CN109602643B - BB cream and preparation method thereof - Google Patents
BB cream and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/90—Block copolymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses BB cream which comprises a film-forming agent, mixed toner, an emulsifier, grease, a thickener, a humectant, a pH regulator, a skin feel regulator, perfume, a preservative, other functional components, EDTA disodium and water. The BB cream disclosed by the invention is easy to remove makeup and has no residue on the basis of good makeup holding effect, has small harm to the skin of a user, is reasonable in component matching, and can achieve good effects in the aspects of moistening degree, humidity preservation, blemish covering capability, makeup holding effect and the like.
Description
Technical Field
The invention relates to the field of cosmetics, and particularly relates to BB cream and a preparation method thereof.
Background
In recent years, with the continuous development of cosmetics and the increase of the demand of beauty-conscious women, BB creams are more and more sought after and become a popular trend. The fundamental reason is that the BB cream is not only convenient to use, but also has the effects of foundation make-up, sun protection and isolation products. Beauty-conscious women can have perfect skin and skin feel only by using the BB cream. BB cream can make female friends go out with confidence; can help women who love beauty to make perfect base makeup and keep makeup for one day.
BB cream, called BlemishBalm for short, mainly has the functions of concealing blemishes, adjusting skin colors, preventing sun and refining pores, and can make basic makeup with bare effect. It originates from Germany and is originally applied to medical cosmetology, named as 'scar moisturizing cream' and mainly has the functions of concealing blemishes, adjusting skin color, preventing sunlight and refining pores. The later change is made once, so that the BB cream is combined with skin care, becomes more breathable, moist and moist from the BB cream which is not breathable after being used on the face initially, and even has acne after being used for a long time, and also becomes easier to remove makeup.
Most of the BB creams in the market are water-in-oil emulsified structures due to the considerations of makeup durability and stability, and in a water-in-oil system, the stability of the BB cream is relatively good, but due to the structure that an oil phase is used as an external phase to wrap an emulsified water phase, the water-in-oil BB cream inevitably feels relatively oily in skin in use. In patent CN105687045A, it can achieve relative soft and smooth water-moistening in similar water-in-oil system products, but because the external phase of itself is the structure of oil phase, the main skin feeling experience is still biased to oil, so there is inevitably a feeling of oil-moistening, and it is more obvious in summer and other environments where oil is easily produced.
With the market demand of moisturizing and refreshing skin feel, the oil-in-water BB cream is gradually increased, and the shortcomings of the makeup-sustaining effect are gradually exposed. The oil-in-water BB cream generally has a common makeup holding effect and cannot resist water and sweat. In patent CN108371637A, the foundation has a certain makeup-holding effect, but is still insufficient, and has poor water resistance and sweat resistance, so that the makeup is easy to be made in the damp or sweat-prone occasions. In addition, since a refreshing cosmetic such as a general oil-in-water foundation is mainly used in a case where sweat is easily generated due to heat such as summer, the problem is also highlighted in severity.
On the aspect of the makeup maintaining effect, if the makeup maintaining effect of the product is relatively general or even deviated, a user needs to make up regularly; but the over-strong make-up holding effect brings new problems to the make-up holding agent. For example: patent CN106963659A and patent CN 108294996A. The makeup-removing product has a strong makeup-removing effect, can make makeup for 7-8 hours, however, after the makeup-removing product is used, the makeup-removing product is needed to remove makeup from the makeup-removing product, and the general makeup-removing product does not necessarily have enough cleaning power to clean the makeup-removing product, so that the makeup-removing product can cause residual and accumulation of makeup components, and a series of skin problems such as inflammation and acne are easily caused after the makeup-removing product is accumulated for a certain time. Thus, there is a need for a product that has sufficient makeup retention, but is easy to remove.
Disclosure of Invention
The invention aims to provide BB cream and a preparation method thereof.
The technical scheme adopted by the invention is as follows:
BB cream comprises 0.2-3 wt% of film forming agent, 6-20 wt% of mixed toner, 2-7 wt% of emulsifier, 7-20 wt% of grease, 0.2-3 wt% of thickening agent, 5-20 wt% of humectant, 0-0.2 wt% of pH regulator, 2-10 wt% of skin-feel regulator, 0.05-0.2 wt% of perfume, 0.5-4 wt% of preservative, 0.4-2.0 wt% of other functional components, 0.05-0.1 wt% of disodium EDTA and the balance of water; wherein the film forming agent is selected from at least one of polyquaternium-46, polyquaternium-44, polyquaternium-16, polyvinylpyrrolidone, VP/methacrylamide/vinyl imidazole copolymer, VP/VA copolymer and acrylic acid (ester)/tert-butyl acrylamide copolymer.
Further, the mixed toner contains titanium dioxide and ferric oxide toner, wherein the ferric oxide toner is selected from at least one of ferric oxide yellow, ferric oxide red and ferric oxide black.
Further, the emulsifier is at least one selected from the group consisting of polyglyceryl emulsifier selected from the group consisting of polyglyceryl-10 decaoleate, polyglyceryl-10 decanoate caprylate, polyglyceryl-10 stearate, polyglyceryl-6 distearate, and polyglyceryl-3 stearate, and the oil-in-water emulsifier is at least one selected from the group consisting of glyceryl stearate citrate, glyceryl stearate (and) PEG-100 stearate, sucrose polystearate (and) hydrogenated polyisopropylene, sodium stearyl polyglutamate, disodium cetearyl sulfosuccinate, and monoglycerides.
Further, the oil and fat is selected from at least one of isononyl isononanoate, dioctyl carbonate, propylheptyl caprylate, undecane (and) tridecane, caprylic/capric triglyceride, dibutyl adipate, cyclopentyldimethicone, dimethicone, C20-24 olefin, mineral oil, isopropyl myristate, isopropyl palmitate, cetyl sodium stearyl alcohol, behenyl alcohol, propylheptyl caprylate, coco-caprylic/capric acid ester, and silicone oil.
Further, the thickener is selected from at least one of a biopolysaccharide gum, carbomer, magnesium aluminum silicate, polyacrylamide (and) polyethylene glycol diacrylate, sodium acrylate/sodium acryloyldimethyl taurate copolymer, sodium polyacrylate (and) dioctyl carbonate (and) polyglycerol-3 decanoate; preferably, the biopolysaccharide gum is selected from one or more of agarose, xanthan gum, gellan gum, carrageenan, cellulose.
Further, the humectant is at least one selected from glycerin, propylene glycol, 1, 3-butylene glycol, hyaluronic acid, and saccharide isomer.
Further, the skin feel modifier is selected from at least one of silica gel elastomer, silica powder, fungus plant gum, brown algae extract, boron nitride, mica and bismuth oxychloride, wherein the silica gel elastomer is selected from at least one of cyclopentadimethylsiloxane (and) polydimethylsiloxane/vinyl polydimethylsiloxane cross-polymer and octyl-methicone (and) cyclopentadimethylsiloxane (and) polydimethylsiloxane cross-polymer, and the silica powder is selected from at least one of polymethylsilsesquioxane and vinyl polydimethylsiloxane/polymethylsilsesquioxane cross-polymer.
Further, the preservative consists of 0.1 wt% of propyl hydroxybenzoate, 0.1 wt% of methyl hydroxybenzoate and 0.5 wt% of phenoxyethanol.
Further, other effective components are selected from at least one of antioxidant, soothing and anti-allergy, and components;
preferably, the antioxidant is at least one of tocopherol acetate, lecithin, ascorbic acid, astaxanthin, lycopene, lipoic acid, ubiquinone and tea polyphenol;
preferably, the soothing and anti-allergy ingredient is at least one selected from bisabolol, hydroxyphenylpropionamide benzoic acid, chamomile extract, licorice root extract, glycyrrhizic acid, allantoin, ceramide, lavender extract.
Further, the pH adjuster is sodium hydroxide.
The invention has the beneficial effects that:
the BB cream disclosed by the invention adopts a film forming agent different from a traditional film forming agent, and the film forming agent adopted by the invention comprises the following components: polyquaternium-46, VP/methacrylamide/vinylimidazole copolymers, VP/VA copolymers, and the like. The film-forming agent is generally used as a hair styling agent, and compared with a mainstream film-forming agent, the film-forming effect of the film-forming agent is possibly slightly weaker, but the effect after film formation is relatively more continuous, light, thin and flexible. Secondly, the film forming agent has good water solubility and can be used as a film forming protective agent of a water phase external phase, after the BB cream is smeared, water is gradually evaporated, the product is gradually formed into a film, and the makeup holding effect of the BB cream can be effectively improved.
The BB cream disclosed by the invention is easy to remove makeup and has no residue on the basis of good makeup holding effect, and has little harm to the skin of a user.
The BB cream disclosed by the invention is reasonable in component matching, and can achieve better effects in the aspects of moistening degree, humidity preservation, blemish covering capability, makeup holding effect and the like.
Drawings
Fig. 1 shows the result of the makeup removal effect test.
Detailed Description
The present invention will be further illustrated with reference to the following examples, which are intended to illustrate the invention and are not intended to limit the scope of the invention.
Examples 1 to 3
The formulations of the BB creams of examples 1 to 3 are shown in the following table:
the oil-in-water BB cream of the above example 1 is prepared by the following steps:
1) dispersing titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate and C20-24 olefin uniformly by using a homogenizer or a colloid mill for later use.
2) Putting polyglycerol-10 decaoleate, cetyl sodium stearate alcohol, propyl heptyl caprylate, tocopherol acetate, bisabolol, coconut oil alcohol-caprylic/capric acid ester, propyl hydroxybenzoate, glyceryl stearate citrate and the mixture obtained in the step 1 into an oil phase pot, heating to 85 ℃, and stirring, homogenizing and dispersing uniformly.
3) Putting glycerol, propylene glycol, disodium EDTA, xanthan gum, magnesium aluminum silicate, gellan gum, methylparaben, disodium cetyl stearyl sulfosuccinate, ethanol and polyquaternium-46 into an emulsifying pot, stirring and dispersing uniformly, adding pure water, gradually heating to 85 ℃, and keeping the temperature and stirring.
4) Simethicone, cyclopenta dimethyl silicone/vinyl dimethyl silicone cross-linked polymer and sodium polyacrylate (and) dioctyl carbonate (and) polyglycerol-3 decanoate are stirred and dispersed uniformly for later use.
5) And (3) adding the mixture obtained in the step (2) into an emulsifying pot while stirring, and homogenizing and emulsifying.
6) And (5) adding the mixture obtained in the step (4) into an emulsifying pot in homogenization.
7) Cooling to 45 deg.C, and adding the rest raw materials one by one.
The oil-in-water BB cream of the above example 2 is prepared by the following specific steps:
1) dispersing titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate and C20-24 olefin uniformly by using a homogenizer or a colloid mill for later use.
2) Putting polyglycerol-10 decaoleate, cetyl sodium stearate alcohol, propyl heptyl caprylate, tocopherol acetate, bisabolol, coconut oil alcohol-caprylic/capric acid ester, propyl hydroxybenzoate, glyceryl stearate citrate and the mixture obtained in the step 1 into an oil phase pot, heating to 85 ℃, and stirring, homogenizing and dispersing uniformly.
3) Putting glycerol, propylene glycol, disodium EDTA, xanthan gum, magnesium aluminum silicate, gellan gum, methylparaben, disodium cetyl stearyl sulfosuccinate, ethanol and VP/VA copolymer (copolymer) into an emulsifying pot, stirring and dispersing uniformly, adding pure water, gradually heating to 85 ℃, and keeping the temperature and stirring.
4) Simethicone, cyclopenta dimethyl silicone/vinyl dimethyl silicone cross-linked polymer and sodium polyacrylate (and) dioctyl carbonate (and) polyglycerol-3 decanoate are stirred and dispersed uniformly for later use.
5) And (3) adding the mixture obtained in the step (2) into an emulsifying pot while stirring, and homogenizing and emulsifying.
6) And (4) adding the mixture obtained in the step (4) into an emulsifying pot in homogenizing.
7) Cooling to 45 deg.C, and adding the rest raw materials one by one.
The oil-in-water BB cream of the above example 3 is prepared by the following specific steps:
1) dispersing titanium dioxide, iron oxide red, iron oxide black, iron oxide yellow, isononyl isononanoate and C20-24 olefin uniformly by using a homogenizer or a colloid mill for later use.
2) Putting polyglycerol-10 decaoleate, cetyl sodium stearate alcohol, propyl heptyl caprylate, tocopherol acetate, bisabolol, coconut oil alcohol-caprylic/capric acid ester, propyl hydroxybenzoate, glyceryl stearate citrate and the mixture obtained in the step 1 into an oil phase pot, heating to 85 ℃, and stirring, homogenizing and dispersing uniformly.
3) The acrylic acid (ester)/tert-butyl acrylamide copolymer is mixed with alcohol uniformly, and then sodium hydroxide aqueous solution is added.
4) Putting the mixture in the step 3 and glycerin, propylene glycol, EDTA disodium, xanthan gum, magnesium aluminum silicate, gellan gum, methylparaben, cetyl stearyl alcohol disodium sulfosuccinate into an emulsifying pot, stirring and dispersing uniformly, adding pure water, gradually heating to 85 ℃, preserving heat and stirring.
5) Simethicone, cyclopenta dimethyl silicone/vinyl dimethyl silicone cross-linked polymer, sodium polyacrylate (and) dioctyl carbonate (and) polyglycerol-3 decanoate are stirred and dispersed uniformly for later use.
6) And (3) adding the mixture obtained in the step (2) into an emulsifying pot while stirring, and homogenizing and emulsifying.
7) And (4) adding the mixture obtained in the step (5) into an emulsifying pot in homogenizing.
8) Cooling to 45 deg.C, and adding the rest raw materials one by one.
Stability detection
The stability test results are shown in the following table:
the BB cream in the embodiments 1 to 3 has no obvious change after long-term storage (normal temperature for 1 year), cold resistance (-15 ℃) and heat resistance (45 ℃) long-term destructive tests, and all sensory indexes and physical and chemical indexes meet related national regulations.
Product effect evaluation
The BB cream obtained in examples 1 to 3 was used for clinical laboratory evaluation (in contrast to commercially available oil-in-water BB cream and water-in-oil BB cream, the commercially available oil-in-water BB cream was designated as comparative example 1, and the water-in-oil BB cream was designated as comparative example 2).
The clinical experimental conditions were: random volunteers 50, aged 20-40 years, wherein 10 people who had taken sensitive skin (i.e. thin skin, easy allergy, obvious red blood streak on face, easy skin redness and fever, skin sensitive to environmental factors, seasonal changes and irritation of facial care products) were assured. The test personnel are divided into 5 groups, the BB cream obtained in the examples 1-3 and two commercially available BB cream products are used once a day, the used products are evaluated to be 5 points, preferably 4 points, generally 3 points, not preferably 2 points and very poorly 1 point according to the using effect after one month of use, and part of the items are the number of people with corresponding feelings.
| Test item | Example 1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 |
| Moistening degree | 3.7 | 3.4 | 3.6 | 3.5 | 4.2 |
| Moisture retention | 4.0 | 3.6 | 3.7 | 3.4 | 3.2 |
| Concealing capability | 4.0 | 3.9 | 4.1 | 4.0 | 4.0 |
| Make-up effect | 4.1 | 4.3 | 4.2 | 3.6 | 4.5 |
| Greasy feeling | 5 | 4 | 6 | 3 | 18 |
| |
0 | 1 | 0 | 2 | 3 |
Five groups of testers applied 0.5g of corresponding samples on the backs of hands respectively on 5 × 5cm of skin (with 0.5cm grid areas scribed), and counted the coverage area before testing, after flushing for 1 minute, after gently sucking off water, after washing with clean water and after gently kneading for 15 seconds with common makeup remover. The results are shown in the table below, with the line diagrams in FIG. 1.
| Before testing | After flushing | After absorbing water | After scrubbing and washing | After makeup removal | |
| Example 1 | 100 | 100 | 92 | 0 | 0 |
| Example 2 | 100 | 100 | 96 | 0 | 0 |
| |
100 | 100 | 93 | 0 | 0 |
| Comparative example 1 | 100 | 95 | 83 | 13 | 0 |
| Comparative example 2 | 100 | 100 | 98 | 46 | 6 |
Claims (10)
1. BB cream is characterized by comprising 0.2-3 wt% of film forming agent, 6-20 wt% of mixed toner, 2-7 wt% of emulsifier, 7-20 wt% of grease, 0.2-3 wt% of thickener, 5-20 wt% of humectant, 0-0.2 wt% of pH regulator, 2-10 wt% of skin feel regulator, 0.05-0.2 wt% of perfume, 0.5-4 wt% of preservative, 0.4-2.0 wt% of other functional components, 0.05-0.1 wt% of disodium EDTA and the balance of water;
the film-forming agent is acrylic acid (ester)/tert-butyl acrylamide copolymer;
the mixed toner contains titanium dioxide and ferric oxide toner, wherein the ferric oxide toner is selected from at least one of ferric oxide yellow, ferric oxide red and ferric oxide black;
the other functional components are at least one of antioxidant and anti-allergy relieving component.
2. The BB cream of claim 1, wherein the emulsifier is selected from at least one of a polyglycerol emulsifier selected from at least one of polyglycerol-10 oleate, polyglycerol-10 caprate caprylate, polyglycerol-10 stearate, polyglycerol-6 distearate, polyglycerol-3 stearate, and an oil-in-water emulsifier selected from at least one of glycerol stearate citrate, glycerol stearate (and) PEG-100 stearate, sucrose polystearate (and) hydrogenated polyisopropene, sodium stearoylpolyglutamate, disodium cetostearyl sulfosuccinate, and monoglycerides.
3. The BB cream of claim 2, wherein the grease is selected from at least one of isononyl isononanoate, dioctyl carbonate, propylheptyl caprylate, undecane (and) tridecane, caprylic/capric triglyceride, dibutyl adipate, C20-24 olefin, mineral oil, isopropyl myristate, isopropyl palmitate, cetostearyl alcohol, behenyl alcohol, propylheptyl caprylate, coco-caprylic/capric acid ester, and silicone oil.
4. The BB cream of claim 3, wherein the thickener is selected from at least one of a biopolysaccharide gum, carbomer, veegum, polyacrylamide (and) polyethylene glycol diacrylate, sodium acrylate/sodium acryloyldimethyl taurate copolymer, sodium polyacrylate (and) dioctyl carbonate (and) polyglycerol-3 decanoate.
5. The BB cream according to claim 4, wherein the biopolysaccharide gum is selected from one or more of agarose, xanthan gum, gellan gum, carrageenan and cellulose.
6. The BB cream of any one of claims 1 to 5, wherein the humectant is at least one selected from glycerin, propylene glycol, 1, 3-butylene glycol, hyaluronic acid and saccharide isomers.
7. The BB cream according to any one of claims 1 to 5, wherein the skin-feel modifier is selected from at least one of a silica gel elastomer selected from at least one of cyclopentadimethylsiloxane (and) at least one of polydimethylsiloxane/vinyl polydimethylsiloxane crosspolymer and octylmethicone (and) cyclopentadimethylsiloxane (and) at least one of vinyl dimethicone/methicone silsesquioxane crosspolymer, silica powder, and silicone oxide, and a mixture thereof.
8. The BB cream of claim 7, wherein the preservative comprises propylparaben 0.1 wt%, methylparaben 0.1 wt%, and phenoxyethanol 0.5 wt%.
9. The BB cream of claim 8, wherein the antioxidant is at least one of tocopherol acetate, lecithin, ascorbic acid, astaxanthin, lycopene, lipoic acid, ubiquinone, and tea polyphenol.
10. The BB cream according to claim 9, wherein the soothing and anti-allergy ingredient is at least one selected from the group consisting of bisabolol, hydroxyphenylpropionamide benzoic acid, chamomile extract, licorice root extract, glycyrrhizic acid, allantoin, ceramide, and lavender extract.
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| CN110037931A (en) * | 2019-05-31 | 2019-07-23 | 福建省梦娇兰日用化学品有限公司 | A kind of infant's efficient moisture-retention moisturizing lotion of the component containing antipollution |
| CN111759744A (en) * | 2020-08-03 | 2020-10-13 | 上海绵花棠生物科技有限公司 | Cosmetic composition, preparation method thereof and cosmetic product |
| CN112294700A (en) * | 2020-11-17 | 2021-02-02 | 广州美赢东方生物科技有限公司 | Foundation cream and preparation method thereof |
| CN113208940B (en) * | 2021-04-30 | 2022-12-23 | 广州市科能化妆品科研有限公司 | Refreshing and stable sun-screening composition and preparation method thereof |
| CN113940899B (en) * | 2021-09-29 | 2024-03-12 | 广州卓芬化妆品有限公司 | Waterproof foundation composition and preparation method thereof |
| CN115400041B (en) * | 2022-06-17 | 2023-09-29 | 诺斯贝尔化妆品股份有限公司 | Cosmetic composition with alpha gel structure and preparation method thereof |
| CN118078654A (en) * | 2024-04-03 | 2024-05-28 | 广州亿彩生物科技有限公司 | BB cream and preparation method thereof |
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| EP2221045A1 (en) * | 2009-02-20 | 2010-08-25 | Beiersdorf AG | Skin care formulations with an immediate tautening effect |
| US10105297B2 (en) * | 2016-04-01 | 2018-10-23 | L'oreal | Sunscreen compositions and methods for boosting efficacy |
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| US20150274972A1 (en) * | 2012-10-12 | 2015-10-01 | Alzo International, Inc. | Enhanced water and transfer resistant film forming |
| CN105168023B (en) * | 2015-10-14 | 2018-05-22 | 许龙 | Aqueous foundation cream and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2221045A1 (en) * | 2009-02-20 | 2010-08-25 | Beiersdorf AG | Skin care formulations with an immediate tautening effect |
| US10105297B2 (en) * | 2016-04-01 | 2018-10-23 | L'oreal | Sunscreen compositions and methods for boosting efficacy |
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