CN112294700A - Foundation cream and preparation method thereof - Google Patents

Abstract

The invention belongs to the technical field of cosmetics and preparation thereof, and provides a foundation cream and a preparation method thereof, wherein the foundation cream comprises 14-18 parts by weight of phase A (forming agent), 43-51 parts by weight of phase B (film forming agent, hydrogenated C6-20 polyolefin, antioxidant, emollient and conditioner mixture, the hydrogenated C6-20 polyolefin is 3-6 parts by weight, 8-10 parts by weight of phase C (lubricant) and 21-28 parts by weight of phase D (colorant) is 0.2-0.6 part by weight of phase E (preservative), the foundation cream prepared by the invention not only has good makeup effect, high coverage, long-lasting makeup, water and sweat resistance, but also has the effect of being free of floating powder, the contents of heavy metals of mercury, lead, arsenic and cadmium all reach the standard, and has no contamination of microorganisms such as heat-resistant Escherichia coli, Staphylococcus aureus and Pseudomonas aeruginosa.

Description

Foundation cream and preparation method thereof

Technical Field

The invention belongs to the technical field of cosmetics and preparation thereof, and particularly relates to foundation cream and a preparation method thereof.

Background

Foundation make-up is the basis of makeup, and powder foundation make-up is the most common, and the application on face appears gentle and natural, is the best choice of daily makeup. When makeup is carried out, people always forget to make a layer of foundation make-up for themselves. Therefore, the foundation is a foundation for women's makeup and is better than the foundation in a certain degree, and the care of the skin is more delicate and gentle.

Foundations generally include three use effects: moisture retention and water locking, light weight, smoothness and perfect defect covering. However, the traditional foundation has the advantages that the mineral components and the chemical synthetic raw materials cause unnecessary damage to the skin and even cause allergy. Especially people with special skin, such as people with allergic constitution. With the development of science and technology, natural, safe and environment-friendly products are sought in europe, america and taiwan as early as 2010 so as to meet the requirements of consumers on safe products and make the market prospect of cosmetics wider.

Disclosure of Invention

In order to solve the problems, the invention provides a safe foundation cream with low heavy metal content and no microbial pollution so as to meet the requirements of people on the safety performance of products, and the concrete contents of the invention are as follows:

the first object of the present invention is to provide a foundation cream, which has the following technical points: the foundation cream is prepared by mixing 14-18 parts by weight of phase A, 43-51 parts by weight of phase B, 8-10 parts by weight of phase C and 21-28 parts by weight of phase D, and 0.2-0.6 part by weight of phase E;

the phase A is a forming agent;

the phase B is a mixture of a film forming agent, hydrogenated C6-20 polyolefin, an antioxidant, an emollient and a conditioner, and the weight part of the hydrogenated C6-20 polyolefin is 3-6;

the phase C is a lubricant;

the phase D is a colorant;

the phase E is a preservative.

In some embodiments of the present invention, the film forming agent in the formulation system of the foundation cream is polyvinylpyrrolidone.

In some embodiments of the present invention, the forming agent in the formulation system of the foundation cream is a mixture of ozokerite, synthetic wax, microcrystalline wax, beeswax, and polyethylene.

In some embodiments of the present invention, the preservative in the foundation cream formulation is a mixture of ethylhexyl glycerin and phenoxyethanol.

In some embodiments of the present invention, the antioxidant in the foundation cream formulation system is tocopherol.

In some embodiments of the present invention, the emollient is a mixture of sodium hyaluronate, octyldodecanol, tridecyl alcohol trimellitate, macadamia nut seed oil, phytosterol isostearate, and jojoba fat.

In some embodiments of the present invention, the lubricant in the foundation cream formulation is a mixture of boron nitride, silica, and polymethyl methacrylate.

In some embodiments of the present invention, the conditioner in the formulation system of the foundation cream is a mixture of Rosa canina fruit oil, glycerol tri (ethyl hexanoate), hydrogenated shea butter, and Olea europaea fruit oil.

In some embodiments of the present invention, the colorant in the foundation cream is a mixture of titanium dioxide, black iron oxide, yellow iron oxide, and red iron oxide.

The second object of the present invention is to provide a foundation cream preparation method comprising the steps of:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 60-70 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenization condition, and homogenizing for 5-10 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring and heating to 80-85 ℃, preserving heat for 10-40 minutes, and cooling to 60-70 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.

Compared with the prior art, the invention has the beneficial effects that:

the foundation cream is prepared by mixing 14-18 parts by weight of phase A (forming agent), 43-51 parts by weight of phase B (film forming agent, hydrogenated C6-20 polyolefin, antioxidant, emollient and conditioner mixture, wherein the hydrogenated C6-20 polyolefin is 3-6 parts by weight, 8-10 parts by weight of phase C (lubricant) and 21-28 parts by weight of phase D (colorant) is 0.2-0.6 part by weight of phase E (preservative).

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below so that those skilled in the art can better understand the advantages and features of the present invention, and thus the scope of the present invention will be more clearly defined. The embodiments described herein are only a few embodiments of the present invention, rather than all embodiments, and all other embodiments that can be derived by one of ordinary skill in the art without inventive faculty based on the embodiments described herein are intended to fall within the scope of the present invention.

Example 1

A foundation cream is prepared by mixing 16 weight parts of phase A, 49.9 weight parts of phase B, 9 weight parts of phase C and 24.5 weight parts of phase D, and 0.6 weight parts of phase E;

the phase A is polyvinylpyrrolidone;

the phase B is a mixture of a film forming agent (ozokerite: synthetic wax: microcrystalline wax: beeswax: polyethylene: 1:1:1:1), hydrogenated C6-20 polyolefin, tocopherol, an emollient (sodium hyaluronate: octyldodecanol: tridecanol trimellitate: macadamia nut seed oil: phytosterol isostearate: jojoba fat: 1:1:1) and a conditioner (Rosa canina oil: glycerol tri (ethyl hexanoate) ester: hydrogenated shea butter: olive oil: 1:1:1:1), wherein the weight part of the hydrogenated C6-20 polyolefin is 4;

the phase C is a lubricant (boron nitride: silica: polymethyl methacrylate: 1:1: 1);

the phase D is a colorant (titanium dioxide: black iron oxide: yellow iron oxide: red iron oxide: 1:1: 1);

the phase E is preservative (ethylhexyl glycerol: and phenoxyethanol ═ 1: 1).

According to the above formulation, the foundation cream of the present application is prepared by a method comprising the steps of:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 65 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenization condition, and homogenizing for 8 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring and heating to 82 ℃, preserving heat for 30 minutes, and cooling to 65 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.

The foundation cream prepared by the embodiment is a paste, has the same color and luster with the sample plate, is tasteless, and has no obvious difference from the original cream before the test after being treated at the temperature of 45 +/-1) DEG C for 24 hours, and has no obvious difference from the original cream before the test after being treated at the temperature of minus 5 to minus 10℃ for 24 hours.

Example 2

A foundation cream is prepared by mixing 18 parts by weight of phase A, 51 parts by weight of phase B, 9.8 parts by weight of phase C and 21 parts by weight of phase D, and 0.2 part by weight of phase E;

the phase A is polyvinylpyrrolidone;

the phase B is a mixture of a film forming agent (ozokerite: synthetic wax: microcrystalline wax: beeswax: polyethylene: 1:2:0.5:1:1), hydrogenated C6-20 polyolefin, tocopherol, an emollient (sodium hyaluronate: octyldodecanol: tridecanol trimellitate: macadamia nut seed oil: phytosterol isostearate: jojoba fat: 2:0.5:0.5:1:1:1) and a conditioner (Rosa canina oil: glycerol tri (ethyl hexanoate) ester: hydrogenated shea butter: olive fruit oil: 2:0.5:0.5:1), wherein the weight part of the hydrogenated C6-20 polyolefin is 3;

the phase C is a lubricant (boron nitride: silica: polymethyl methacrylate: 2:1: 1);

the phase D is a colorant (titanium dioxide: black iron oxide: yellow iron oxide: red iron oxide: 2:1:1: 1);

the phase E is preservative (ethylhexyl glycerol: and phenoxyethanol ═ 2: 1).

According to the above formulation, the foundation cream of the present application is prepared by a method comprising the steps of:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 60 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenizing condition, and homogenizing for 10 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring and heating to 80 ℃, preserving heat for 40 minutes, and cooling to 60 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.

The foundation cream prepared by the embodiment is a paste, has the same color and luster with the sample plate, is tasteless, and has no obvious difference from the original cream before the test after being treated at the temperature of 45 +/-1) DEG C for 24 hours, and has no obvious difference from the original cream before the test after being treated at the temperature of minus 5 to minus 10℃ for 24 hours.

Example 3

A foundation cream is prepared by mixing 18 weight parts of phase A, 43.4 weight parts of phase B, 10 weight parts of phase C and 28 weight parts of phase D, and 0.6 weight parts of phase E;

the phase A is polyvinylpyrrolidone;

the phase B is a mixture of a film forming agent (ozokerite: synthetic wax: microcrystalline wax: beeswax: polyethylene: 1:1:1:2), hydrogenated C6-20 polyolefin, tocopherol, an emollient (sodium hyaluronate: octyldodecanol: tridecanol trimellitate: macadamia nut seed oil: phytosterol isostearate: jojoba fat: 1:2:1:1: 1) and a conditioner (Rosa canina oil: glycerol tri (ethyl hexanoate) ester: hydrogenated shea butter: olive oil: 1:2:1:1), wherein the weight part of the hydrogenated C6-20 polyolefin is 6;

the phase C is a lubricant (boron nitride: silica: polymethyl methacrylate: 1:2: 1);

the phase D is a colorant (titanium dioxide: black iron oxide: yellow iron oxide: red iron oxide: 1:1: 2);

the phase E is preservative (ethylhexyl glycerol: and phenoxyethanol ═ 1: 2).

According to the above formulation, the foundation cream of the present application is prepared by a method comprising the steps of:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 70 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenization condition, and homogenizing for 5 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring and heating to 85 ℃, preserving heat for 10 minutes, and cooling to 70 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.

The foundation cream prepared by the embodiment is a paste, has the same color and luster with the sample plate, is tasteless, and has no obvious difference from the original cream before the test after being treated at the temperature of 45 +/-1) DEG C for 24 hours, and has no obvious difference from the original cream before the test after being treated at the temperature of minus 5 to minus 10℃ for 24 hours.

Example 4

A foundation cream is prepared by mixing 15 weight parts of phase A, 50 weight parts of phase B, 9.5 weight parts of phase C and 25 weight parts of phase D, and 0.5 weight parts of phase E;

the phase A is polyvinylpyrrolidone;

the phase B is a mixture of a film forming agent (ozokerite: synthetic wax: microcrystalline wax: beeswax: polyethylene: 1:1:2:1), hydrogenated C6-20 polyolefin, tocopherol, an emollient (sodium hyaluronate: octyldodecanol: tridecanol trimellitate: macadamia nut seed oil: phytosterol isostearate: jojoba fat: 2:1:1:1:1:1) and a conditioner (Rosa canina oil: glycerol tri (ethyl hexanoate) ester: hydrogenated shea butter: olive oil: 1:1:2:1), wherein the weight part of the hydrogenated C6-20 polyolefin is 5;

the phase C is a lubricant (boron nitride: silica: polymethyl methacrylate: 1: 2);

the phase D is a colorant (titanium dioxide: black iron oxide: yellow iron oxide: red iron oxide: 1:2: 1);

the phase E is preservative (ethylhexyl glycerol: and phenoxyethanol ═ 3: 1).

According to the above formulation, the foundation cream of the present application is prepared by a method comprising the steps of:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 65 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenization condition, and homogenizing for 7 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring, heating to 82.5 ℃, preserving heat for 30 minutes, and cooling to 65 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.

The foundation cream prepared by the embodiment is a paste, has the same color and luster with the sample plate, is tasteless, and has no obvious difference from the original cream before the test after being treated at the temperature of 45 +/-1) DEG C for 24 hours, and has no obvious difference from the original cream before the test after being treated at the temperature of minus 5 to minus 10℃ for 24 hours.

Test examples

The foundation creams prepared in examples 1 to 4 were submitted to microbiological and physicochemical tests according to technical standards for cosmetic safety (2015), and the results are shown in tables 1 and 2:

TABLE 1 results of microbial detection

Detecting items	Unit of	The result of the detection	Limit value
				Total number of colonies	CFU/g	＜10	≤1000
Total number of mold and yeast	CFU/g	＜10	≤100
				Heat-resistant coliform bacteria colony	/g	Not detected out	Cannot be detected
Staphylococcus aureus	/g	Not detected out	Cannot be detected
				Pseudomonas aeruginosa	/g	Not detected out	Cannot be detected

TABLE 2 results of physical and chemical tests

The makeup efficiency of the foundation creams prepared in examples 1 to 4 was tested, the prepared foundation creams were washed under tap water to observe the waterproof and antiperspirant effects, the prepared foundation creams were subjected to a makeup duration test, the same amount of foundation cream was applied to human faces with mixed oil skin texture, and a persistence test was performed, and the specific results are shown in table 3:

TABLE 3 cosmetic results for foundation cream

	Powder material	Water-proof effect	Covering effect	Hand-held makeupTime of day	Whether or not to float powder
						Example 1	Fineness of fineness	Good taste	Good taste	＞8h	Whether or not
Example 2	Fineness of fineness	Good taste	Good taste	＞8h	Whether or not
						Example 3	Fineness of fineness	Good taste	Good taste	＞8h	Whether or not
Example 4	Fineness of fineness	Good taste	Good taste	＞8h	Whether or not

The makeup cream prepared by the embodiment has a matte surface, no oil light and good covering power when being applied to the surface of skin, and the makeup surface is still clean and has no dark color after the makeup cream is kept for 6 hours and the nose is slightly oily; after the makeup is kept for 8 hours, the nose is slightly oily and dark, and the covering power is still unchanged; after the makeup is kept for 10 hours, the T area becomes oily and bright, the color is dark, and the covering power is still unchanged. Therefore, the foundation cream prepared by the invention is suitable for being applied to the foundation made by swimming, diving, photography in a studio, stage deduction and theater photography.

Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (10)

1. A foundation cream characterized by: the foundation cream is prepared by mixing 14-18 parts by weight of phase A, 43-51 parts by weight of phase B, 8-10 parts by weight of phase C and 21-28 parts by weight of phase D, and 0.2-0.6 part by weight of phase E;

the phase A is a forming agent;

the phase B is a mixture of a film forming agent, hydrogenated C6-20 polyolefin, an antioxidant, an emollient and a conditioner, and the weight part of the hydrogenated C6-20 polyolefin is 3-6;

the phase C is a lubricant;

the phase D is a colorant;

the phase E is a preservative.

2. Foundation cream according to claim 1, characterized in that: the film forming agent is polyvinylpyrrolidone.

3. Foundation cream according to claim 1, characterized in that: the forming agent is a mixture of ozokerite, synthetic wax, microcrystalline wax, beeswax and polyethylene.

4. Foundation cream according to claim 1, characterized in that: the preservative is a mixture of ethylhexyl glycerol and phenoxyethanol.

5. Foundation cream according to claim 1, characterized in that: the antioxidant is tocopherol.

6. Foundation cream according to claim 1, characterized in that: the emollient is a mixture of sodium hyaluronate, octyldodecanol, tridecanol trimellitate, macadamia nut seed oil, phytosterol isostearate and jojoba fat.

7. Foundation cream according to claim 1, characterized in that: the lubricant is a mixture of boron nitride, silica and polymethyl methacrylate.

8. Foundation cream according to claim 1, characterized in that: the conditioner is a mixture of Rosa canina fruit oil, glyceryl tri (ethyl hexanoate), hydrogenated shea butter and olive fruit oil.

9. Foundation cream according to claim 1, characterized in that: the colorant is a mixture of titanium dioxide, black iron oxide, yellow iron oxide and red iron oxide.

10. A foundation cream according to any one of claims 1 to 9, characterized in that: the preparation method of the foundation cream comprises the following steps:

the method comprises the following steps: sequentially adding the raw materials in the phase A into a water phase pot, stirring and heating to 60-70 ℃, stirring until the powder is fully dissolved and transparent, and cooling to room temperature for later use;

step two: sequentially adding the phase B oil phase raw materials into an emulsifying pot, and fully stirring or homogenizing uniformly; slowly pumping the A-phase pot body into an emulsifying pot under the homogenization condition, and homogenizing for 5-10 minutes;

step three: sequentially adding the C-phase raw materials into an emulsifying pot, stirring and heating to 80-85 ℃, preserving heat for 10-40 minutes, and cooling to 60-70 ℃;

step four: grinding the D-phase raw material, adding the D-phase raw material into an emulsifying pot, adding the E-phase raw material, homogenizing again, taking out of the pot, detecting and filling.