Summary of the invention
The objective of the invention is in order to overcome weak point of the prior art, provide a kind of fast, the whitening spot-relieving cream cosmetic of efficient, green safety;
Another object of the present invention is for a kind of preparation method of this whitening spot-relieving cream cosmetic is provided.
In order to achieve the above object, the present invention adopts following scheme:
A kind of whitening spot-relieving cream cosmetic, percentage composition comprises following component by weight:
A, main body Whitening, spot component 5.21~21%
B, auxiliary Whitening, spot component 0.4~3.0%
C, oil phase components 13.5~32.5%
D, water component 41.5~80.19%
E, thickening stabilization component 0.5~1.0%
F, auxiliary agent component 0.3~1.0%.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said main body Whitening, spot component is made up of following components in weight percentage content:
Glycyrrhiza glabra L. (GLYCYRRHIZA GLABRA) root extract 0.01~5.0%
Nicotiamide (VB3) 2.0~6.0%
Arbutin 2.0~6.0%
Hydroxy decyl ubiquinone 0.2~1.0%
Superfine titanium white (TiO2) 1.0~3.0%.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said auxiliary Whitening, spot component is made up of following components in weight percentage content:
Tioxolone 0.2~1.0%
Tocopherol acetas 0.2~2.0%.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said oil phase components is made up of following components in weight percentage content:
PEG-100 stearate 1.0~3.0%
Cetearyl alcohol 1.5~3.5%
Polydimethylsiloxane 3.0~5.0%
Caprylic/capric triglyceride 4.0~8.0%
Hydrogenated polydecene 3.0~10.0%
Ermine oil 1.0~3.0%.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said water component is made up of following components in weight percentage content:
EDTA disodium 0.01~0.20%
Allantoin 0.1~0.5%
Glycerol 1.0~10.0%
1,3 butylene glycol 1.0~10.0%
Xanthan gum 0.1~0.3%
Water 21.5~77.98%.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said thickening stabilization component are one or more the mixture in polyacrylamide, C13-14 isoparaffin, the lauryl alcohol-7.
Aforesaid a kind of whitening spot-relieving cream cosmetic, wherein said auxiliary agent component are one or both the mixture in essence, the antiseptic.
A kind of method for preparing above-mentioned whitening spot-relieving cream cosmetic, comprising following steps:
A, C is warmed up to 65~95 ℃ mutually, is incubated 75~85 ℃, add the B phase, stirring and dissolving is complete;
B, D is warmed up to 65~95 ℃ mutually, is incubated 75~85 ℃, stirring and dissolving is complete;
C, earlier with C mixed phase suction emulsifying pot, suction D phase slowly adds the A phase, homogenizing 5~15min, insulated and stirred 5~15min, evacuation cooling more again;
D, add the E phase 50~70 ℃ the time, homogenizing 2-3min stirs;
E, add the F phase 30~50 ℃ the time, stir, promptly get product of the present invention.
In sum, beneficial effect of the present invention:
1, Main Ingredients and Appearance effect among the present invention: glabridin (Glabridin) is the natural whiting agent of extracting from the certain species Radix Glycyrrhizae, the activity of its energy restraint of tyrosinase, can suppress the oxidasic activity of dopachrome change and DHICA again, it is a kind of quick, efficient, green whitening cosmetics additive, ability with removing oxygen-derived free radicals similar to SOD (superoxide dismutase) has the antioxidant radical ability close with vitamin E.Glabridin is the most effective natural whiting of generally acknowledging in the world at present, brighten, speckle dispelling, sun care preparations additive; The price of 90% content glabridin is about 200,000 yuan/KG on the market at present, is described as " gold of whitening " at cosmetics circle.This product is taken from the glabridin that Glycyrrhiza glabra L. extracts, as main whitening and speckle dispelling active ingredient, cooperate nicotiamide (VB3), arbutin, idebenone, superfine titanium white, play synergistic function, the Whitening, spot component is assisted in collocation again: tioxolone (short infiltration), tocopherol acetas (antioxidation, maintenance).
2, product of the present invention all has good effect for the problem of various skin matter, but uses the just onset of about two weeks, and one month effect is fairly obvious;
3, product of the present invention has splendid desalination effect for symptoms such as freckle, the skin ulcer of fullying recover from an illness, acne, blackhead, chloasma, withered and yellow black face, chloasma, sun speckles, and whitening effect is preferably arranged.
The specific embodiment
Below in conjunction with the specific embodiment the present invention is described further:
Embodiment 1
Whitening spot-relieving cream cosmetic of the present invention, percentage composition comprises following component by weight:
A, main body Whitening, spot component 5.21%
B, auxiliary Whitening, spot component 3.0%
C, oil phase components 32.5%
D, water component 57.29%
E, thickening stabilization component 1.0%
F, auxiliary agent component 1.0%,
Wherein said main body Whitening, spot component is made up of following components in weight percentage content:
Glycyrrhiza glabra L. (GLYCYRRHIZA GLABRA) root extract 0.01%
Nicotiamide (VB3) 2.0%
Arbutin 2.0%
Hydroxy decyl ubiquinone 0.2%
Superfine titanium white (TiO2) 1.0%;
Wherein said auxiliary Whitening, spot component is made up of following components in weight percentage content:
Tioxolone 1.0%
Tocopherol acetas 2.0%;
Wherein said oil phase components is made up of following components in weight percentage content:
PEG-100 stearate 3.0%
Cetearyl alcohol 3.5%
Polydimethylsiloxane 5.0%
Caprylic/capric triglyceride 8.0%
Hydrogenated polydecene 10.0%
Ermine oil 3.0%;
Wherein said water component is made up of following components in weight percentage content:
EDTA disodium 0.2%
Allantoin 0.5%
Glycerol 10.0%
1,3 butylene glycol 10.0%
Xanthan gum 0.3%
Water 36.29%;
Wherein said thickening stabilization component is 1.0% polyacrylamide;
Wherein said auxiliary agent component is 1.0% the essence and the mixture of antiseptic.
The described whitening spot-relieving cream cosmetic of present embodiment is to prepare by following steps:
A, C is warmed up to 65 ℃ mutually, is incubated 75 ℃, add the B phase, stirring and dissolving is complete;
B, D is warmed up to 65 ℃ mutually, is incubated 75 ℃, stirring and dissolving is complete;
C, earlier with C mixed phase suction emulsifying pot, suction D phase slowly adds the A phase, homogenizing 5min, insulated and stirred 5min, evacuation cooling more again;
D, add the E phase 50 ℃ the time, homogenizing 2-3min stirs;
E, add the F phase 30 ℃ the time, stir, promptly get product of the present invention.
Embodiment 2
Whitening spot-relieving cream cosmetic of the present invention, percentage composition comprises following component by weight:
A, main body Whitening, spot component 21%
B, auxiliary Whitening, spot component 0.4%
C, oil phase components 13.5%
D, water component 64.3%
E, thickening stabilization component 0.5%
F, auxiliary agent component 0.3%,
Wherein said main body Whitening, spot component is made up of following components in weight percentage content:
Glycyrrhiza glabra L. (GLYCYRRHIZA GLABRA) root extract 5%
Nicotiamide (VB3) 6.0%
Arbutin 6.0%
Hydroxy decyl ubiquinone 1.0%
Superfine titanium white (TiO2) 3.0%;
Wherein said auxiliary Whitening, spot component is made up of following components in weight percentage content:
Tioxolone 0.2%
Tocopherol acetas 0.2%;
Wherein said oil phase components is made up of following components in weight percentage content:
PEG-100 stearate 1.0%
Cetearyl alcohol 1.5%
Polydimethylsiloxane 3.0%
Caprylic/capric triglyceride 4.0%
Hydrogenated polydecene 3.0%
Ermine oil 1.0%;
Wherein said water component is made up of following components in weight percentage content:
EDTA disodium 0.01%
Allantoin 0.1%
Glycerol 1.0%
1,3 butylene glycol 1.0%
Xanthan gum 0.1%
Water 62.09%;
Wherein said thickening stabilization component is 0.5% C13-14 isoparaffin;
Wherein said auxiliary agent component is 0.3% essence.
The described whitening spot-relieving cream cosmetic of present embodiment is to prepare by following steps:
A, C is warmed up to 95 ℃ mutually, is incubated 85 ℃, add the B phase, stirring and dissolving is complete;
B, D is warmed up to 95 ℃ mutually, is incubated 85 ℃, stirring and dissolving is complete;
C, earlier with C mixed phase suction emulsifying pot, suction D phase slowly adds the A phase, homogenizing 15min, insulated and stirred 15min, evacuation cooling more again;
D, add the E phase 70 ℃ the time, homogenizing 2-3min stirs;
E, add the F phase 50 ℃ the time, stir, promptly get product of the present invention.
Embodiment 3
Whitening spot-relieving cream cosmetic of the present invention, percentage composition comprises following component by weight:
A, main body Whitening, spot component 10%
B, auxiliary Whitening, spot component 2%
C, oil phase components 25%
D, water component 61.8%
E, thickening stabilization component 0.7%
F, auxiliary agent component 0.5%,
Wherein said main body Whitening, spot component is made up of following components in weight percentage content:
Glycyrrhiza glabra L. (GLYCYRRHIZA GLABRA) root extract 2.0%
Nicotiamide (VB3) 3.0%
Arbutin 3.0%
Hydroxy decyl ubiquinone 0.5%
Superfine titanium white (TiO2) 1.5%;
Wherein said auxiliary Whitening, spot component is made up of following components in weight percentage content:
Tioxolone 0.5%
Tocopherol acetas 1.5%;
Wherein said oil phase components is made up of following components in weight percentage content:
PEG-100 stearate 2.0%
Cetearyl alcohol 2.0%
Polydimethylsiloxane 4.0%
Caprylic/capric triglyceride 6.0%
Hydrogenated polydecene 9.0%
Ermine oil 2.0%;
Wherein said water component is made up of following components in weight percentage content:
EDTA disodium 0.1%
Allantoin 0.3%
Glycerol 5.0%
1,3 butylene glycol 5.0%
Xanthan gum 0.2%
Water 51.2%;
Wherein said thickening stabilization component is 0.7% C13-14 isoparaffin and the mixture in the lauryl alcohol-7;
Wherein said auxiliary agent component is 0.5% antiseptic.
The described whitening spot-relieving cream cosmetic of present embodiment is to prepare by following steps:
A, C is warmed up to 85 ℃ mutually, is incubated 80 ℃, add the B phase, stirring and dissolving is complete;
B, D is warmed up to 85 ℃ mutually, is incubated 80 ℃, stirring and dissolving is complete;
C, earlier with C mixed phase suction emulsifying pot, suction D phase slowly adds the A phase, homogenizing 10min, insulated and stirred 10min, evacuation cooling more again;
D, add the E phase 60 ℃ the time, homogenizing 2-3min stirs;
E, add the F phase 40 ℃ the time, stir, promptly get product of the present invention.
Whitening spot-relieving cream cosmetic to embodiment 1 to 3 is done some testing performance indexes, and its test is as follows
1. outward appearance: yellow fine and smooth cream frost
2.pH value: 4.5-6.5
3. viscosity: 100000-150000mpa.s
4. heat-resistant stability investigation (48 ℃ * 24h): qualified
5. cold-resistant study on the stability (15 ℃ * 24h): qualified.
The control experiment of whitening spot-relieving cream cosmetic result of use of the present invention:
The beauty treatment circle generally is divided into skin seven classes: seven classes such as neutral skin (normal skin), oily skin, dry skin, sensitive skin, mixed skin, aging skin, problem skin.Specifically:
1, oily skin: this type of skin complexion is dark, corse sweat pore, and sebum secretion is vigorous, and skin greasing is not easy to produce wrinkle, long easily acne, the seat skin ulcer, its pH value is between 5.6-6.6, and is defeated and dispersed immediately when foundation cream is relatively poor during cosmetic, sweats easily.
2, dry skin: the sebum secretion amount is few, does not have greasy feeling, and long easily tiny wrinkle stimulates relatively sensitivity to external world, and xerosis cutis is chapped easily, washes back skin with fancy soap and tingles, and can be divided into two kinds of hydropenia and oil starvations.The preceding kind is more common in more than 35 years old and the old people, and the back is planted and is more common in youngster, and its pH value is between 4.5-5;
3, neutral skin: be exactly normal skin, its pH value is between 5-5.6, and it is healthy desirable skin, and the moist high resilience of non-greasy loses pore, and is ruddy glossy, is not easy to wear out.
4, mixed skin: between dryness and oily skin, showing in the trigonum of having is greasy, and hole skin is thick then to show dry skin at eye and other place.Be more common in the 25-35 age in year;
5, allergic skin: skin stimulates responsive to external world, and allergic phenomenas such as skin is red, swollen, twinge, erythra just appear in (as: make apply some make up etc.) when being subjected to environmental stimuli.All medicines, pollen, cosmetics (as cosmetics such as lipstick, speckle dispelling class, fat-reducing class, hair dye, perfume), chemical substance (as paint etc.), animal skin, seafood (as Eriocheir sinensis etc.), plant (as Fructus Mangifera Indicae, Toxicodendron verniciflnum (Stokes) F. A. Barkley (Rhus verniciflua Stokes) etc.) are hot and cold, metal etc. all allergic phenomena can occur.
6, aging skin: skin occurs lax, dry, matt, and sebum secretion is few, wrinkle often occurs.Be more common in middle-aged and elderly people and sentimental women.
7, problem skin: all Symptomatic skin that goes wrong all is referred to as it problem skin.Problem skin mainly comprises mottle skin (chloasma, freckle, cyasma, butterfly spot, radiation spot etc.), acne, seat skin ulcer, speckle tinea, red blood streak, folliculitis, decortication, eczema, erythra, fester, various dermatitis, facial paralysed trace, nevus, carbuncle, cellulitis, treatment, skin ulcer or the like.
Object of study:
Choose the trier who suffers from mottle of above-mentioned 7 class skin attributes from the beauty treatment place, especially face's actual state is relatively poor, as test crowd of the present invention.
Specifically be divided into 7 and organize greatly, its principal character is:
(1) oiliness group; (2) dryness group; (3) neutral group; (4) Combination group; (5) anaphylaxis group; (6) aging group; (7) problem group.
Every big group is divided into three groups again, and wherein group one is a matched group, and 100 examples are observed by every group.
Experimental technique:
Common cosmetics on the group one usefulness market, used 1 month continuously at every day 3 times.
The whitening spot-relieving cream cosmetic of group's dual-purpose embodiment of the invention 1, used 1 month continuously at every day 3 times.
The whitening spot-relieving cream cosmetic of group's three usefulness embodiment of the invention 2, used 1 month continuously at every day 3 times.
The whitening spot-relieving cream cosmetic of group's four-function embodiment of the invention 3, used 1 month continuously at every day 3 times.
Experimental result sees Table 1
Table 1
Interpretation of result:
1, product of the present invention all has good effect for the problem of various skin matter, compares the improvement that all has in various degree with general cosmetics.But the just onset of about two weeks, one month effect is fairly obvious.2, by the record to client, product of the present invention has splendid desalination effect for symptoms such as freckle, the skin ulcer of fullying recover from an illness, acne, blackhead, chloasma, withered and yellow black face, chloasma, sun speckles, and whitening effect is preferably arranged.