CN115068389A - Multi-effect composition, essence cream and preparation method thereof - Google Patents

Multi-effect composition, essence cream and preparation method thereof Download PDF

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CN115068389A
CN115068389A CN202210873166.9A CN202210873166A CN115068389A CN 115068389 A CN115068389 A CN 115068389A CN 202210873166 A CN202210873166 A CN 202210873166A CN 115068389 A CN115068389 A CN 115068389A
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extract
skin
essence cream
essence
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CN115068389B (en
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苏剑君
王明奎
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Guangzhou Dongsen Medicine Science & Technology Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

Abstract

The invention discloses a multi-effect composition, essence cream and a preparation method thereof, and relates to the technical field of cosmetics, wherein the multi-effect composition comprises the following components in parts by weight: 0.1-0.6 part of lactalbumin, 0.2-2.5 parts of Daisy chrysanthemum extract, 0.3-1.2 parts of magnolia liliflora bark extract and 0.2-5.0 parts of gentian root extract. The multi-effect composition disclosed by the invention is free of stimulation and high in safety, and has multiple effects of resisting wrinkles, tightening, moistening, brightening skin and the like. The invention also discloses an essence cream containing the multi-effect composition, and the essence cream has good stability and skin feel, and can effectively improve skin elasticity, deeply moisturize and brighten skin.

Description

Multi-effect composition, essence cream and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a multi-effect composition, essence cream and a preparation method thereof.
Background
The skin care product has the advantages of whitening and tendering skin, improving the external image of people and enhancing the self-confidence of people. Dry, dull and rough skin is not desired by everyone, but with the age and the stimulation of the living environment including ultraviolet rays and dust, various problems inevitably exist. Aiming at the problems of dry, rough, loose, dull skin and the like, people adopt corresponding skin care products to carry out maintenance and care, thereby improving the condition of gradually worsening skin and enabling the skin to recover young.
The essence care products, including essence cream, essence liquid, essence lotion and the like, have high-efficiency and long-lasting skin care effects. However, most of the existing essence care products have strong single function and lack multiple effects, only have strong effects of single moisturizing, whitening and the like, and cannot solve various problems of the skin at the same time. In addition, most of the existing essences are mainly dependent on the addition of various skin conditioning agents in providing skin feel, so that the skin feel conditioner is expensive, is easy to cause dependence, and is easy to form a new stimulus to cause other damages to the skin.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a multi-effect composition, essence cream and a preparation method thereof, wherein the multi-effect composition has the advantages of no stimulation, high safety, good stability and skin feeling, wrinkle resistance, firmness, moistening and skin brightening.
In order to achieve the purpose, the invention adopts the technical scheme that: a multi-effect composition comprises the following components in parts by weight: 0.1-0.6 part of lactalbumin, 0.2-2.5 parts of Daisy chrysanthemum extract, 0.3-1.2 parts of magnolia sieboldii bark extract and 0.2-5.0 parts of gentian root extract.
In the technical scheme of the invention, the lactalbumin is an active natural signal molecule extracted from milk and can help the regeneration and recovery of mature skin; it can induce the synthesis of extracellular matrix molecules (such as type I collagen) in the dermis, making the skin more firm and increasing elasticity.
Extract of daisy (BELLIS PERENNIS): a skin whitening agent extracted from organic Daisy flower has effects of reducing melanin activity, making pigmentation more uniform, and lightening mottle. Meanwhile, the daisy extract contains a plurality of components such as tannin, saponin, mucus and the like, and has the functions of anti-inflammation, sedation and relaxation.
Magnolia GRANDIFLORA (Magnolia GRANDIFLORA) bark extract: can be used for treating sensitive skin, relieving neurogenic inflammation, and relieving skin redness.
The extract of radix Gentianae (GENTIANA SCABRA) mainly contains gentiopicroside, gentiobiose and gentisic acid, and has effects of resisting oxidation, and relieving and tranquilizing.
Through the matching combination of the natural ingredients, the obtained multi-effect composition has no stimulation and high safety, and has the effects of obviously cooperating with wrinkle resistance, tightening, moistening and skin brightening.
Preferably, the multi-effect composition comprises the following components in parts by weight: 0.2-0.4 part of lactalbumin, 0.6-1.5 parts of Daisy chrysanthemum extract, 0.3-0.8 part of magnolia sieboldii bark extract and 1.0-3.8 parts of gentian root extract.
The invention also aims to provide essence cream which contains the multi-effect composition and also comprises the following components: emulsifier, humectant, emollient, thickener, antioxidant, preservative, emulsion stabilizer, pH regulator, chelating agent and water; wherein, the emulsifier comprises potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate.
In the existing common cosmetic components, the emulsifier mainly plays roles in emulsification, dispersion, solubilization, lubrication and the like, and mainly comprises an anionic emulsifier and a nonionic emulsifier. Among them, anionic emulsifiers have poor hard water resistance, are slightly irritating, and have limited compatibility with the ingredients of the formulation. The non-ionic emulsifier has wide selectivity, hard water resistance, wide pH application range, strong emulsifying power, strong formula adaptability and low irritation.
Based on multiple effects brought by the multi-effect composition, when the multi-effect composition is further prepared into an essence cream product, the inventor adopts a unique emulsifying system and utilizes the anionic emulsifier and the nonionic emulsifier to carry out compounding, so that not only can a good emulsifying effect be ensured, but also an additional technical effect is brought at the same time under a specific proportion.
In the components of the essence cream, potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate are compounded to serve as emulsifying components, the emulsifying components can act together with a multi-effect composition under a specific proportion, no additional skin regulator is needed to be added, a good moisturizing effect and skin feel are provided, and the effects of wrinkle resistance, firmness, moisturizing and skin brightening are influenced by the synergistic effect of the emulsifying components and the multi-effect composition. If the proportion of the emulsified components is not proper, the stability of the essence cream is poor, and the effects of improving the elasticity, moisturizing and skin glossiness and using the essence cream are obviously reduced.
Preferably, the essence cream comprises the following components in percentage by mass: 0.8-9.3% of multi-effect composition, 1.9-7.0% of emulsifier, 1.3-6.64% of humectant, 5.0-17.0% of softening agent, 0.1-0.5% of thickening agent, 0.1-1.0% of antioxidant, 0.3-1.0% of preservative, 0.85-2.2% of emulsion stabilizer, 0.1-0.6% of pH regulator, 0.01-0.1% of chelating agent and the balance of water.
Preferably, the mass ratio of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate is (0.2-1.0): (1.2-4.0): (0.5-2.0).
Preferably, the mass ratio of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate is (0.4-0.6): (3.0-3.5): (0.5-1.0).
Preferably, the mass ratio of the potassium cetyl phosphate to the PEG-20 tribehenate to the PEG-100 stearate is 0.6:3.0: 1.0.
Preferably, the moisturizer comprises butylene glycol, rehmannia glutinosa extract, acetylated sodium hyaluronate, ethylhexyl glycerin and 1, 2-hexanediol;
the emollient comprises isononyl isononanoate, polydimethylsiloxane and shea butter;
the thickening agent is an acryloyl dimethyl ammonium taurate/VP copolymer;
the antioxidant is tocopherol acetate;
the preservative is phenoxyethanol;
the emulsion stabilizer comprises acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and C14-22 alcohol;
the pH regulator comprises arginine and sodium citrate;
the chelating agent is disodium EDTA.
Preferably, the essence cream comprises the following components in percentage by mass: 0.1-0.6% of whey protein, 0.2-2.5% of Daisy chrysanthemum extract, 0.3-1.2% of Magnolia liliiflora bark extract, 0.2-5.0% of gentian root extract, 0.2-1.0% of potassium cetyl phosphate, 1.2-4.0% of behenyl PEG-20 esters, 0.5-2.0% of PEG-100 stearate, 1.0-5.0% of butanediol, 0.02-0.2% of Chinese rehmannia root extract, 0.03-0.24% of sodium hyaluronate, 0.05-0.2% of ethylhexyl glycerol, 0.2-1.0% of 1, 2-hexanediol, 2.0-7.0% of isononyl isononanoate, 2.0-6.0% of polydimethylsiloxane, 1.0-4.0% of shea butter, 0.1-0.5% of ammonium acryloyl dimethyl taurate/VP copolymer, and 0.1-1.0% of tocopherol acetate; 0.3 to 1.0 percent of phenoxyethanol, 0.05 to 0.2 percent of acrylic acid (ester)/C10 to 30 percent of alkanol acrylate cross-linked polymer, 0.8 to 2.0 percent of C14 to 22 alcohol, 0.05 to 0.4 percent of arginine, 0.05 to 0.2 percent of sodium citrate and 0.01 to 0.1 percent of EDTA disodium.
Further, the invention provides a preparation method of the essence cream, and the preparation method comprises the following steps:
(1) sequentially adding EDTA disodium, acryloyl dimethyl ammonium taurate/VP copolymer, butanediol, potassium cetyl phosphate, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, Chinese rehmannia root extract and sodium acetylhyaluronate into an emulsifying pot, heating to 80-85 ℃, and uniformly stirring to obtain phase A;
(2) sequentially adding PEG-20 esters of behenyl trimaran, PEG-100 stearate, isononyl isononanoate, C14-22 alcohol, polydimethylsiloxane, tocopheryl acetate and shea butter into an oil phase pot, and heating to 80-82 ℃ to obtain a phase B;
(3) sucking the phase B into an emulsifying pot, homogenizing at the speed of 2800-3200 rpm for 4-6 minutes, adding arginine, uniformly stirring, and cooling to below 45 ℃ to obtain phase C;
(4) adding pre-dispersed water, sodium citrate and whey protein into the phase C, and homogenizing at the speed of 1800-2200 rpm for 4-6 minutes to obtain a phase D;
(5) adding pre-dissolved Daisy extract, Magnolia liliflora bark extract, phenoxyethanol, ethylhexylglycerin, 1, 2-hexanediol, and radix Gentianae extract into phase D, stirring, and cooling to below 40 deg.C to obtain the essence cream.
The preparation method of the essence cream has simple operation steps, has low requirement on processing equipment, and can realize industrial mass production.
Compared with the prior art, the invention has the following beneficial effects:
(1) the multi-effect composition takes whey protein, a marguerite extract, a magnolia sieboldii bark extract and a gentian root extract as components, and when the multi-effect composition is prepared according to a specific proportion, the components can act synergistically, so that the multi-effect composition has multiple effects of resisting wrinkles, tightening, moistening and brightening skin. In addition, the added gentian root extract and magnolia liliflora bark extract are used as anti-allergy and relieving components, so that the product is free of irritation and high in safety, and is suitable for various skin people.
(2) The essence cream disclosed by the invention is further matched with a unique emulsifying system consisting of potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate on the basis of introducing a multi-effect composition, so that the stability of the product is guaranteed, a special moisturizing effect and skin feel are provided, a plurality of skin conditioning agents are not required to be additionally added for skin feel conditioning, and the obtained essence cream can effectively improve the skin elasticity, deeply moisturize and brighten the skin.
Detailed Description
To better illustrate the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to specific examples, but the scope of the present invention and the embodiments are not limited thereto.
Example 1
According to one embodiment of the essence cream, the raw material proportion of the essence cream is shown in table 1, and the preparation method of the essence cream comprises the following steps:
(1) accurately weighing each component material in the formula components, and simultaneously cleaning production equipment;
(2) sequentially adding EDTA disodium, acryloyl dimethyl ammonium taurate/VP copolymer, butanediol, potassium cetyl phosphate, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, Chinese rehmannia root extract and sodium acetylhyaluronate into an emulsifying pot, heating to 80-85 ℃, and uniformly stirring to obtain phase A;
(3) sequentially adding PEG-20 esters of Tribehenyl alcohol, PEG-100 stearate, isononyl isononanoate, C14-22 alcohol, polydimethylsiloxane, tocopheryl acetate and shea butter into an oil phase pot, and heating to 80-82 ℃ to obtain a phase B;
(4) sucking phase B into emulsifying pot, homogenizing at 3000rpm for 5 min, adding arginine, stirring, and cooling to below 45 deg.C to obtain phase C;
(5) adding pre-dispersed water, sodium citrate and whey protein into phase C, and homogenizing at 2000rpm for 5 min to obtain phase D;
(6) adding pre-dissolved Daisy extract, Magnolia liliflora bark extract, phenoxyethanol, ethylhexylglycerin, 1, 2-hexanediol, and radix Gentianae extract, stirring, and cooling to below 40 deg.C to obtain the essence cream.
Examples 2 to 6
The raw material proportions of the essence cream in the examples of the invention, examples 2-6 are shown in table 1. The preparation method is the same as that of example 1.
Table 1 composition of essence creams of examples 1 to 6 in percentage by mass (%)
Figure BDA0003761208580000051
Figure BDA0003761208580000061
Comparative example 1
The comparative example is different from example 2 only in that the components of the essence cream of the comparative example do not contain potassium cetyl phosphate.
Comparative example 2
The difference between the comparative example and the example 2 is that the components of the essence cream of the comparative example do not contain the behenyl alcohol PEG-20 ester and the PEG-100 stearate.
Comparative example 3
The comparative example differs from example 2 only in that the components of the essence cream of the comparative example do not contain potassium cetyl phosphate and PEG-20 tribehenate.
Comparative example 4
The difference between the comparative example and the example 2 is only that the addition amounts of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate in the components of the essence cream of the comparative example are respectively 0.1%, 0.5% and 0.2%.
Comparative example 5
The difference between the comparative example and the example 2 is that the addition amounts of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate in the components of the essence cream of the comparative example are respectively 2.0%, 0.3% and 3.5%.
Comparative example 6
The difference between the comparative example and the example 2 is only that the addition amounts of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate in the components of the essence cream of the comparative example are 3.0%, 6.8% and 0.1% respectively.
Comparative example 7
The difference between the comparative example and the example 2 is only that the addition amounts of the potassium cetyl phosphate, the PEG-20 tribehenate and the PEG-100 stearate in the components of the essence cream of the comparative example are respectively 0.05%, 7.0% and 3.2%.
Comparative example 8
The comparative example is different from example 2 only in that the components of the essence cream of the comparative example comprise 0.05%, 0.1% and 0.1% of whey protein, 0.1% of daisy extract and 0.1% of magnolia liliflora bark extract.
Comparative example 9
The comparative example is different from example 2 only in that the components of the essence cream of the comparative example comprise 0.8%, 0.08% and 0.05% of whey protein, an extract of marguerite and an extract of magnolia liliiflora bark.
Comparative example 10
The comparative example is different from example 2 only in that the components of the essence cream of the comparative example comprise 0.03%, 4.0% and 0.02% of whey protein, an extract of marguerite and an extract of magnolia liliiflora bark.
Comparative example 11
The comparative example is different from example 2 only in that the addition amounts of the gentian root extract and the magnolia liliflora bark extract in the components of the essence cream of the comparative example are 0.6% and 0.08%, respectively.
Comparative example 12
The comparative example is different from example 2 only in that the addition amounts of the gentian root extract and the magnolia liliflora bark extract in the components of the essence cream of the comparative example are 0.01% and 6.8% respectively.
Comparative example 13
The comparative example differs from example 2 only in that potassium cetyl phosphate in the components of the essence cream of the comparative example is replaced with span 80, a conventional emulsifier.
Comparative example 14
The comparative example is different from example 2 only in that the components of the essence cream of the comparative example do not contain whey protein, and the addition amounts of the daisy extract, the magnolia liliflora bark extract and the gentian root extract are respectively 1.5%, 0.8% and 1.0%.
Comparative example 15
The comparative example differs from example 2 only in that the whey protein in the components of the comparative example cream was replaced with oat peptide.
The essence creams of comparative examples 1 to 15 were prepared in the same manner as in example 1.
Effect example 1
In order to verify the stability performance of the essence cream of the present invention under different conditions, physicochemical performance tests were performed on the essence creams prepared in examples 1 to 6 and comparative examples 1 to 15. The results of the physicochemical properties of the essence cream, including appearance, pH, heat resistance (45. + -. 2 ℃ for 2 months), cold resistance-17. + -. 2 ℃ for 2 months, and cycle (45 ℃ at room temperature, -17 ℃ for 3 cycles), are shown in Table 2.
Table 2 results of physicochemical property test of the essence creams of examples 1 to 6 and comparative examples 1 to 15
Figure BDA0003761208580000091
As can be seen from Table 2, the essence creams of examples 1 to 6, comparative examples 8 to 12 and comparative examples 14 to 15 all have good stability under heat resistance (45 + -2 ℃,2 months), cold resistance-17 + -2 ℃,2 months), and cycling (45 ℃, room temperature, -17 ℃, 3 cycles). The comparative examples 1 to 3 do not completely contain the whole emulsifier components of the present invention, the amounts of potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate in the comparative examples 4 to 7 are out of the range of the present invention, the potassium cetyl phosphate in the comparative example 13 is replaced with other emulsifiers, and the obtained essence cream shows a phenomenon of delamination or slight delamination.
Effect example 2
In order to verify the performance effects of the essence cream of the invention on resisting wrinkles, tightening, moistening and moisturizing and brightening skin, the skin elasticity, the skin moisture content and the skin glossiness of the products of examples 1-6 and comparative examples 1-15 are tested, and the specific steps are as follows:
test object(s): 63 female volunteers, 30-55 years old, had wrinkles on the cheeks, dry skin, poor facial skin elasticity, and no other obvious skin problems. The random division into 21 groups, each corresponding to the compositions of test examples 1-6 and comparative examples 1-15, respectively.
The test method comprises the following steps: applying the corresponding test sample to cheek 2 times a day, once in the morning and once in the evening; the sample is pushed evenly by finger abdomen during smearing process, and the skin is massaged to make the sample be absorbed sufficiently. The application is continued for 4 weeks.
1. Skin elasticity test
By using
Figure BDA0003761208580000102
The MPA580 tester measures the skin tightness F4 value and the skin tightness F4 value of the skin of a test object before and after using the essence creamA smaller F4 value indicates a tighter skin. The results of the skin tightness F4 values tested are shown in table 3.
Table 3 skin tightening test results of the essences of examples 1 to 6 and comparative examples 1 to 15
Figure BDA0003761208580000101
Figure BDA0003761208580000111
As can be seen from Table 3, after the essence cream of the invention is continuously used for 4 weeks, the F4 value of skin firming is reduced, and the essence cream of the invention has the effects of resisting wrinkles and firming. Comparative examples 1 to 12 and comparative examples 14 to 15, which are inferior to the present invention in skin firmness improving effects.
2. Deep moisturizing efficacy test
The skin moisture content of the test subjects before and after the application of the essence cream was measured using a skin moisture tester (CKCorneometer CM 825, germany), and the test results are shown in table 4.
Table 4 skin moisture content test results of the essences of examples 1 to 6 and comparative examples 1 to 15
Figure BDA0003761208580000112
Figure BDA0003761208580000121
As can be seen from table 4, the essence cream of the present invention has a more significant moisturizing effect than the comparative example.
3. Skin gloss test
The skin gloss was tested using a multifunctional skin tester (CK, Germany, model GL 200).
Skin gloss increase (%) - (An-a0)/a0 × 100%.
Table 5 skin gloss test results of the essences of examples 1 to 6 and comparative examples 1 to 15
Figure BDA0003761208580000122
Figure BDA0003761208580000131
As can be seen from table 5, the essence cream of the present invention significantly increased skin gloss after 4 weeks of use.
4. Evaluation of Using Effect
In order to evaluate the comprehensive use effect of the essence cream, the use effect of a corresponding test sample is graded and evaluated by a test object, and the full score is 10.
Table 6 results of evaluation of use effects of the essences of examples 1 to 6 and comparative examples 1 to 15
Figure BDA0003761208580000132
Figure BDA0003761208580000141
Figure BDA0003761208580000151
From the results in table 6, in examples 1 to 6, the irritation evaluations of all the test subjects were non-irritating, and in terms of the use experience, the effects of improving the firmness and elasticity of the skin, brightening and shining the skin, achieving a good moisturizing effect, and providing fine and smooth skin feel were shown. The essence cream prepared by the invention has no stimulation and high safety, and has multiple effects of resisting wrinkles, tightening, moistening and brightening skin. From the evaluation of the effects of comparative examples 1 to 15, it was found that the essence cream of the present invention was inferior in irritation, moisturizing effect, skin feel, and improvement of skin firmness, elasticity and glossiness.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (9)

1. The multi-effect composition is characterized by comprising the following components in parts by weight: 0.1-0.6 part of lactalbumin, 0.2-2.5 parts of Daisy chrysanthemum extract, 0.3-1.2 parts of magnolia liliflora bark extract and 0.2-5.0 parts of gentian root extract.
2. The composition of claim 1, comprising the following components in parts by weight: 0.2-0.4 part of lactalbumin, 0.6-1.5 parts of Daisy chrysanthemum extract, 0.3-0.8 part of magnolia sieboldii bark extract and 1.0-3.8 parts of gentian root extract.
3. The essence cream is characterized by comprising the following components: the multi-effect composition of any one of claims 1-2, an emulsifier, a humectant, an emollient, a thickener, an antioxidant, a preservative, an emulsion stabilizer, a pH adjuster, a chelating agent, and water;
wherein the emulsifier comprises potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate.
4. The essence cream of claim 3, characterized by comprising the following components in percentage by mass: 0.8-9.3% of multi-effect composition, 1.9-7.0% of emulsifier, 1.3-6.64% of humectant, 5.0-17.0% of softening agent, 0.1-0.5% of thickening agent, 0.1-1.0% of antioxidant, 0.3-1.0% of preservative, 0.85-2.2% of emulsion stabilizer, 0.1-0.6% of pH regulator, 0.01-0.1% of chelating agent and the balance of water.
5. The essence of any of claims 3 to 4 wherein the mass ratio of potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate is (0.2-1.0): (1.2-4.0): (0.5-2.0).
6. The essence of claim 5 wherein the mass ratio of potassium cetyl phosphate, PEG-20 tribehenate and PEG-100 stearate is (0.4-0.6): (3.0-3.5): (0.5-1.0).
7. The essence of any one of claims 3 to 4, wherein the moisturizer comprises butylene glycol, rehmannia root extract of China, sodium hyaluronate acetylated, ethylhexylglycerin and 1, 2-hexanediol;
the emollient comprises isononyl isononanoate, polydimethylsiloxane and shea butter;
the thickening agent is an acryloyl dimethyl ammonium taurate/VP copolymer;
the antioxidant is tocopherol acetate;
the preservative is phenoxyethanol;
the emulsion stabilizer comprises acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer and C14-22 alcohol;
the pH regulator comprises arginine and sodium citrate;
the chelating agent is disodium EDTA.
8. The essence cream according to claim 7, which comprises the following components in percentage by mass: 0.1-0.6% of whey protein, 0.2-2.5% of Daisy chrysanthemum extract, 0.3-1.2% of Magnolia liliiflora bark extract, 0.2-5.0% of gentian root extract, 0.2-1.0% of potassium cetyl phosphate, 1.2-4.0% of behenyl PEG-20 esters, 0.5-2.0% of PEG-100 stearate, 1.0-5.0% of butanediol, 0.02-0.2% of Chinese rehmannia root extract, 0.03-0.24% of sodium hyaluronate, 0.05-0.2% of ethylhexyl glycerol, 0.2-1.0% of 1, 2-hexanediol, 2.0-7.0% of isononyl isononanoate, 2.0-6.0% of polydimethylsiloxane, 1.0-4.0% of shea butter, 0.1-0.5% of ammonium acryloyl dimethyl taurate/VP copolymer, and 0.1-1.0% of tocopherol acetate; 0.3 to 1.0 percent of phenoxyethanol, 0.05 to 0.2 percent of acrylic acid (ester)/C10 to 30 percent of alkanol acrylate cross-linked polymer, 0.8 to 2.0 percent of C14 to 22 alcohol, 0.05 to 0.4 percent of arginine, 0.05 to 0.2 percent of sodium citrate and 0.01 to 0.1 percent of EDTA disodium.
9. The method for preparing the essence cream according to claim 8, comprising the steps of:
(1) sequentially adding EDTA disodium, acryloyl dimethyl ammonium taurate/VP copolymer, butanediol, potassium cetyl phosphate, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, Chinese rehmannia root extract and sodium acetylhyaluronate into an emulsifying pot, heating to 80-85 ℃, and uniformly stirring to obtain phase A;
(2) sequentially adding PEG-20 esters of behenyl trimaran, PEG-100 stearate, isononyl isononanoate, C14-22 alcohol, polydimethylsiloxane, tocopheryl acetate and shea butter into an oil phase pot, and heating to 80-82 ℃ to obtain a phase B;
(3) sucking the phase B into an emulsifying pot, homogenizing at the speed of 2800-3200 rpm for 4-6 minutes, adding arginine, uniformly stirring, and cooling to below 45 ℃ to obtain phase C;
(4) adding pre-dispersed water, sodium citrate and whey protein into the phase C, and homogenizing at the speed of 1800-2200 rpm for 4-6 minutes to obtain a phase D;
(5) adding pre-dissolved Daisy extract, Magnolia liliflora bark extract, phenoxyethanol, ethylhexylglycerin, 1, 2-hexanediol, and radix Gentianae extract into phase D, stirring, and cooling to below 40 deg.C to obtain the essence cream.
CN202210873166.9A 2022-07-22 Multi-effect composition, essence cream and preparation method thereof Active CN115068389B (en)

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CN107961211A (en) * 2011-05-10 2018-04-27 玫琳凯有限公司 Cosmetic composition
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