Summary of the invention
The objective of the invention is to overcome the deficiency of prior art, a kind of combination various plants composition is provided, collection is isolated, and whitens; The triple effect of preserving moisture unification, skin care, moisturizing comprehensively; The adjustment colour of skin keeps skin health, strengthens elastic skin whitening lotion of skin and preparation method thereof.
The object of the invention is achieved through following technical proposals
A kind of skin whitening lotion, the quality sum of each component is 100 mass parts, is made up of following component:
The quality sum of each component of the present invention is 100 mass parts, and each components contents is preferably following:
Said component A is acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer; Mainly be used as the cosmetics thickener; Be used in hair and the skin-protection product; Wiping can form thin film and have adhesion, hold moistening effect that moisture provides continuation to skin on skin, make dermal sensation such as silkiness soft, for example the commodity ULRVEZ-21 of the sharp biochemical industry in sky, Beijing Co., Ltd.
Said B component is the copolymer of PEG and PPG; UCON Fluids is the Polyethylene Glycol propylene glycol, and the liquid with midium-viscosity can make emollient cream, water-activated eye make-up remover, hidroschesis reveal and moist suitable cunning of deodorizer, can bring a series of additional effects simultaneously; For example: can make the rapid humidifying of color make-up; In use can produce heat rapidly, perhaps control the viscosity of shampoo, for example PEG/PPG-17/6 copolymer 75-H 450.
Said component C is the mixture of ammonium acrylate/acrylamide copolymer, polyisobutylene and polysorbas20, belongs to hydration expansion drop (HSD) polymer of a new generation, has improved electrolytical resistance and stronger emulsification function is arranged.The thickener/emulsifier of wieldy liquid state, for example France's match commodity Sepiplus of BIC Corp 265.
Said component D is the ring-type dimethyl siloxane; It has the compatibility highly with many components in all kinds of cosmetics; Reduce greasy feeling in the prescription; Make cosolvency, solid powder dispersant, gentle light, smooth tender, be used for light cream frost, emulsion, cleansing milk, astringent, color make-up, shampoo water.Make hair increase gloss, significantly improve cardability, noresidue deposition, for example the commodity DC345 of Dow corning company.
Said component E is dimethicone/ring penta dimethyl-silicon oleogel; Form by the polydimethylsiloxane of mass percent 45.0~50.0wt%, ring penta siloxanes of 36.0~42.0wt% and the GRANSIL GCM-5 of 12.0~16.0wt%; Be that the spongy dimethyl siloxane crosslinked spherical powder that will have oily swelling character is scattered in dimethicone and is prepared from ring penta dimethicone; Can be applicable to the color make-up prescription as face's fat absorption agent; Reach inferior light, smoothly with the appearance of not having oil.It shows similar smooth silica flour, can give the unusual silk of skin sliding skin sense, can add essence or directly uses as the skin protection finished product; Or composite with other active matters, like vitamin, antibacterial; Cholesterol or sunscreen etc., for example Guangzhou joins and gathers the commodity Gransil DMCM-5 of trade Co., Ltd.
Said component F can combine with the epsilon-amino acid functional group in the cutin for lock hydromagnetic stone, brings into play powerful aquation and reaches long-acting moisture-keeping function; Even the water flushing is flush away easily, just as magnetite firmly is incorporated into skin surface, its another group is then brought into play powerful aquation; Prevent that moisture content scatters and disappears; And, dynamically keep the water balance of skin, for example the lock hydromagnetic stone of Switzerland Pan Defa company from the external environment suction.
Said component G is the three kind of plant extracts of scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit; Prepare according to following step: at first with quality such as scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit put in the agitated reactor, add sterile deionized water to submergence material, soak and remove impurity after 1-3 hour; Add the sterile deionized water that material gross mass 8-10 doubly measures again; Heat boil 2-4 hour after, discharging is also filtered, and obtains plant extract.
Said component H is a Tricholoma matsutake (lto et lmai) Singer extract; Prepare according to following step: at first Tricholoma matsutake (lto et lmai) Singer is put in the agitated reactor, added sterile deionized water to submergence Tricholoma matsutake (lto et lmai) Singer, soak and remove impurity after 1-3 hour; Add the sterile deionized water that Tricholoma matsutake (lto et lmai) Singer gross mass 8-10 doubly measures again; Heat boil 2-4 hour after, discharging is also filtered, and obtains Tricholoma matsutake (lto et lmai) Singer extract.
Said component I is bisabolol, ginger-root extract, aspect the skin that the reduction product stimulates, reparation has inflammation damnification effect preferably being arranged, is used in the sunscreen product, can reduce the injury of ultraviolet to skin effectively; Be used in the product for resolving poxes, can alleviate the acne of skin; In the flush away product, skin there is certain tack, sustainable performance effect, the commodity SymRelief of place of production Germany Symrise (fragrant quick relaxing) for example, oil-soluble is pale yellow to light brown liquid.
Said component J be the methyl isothiazolone (with) iodine propilolic alcohol butyl mephenesin Carbamate, i.e. the Microcare MTI of ACTI-ch em company, it is dissolved in the water preparation system fully, need not use the solubilizing agent solubilising, non-volatile formaldehyde is fine to the mycete antiseptic effect.
Said essence is selected food stage essence W1005238.
A kind of method for preparing the skin whitening lotion of the present invention, carry out according to following step:
(1) deionized water is put into the vacuum emulsification still; Add triethanolamine, hyaluronate sodium, sodium metabisulfite, methyl propanediol, endecatylene acyl group phenylalanine, component F, essence, citric acid again; After being uniformly dispersed, extracting vacuum is warming up to 80-90 ℃ simultaneously to 5-10Pa;
(2) component A, B component, hydrolecithin, hydrogenated polydecene, plant sterol isostearate, Ascorbyl Tetraisopalmitate, component C, component D, polydimethylsiloxane, component E, component J are put into the oil phase still, be warming up to 80-90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5-10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40-45 ℃, adds component G, component H, component I, and keep 5-10Pa;
When (5) treating that mixture temperature is reduced to 36-38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion of the present invention.
In the said step (1), be warming up to 80-85 ℃.
In the said step (1), extracting vacuum is to 5-10Pa.
In the said step (2), be warming up to 80-85 ℃.
In said step (3) and (4), pressure maintains 5-8Pa.
Compared with prior art, technical scheme of the present invention is concentrated the elite of several plant composition, and collection is isolated; Whiten the triple effect of preserving moisture unification, skin care; Moisturizing comprehensively, the adjustment colour of skin keeps skin health; Strengthen skin elasticity, make skin present natural gloss again, can isolate the infringement to skin such as extraneous in the daytime various dirts and radiation simultaneously.Except that the above-mentioned component of having made description, also have:
1. Ascorbyl Tetraisopalmitate; As a kind of oil-soluble VC of uniqueness, can suppress intracellular tyrosine enzyme and melanin and generate. antioxidation, remove free radical; Reduce cell and DNA damage that UV brings; Prevent greasy peroxidating and skin aging, have outstanding heat and oxidation stability, can recover cytoactive.
2. the undecanoyl phenylalanine as a kind of melanin inhibitor, can promote skin to be converted into normal chromogenesis; Prevent that melanin from forming, warp is to the Asia tuerculoderma, and every day is with 2 times; Through 3 months, measure glossiness before using and with the back, effect shows very good; Can remedy the single deficiency of traditional whitening agent action pathway, effect more obviously with lasting, has multiple whitening function simultaneously; Skin is whitened at many levels, and antagonism produces melanic a plurality of links, can suppress melanin comprehensively and generate.
3. Tricholoma matsutake (lto et lmai) Singer extract; Use as the whitening anti-wrinkling concentrating agents, directly, established melanin is converted into the light black element to the melanin effect that has generated; The melanin generation that suppresses new of comparing needs a physiological period, the fast and safety of whitening and speckle dispelling speed.
The specific embodiment
Further specify technical scheme of the present invention below in conjunction with specific embodiment.
In an embodiment of the present invention, component A is acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, adopts the commodity ULRVEZ-21 of the sharp biochemical industry company limited in sky, Beijing.B component is the copolymer of PEG and PPG, adopts PEG/PPG-17/6 copolymer 75H-450.Component C is the mixture of ammonium acrylate/acrylamide copolymer, polyisobutylene and polysorbas20, adopts the France match commodity Sepiplus of BIC Corp 265.Component D is the ring-type dimethyl siloxane, adopts the commodity DC345 of Dow corning company.Component E is dimethicone/ring penta dimethyl-silicon oleogel, adopts Guangzhou to join and gathers the commodity Gransil DMCM-5 of trade Co., Ltd.Component F is the lock hydromagnetic stone of Switzerland Pan Defa company.Component G is the three kind of plant extracts of scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit; Prepare according to following step: at first with quality such as scutellariae,radix, Glycyrrhiza glabra L. root and Fructus Jujubae fruit put in the agitated reactor, add sterile deionized water to submergence material, soak and remove impurity after 1-3 hour; Add the sterile deionized water that material gross mass 8-10 doubly measures again; Heat boil 2-4 hour after, discharging is also filtered, and obtains plant extract.Component H is a Tricholoma matsutake (lto et lmai) Singer extract; Prepare according to following step: at first Tricholoma matsutake (lto et lmai) Singer is put in the agitated reactor, added sterile deionized water to submergence Tricholoma matsutake (lto et lmai) Singer, soak and remove impurity after 1-3 hour; Add the sterile deionized water that Tricholoma matsutake (lto et lmai) Singer gross mass 8-10 doubly measures again; Heat boil 2-4 hour after, discharging is also filtered, and obtains Tricholoma matsutake (lto et lmai) Singer extract.Component I is bisabolol, ginger-root extract, adopts the commodity SymRelief (fragrant quick relaxing) of place of production Germany Symrise, and oil-soluble is pale yellow to light brown liquid.Component J is the Microcare MTI of ACTI-chem company.The quality sum of each component is 100kg.
Embodiment 1
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.025kg, hyaluronate sodium 0.2kg, sodium metabisulfite 0.5kg, methyl propanediol 2kg, endecatylene acyl group phenylalanine 0.08kg, component F 6kg, essence 0.05kg, citric acid 0.05kg again; After being uniformly dispersed; Extracting vacuum is warming up to 80 ℃ simultaneously to 5Pa;
(2) component A 0.3kg, B component 1kg, hydrolecithin 0.5kg, hydrogenated polydecene 4kg, plant sterol isostearate 0.1kg, Ascorbyl Tetraisopalmitate 1kg, component C 1kg, component D 1kg, polydimethylsiloxane 1kg, component E 1.5kg, component J 0.05kg are put into the oil phase still, be warming up to 80 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 45 ℃, adds component G 3kg, component H 0.2kg, component I 1kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 1 of the present invention.
Embodiment 2
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.4kg, hyaluronate sodium 0.005kg, sodium metabisulfite 0.2kg, methyl propanediol 5kg, endecatylene acyl group phenylalanine 0.03kg, component F 2kg, essence 0.1kg, citric acid 0.01kg again; After being uniformly dispersed; Extracting vacuum is warming up to 90 ℃ simultaneously to 8Pa;
(2) component A 0.1kg, B component 0.5kg, hydrolecithin 1.5kg, hydrogenated polydecene 1kg, plant sterol isostearate 0.5kg, Ascorbyl Tetraisopalmitate 4kg, component C 3kg, component D 3kg, polydimethylsiloxane 3kg, component E 0.5kg, component J 0.1kg are put into the oil phase still, be warming up to 90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 8Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40 ℃, adds component G 0.5kg, component H 1kg, component I 0.1kg, and keep 8Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 2 of the present invention.
Embodiment 3
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.3kg, hyaluronate sodium 0.015kg, sodium metabisulfite 0.3kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.08kg, citric acid 0.02kg again; After being uniformly dispersed; Extracting vacuum is warming up to 85 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 2kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 85 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 2kg, component H 0.5kg, component I 0.8kg, and keep 10Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 3 of the present invention.
Embodiment 4
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.3kg, hyaluronate sodium 0.01kg, sodium metabisulfite 0.4kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.08kg, citric acid 0.02kg again; After being uniformly dispersed; Extracting vacuum is warming up to 90 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 3kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 90 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 40 ℃, adds component G 2kg, component H 0.5kg, component I 0.8kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 4 of the present invention.
Embodiment 5
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.35kg, hyaluronate sodium 0.2kg, sodium metabisulfite 0.4kg, methyl propanediol 4kg, endecatylene acyl group phenylalanine 0.06kg, component F 4kg, essence 0.07kg, citric acid 0.02kg again; After being uniformly dispersed; Extracting vacuum is warming up to 80 ℃ simultaneously to 5Pa;
(2) component A 0.3kg, B component 0.8kg, hydrolecithin 1.2kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.4kg, Ascorbyl Tetraisopalmitate 3kg, component C 1.5kg, component D 1.5kg, polydimethylsiloxane 2.5kg, component E 1kg, component J 0.08kg are put into the oil phase still, be warming up to 80 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 5Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 45 ℃, adds component G 2kg, component H 0.5kg, component I 0.5kg, and keep 5Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 5 of the present invention.
Embodiment 6
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.3kg, hyaluronate sodium 0.008kg, sodium metabisulfite 0.5kg, methyl propanediol 3kg, endecatylene acyl group phenylalanine 0.07kg, component F 5kg, essence 0.05kg, citric acid 0.02kg again; After being uniformly dispersed; Extracting vacuum is warming up to 82 ℃ simultaneously to 8Pa;
(2) component A 0.3kg, B component 0.8kg, hydrolecithin 1.5kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.5kg, Ascorbyl Tetraisopalmitate 2kg, component C 2kg, component D 2kg, polydimethylsiloxane 2kg, component E 1.5kg, component J 0.6kg are put into the oil phase still, be warming up to 82 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 8Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 2.5kg, component H 1kg, component I 0.3kg, and keep 8Pa;
When (5) treating that mixture temperature is reduced to 36 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 6 of the present invention.
Embodiment 7
(1) deionized water (quality that promptly deducts behind all the other constituent masses with 100kg takes by weighing) is put into the vacuum emulsification still; Add triethanolamine 0.025kg, hyaluronate sodium 0.01kg, sodium metabisulfite 0.4kg, methyl propanediol 5kg, endecatylene acyl group phenylalanine 0.05kg, component F 5kg, essence 0.08kg, citric acid 0.02kg again; After being uniformly dispersed; Extracting vacuum is warming up to 85 ℃ simultaneously to 10Pa;
(2) component A 0.2kg, B component 0.8kg, hydrolecithin 1kg, hydrogenated polydecene 3kg, plant sterol isostearate 0.3kg, Ascorbyl Tetraisopalmitate 2.5kg, component C 2kg, component D 3kg, polydimethylsiloxane 1kg, component E 0.5kg, component J 0.1kg are put into the oil phase still, be warming up to 85 ℃;
(3) oil phase component after step (2) preparation is sucked in the vacuum emulsification still, and keep 10Pa;
(4) the vacuum emulsification temperature in the kettle is cooled to 42 ℃, adds component G 1kg, component H 0.5kg, component I 0.8kg, and keep 10Pa;
When (5) treating that mixture temperature is reduced to 38 ℃ naturally in the emulsion reactor, discharging is also filtered, and promptly gets skin whitening lotion sample 7 of the present invention.
Investigate the whiten action effect of sample 1-7 of skin of the present invention, the personnel that choose 50 all ages and classes use, and life cycle is fortnight, and 99% user is good to above-mentioned sample performance, and effectively skin protection and whitening of sample comprehensively solves skin problem.
More than the present invention has been done exemplary description; Should be noted that; Under the situation that does not break away from core of the present invention, the replacement that is equal to that any simple distortion, modification or other those skilled in the art can not spend creative work all falls into protection scope of the present invention.