CN107320395A - A kind of eye shadow and preparation method thereof - Google Patents
A kind of eye shadow and preparation method thereof Download PDFInfo
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- CN107320395A CN107320395A CN201710690178.7A CN201710690178A CN107320395A CN 107320395 A CN107320395 A CN 107320395A CN 201710690178 A CN201710690178 A CN 201710690178A CN 107320395 A CN107320395 A CN 107320395A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/34—Alcohols
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8123—Compositions of homopolymers or copolymers of compounds having one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers, e.g. PVC, PTFE
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
The invention discloses a kind of eye shadow and preparation method thereof, wherein eye shadow includes the component of following percentage by weight：Lubricant 15 28%；Anti-caking agent 1 5%；Filler 10 18%；Colouring agent 0.1 5%；Preservative 0.7 1.34%；Tin oxide 0.1 5%；Boron sikicate aluminum calcium 0.1 5%；NMF 6.1 10.2%；Emollient 18 25%；Surfactant 2 4%；Stearyl alcohol 1 2%；The ester 0.1 0.5% of pentaerythrite four；Elderberry extract 1 3%；Camellia flower extract 1 3%；Bermuda lily flower extract 1 3%；Surplus is water.It has the advantages that makeup process is submissive, not stimulated gently, moisturizing moisturizing and repair skin, is full of damp, soft and moist high resilience using rear skin water profit, effectively reduces microgroove and foxiness.
Description
Technical field
The present invention relates to cosmetic technical field, more specifically, it relates to a kind of eye shadow and preparation method thereof.
Background technology
Eye shadow is, for the cosmetics to circumference of eyes, eyes is had third dimension with color and shadow.Eye shadow has powdered, rod
Shape, paste, emulsion form and pencil-shaped.Color is very various, warm tones, cool tone and netrual colour can be divided to adjust several.In general,
The primary effect of eye shadow seeks to assign eye third dimension and makes eye more tensioned through color.
A kind of powdery eye shadow block is disclosed in Publication No. CN101804020A Chinese invention patent, with parts by weight
Meter, by following material composition：Kaolin：50~60, ultramarine：10~20, titanium dioxide：3~5, bismuth hydroxide：15~25, honeybee
Wax：2~5, isopropyl palmitate：4~8, glycerin monostearate：0.5~1, essence：0.3~0.6.This eye shadow is with tradition
Powder composition based on, the problem of existing that smearing is dry when using, be not easy to sprawl, adornment of easily swooning；And powder is to skin
Injury it is more serious, be used for a long time cause circumference of eyes red swelling of the skin, it is dry itch, astringent, pigment deposition, cutis laxa etc. are asked
Topic.
It is, therefore, desirable to provide a kind of new scheme solves the above problems.
The content of the invention
In view of the deficienciess of the prior art, the purpose of the present invention one is to provide a kind of eye shadow, by add emollient,
NMF and active botanical, the problem of solving strong, dry eye shadow excitant, injury eye skin, it has gentle
Do not stimulate, moisturizing moisturizing, repair skin advantage.
To achieve the above object one, the invention provides following technical scheme：
A kind of eye shadow, includes the component of following percentage by weight：
Lubricant 15-28%；
Anti-caking agent 1-5%；
Filler 10-18%；
Colouring agent 1-5%；
Preservative 0.7-1.34%；
Tin oxide 0.1-5%；
Boron sikicate aluminum calcium 0.1-5%；
NMF 6.1-10.2%；
Emollient 18-25%；
Surfactant 2-4%；
Stearyl alcohol 1-2%；
Pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamate) 0.1-0.5%；
Elder (SAMBUCUS NIGRA) extract 1-3%；
Camellia (CAMELLIA JAPONICA) flower extract 1-3%；
Bermuda lily (LILIUM CANDIDUM) flower extract 1-3%；
Surplus is water.
Using above-mentioned technical proposal, contain flavone compound and hydrochloric acid in elder (SAMBUCUS NIGRA) extract
Jamaicin etc. has the active material of anti-inflammation, not only has stronger inhibitory action to animal fungal and bacterium, also has
The effect of antioedematous；Camellia (CAMELLIA JAPONICA) flower extract contains several mineral materials and vitamin, phosphorus, calcium, iron,
Manganese, magnesium；Vitamin B, vitamin C (ascorbic acid), vitamin E (tocopherol), with releiving, pacify, soften, it is moisturizing, anti-ageing
Wait for a long time a variety of effects；Bermuda lily (LILIUM CANDIDUM) flower extract is applied to sensitiveness, impaired skin, particularly eye
Portion's surrounding skin, with anti-oxidant, softening, convergence and the effect for rebuilding reparation skin, three coordinates Synergistic, keeps eye
Skin health.NMF in formula, can make eye skin replenishing water and preserving moisture, lubricant, emollient with the moisture content in absorption air
The frictional force between flour and skin in eye shadow is reduced, increases smoothness, eye shadow is not stimulated gently.Pentaerythrite four (double-
Tert-butyl hydroxy hydrocinnamic acid) ester as antioxidant, effectively prevents extract, grease, aliphatic acid in eye shadow etc. by oxygen
Change.
More preferably：The emollient includes the component of following percentage by weight：
Cetanol ethylhexoate 8-10%；
Three different stearin 6-8%；
Phenyl trimethicone 3-5%；
Dimethyl silicone polymer 1-2%.
Using above-mentioned technical proposal, cetanol ethylhexoate can increase the soft and moist property of skin, and skin quality is moist, phenyl
Poly- trimethicone can reduce surface tension, product is clearly easily smeared, and not stick greasy；Dimethyl silicone polymer has eye shadow
There is sliding soft and silk-like handle, and film is formed on skin, do not stick clearly greasy.
More preferably：The NMF includes the component of following percentage by weight：Glycerine 3-5%；Saualane 3-
5%；Pungent glycol 0.1-0.2%.
Using above-mentioned technical proposal, glycerine can make eye skin replenishing water and preserving moisture with the moisture content in absorption air, and saualane is
The hydrogenated obtained a kind of squalene extracting of excellent performance of squalene extracted from hydrogenated hydro carbons grease, therefore also known as deepwater shark liver
Oil.Saualane has preferable compatibility to skin, will not cause allergy and stimulation, and can accelerate elder in formula
(SAMBUCUS NIGRA) extract, camellia (CAMELLIA JAPONICA) flower extract, bermuda lily (LILIUM
CANDIDUM) flower extract permeates into skin, and it has relatively low polarity and medium spreadability, moreover it is possible to press down mycostatic life
It is long.
More preferably：The lubricant includes the component of following percentage by weight：Mica 10-20%；Polytetrafluoroethyl-ne
Alkene 5-8%.
Using above-mentioned technical proposal, polytetrafluoroethylene (PTFE) and mica can increase smooth degree, and polytetrafluoroethylene (PTFE) also has sun-proof ability,
Low oil suction water imbibition, can be greatly reduced eye shadow and float powder situation.
More preferably：The surfactant includes the component of following percentage by weight：The stearate of polyglycereol -2
1-2%；Stearine 1-2%.
Using above-mentioned technical proposal, the stearate of polyglycereol -2 and stearine can reduce the surface tension of water,
The emulsifying capacity between each component is improved, each component more efficiently mixed, be uniformly dispersed.
More preferably：The anti-caking agent includes the component of following percentage by weight：HDI/ trihydroxy methyl hexyls Inner
Ester cross-linked polymer 0.5-2.5%；Silica 0.5-2.5%.
Using above-mentioned technical proposal, HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymers and silica surface are more smooth, as
Anti-caking agent, plays lubrication between powdered granule, reduces intergranular frictional force, powder granule is kept apart, it is to avoid
Caking.
More preferably：The filler includes the component of following percentage by weight：Polyamide fibre -125-10%；Lauroyl
Lysine 4-6%；Triethoxy octyl group silane 1-2%.
Using above-mentioned technical proposal, polyamide fibre -12 can increase product and slide soft feeling, and floating powder can be greatly reduced in low oil suction water imbibition
Situation, and degree of safety is all higher than inorganic particle with transparency；Lauroyl lysine has high-lubricity, soft and smooth skin sense, low mill
Wipe coefficient, with antistatic, inoxidizability, powder can be assigned and paste skin sense, soft and smooth sense well.
More preferably：The colouring agent include CI 77891, CI 77492, CI 77499, CI 77491,
At least one of CI77742, CI 15850, CI 19140, CI 77510, CI 77288.
Using above-mentioned technical proposal, used by the collocation of a variety of colouring agents, assign eye shadow abundant color, and will not
Skin is caused to stimulate.
More preferably：The preservative includes the component of following percentage by weight：Methyl hydroxybenzoate 0.1-0.2%；Hydroxyl
Phenylpropyl alcohol ester 0.1-0.14%；Phenoxyethanol 0.5-1.0%.
Using above-mentioned technical proposal, using cooperatively for three kinds of preservatives effectively prevents eye shadow moldy metamorphism.
The purpose of the present invention two is to provide a kind of preparation method of eye shadow, and the eye shadow prepared using this method is solved
Eye shadow excitant is strong, dry, injury eye skin the problem of, it has the advantages that not stimulate gently, moisturizing moisturizing, reparation skin.
To achieve the above object two, the invention provides following technical scheme：
A kind of preparation method of eye shadow, it is characterised in that comprise the following steps：
Step one, by mica, polytetrafluoroethylene (PTFE), HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, polyamide fibre -12, bay
Acyl lysine, triethoxy octyl group silane, methyl hydroxybenzoate, Nipasol mix 5-10min, and rotating speed is 2500-
3000rpm, is well mixed, and forms A phases, stand-by；
Step 2,5-10min is mixed by colouring agent, and rotating speed is 2500-3000rpm, is well mixed, and forms B phases, stand-by；
Step 3, A phases, B phases are put into reducing mechanism and crushed, rotating speed is 5000-6000rpm；
Step 4, the A phases after crushing, B are added in stirring container, then tin oxide, boron sikicate aluminum calcium are added into stirring container
It is interior, stir, mixing speed is 2500-3000rpm, mixing time is 5-10min, form C phases；
Step 5, water, glycerine are added in main emulsification pot, is heated to after 75 DEG C, starts stirring, rotating speed is 1000-1500rpm,
Form D1 phases；
Step 6, by saualane, pungent glycol, cetanol ethylhexoate, three different stearins, phenyl trimethicone, poly-
Dimethyl siloxane, the stearate of polyglycereol -2, stearine, stearyl alcohol, Phenoxyethanol, (double-tertiary fourths of pentaerythrite four
Base hydroxyhydrocinnamic acid) ester adds in secondary emulsification pot, is heated to after 75 DEG C, starts stirring, rotating speed is 1000-1500rpm, shape
Into D2 phases；
Step 7, expects that body is pumped into main emulsification pot by D2 phases, starts homogeneous, rotating speed is 2500-300rpm, and the time is 5-10min,
10-20min is incubated after the completion of homogeneous；
Step 8, the material in step 7 is cooled to 40 DEG C, sequentially adds elder (SAMBUCUS NIGRA) extraction
Thing, camellia (CAMELLIA JAPONICA) flower extract, bermuda lily (LILIUM CANDIDUM) flower extract stir,
- 0.1Mpa is evacuated to after well mixed；
Step 9, the material in step 8 is cooled to 30 DEG C, forms D phases；
Step 10, C phases, D are mixed and are formed uniformly lotion, lotion are injected into compressing in mould, using dehumidifier by cream
Moisture in body is taken away, obtains eye shadow.
Using above-mentioned technical proposal, because the A phases in the application and B phases are mostly hydrophobicity powder, it is difficult to water, glycerine
It is uniformly dispersed with extract.It has been investigated that, first, the components such as the grease in formula, glycerine, extract are emulsified as emulsion；
Secondth, by emulsion and powder under high velocity agitation, the material body as paste；3rd, the material body of paste is injected in mould and suppressed
Shaping；4th, the function using dehumidifier, will expect that the moisture content in body is siphoned away, while remaining the effective ingredient in formula, make each
Component is dispersed, thus be made with not stimulating gently, moisturizing moisturizing, the eye shadow of reparation skin effect.
In summary, the invention has the advantages that：
It has been investigated that, elder (SAMBUCUS NIGRA) extract, camellia (CAMELLIA JAPONICA) flower extract,
Bermuda lily (LILIUM CANDIDUM) flower extract is applied to sensitiveness, impaired skin, particularly circumference of eyes skin, tool
There are anti-oxidant, softening, convergence and rebuild to repair skin, three coordinates Synergistic, keeps eye part skin health.Spiny dogfish
Alkane has preferable compatibility to skin, will not cause allergy and stimulation, and can accelerate elder (SAMBUCUS in formula
NIGRA) extract, camellia (CAMELLIA JAPONICA) flower extract, bermuda lily (LILIUM CANDIDUM) flower are extracted
Thing permeates into skin.
Glycerine in formula can make eye skin replenishing water and preserving moisture, lubricant, emollient reduction with the moisture content in absorption air
Frictional force in eye shadow between flour and skin, increases smoothness, eye shadow is not stimulated gently and is easily smeared, do not stick clearly
It is greasy, make eye shadow that there is sliding soft and silk-like handle, and be easy on skin form film.(double-tert-butyl hydroxy the hydrogenation of pentaerythrite four
Cinnamic acid) ester as antioxidant, effectively prevents extract, grease, aliphatic acid in eye shadow etc. to be oxidized.Polyamide fibre -12, poly- four
PVF has low oil suction water imbibition, and eye shadow can be greatly reduced and floats powder situation.
Brief description of the drawings
Fig. 1 is preparation method flow chart of the invention.
Embodiment
With reference to embodiment and accompanying drawing, the present invention will be described in detail.
Embodiment 1：As shown in figure 1, a kind of eye shadow, each component and its corresponding percentage by weight are as shown in table 1, and pass through
Following steps are prepared：
Step one, by mica, polytetrafluoroethylene (PTFE), HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, polyamide fibre -12, bay
Acyl lysine, triethoxy octyl group silane, methyl hydroxybenzoate, Nipasol stirring 5-10min, rotating speed is 2500-3000rpm, is mixed
Close uniform, form A phases, it is stand-by；
Step 2,5-10min is stirred by colouring agent, and rotating speed is 2500-3000rpm, is well mixed, and forms B phases, stand-by；
Step 3, A phases, B phases are put into reducing mechanism and crushed, rotating speed is 5000-6000rpm；
Step 4, the A phases after crushing, B are added in stirring container, then tin oxide, boron sikicate aluminum calcium are added into stirring container
It is interior, stir, mixing speed is 2500-3000rpm, mixing time is 5-10min, form C phases；
Step 5, water, glycerine are added in main emulsification pot, is heated to after 75 DEG C, starts stirring, rotating speed is 1000-1500rpm,
Form D1 phases；
Step 6, by saualane, pungent glycol, cetanol ethylhexoate, three different stearins, phenyl trimethicone, poly-
Dimethyl siloxane, the stearate of polyglycereol -2, stearine, stearyl alcohol, Phenoxyethanol, (double-tertiary fourths of pentaerythrite four
Base hydroxyhydrocinnamic acid) ester adds in secondary emulsification pot, is heated to after 75 DEG C, starts stirring, rotating speed is 1000-1500rpm, shape
Into D2 phases；
Step 7, expects that body is pumped into main emulsification pot by D2 phases, starts homogeneous, rotating speed is 2500-300rpm, and the time is 5-10min,
10-20min is incubated after the completion of homogeneous；
Step 8, the material in step 7 is cooled to 40 DEG C, sequentially adds elder (SAMBUCUS NIGRA) extraction
Thing, camellia (CAMELLIA JAPONICA) flower extract, bermuda lily (LILIUM CANDIDUM) flower extract stir,
- 0.1Mpa is evacuated to after well mixed；
Step 9, the material in step 8 is cooled to 30 DEG C, forms D phases；
Step 10, C phases, D are mixed and are formed uniformly lotion, lotion are injected into compressing in mould, using dehumidifier by cream
Moisture in body is taken away, obtains eye shadow.
Embodiment 2-10：A kind of eye shadow, is with the difference of embodiment 1, each component and its corresponding weight percent
Than as shown in table 1.
Each component and its percentage by weight in the embodiment 1-10 of table 1
Embodiment 11-20：A kind of eye shadow, is with the difference of embodiment 3, and each component and its corresponding weight percent are such as
Shown in table 2.
Each component and its percentage by weight in the embodiment 11-20 of table 2
Embodiment 21-26：A kind of eye shadow, is with the difference of embodiment 3, and each component and its corresponding weight percent are such as
Shown in table 3.
Each component and its percentage by weight in the embodiment 11-20 of table 3
Comparative example 1：A kind of eye shadow, is with the difference of embodiment 3, and cetanol ethylhexoate, three different tristearin are not added
Essence, phenyl trimethicone, dimethyl silicone polymer.
Comparative example 2：A kind of eye shadow, is with the difference of embodiment 3, and glycerine, saualane, pungent glycol are not added.
Comparative example 3：A kind of eye shadow, is, NMF only adds 1% glycerine with the difference of embodiment 3.
Comparative example 4：A kind of eye shadow, is with the difference of embodiment 3, and bermuda lily flower extract is not added.
Comparative example 5：A kind of eye shadow, is with the difference of embodiment 3, and camellia flower extract is not added.
Comparative example 6：A kind of eye shadow, is with the difference of embodiment 3, and camellia flower extract and bermuda lily are not added
Flower extract.
Comparative example 7：A kind of eye shadow, is with the difference of embodiment 3, do not add polyamide fibre -12, lauroyl lysine,
Triethoxy octyl group silane.
Comparative example 8：A kind of eye shadow, is with the difference of embodiment 3, and acquisition is made by the steps：Weigh each
Component, all components are well mixed and remove moisture obtain eye shadow.
Test a makeup and preserving moisture and protecting skin effect test
Test specimen：Using the eye shadow obtained in embodiment 1-26 as test specimen 1-26, using what is obtained in comparative example 1-8
Eye shadow is used as control sample 1-8.
Test method：Eye part skin that choose areal, that the age is 18-35 one full year of life has drying, pigment deposition, skin
The women white collar subject 3400 of the problems such as relaxation, is divided into 34 groups, number consecutively 1-34 groups.Subject is respectively using examination
Sample 1-26 and control sample 1-8 are tested, record subject gives up every group most using use feeling and effect after one month
5 values of big 5 values and minimum, it is remaining to take its average value.
Result of the test：The use feeling and effect of 1-34 group subjects is as shown in table 4.As shown in Table 4, in the application
Cetanol ethylhexoate, three different stearins, phenyl trimethicone and dimethyl silicone polymer are used cooperatively, can
The excitant of eye shadow is reduced, makeup process is submissive, does not stimulate gently；Glycerine, saualane, using cooperatively for pungent glycol enhance eye
The moisturizing moisturizing performance of shadow, after camellia (CAMELLIA JAPONICA) flower extract, moistening effect is obtained significantly
Lifting；The addition of lubricant, anti-caking agent and filler, improves the smoothness of eye shadow, can assign powder and paste well
Skin sense, soft and smooth sense.
The use feeling and effect of the 1-34 group subjects of table 4
Test the test of two physical indexs
Test specimen：Using the eye shadow obtained in embodiment 1-5 as test specimen 1-5.
Test method：With reference to QB/T1976-2004《Cosmetic powder agglomates》Specified in method test specimen 1-5 is examined
Survey, examination criteria is as shown in table 5.
Result of the test：Test specimen 1-5 physical index test result is as shown in table 5.
The testing result of the examination criteria of table 5 and test specimen 1-5
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-described embodiment,
All technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
For those of ordinary skill, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (10)
1. a kind of eye shadow, it is characterised in that include the component of following percentage by weight：
Lubricant 15-28%；
Anti-caking agent 1-5%；
Filler 10-18%；
Colouring agent 0.1-5%；
Preservative 0.7-1.34%；
Tin oxide 0.1-5%；
Boron sikicate aluminum calcium 0.1-5%；
NMF 6.1-10.2%；
Emollient 18-25%；
Surfactant 2-4%；
Stearyl alcohol 1-2%；
Pentaerythrite four（Double-tert-butyl hydroxy hydrocinnamic acid）Ester 0.1-0.5%；
Elder（SAMBUCUS NIGRA）Extract 1-3%；
Camellia（CAMELLIA JAPONICA）Flower extract 1-3%；
Bermuda lily（LILIUM CANDIDUM）Flower extract 1-3%；
Surplus is water.
2. eye shadow according to claim 1, it is characterised in that the emollient includes the component of following percentage by weight：
Cetanol ethylhexoate 8-10%；
Three different stearin 6-8%；
Phenyl trimethicone 3-5%；
Dimethyl silicone polymer 1-2%.
3. eye shadow according to claim 1, it is characterised in that the NMF includes the component of following percentage by weight：
Glycerine 3-5%；Saualane 3-5%；Pungent glycol 0.1-0.2%.
4. eye shadow according to claim 1, it is characterised in that the surfactant includes the group of following percentage by weight
Point：The stearate of polyglycereol -2 1-2%；Stearine 1-2%.
5. eye shadow according to claim 1, it is characterised in that the lubricant includes the component of following percentage by weight：
Mica 10-20%；Polytetrafluoroethylene (PTFE) 5-8%.
6. eye shadow according to claim 1, it is characterised in that the anti-caking agent includes the group of following percentage by weight
Point：HDI/ trihydroxy methyl hexyl Inner ester cross-linked polymers 0.5-2.5%；Silica 0.5-2.5%.
7. eye shadow according to claim 1, it is characterised in that the filler includes the component of following percentage by weight：
The 5-10% of polyamide fibre -12；Lauroyl lysine 4-6%；Triethoxy octyl group silane 1-2%.
8. eye shadow according to claim 1, it is characterised in that the colouring agent includes CI 77891, CI 77492, CI
77499th, at least one of CI 77491, CI 77742, CI 15850, CI 19140, CI 77510, CI 77288.
9. eye shadow according to claim 1, it is characterised in that the preservative includes the component of following percentage by weight：
Methyl hydroxybenzoate 0.1-0.2%；Nipasol 0.1-0.14%；Phenoxyethanol 0.5-1.0%.
10. a kind of preparation method of eye shadow, it is characterised in that comprise the following steps：
Step one, by mica, polytetrafluoroethylene (PTFE), HDI/ trihydroxy methyl hexyl Inner esters cross-linked polymer, silica, polyamide fibre -12, bay
Acyl lysine, triethoxy octyl group silane, methyl hydroxybenzoate, Nipasol mix 5-10min, and rotating speed is 2500-
3000rpm, is well mixed, and forms A phases, stand-by；
Step 2,5-10min is mixed by colouring agent, and rotating speed is 2500-3000rpm, is well mixed, and forms B phases, stand-by；
Step 3, A phases, B phases are put into reducing mechanism and crushed, rotating speed is 5000-6000rpm；
Step 4, the A phases after crushing, B are added in stirring container, then tin oxide, boron sikicate aluminum calcium are added into stirring container
It is interior, stir, mixing speed is 2500-3000rpm, mixing time is 5-10min, form C phases；
Step 5, water, glycerine are added in main emulsification pot, is heated to after 75 DEG C, starts stirring, rotating speed is 1000-1500rpm,
Form D1 phases；
Step 6, by saualane, pungent glycol, cetanol ethylhexoate, three different stearins, phenyl trimethicone, poly-
Dimethyl siloxane, the stearate of polyglycereol -2, stearine, stearyl alcohol, Phenoxyethanol, pentaerythrite four（Double-tertiary fourths
Base hydroxyhydrocinnamic acid）Ester is added in secondary emulsification pot, is heated to after 75 DEG C, is started stirring, rotating speed is 1000-1500rpm, shape
Into D2 phases；
Step 7, expects that body is pumped into main emulsification pot by D2 phases, starts homogeneous, rotating speed is 2500-300rpm, and the time is 5-10min,
10-20min is incubated after the completion of homogeneous；
Step 8, the material in step 7 is cooled to 40 DEG C, elder is sequentially added（SAMBUCUS NIGRA）Extract
Thing, camellia（CAMELLIA JAPONICA）Flower extract, bermuda lily（LILIUM CANDIDUM）Flower extract stirs,
- 0.1Mpa is evacuated to after well mixed；
Step 9, the material in step 8 is cooled to 30 DEG C, forms D phases；
Step 10, C phases, D are mixed and are formed uniformly lotion, lotion are injected into compressing in mould, using dehumidifier by cream
Moisture in body is taken away, obtains eye shadow.
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| CN108309827A (en) * | 2018-02-06 | 2018-07-24 | 陈云 | A kind of flexible glue eye shadow and preparation method thereof |
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| CN113244135A (en) * | 2021-05-28 | 2021-08-13 | 美尚(广州)化妆品股份有限公司 | Oil wax type makeup cosmetic powder and preparation method thereof |
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