CN110200882A - A kind of Whitening, spot essence dew and preparation method thereof - Google Patents
A kind of Whitening, spot essence dew and preparation method thereof Download PDFInfo
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- CN110200882A CN110200882A CN201910473134.8A CN201910473134A CN110200882A CN 110200882 A CN110200882 A CN 110200882A CN 201910473134 A CN201910473134 A CN 201910473134A CN 110200882 A CN110200882 A CN 110200882A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Abstract
The present invention discloses a kind of Whitening, spot essence dew and preparation method thereof, comprising steps of 1) putting into component A in water phase pot, is heated with stirring to 80-85 DEG C, makes it dissolve completely;2) B component is put into oily phase pot, is heated with stirring to 80-85 DEG C, homogeneous makes it dissolve completely;3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 80-85 DEG C of homogeneous 1-3min of temperature, heat preservation stirring cooling after ten minutes;4) when temperature drops to 60 DEG C, component C is added;5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;6) when being cooled to 40 DEG C, stop agitation and filtration discharging.The essence dew more pro-skin, also added the whitening active ingredients such as glabridin, microalgae skin lightening agent, niacinamide while naturally, making nude look effect, really conserve skin, have the effect of Whitening, spot, improvement facial defect.
Description
Technical field
The present invention relates to a kind of Whitening, spot essence dew and preparation method thereof, belong to cosmetic technical field.
Background technique
Although element Yan Shuan can play the effect brightened on the market, the main component of plain face frost is titanium dioxide (dioxy
Change titanium), if a kind of low oil content of patent does not clearly take off adornment element Yan Shuan (107982167 A of CN), which includes oiliness
Emollient, polyol humectant, skin conditioning agent, polymeric rheology regulator, titanium dioxide class covering agent, synergist, preservative
And essence.
Separately have, a kind of element Yan Shuan and its preparation process (108403483 A of CN), which includes following parts by weight
Component: 40-52 parts of pure water;2-3 parts of titanium dioxide;0.03-0.08 parts of triethoxy octyl silane;35-38 parts of moisturizer;At
4-6.5 parts of film;First 4-6 parts of emollient;Second 2-4 parts of emollient;1.08-1.52 parts of thickener/emulsifier;Glycine betaine 1-5
Part;Palmityl tripeptides -1 are 0.5-2 parts;0.402-0.5825 parts of preservative;Moisturizer is by yellow tang extract, niacinamide, general
Alcohol, glycerine, butanediol composition;Film forming agent is made of Jojoba esters, sunflower seed wax, Acacia decurrens floral wax, polyglycereol -3;Increase
Ropy milk agent is made of sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, Polyoxyethylene Sorbitan Monooleate.
Though there is titanium dioxide excellent covering power, which to reach, reduces microgroove and wrinkle effect, due to its impermeable light-proofness and
High refractive index (RI about 2.5-2.6) makes skin seem to whiten unnatural, and floating powder is intractable, and oil sense is too strong.
Summary of the invention
In view of the above existing problems in the prior art, the present invention provides a kind of Whitening, spot essence dew, quality silk is sliding to be moistened,
It easily absorbs, can allow skin immediately and long-acting Whitening, spot.The present invention goes back while providing the system of Whitening, spot essence dew
Preparation Method.
To achieve the goals above, a kind of Whitening, spot essence dew that the present invention uses, by weight, including with the following group
Point;
Component A: 0.01-0.5 parts of carbomer, 0.01-0.5 parts of methyl hydroxybenzoate, 10-15 parts of moisturizer, deionized water 60-70
Part;
B component: 1.5-5 parts of emulsifier, 1-6 parts of caprylic/capric triglyceride, 3-10 parts of polymethylsilsesquioxane, nitrogen
Change boron 3-10 parts, 1-5 parts of octyl polymethyl siloxane, 4-10 parts of ring five dimethyl silicone polymer, 2-8 parts of Nexbase 2004, gathers
1-5 parts of dimethyl siloxane, 1-6 parts of (thylhexoic acid) ester of glycerol three;
Component C: 0.01-0.5 parts of pH adjusting agent;
D component: 0.01-0.5 parts of glycyrrhiza glabra root extract, 2-5 parts of preservative;
Component E: 1-5 parts of niacinamide, 2-10 parts of deionized water;
F component: 0.1-0.5 parts of extraction of high mountain plant, 0.01-0.5 parts of multiflora rose extract, Herba Saussureae Involueratae extract 0.01-0.5
Part, 0.01-2 parts of microalgae skin lightening agent, 0.01-0.5 parts of essence.
The moisturizer uses one of glycerol, 1,3 butylene glycol, dipropylene glycol, sorbierite, trehalose or a variety of
Mixing.
The emulsifier is stearine, PEG-100 stearate, C12-20 alkyl glucoside, polysorbate-
20, one of sucrose stearate/sucrose, stearoyl-glutamic acid sodium, sodium cetyl stearyl sulfate or a variety of mixing.
The pH adjusting agent is one of triethanolamine, arginine, tromethamine, potassium hydroxide, sodium hydroxide or more
Kind mixing.
The preservative is 1,2- pentanediol, parahydroxyacet-ophenone, Phenoxyethanol, 1,2- hexylene glycol, methyl hydroxybenzoate, oxybenzene
One of propyl ester, glycerol caprylate or a variety of mixing.
It is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng extraction that the high mountain, which plants extraction,
Object, tomonea extract, Chinese herbaceous peony root extract according to 1:2:1:1:3:4 mixing.
The microalgae skin lightening agent is using one of lutein, lecithin/sodium ascorbate, tocopherol or a variety of mixed
It closes.
In addition, the present invention also provides the preparation methods of Whitening, spot essence dew, comprising steps of
1) component A is put into water phase pot, is heated with stirring to 80-85 DEG C, made it dissolve completely;
2) B component is put into oily phase pot, is heated with stirring to 80-85 DEG C, homogeneous makes it dissolve completely;
3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 80-85 DEG C of homogeneous 1-3min of temperature, heat preservation
Cooling is stirred after 10 minutes;
4) when temperature drops to 60 DEG C, component C is added;
5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;
6) when being cooled to 40 DEG C, stop agitation and filtration discharging.
The performance or the mechanism of action of used part material are as follows in inventive formulation:
1. high mountain plants the Chinese medicine beauty that extraction is derived from the Yunnan genunie medicinal materials such as the plant HERBA DENDROBII, Radix Angelicae Sinensis, Radix Notoginseng in Yunnan composition
Skin side is compounded according to the prescription thought of Traditional Chinese Medicine " monarch, minister, help, make ", is had good antioxidant activity and is inhibited junket
Propylhomoserin enzymatic activity, and have the function of good improvement skin microcirculation, good moist skin, balanced pigment and taste can be played
The effect of supporting skin.
2. polymethylsilsesquioxane is organic silica microsphere, enhances the ductility and smoothness of cosmetics, increase for it
Gloss promotes smooth feeling, glossiness, powder sense and soft light effect, prevents from agglomerating, and smooth surface promotes sense of touch, and it is unrestrained saturating to improve light
Rate is penetrated, light route is changed, brings skin soft focus effec, wrinkle and flaw are covered in help.
3. boron nitride light sensation is thoroughly white, laminated structure, there is triple function: first is that light sensation reflection factor, even skin tone, new one
For skin care science and technology, bright natural dressing is made, microgroove is covered;Second is that the super light skin of smooth texture height, smooth skin quality, stealthy hair
Hole, super-thin sheet-shaped possess the docile fine and smooth texture of ultra micro, are bonded skin surface remarkably, smooth skin, moment stealth pore, but
Pore is not blocked, skin freely breathes free of a burden;Third is that Separate Fine-grained Minerals whitening composition, Separate Fine-grained Minerals whitening composition, meet women
The colour of skin, at once promoted skin and muscles are fair degree, enable skin shine fair and tender brilliance, glossy dressing.
4. glycyrrhiza glabra root extract (glabridin): the glabridin in licorice can not only inhibit melanin to be formed,
It can also be anti-inflammatory.
5. niacinamide: the coenzyme premise in cell metabolism, enhance skin barrier function, have desalination skin, it is anti-aging and
Anti-acne active has a kind of basic vitamins replenishers in very high safety and the treatment of clinic skin section, wide
It is general to be used to treat photosensitive dermatitis, acne etc..It inhibit melanin pigmentation, in terms of also have good curative effect;It is based on
This feature, niacinamide cosmetic field application obtained further extension, other than traditional whitening effect, also by
For reducing the melanin for having generated, having precipitated, its transfer to cells of superficial layer is obstructed, accelerates cell metabolism, quickening black
Pigment horn cell falls off.Niacinamide is able to maintain that skin water content, promotes skin corium microcirculation.Niacinamide can also greatly subtract
Less or eliminate skin ageing phenomenon, for example wrinkle, peeling, pore are coarse etc., reduce injury of the free radical to skin, play prevention
Aging repairs skin and reduces the obscure effect of face.
Essence dew of the invention is the upgrading for having made more to accord with the demands of the market in the simple and fast theory of plain face frost, addition
Boron nitride, with slightly lower index of refraction (RI about 1.4-2.1), the brighter powder of structure is easier to make clear naked adornment effect
Fruit solves general plain face frost because too white unnatural caused by titanium dioxide is added, and floating powder is intractable, and oil feels too strong defect.It should
Essence dew more pro-skin, also added the beauty such as glabridin, microalgae skin lightening agent, niacinamide while naturally, making nude look effect
White active constituent, really conserves skin, has the effect of Whitening, spot, improves facial defect.
Detailed description of the invention
Fig. 1 is the influence VISIA figure one using sample a pair of spot;
Fig. 2 is the influence VISIA figure two using sample two to spot;
Specific embodiment
In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention is carried out below further detailed
It describes in detail bright.However, it should be understood that the specific embodiments described herein are merely illustrative of the present invention, it is not limited to this hair
Bright range.
Unless otherwise defined, all technical terms and scientific terms used herein are led with technology of the invention is belonged to
The normally understood meaning of the technical staff in domain is identical, and term as used herein in the specification of the present invention is intended merely to retouch
State the purpose of specific embodiment, it is not intended that in the limitation present invention.
Embodiment 1
A kind of Whitening, spot essence dew, by weight, including following components;
Component A: 0.02 part of carbomer, 0.03 part of methyl hydroxybenzoate, 10 parts of moisturizer, 60 parts of deionized water;
B component: 1.5 parts of emulsifier, 2 parts of caprylic/capric triglyceride, 3.5 parts of polymethylsilsesquioxane, boron nitride 4
Part, 2 parts of octyl polymethyl siloxane, 5 parts of ring five dimethyl silicone polymer, 2 parts of Nexbase 2004, dimethyl silicone polymer 2
Part, 2 parts of ester of glycerol three (thylhexoic acid);
Component C: 0.1 part of pH adjusting agent;
D component: 0.1 part of glycyrrhiza glabra root extract, 2.5 parts of preservative;
Component E: 1.5 parts of niacinamide, 2 parts of deionized water;
F component: 0.1 part of extraction of high mountain plant, 0.1 part of multiflora rose extract, 0.1 part of Herba Saussureae Involueratae extract, microalgae skin lightening agent 0.1
Part, 0.1 part of essence.
Wherein, moisturizer uses glycerol;Emulsifier is stearine;PH adjusting agent is triethanolamine;Preservative is
1,2- pentanediol;It is HERBA DENDROBII stem extraction, Angelica roots, Herba Verbenae, Roots of Panax Notoginseng extraction that high mountain, which plants extraction,
Object, tomonea extract, Chinese herbaceous peony root extract according to 1:2:1:1:3:4 mixing;Microalgae skin lightening agent uses lutein, lecithin
Rouge/sodium ascorbate, tocopherol according to 2:1:1 mixing.
The preparation method of the Whitening, spot essence dew, comprising steps of
1) component A is put into water phase pot, is heated with stirring to 80 DEG C, made it dissolve completely;
2) B component is put into oily phase pot, is heated with stirring to 80 DEG C, homogeneous makes it dissolve completely;
3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 80 DEG C of homogeneous 1min of temperature, keep the temperature 10 points
Cooling is stirred after clock;
4) when temperature drops to 60 DEG C, component C is added;
5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;
6) when being cooled to 40 DEG C, stop agitation and filtration discharging.
Embodiment 2
A kind of Whitening, spot essence dew, by weight, including following components;
Component A: 0.3 part of carbomer, 0.3 part of methyl hydroxybenzoate, 12 parts of moisturizer, 65 parts of deionized water;
B component: 3 parts of emulsifier, 2 parts of caprylic/capric triglyceride, 5 parts of polymethylsilsesquioxane, 5 parts of boron nitride, pungent
It is 3 parts of base polymethyl siloxane, 6 parts of ring five dimethyl silicone polymer, 5 parts of Nexbase 2004,3.5 parts of dimethyl silicone polymer, sweet
Oily three 3 parts of (thylhexoic acid) esters;
Component C: 0.3 part of pH adjusting agent;
D component: 0.3 part of glycyrrhiza glabra root extract, 4 parts of preservative;
Component E: 4 parts of niacinamide, 6 parts of deionized water;
F component: 0.3 part of extraction of high mountain plant, 0.3 part of multiflora rose extract, 0.4 part of Herba Saussureae Involueratae extract, microalgae skin lightening agent 1
Part, 0.3 part of essence.
Wherein, moisturizer is mixed using 1,3-BDO, dipropylene glycol according to 1:1;Emulsifier is PEG-100 stearic acid
Ester;PH adjusting agent is arginine;Preservative is parahydroxyacet-ophenone;High mountain is planted extraction and is mentioned for HERBA DENDROBII stem extraction, angelica root
Take object, Herba Verbenae, Radix Notoginseng root extract, tomonea extract, Chinese herbaceous peony root extract according to the mixed of 1:2:1:1:3:4
It closes;Microalgae skin lightening agent using lutein, lecithin/sodium ascorbate, tocopherol according to 1:2:2 mixing.
The preparation method of the Whitening, spot essence dew, comprising steps of
1) component A is put into water phase pot, is heated with stirring to 83 DEG C, made it dissolve completely;
2) B component is put into oily phase pot, is heated with stirring to 83 DEG C, homogeneous makes it dissolve completely;
3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 83 DEG C of homogeneous 2min of temperature, keep the temperature 10 points
Cooling is stirred after clock;
4) when temperature drops to 60 DEG C, component C is added;
5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;
6) when being cooled to 40 DEG C, stop agitation and filtration discharging.
Embodiment 3
A kind of Whitening, spot essence dew, by weight, including following components;
Component A: 0.4 part of carbomer, 0.5 part of methyl hydroxybenzoate, 13 parts of moisturizer, 70 parts of deionized water;
B component: 4.5 parts of emulsifier, 5 parts of caprylic/capric triglyceride, 8 parts of polymethylsilsesquioxane, 8 parts of boron nitride,
It is 4 parts of octyl polymethyl siloxane, 8 parts of ring five dimethyl silicone polymer, 8 parts of Nexbase 2004,5 parts of dimethyl silicone polymer, sweet
Oily three 5 parts of (thylhexoic acid) esters;
Component C: 0.5 part of pH adjusting agent;
D component: 0.5 part of glycyrrhiza glabra root extract, 4.5 parts of preservative;
Component E: 5 parts of niacinamide, 9 parts of deionized water;
F component: 0.5 part of extraction of high mountain plant, 0.5 part of multiflora rose extract, 0.5 part of Herba Saussureae Involueratae extract, microalgae skin lightening agent 2
Part, 0.5 part of essence.
Wherein, moisturizer uses sorbierite;Emulsifier is polysorbate -20;PH adjusting agent is triethanolamine;Preservative
It is mixed for 1,2- hexylene glycol, methyl hydroxybenzoate according to 1:2;It is HERBA DENDROBII stem extraction, Angelica roots, horsewhip that high mountain, which plants extraction,
Careless extract, Radix Notoginseng root extract, tomonea extract, Chinese herbaceous peony root extract are mixed by 1:2:1:1:3:4;Microalgae skin lightening agent is
The mixing of lutein, lecithin/sodium ascorbate, tocopherol (vitamin E).
The preparation method of the Whitening, spot essence dew, comprising steps of
1) component A is put into water phase pot, is heated with stirring to 85 DEG C, made it dissolve completely;
2) B component is put into oily phase pot, is heated with stirring to 85 DEG C, homogeneous makes it dissolve completely;
3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 85 DEG C of homogeneous 3min of temperature, keep the temperature 10 points
Cooling is stirred after clock;
4) when temperature drops to 60 DEG C, component C is added;
5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;
6) when being cooled to 40 DEG C, stop agitation and filtration discharging.
Whitening, spot essence made from above-described embodiment 1-3 is revealed, according to the wholesomeness of " cosmetics health specification "
It examines and carries out Micro biological Tests and service check, specific inspection result is as shown in the following table 1,2.
The Micro biological Tests result of 1 essence of table dew
Analytical table 1 is it is found that total plate count, mould and the yeast sum, fecal coliform that Whitening, spot essence of the invention is revealed
The inspection of the projects such as class, staphylococcus aureus and pseudomonas aeruginosa meets the requirements, and illustrates Whitening, spot essence dew peace
It is complete reliable.
The detection performance result of 2 essence of table dew
Analytical table 2 glues it is found that the pH value revealed of Whitening, spot essence of the invention is 6.39-7.12 (standard 4.5-8.5)
Spending performance is 7960-11000cps (standard 7000-20000cps), and relative density is 0.998-1.001 (standard 0.98-
1.20), in addition, its appearance, odor type comply with standard, cold-resistant, resistance to Thermal test, centrifugation test are without exception.
Essence dew is made into effect test comparison with Whitening, spot product on sale below:
1. tested material: 2 essence of the embodiment of the present invention reveals (sample one), commercially available Whitening, spot product (sample two);
2. the testing time: on 08 22nd, 1 on the 09th 07 month 2018;
3. experimental method
3.1 Subject characteristics, 35 people, 4 male 31 female;
3.2 recipient sites: at cheek spottiness;
3.3 product smearing methods: smearing at spottiness, use sooner or later, persistently uses 4 weeks;
3.4 test indexs and instrument: keratoderma L value, ITA value (Skin-Colorimrter CL400), melanin
Content (Mexameter MX18), spot gray scale and area (VISIA face imager is taken pictures, FrameScan software is analyzed);
3.5 experimental procedures: first cleaning test position with clear water before tester's test, after the 20min that sits quietly, carries out VISIA bat
Each test index value of 0W (T0) before smearing according to, the tested sample segment of test, then smears tested material according to regulation dosage, and in painting
It smears tested material 2W (T1), 4W (T2) and carries out VISIA afterwards and take pictures, test recipient site skin.In experimentation, recipient site is sudden and violent
Dew is placed in test mode, keeps loosening;
3.6 analysis methods: by comparing recipient site in the mutation analysis of each test index of each testing time point
Changing value=T2 1. (4 weeks values after use)-T0 (basic value when any product initial value: is not used)
2. index expression: L* value is higher, and skin is whiter, pigment content is fewer;ITA value is higher, and skin is more transparent;Melanin
Value is lower, and melanin content is lower;Speckle regions area is smaller, and spot is smaller;Spot gray value is bigger, and spot is more shallow.
It is specific that test result is as follows.
The skin L* value of each tester of table 3
As known from Table 3, sample one increases whitening skin degree 2.18%, and sample two increases whitening skin degree 0.74%.Sample
One effect is more significant.
Each tester's skin I TA value of table 4
As known from Table 4, sample one increases skin transparency 11%, and sample two increases skin transparency 5.47%.Sample one
Effect is more significant.
Each tester's dermal melanin value of table 5
As known from Table 5, the melanin average value of sample one reduces 11%, and the melanin average value of sample two reduces 6%.Sample
One effect of product is more significant.
Each tester's speckle regions area value of table 6
As known from Table 6, the speckle regions area value of sample one reduces 11.03%, and the speckle regions area value of sample two subtracts
Few 4.5%.One effect of sample is more significant.
Each tester's spot average gray of table 7
As known from Table 7, the spot of sample one shoals 0.75%, and the spot of sample two shoals 0.13%, and one effect of sample is more
Significantly.
In conjunction with shown in attached drawing 1-2, wherein attached drawing 1,2 is to be schemed using the influence VISIA of sample a pair of spot, and spot becomes
Shallowly, become smaller, tail off;Influence VISIA figure using sample two to spot, spot are unchanged.
Therefore, essence of the invention dew can be realized following effect: whitening skin degree L value is promoted;Skin transparency ITA value
It is promoted;Melanin is reduced;Speckle regions area value is reduced;Speckle regions gray scale is reduced, and each performance is considerably better than whitening on sale
Light spot product.
Claims (8)
1. a kind of Whitening, spot essence dew, which is characterized in that by weight, including following components;
Component A: 0.01-0.5 parts of carbomer, 0.01-0.5 parts of methyl hydroxybenzoate, 10-15 parts of moisturizer, 60-70 parts of deionized water;
B component: 1.5-5 parts of emulsifier, 1-6 parts of caprylic/capric triglyceride, 3-10 parts of polymethylsilsesquioxane, boron nitride
3-10 parts, 1-5 parts of octyl polymethyl siloxane, 4-10 parts of ring five dimethyl silicone polymer, 2-8 parts of Nexbase 2004, poly- diformazan
1-5 parts of radical siloxane, 1-6 parts of (thylhexoic acid) ester of glycerol three;
Component C: 0.01-0.5 parts of pH adjusting agent;
D component: 0.01-0.5 parts of glycyrrhiza glabra root extract, 2-5 parts of preservative;
Component E: 1-5 parts of niacinamide, 2-10 parts of deionized water;
F component: high mountain plants 0.1-0.5 parts of extraction, 0.01-0.5 parts of multiflora rose extract, 0.01-0.5 parts of Herba Saussureae Involueratae extract, micro-
0.01-2 parts of algae skin lightening agent, 0.01-0.5 parts of essence.
2. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that the moisturizer using glycerol,
One of 1,3 butylene glycol, dipropylene glycol, sorbierite, trehalose or a variety of mixing.
3. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that the emulsifier is glycerol stearate
Ester, PEG-100 stearate, C12-20 alkyl glucoside, polysorbate -20, sucrose stearate/sucrose, stearoyl paddy ammonia
One of sour sodium, sodium cetyl stearyl sulfate or a variety of mixing.
4. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that the pH adjusting agent is three ethyl alcohol
One of amine, arginine, tromethamine, potassium hydroxide, sodium hydroxide or a variety of mixing.
5. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that the preservative is 1,2- penta 2
One of alcohol, parahydroxyacet-ophenone, Phenoxyethanol, 1,2- hexylene glycol, methyl hydroxybenzoate, Nipasol, glycerol caprylate are more
Kind mixing.
6. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that it is HERBA DENDROBII that the high mountain, which plants extraction,
Stem extraction, Angelica roots, Herba Verbenae, Radix Notoginseng root extract, tomonea extract, Chinese herbaceous peony root extract according to
The mixing of 1:2:1:1:3:4.
7. a kind of Whitening, spot essence dew according to claim 1, which is characterized in that the microalgae skin lightening agent is yellow using leaf
One of element, lecithin/sodium ascorbate, tocopherol or a variety of mixing.
8. a kind of preparation method of any one of claim 1-7 Whitening, spot essence dew, which is characterized in that comprising steps of
1) component A is put into water phase pot, is heated with stirring to 80-85 DEG C, made it dissolve completely;
2) B component is put into oily phase pot, is heated with stirring to 80-85 DEG C, homogeneous makes it dissolve completely;
3) water phase material and oil phase material are sucked in succession in emulsifying kettle, keeps 80-85 DEG C of homogeneous 1-3min of temperature, keep the temperature 10 points
Cooling is stirred after clock;
4) when temperature drops to 60 DEG C, component C is added;
5) when temperature drops to 45 DEG C, the good D component of predissolve, component E, F component is added;
6) when being cooled to 40 DEG C, stop agitation and filtration discharging.
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CN112353725A (en) * | 2020-11-19 | 2021-02-12 | 广州领衔生物科技有限公司 | Efficacy composition in eye cream, eye cream and preparation method thereof |
CN113893310A (en) * | 2020-07-06 | 2022-01-07 | 安琪纽特股份有限公司 | Mountain plant fermentation composition and preparation method and application thereof |
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CN113893310A (en) * | 2020-07-06 | 2022-01-07 | 安琪纽特股份有限公司 | Mountain plant fermentation composition and preparation method and application thereof |
CN112137927A (en) * | 2020-09-12 | 2020-12-29 | 荣鼎(广东)生物科技有限公司 | Fibronectin essence emulsion with high penetration and light sensation reproduction and tissue regeneration initiation and preparation method thereof |
CN112353725A (en) * | 2020-11-19 | 2021-02-12 | 广州领衔生物科技有限公司 | Efficacy composition in eye cream, eye cream and preparation method thereof |
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