CN109602643A - A kind of BB frost and preparation method thereof - Google Patents
A kind of BB frost and preparation method thereof Download PDFInfo
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- CN109602643A CN109602643A CN201811504739.0A CN201811504739A CN109602643A CN 109602643 A CN109602643 A CN 109602643A CN 201811504739 A CN201811504739 A CN 201811504739A CN 109602643 A CN109602643 A CN 109602643A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/90—Block copolymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of BB frosts, contain film forming agent, mixing toner, emulsifier, grease, thickener, moisturizer, pH adjusting agent, skin sense regulator, fragrance, preservative, other functional components, EDETATE SODIUM, water.BB frost in the present invention, hold adornment effect it is preferable on the basis of, be easy makeup removing and noresidue, small to the skin damage of user, the collocation of each ingredient rationally, moistens degree, moisturizing degree, concealing ability, holds adornment effect etc. and can reach preferable effect.
Description
Technical field
The present invention relates to cosmetic field, in particular to a kind of BB frost and preparation method thereof.
Background technique
In recent years, with the increase of the continuous development of cosmetics and the demand for the women that likes to be beautiful, BB frost is increasingly pursued by people
And become fashion trend.Its underlying cause is that BB frost is not only easy to use, but also has both foundation cream, sun-proof and isolated product
Effect.The women to like to be beautiful need to only use BB frost that can possess flawless skin quality and skin sense.BB frost can allow female friend
It gos out in proud array；It can more help the women to like to be beautiful to make perfect bottom adornment, persistently keep dressing in one day.
BB frost, is the abbreviation of BlemishBalm, and effect is mainly concealing, adjusts the colour of skin, is sun-proof, careful pore, can be made
Basic nude look effect out.It initially applies to medical cosmetology, entitled " scar moisturiser ", effect is mainly originating from Germany
Concealing adjusts the colour of skin, is sun-proof, careful pore.After experienced again and again change so that its with maintenance skin care in conjunction with, exist from initially
Become more ventilative using the BB frost that skin president small pox is even used for a long time in rear airtight, dry skin on the face, moisten moisturizing, and
And it also becomes to be more easier to remove ornaments and formal dress.
BB frost on the market is mostly Water-In-Oil emulsification structure, water-in-oil system for the considerations of holding adornment and stability
In, the stability of BB frost is relatively preferable, but the structure of water phase, Water-In-Oil are emulsified due to itself wrapping up using oily phase as foreign minister
BB frost inevitably may feel that skin sense is relatively glossy in use.In patent CN105687045A, produced in similar water-in-oil system
It can accomplish opposite soft and smooth water profit in product, but due to the structure that foreign minister itself is oily phase, main skin sense experience is still biased to
Oil, so can inevitably have glossy sense, wherein being easy to become apparent under fuel-displaced environment in summer etc..
As skin sense water moistens the salubrious market demand, the shortcomings that oil-in-water BB frost starts gradually to increase, and it holds adornment effect
Also gradually it is exposed.The generally existing adornment effect of holding of oil-in-water BB frost is general, can not the anti-sweat of waterproof.Patent CN108371637A
In, foundation cream itself have it is certain hold adornment effect, but still insufficient, the anti-sweat ability of water resistant is poor, so that moist or hold
The occasion easily perspired be easy to cause colored adornment.And since the light cosmetics such as general oil-in-water foundation cream are mainly used for summer etc.
When sweltering heat is easy to perspire, so the problem severity is also more prominent.
On the problem of holding adornment effect, if product its hold the relatively general even deviation of adornment effect, user needs regular
Refine the make-up；But it holds too strong also my the new problem of its bring of adornment effect.Such as: patent CN106963659A and patent
CN108294996A etc..It holds that adornment effect is stronger, can accomplish 7-8 hours adornments of holding, however after use, cleaning dressing needs make
It is removed ornaments and formal dress with makeup removal products, and general makeup removal products may not have enough cleaning force to clean it, cause Cosmetic Ingredient
Residual and accumulation, inflammation is easily caused after the accumulation of certain time and plays a series of skin problems such as acne.It is therefore desirable to have
One kind holds that adornment ability is enough, but is easy the product of makeup removing.
Summary of the invention
The purpose of the present invention is to provide a kind of BB frosts and preparation method thereof.
The technical solution used in the present invention is:
A kind of BB frost, containing film forming agent 0.2wt%~3wt%, mix toner 6wt%~20wt%, emulsifier 2wt%~
7wt%, grease 7wt%~20wt%, thickener 0.2wt%~3wt%, moisturizer 5wt%~20wt%, pH adjusting agent
0wt%~0.2wt%, skin sense regulator 2wt%~10wt%, fragrance 0.05wt%~0.2wt%, preservative 0.5wt%~
4wt%, other functional components 0.4wt%~2.0wt%, EDETATE SODIUM 0.05wt%~0.1wt%, water surplus；Wherein form a film
Agent is selected from polyquaternium -46, polyquaternium -44, polyquaternium -16, polyvinylpyrrolidone, VP/ Methacrylamide/ethylene
At least one of base imidazoles copolymer, VP/VA copolymer, acrylic acid (ester) class/N-tert-butyl acrylamide copolymer.
Further, it mixes and contains titanium dioxide and iron oxide toner in toner, wherein iron oxide toner is selected from iron oxide
At least one of Huang, iron oxide red, iron oxide black.
Further, emulsifier is selected from least one of Polyglycerol emulsifiers, oil-water emulsifiers, wherein polyglycereol cream
Agent is selected from Polyaldo DGDO(10-10-0), Natrulon H-10 decylate caprylate, Natrulon H-10 stearate, polyglycereol -6 two
At least one of stearate, -3 stearate of polyglycereol, oil-water emulsifiers are selected from Glyceryl stearate citrate, sweet
Oleostearin acid esters (and) PEG-100 stearate, Sucrose Polystearic Acid Esters (and) hydrogenation polyisobutylene, stearoyl polyglutamic acid
At least one of sodium, cetostearyl alcohol sulfosuccinate disodium, monoglyceride.
Further, grease be selected from isononyl isononanoate, carbonic acid dioctyl ester, sad Propylheptyl, hendecane (and) 13
Alkane, caprylic/capric triglyceride, dibutyl adipate, ring five dimethyl silicone polymer, dimethyl silicone polymer, C20-24 alkene
Hydrocarbon, dormant oil, isopropyl myristate, isopropyl palmitate, whale sodium stearyl alcohol, docosyl alcohol, propylheptyl caprylate, lauric alcohol-
At least one of caprylic/capric ester, silicone oil.
Further, thickener be selected from biological polyoses glue, carbomer, aluminium-magnesium silicate, polyacrylamide (and) polyethylene glycol
Diacrylate, sodium acrylate/sodium acryloyldimethyl taurate copolymers, isohexadecane, Polyoxyethylene Sorbitan Monooleate, polypropylene
At least one of sour sodium, carbonic acid dioctyl ester, -3 decylate of polyglycereol；Preferably, biological polyoses glue is selected from agarose, xanthan
One of glue, gellan gum, carragheen, cellulose are a variety of.
Further, moisturizer is in glycerol, propylene glycol, 1,3-BDO, hyaluronic acid, carbohydrate isomer
It is at least one.
Further, skin sense regulator be selected from silicone elastomer body, silicon powder, fungi plant glue, brown alga extract, boron nitride,
At least one of mica, bismuth oxychloride, wherein silicone elastomer body be selected from ring five dimethyl silicone polymer (and) poly dimethyl silicon
Oxygen alkane/vinyl dimethicone cross polymer and octyl polymethyl siloxane (and) ring five dimethyl silicone polymer
At least one of (and) Dimethicone Crosspolymer, silicon powder is selected from polymethylsilsesquioxane and vinyl is poly-
At least one of dimethyl siloxane/polymethyl siloxane silsesquioxane cross-linked polymer.
Further, preservative is selected from least one of Nipasol, methyl hydroxybenzoate, Phenoxyethanol.
Further, other functional components are selected from least one of antioxidant, antiallergic of releiving, ingredient；
Preferably, antioxidant be tocopherol acetate, lecithin, ascorbic acid, astaxanthin, lycopene, lipoic acid,
At least one of ubiquinone, tea polyphenols；
Preferably, antiallergic of releiving ingredient is selected from bisabolol, hydroxy phenylpropionyl amine benzoic acid, Flos Chrysanthemi extract, licorice
At least one of extract, glycyrrhizic acid, allantoin, ceramide, Herba Lysimachiae foenumgraeci extract.
Further, pH adjusting agent is sodium hydroxide.
The beneficial effects of the present invention are:
BB frost in the present invention uses the film forming agent different from traditional film forming agent, and the film forming agent that the present invention uses includes:
Polyquaternium -46, VP/ Methacrylamide/Nvinylimidazole copolymers, VP/VA copolymer etc..Such film forming agent original purposes one
As be hair styling agent, relative to the film forming agent of mainstream, film-formation result may be slightly weak, but its film forming after effect relatively more
Continuously, frivolous flexible.Secondly, such film forming agent itself has preferable water solubility, can as the film-forming protecting agents of water phase foreign minister,
After BB frost is smeared, moisture gradually evaporates, and product gradually forms a film, and can effectively improve BB frost holds adornment effect.
In the present invention BB frost, hold adornment effect it is preferable on the basis of, be easy makeup removing and noresidue, to the skin of user
It injures small.
BB frost in the present invention, the collocation of each ingredient rationally, moisten that degree, moisturizing degree, concealing ability, to hold adornment effect etc. equal
Preferable effect can be reached.
Detailed description of the invention
Fig. 1 is makeup removing effect experimental result.
Specific embodiment
Below in conjunction with embodiment, the present invention is further explained, it should be appreciated that following embodiment be merely to illustrate the present invention and
It is not used in and limits the scope of the invention.
Examples 1 to 3
The formula of BB frost in Examples 1 to 3 is as shown in the table:
Specific preparation process is as follows for the oil-in-water BB frost of above-described embodiment 1:
1) by titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate, C20-24 alkene use equal
Matter machine or colloid mill are uniformly dispersed, spare to make.
2) by Polyaldo DGDO(10-10-0), the hard ester alcohol of whale sodium, propylheptyl caprylate, tocopherol acetate, opopanax
Mixture puts into oily phase in alcohol, lauric alcohol-caprylic/capric ester, Nipasol, Glyceryl stearate citrate and step 1
Pot is heated to 85 DEG C, and stirring homogenous disperse is uniform.
3) by glycerol, propylene glycol, EDETATE SODIUM, xanthan gum, aluminium-magnesium silicate, gellan gum, methyl hydroxybenzoate, the hard ester alcohol sulphur of whale sodium
Base succinate disodium, ethyl alcohol and polyquaternium -46 put into emulsion pot, are dispersed with stirring uniformly, pure water is added, is gradually warmed up
85 DEG C, insulated and stirred.
4) by dimethicone, ring five dimethyl silicone polymer/Dimethicone/Vinyl Dimethicone
- 3 decylate of cross-linked polymer and Sodium Polyacrylate (and) carbonic acid dioctyl ester (and) polyglycereol is dispersed with stirring uniformly spare to make.
5) emulsion pot in stirring, emulsifying is added in step 2 gained mixture.
6) step 4 gained mixture is added to the emulsion pot in homogeneous.
7) 45 DEG C are cooled to, adds surplus stock one by one.
Specific preparation process is as follows for the oil-in-water BB frost of above-described embodiment 2:
1) by titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate, C20-24 alkene use equal
Matter machine or colloid mill are uniformly dispersed, spare to make.
2) by Polyaldo DGDO(10-10-0), the hard ester alcohol of whale sodium, propylheptyl caprylate, tocopherol acetate, opopanax
Mixture puts into oily phase in alcohol, lauric alcohol-caprylic/capric ester, Nipasol, Glyceryl stearate citrate and step 1
Pot is heated to 85 DEG C, and stirring homogenous disperse is uniform.
3) by glycerol, propylene glycol, EDETATE SODIUM, xanthan gum, aluminium-magnesium silicate, gellan gum, methyl hydroxybenzoate, the hard ester alcohol sulphur of whale sodium
Base succinate disodium, ethyl alcohol and VP/VA copolymer (copolymer) put into emulsion pot, are dispersed with stirring uniformly, pure water is added, by
85 DEG C are gradually warming up to, insulated and stirred.
4) by dimethicone, ring five dimethyl silicone polymer/Dimethicone/Vinyl Dimethicone
- 3 decylate of cross-linked polymer and Sodium Polyacrylate (and) carbonic acid dioctyl ester (and) polyglycereol is dispersed with stirring uniformly spare to make.
5) emulsion pot in stirring, emulsifying is added in step 2 gained mixture.
6) step 4 gained mixture is added to the emulsion pot in homogeneous.
7) 45 DEG C are cooled to, adds surplus stock one by one.
Specific preparation process is as follows for the oil-in-water BB frost of above-described embodiment 3:
1) by titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate, C20-24 alkene use equal
Matter machine or colloid mill are uniformly dispersed, spare to make.
2) by Polyaldo DGDO(10-10-0), the hard ester alcohol of whale sodium, propylheptyl caprylate, tocopherol acetate, opopanax
Mixture puts into oily phase in alcohol, lauric alcohol-caprylic/capric ester, Nipasol, Glyceryl stearate citrate and step 1
Pot is heated to 85 DEG C, and stirring homogenous disperse is uniform.
3) acrylic acid (rouge) class/N-tert-butyl acrylamide copolymer is uniformly mixed with alcohol, sodium hydroxide is then added
Aqueous solution.
4) by glycerol, propylene glycol, EDETATE SODIUM, xanthan gum, aluminium-magnesium silicate, gellan gum, methyl hydroxybenzoate, the hard ester alcohol sulphur of whale sodium
Mixture puts into emulsion pot in base succinate disodium and step 3, is dispersed with stirring uniformly, pure water is added, is gradually warmed up to 85
DEG C, insulated and stirred.
5) by dimethicone, ring five dimethyl silicone polymer/Dimethicone/Vinyl Dimethicone
Cross-linked polymer, -3 decylate of Sodium Polyacrylate (and) carbonic acid dioctyl ester (and) polyglycereol are dispersed with stirring uniformly spare to make.
6) emulsion pot in stirring, emulsifying is added in step 2 gained mixture.
7) step 5 gained mixture is added to the emulsion pot in homogeneous.
8) 45 DEG C are cooled to, adds surplus stock one by one.
Detection of Stability
Detection of Stability result is as shown in the table:
BB frost in Examples 1 to 3 is long-term by long term storage (room temperature 1 year) and cold-resistant (- 15 DEG C), heat-resisting (45 DEG C)
Destructive testing, product meet national relevant regulations without significant change, every organoleptic indicator, physical and chemical index.
The evaluation and test of product effect
Gained BB frost in Example 1-3 carries out clinical trial evaluation (with commercially available oil-in-water BB frost and Water-In-Oil BB frost
It compares, remembers that commercially available oil-in-water BB frost is comparative example 1, Water-In-Oil BB frost is comparative example 2).
Clinical trial condition are as follows: random volunteer 50, the age 20-40 years old, wherein it is ensured that extracting sensitive skin (i.e. skin
It is relatively thin, be easy allergy, red capillary is obvious on the face, and skin is easy general red fever, skin be easy by environmental factor, seasonal variations and
Facial product stimulate allergy) crowd 10.Tester is divided into 5 groups, respectively using the frost of BB obtained by Examples 1 to 3 and
Two kinds of commercially available BB frost products according to using effect are 5 to using product to be evaluated using after one month daily using primary
Point, preferably 4 points, generally 3 points, it is bad be 2 points, it is very poor be 1 point, some projects are to have the number accordingly felt.
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 |
| Moisten degree | 3.7 | 3.4 | 3.6 | 3.5 | 4.2 |
| Moisturizing degree | 4.0 | 3.6 | 3.7 | 3.4 | 3.2 |
| Concealing ability | 4.0 | 3.9 | 4.1 | 4.0 | 4.0 |
| Hold adornment effect | 4.1 | 4.3 | 4.2 | 3.6 | 4.5 |
| Greasy feeling | 5 | 4 | 6 | 3 | 18 |
| Sense of discomfort | 0 | 1 | 0 | 2 | 3 |
Five groups of testers on the back of the hand, are uniformly applied on the skin of 5*5cm with 0.5g respective sample and (are drawn between having respectively
Be divided into the net region of 0.5cm), respectively before testing, after bath 1 minute, gently after suck dry moisture, clear water wash by rubbing with the hands after and make
Masked area is counted after gently rubbing 15s with general makeup remover.As a result such as following table, line chart such as Fig. 1.
| Before test | After bath | After water suction | After washing by rubbing with the hands | After makeup removing | |
| Embodiment 1 | 100 | 100 | 92 | 0 | 0 |
| Embodiment 2 | 100 | 100 | 96 | 0 | 0 |
| Embodiment 3 | 100 | 100 | 93 | 0 | 0 |
| Comparative example 1 | 100 | 95 | 83 | 13 | 0 |
| Comparative example 2 | 100 | 100 | 98 | 46 | 6 |
Claims (9)
1. a kind of BB frost, it is characterised in that: contain film forming agent 0.2wt%~3wt%, mixing toner 6wt%~20wt%, emulsification
Agent 2wt%~7wt%, grease 7wt%~20wt%, thickener 0.2wt%~3wt%, moisturizer 5wt%~20wt%, pH
Regulator 0wt%~0.2wt%, skin sense regulator 2wt%~10wt%, fragrance 0.05wt%~0.2wt%, preservative
0.5wt%~4wt%, other functional components 0.4wt%~2.0wt%, EDETATE SODIUM 0.05wt%~0.1wt%, water surplus；
Wherein film forming agent is selected from polyquaternium -46, polyquaternium -44, polyquaternium -16, polyvinylpyrrolidone, VP/ metering system
Amide/Nvinylimidazole copolymers, VP/VA copolymer, at least one in acrylic acid (ester) class/N-tert-butyl acrylamide copolymer
Kind.
2. BB frost according to claim 1, it is characterised in that: contain titanium dioxide and iron oxide toner in mixing toner,
Wherein iron oxide toner is selected from least one of iron oxide yellow, iron oxide red, iron oxide black.
3. BB frost according to claim 1, it is characterised in that: emulsifier is selected from Polyglycerol emulsifiers, oil-water emulsifiers
At least one of, wherein Polyglycerol emulsifiers be selected from Polyaldo DGDO(10-10-0), Natrulon H-10 decylate caprylate, gather it is sweet
At least one of oily -10 stearates, -6 distearate of polyglycereol, -3 stearate of polyglycereol, oil-water emulsifiers choosing
From Glyceryl stearate citrate, stearine (and) PEG-100 stearate, Sucrose Polystearic Acid Esters (and) hydrogenation
At least one of polyisobutylene, stearoyl polyglutamic acid sodium, cetostearyl alcohol sulfosuccinate disodium, monoglyceride.
4. BB frost according to claim 1, it is characterised in that: grease is selected from isononyl isononanoate, carbonic acid dioctyl ester, octanoic acid
Propylheptyl, hendecane (and) tridecane, caprylic/capric triglyceride, dibutyl adipate, ring five dimethyl silicone polymer,
Dimethyl silicone polymer, C20-24 alkene, dormant oil, isopropyl myristate, isopropyl palmitate, whale sodium stearyl alcohol, docosyl alcohol,
At least one of propylheptyl caprylate, lauric alcohol-caprylic/capric ester, silicone oil.
5. BB frost according to claim 1, it is characterised in that: thickener is selected from biological polyoses glue, carbomer, magnesium silicate
Aluminium, polyacrylamide (and) polyethyleneglycol diacrylate, sodium acrylate/sodium acryloyldimethyl taurate copolymers, different ten
At least one of six alkane, Polyoxyethylene Sorbitan Monooleate, Sodium Polyacrylate, carbonic acid dioctyl ester, -3 decylate of polyglycereol；Preferably, raw
Object polysaccharide gum is selected from one of agarose, xanthan gum, gellan gum, carragheen, cellulose or a variety of.
6. BB according to claim 1 frost, it is characterised in that: moisturizer is selected from glycerol, propylene glycol, 1,3-BDO, thoroughly
At least one of bright matter acid, carbohydrate isomer.
7. BB frost according to claim 1, it is characterised in that: skin sense regulator is selected from silicone elastomer body, silicon powder, mushroom and plants
At least one of object glue, brown alga extract, boron nitride, mica, bismuth oxychloride, wherein silicone elastomer body is selected from the poly- diformazan of ring five
Radical siloxane (and) Dimethicone/Vinyl Dimethicone cross-linked polymer and octyl polymethyl siloxane
At least one of (and) ring five dimethyl silicone polymer (and) Dimethicone Crosspolymer, silicon powder is selected from poly- methyl
At least one in silsesquioxane and vinyldimethicone/polymethyl siloxane silsesquioxane cross-linked polymer
Kind.
8. BB frost according to claim 1, it is characterised in that: preservative is selected from Nipasol, methyl hydroxybenzoate, Phenoxyethanol
At least one of.
9. BB according to claim 1 frost, it is characterised in that: other functional components be selected from antioxidant, antiallergic of releiving, at
At least one of point；
Preferably, antioxidant be tocopherol acetate, it is lecithin, ascorbic acid, astaxanthin, lycopene, lipoic acid, general
At least one of quinone, tea polyphenols；
Preferably, antiallergic of releiving ingredient is selected from bisabolol, hydroxy phenylpropionyl amine benzoic acid, Flos Chrysanthemi extract, licorice and extracts
At least one of object, glycyrrhizic acid, allantoin, ceramide, Herba Lysimachiae foenumgraeci extract.
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| CN111759744A (en) * | 2020-08-03 | 2020-10-13 | 上海绵花棠生物科技有限公司 | Cosmetic composition, preparation method thereof and cosmetic product |
| CN112294700A (en) * | 2020-11-17 | 2021-02-02 | 广州美赢东方生物科技有限公司 | Foundation cream and preparation method thereof |
| CN113208940A (en) * | 2021-04-30 | 2021-08-06 | 广州市科能化妆品科研有限公司 | Refreshing and stable sunscreen composition and preparation method thereof |
| CN113208940B (en) * | 2021-04-30 | 2022-12-23 | 广州市科能化妆品科研有限公司 | Refreshing and stable sun-screening composition and preparation method thereof |
| CN113940899A (en) * | 2021-09-29 | 2022-01-18 | 广州卓芬化妆品有限公司 | Waterproof foundation composition and preparation method thereof |
| CN113940899B (en) * | 2021-09-29 | 2024-03-12 | 广州卓芬化妆品有限公司 | Waterproof foundation composition and preparation method thereof |
| CN115400041A (en) * | 2022-06-17 | 2022-11-29 | 诺斯贝尔化妆品股份有限公司 | Cosmetic composition with alpha gel structure and preparation method thereof |
| CN115400041B (en) * | 2022-06-17 | 2023-09-29 | 诺斯贝尔化妆品股份有限公司 | Cosmetic composition with alpha gel structure and preparation method thereof |
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| CN109602643B (en) | 2022-06-03 |
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