857-2013 standards.Will be upper
State Oily women of the product by way of directly smearing between 15-45 year to try out, the people of user 100, usage time
For 15-30 days, the drying of skin can be obviously improved, and the glossy phenomenon having one's face covered with is obviously controlled.
Claims (9)
1. the skin cream that a kind of suitable Oily uses, including emollient 10-35%, stable emulsifying by weight percentage
Agent 3-10%, NMF 1-3%, thickener 0.1-2%, mesh number for 115-1340 mesh natural wooden fiber element powder 0.5- 5% and go
Ion water surplus；Emollient is isobutyl palmitate, caprylic/capric triglyceride, isopropyl stearate, isostearic acid isopropyl
Ester, laurate ethylhexyl, cetearyl caprylate, isononyl isononanoate, saualane, dimethyl silicone polymer, phenyl three
One or more in methyl polysiloxane or cyclopentasiloxane；Emulsion stabilizer is AEO, methyl glucose
Glucosides sesquistearate, polyoxyethylene stearic acid ester, glycerin monostearate, polysorbate, cetostearyl alcohol or spermaceti
One or more in alcohol；Natural wooden fiber's element powder is the auspicious model Vivapur CS for stepping on the production of Mel father and son company of Germany
9 FM, Vitacel CS 20 FC, the FM of 70 FM or Vivapur CS of Vivapur CS 130 natural wooden fiber's element powder.
2. the skin cream that suitable Oily according to claim 1 uses, it is characterised in that：The NMF is sweet
One or more in oil, butanediol, propane diols or polyethylene glycol.
3. the skin cream that suitable Oily according to claim 1 or 2 uses, it is characterised in that：The thickener is
One or more in sodium carboxymethyl starch, carbomer or xanthans.
4. the skin cream that suitable Oily according to claim 3 uses, it is characterised in that：The skin cream also includes
There are preservative and essence, the percentage by weight of preservative and essence in skin cream is preservative 0.25-0.45%, essence 0.1-
0.2%。
5. the skin cream that suitable Oily according to claim 4 uses, it is characterised in that：The preservative is benzene oxygen
One or more in ethanol, parabens, methylisothiazolinone；Essence is flavoring rose essence or lily essence.
6. the skin cream that suitable Oily according to claim 5 uses, it is characterised in that：The skin cream also includes
There is nertralizer, the nertralizer is the one or more in triethanolamine, sodium hydroxide or potassium hydroxide, and nertralizer is in skin cream
Percentage by weight be 0.2-0.3%.
A kind of 7. preparation method for the skin cream that any suitable Oilys of claim 1-3 use, it is characterised in that：Institute
The method of stating is to be heated to 70-80 DEG C after being well mixed emollient, emulsion stabilizer, and oil phase is made；By NMF, thickener,
70-80 DEG C is heated to after natural wooden fiber's element powder, deionized water are well mixed, aqueous phase is made；Oil phase and aqueous phase are added again
The emulsifying 3-5 minutes into vacuum homogenizer, degassing, less than 45 DEG C are cooled to, discharging, obtains skin cream.
8. the preparation method for the skin cream that suitable Oily according to claim 7 uses, it is characterised in that：The system
In Preparation Method, preservative is added after oil phase and aqueous phase emulsifying, stirs 10-30 minutes, when being cooled to 50-60 DEG C, is added
Essence, stir 5-10 minutes, degassing, continue cool to less than 45 DEG C, discharging.
9. the preparation method for the skin cream that the suitable Oily according to claim 7 or 8 uses, it is characterised in that：Institute
That states aqueous phase is added with nertralizer.
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| CN201510463877.9A CN104997653B (en) | 2015-07-31 | 2015-07-31 | Skin cream that a kind of suitable Oily uses and preparation method thereof |
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| CN104997653B true CN104997653B (en) | 2017-12-08 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105623930A (en) * | 2016-01-26 | 2016-06-01 | 四川程立农业科技有限公司 | Tea polyphenol skin-beautifying toilet soap |
| KR20180024463A (en) * | 2016-08-30 | 2018-03-08 | (주)아모레퍼시픽 | Oil-in-water type emulsion having improved stability and cosmetic composition comprising the same |
| CN106619183A (en) * | 2017-03-14 | 2017-05-10 | 广东龙湖科技股份有限公司 | Washing-free powdery shampoo and preparation method thereof |
| CN106974859A (en) * | 2017-04-05 | 2017-07-25 | 广州市聚吉科绿色化学共性技术研究院有限公司 | A kind of water lock skin-moisturizing, skin dew |
| CN108785221A (en) * | 2017-05-04 | 2018-11-13 | 周继伟 | Chinese medicine whitening essence liquid |
| CN108186401A (en) * | 2018-03-08 | 2018-06-22 | 华中科技大学同济医学院附属协和医院 | A kind of preserving moisture and protecting skin frost containing glycogen and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005008548A (en) * | 2003-06-18 | 2005-01-13 | Ikeda Shokken Kk | External preparation for skin |
| CN102603978A (en) * | 2012-01-19 | 2012-07-25 | 大连工业大学 | cellulose based water-absorbing and oil-absorbing material and preparation method thereof |
| CN102762190A (en) * | 2010-02-25 | 2012-10-31 | 株式会社欧肯 | Flat cellulose powder processed with amphiphilic substance, and cosmetic preparation containing same |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20020192245A1 (en) * | 2001-04-17 | 2002-12-19 | Jensen Claude Jarkae | Morinda Citrifolia (Noni) enhanced protective night cream moisturizer |
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2015
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005008548A (en) * | 2003-06-18 | 2005-01-13 | Ikeda Shokken Kk | External preparation for skin |
| CN102762190A (en) * | 2010-02-25 | 2012-10-31 | 株式会社欧肯 | Flat cellulose powder processed with amphiphilic substance, and cosmetic preparation containing same |
| CN102603978A (en) * | 2012-01-19 | 2012-07-25 | 大连工业大学 | cellulose based water-absorbing and oil-absorbing material and preparation method thereof |
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