CN110664634A - Matte water-soluble coloring modeling hair wax and preparation method thereof - Google Patents
Matte water-soluble coloring modeling hair wax and preparation method thereof Download PDFInfo
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- CN110664634A CN110664634A CN201911035741.2A CN201911035741A CN110664634A CN 110664634 A CN110664634 A CN 110664634A CN 201911035741 A CN201911035741 A CN 201911035741A CN 110664634 A CN110664634 A CN 110664634A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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Abstract
A matte water-soluble coloring modeling hair wax and a preparation method thereof relate to the technical field of hair wax, and the hair wax comprises the following components: an emulsifier; a co-emulsifier; an emollient; glycerol; a colorant; a suspending agent; a film-forming agent; a pH adjusting agent; a preservative; and (3) water. The hair wax prepared by the invention contains the coloring agent, can generate a disposable dyeing effect when being used on hair, can not damage the hair under the protection of a polymer film in the hair wax, can not generate phenomena of fading and the like under normal conditions, and in addition, the interaction of various components in the hair wax can close the opened hair scales, so that the problem that the coloring agent in the hair wax and alkaline conditions damage the hair quality is solved, the hair wax has a good shaping effect, has a clear hair layer stereoscopic impression after shaping, is natural and non-greasy, has a matte texture, has a fragrant and natural smell, and can play a role in moistening and improving the hair quality. The invention also provides a preparation method of the hair wax, which is simple and easy to operate and is suitable for batch industrial production.
Description
The technical field is as follows:
the invention relates to the field of hair care, in particular to a water-soluble coloring and styling wax with matte texture and a preparation method thereof.
Background art:
the hair wax is a semi-solid paste-shaped hair styling product of oil, grease and wax, and is used for fixing the hair style by filling gaps among the hair, so that the hair keeps a natural style which is mutually attracted and not hardened. Is a hair setting agent with 'setting hair and no hardening'. According to the raw material source and the product appearance, the hair wax is divided into 3 kinds of plant hair wax, mineral hair wax and water-soluble hair wax. The vegetable hair wax is a hair care product prepared by taking vegetable oil as a main raw material and adding beeswax, ozokerite, an antioxidant, essence and the like, is a semitransparent paste, is rich in luster, and has proper hardness and viscosity. The mineral hair wax is a hair cosmetic prepared by taking mineral oil such as vaseline, white oil and paraffin as main raw materials and adding a proper amount of raw materials such as pigment, essence and the like. The water-soluble hair wax is also called transparent hair wax, is a transparent paste for hair care and shaping, can make the hair have wet and percolated feeling although the water-soluble hair wax does not have greasy feeling when being used, and the solvent is water, so that the shaping effect of the hair wax is reduced after the water is volatilized, the retention force is not durable, and the hair wax needs to be matched with shaping spray to keep the shaping effect. In addition, the aqueous hair wax belongs to one of alkaline products, can open hair scales on the surface layer of the scalp, can lead the hair scales to be incapable of being closed by frequently using the hair wax, thereby causing the phenomena of dry hair, frizziness and the like, and the hair can have greasy feeling in the using process of the hair wax, thus giving people a refreshing visual sensation.
The invention content is as follows:
the invention aims to overcome the defects of the prior art and provide the water-soluble coloring modeling hair wax with matte texture and the preparation method thereof.
The technical scheme adopted by the invention is as follows: a matte water-soluble coloring modeling hair wax comprises the following components in percentage by mass: emulsifier: 3.5% -15%; auxiliary emulsifier: 1% -5%; and (3) an emollient: 2% -16%; glycerol: 0.5% -5%; colorant: 5.51% -18.1%; suspending agent: 0.5% -3%; film-forming agent: 0.1% -0.3%; pH regulators: 0.05% -0.4%; preservative: 0.5% -2.2%; water: and (4) the balance.
Preferably, the emulsifier comprises the following components in percentage by mass: glycerol stearate: 2% -8%; PEG-100 stearate: 1% -5%; laureth-25: 0.5 to 2 percent.
Preferably, the co-emulsifier is cetearyl alcohol.
Preferably, the emollient comprises the following components in percentage by mass: beeswax: 1% -10%; isododecane: 1 to 6 percent.
Preferably, the colorant comprises the following components in percentage by mass: CI 77019: 5% -15%; CI 77891: 0.5% -2.6%; CI 77266: 0.01 to 0.5 percent.
Preferably, the suspending agent is an acrylic acid (ester)/steareth-20 methacrylate copolymer; the film forming agent is polyvinylpyrrolidone.
Preferably, the preservative comprises the following components in percentage by mass: phenoxyethanol: 0.2% -1%; methyl hydroxybenzoate: 0.1% -0.5%; propyl hydroxybenzoate: 0.1% -0.4%; chlorphenesin: 0.1 to 0.3 percent.
Preferably, the hair wax also contains 0% -2.5% of aromatic.
The invention also aims to provide a preparation method of the water-soluble coloring modeling hair wax with the matte texture, which is simple and easy to operate, can be used for batch industrial production and has no dependence on equipment, and the preparation method comprises the following steps:
the method comprises the following steps: adding the emulsifier, the co-emulsifier, the emollient and the preservative with the formula amount of 0.2-0.9% by mass into an emulsifying pot, stirring and mixing, heating to 80-85 ℃, and keeping the temperature for 20-60 min; adding water, film forming agent, glycerol, suspending agent and preservative with the mass percent of 0.1-0.3% into a stirring pot, stirring and mixing, heating to the temperature of 80-85 ℃, and preserving heat for 20-60 min;
step two: pumping the mixture in the stirring pot into an emulsifying pot, homogenizing for 3-5min, adding a pH regulator into the emulsifying pot, continuously homogenizing and stirring uniformly, adding a formula amount of colorant into the emulsifying pot, stirring uniformly, and degassing in vacuum;
step three: cooling the temperature in an emulsifying pot to 48-50 ℃, adding 0.2-1% by mass of preservative and daily essence according to the formula amount into the emulsifying pot, uniformly stirring, taking out the mixture from the emulsifying pot, and screening the mixture by a 80-mesh filter screen after the mixture is detected to be qualified;
step four: and after the detection is qualified, filling and packaging.
The formulation concept of the invention is as follows: in order to reduce the wet percolation feeling of the aqueous hair wax when being coated on the hair, the inventor adds a volatile substance isododecane into the hair wax, utilizes the characteristic that the isododecane carries partial water when volatilizing, solves the wet percolation feeling of the aqueous hair wax when being coated on the hair, simultaneously improves the penetration and moisture-keeping effects of an emollient and a moisture-keeping component in the hair wax, but the addition of the isododecane causes the aqueous hair wax to be incapable of being uniformly coated on the hair because of fast volatilization when being coated, thereby causing the phenomenon of non-uniformity when the hair wax is coated and used, and in order to solve the problem, the inventor tries to add a suspending agent acrylic acid (ester)/steareth-20 methacrylate copolymer and select polyvinylpyrrolidone with good film forming effect into the hair wax, and can excellently improve the film forming property of the hair wax after adding the acrylic acid (ester)/steareth-20 methacrylate copolymer and the polyvinylpyrrolidone, and unexpectedly to the inventors: the two components are added, so that the durability and the toughness of the hair wax are obviously improved, and meanwhile, the flexibility of the hair is also improved through long-term use tests.
The invention has the beneficial effects that: the hair wax prepared by the invention contains the coloring agent, can generate a disposable dyeing effect when being used on hair, can not damage the hair under the protection of a polymer film in the hair wax, can not generate phenomena of fading and the like under normal conditions, and in addition, the interaction of various components in the hair wax can close the opened hair scales, so that the problem that the coloring agent in the hair wax and alkaline conditions damage the hair quality is solved, the hair wax has good shaping effect, has clear hair layer stereoscopic impression after shaping, is natural, non-greasy, non-damp and percolated, has matte texture and fragrant and natural smell, and can play a role in moistening and improving the hair quality.
The specific implementation mode is as follows:
the invention will be further illustrated with reference to specific examples:
examples one to three were prepared using the hair wax formulations in the following table, specifically:
the hair wax prepared in the first to third examples was used by the following method: after hair is cleaned, a proper amount of hair wax is uniformly rubbed in a circle on the palm center, and then the hair wax is lightly smeared from the root of the hair to the top in a lifting and pulling mode by using fingers until the hair wax is uniform.
The hair wax in the first to third embodiments is prepared by the following preparation method, specifically: the method comprises the following steps:
the method comprises the following steps: adding the emulsifier, the co-emulsifier, the emollient and the preservative with the formula amount of 0.2-0.9% by mass into an emulsifying pot, stirring and mixing, heating to 80-85 ℃, and keeping the temperature for 20-60 min; adding water, film forming agent, glycerol, suspending agent and preservative with the mass percent of 0.1-0.3% into a stirring pot, stirring and mixing, heating to the temperature of 80-85 ℃, and preserving heat for 20-60 min;
step two: pumping the mixture in the stirring pot into an emulsifying pot, homogenizing for 3-5min, adding a pH regulator into the emulsifying pot, continuously homogenizing and stirring uniformly, adding a formula amount of colorant into the emulsifying pot, stirring uniformly, and degassing in vacuum;
step three: cooling the temperature in an emulsifying pot to 48-50 ℃, adding 0.2-1% by mass of preservative and daily essence according to the formula amount into the emulsifying pot, uniformly stirring, taking out the mixture from the emulsifying pot, and screening the mixture by a 80-mesh filter screen after the mixture is detected to be qualified;
step four: and after the detection is qualified, filling and packaging.
Comparative examples one to three were prepared using the formulations in the following table, with the specific formulations given in the following table:
the hair wax in comparative examples one to three was prepared by the preparation method in examples one to three of the present invention.
Use effect experiment:
(1) sensory properties:
the hair wax prepared in example one to example three was observed to be a creamy homogeneous liquid having a creamy gray color, free of foreign substances, and having a light fragrance.
(2) The sanitation index is as follows:
the hygiene indexes of the hair wax prepared in the first to third examples are detected, and the specific tested hygiene indexes are shown in the following table:
| detecting items | Basis of inspection method | Restriction (mg/kg) | The result of the detection |
| Mercury | Safety technical Specification for cosmetics 2015 edition | ≤1 | Not detected out |
| Lead (II) | Safety technical Specification for cosmetics 2015 edition | ≤10 | Not detected out |
| Arsenic (As) | Safety technical Specification for cosmetics 2015 edition | ≤2 | Not detected out |
| Partition | Safety technical Specification for cosmetics 2015 edition | ≤5 | Not detected out |
(3) Microorganism indexes are as follows:
the microbiological indicators of the hair wax prepared in the first to third examples were measured, and the specific microbiological indicators tested are shown in the following table:
(4) and (3) testing the use effect:
the test method comprises the following steps:
140 volunteers were selected and divided into seven groups on average, wherein the first group used the hair wax of example one, the second group used the hair wax of example two, the third group used the hair wax of example three, the fourth group used the hair wax of comparative example one, the fifth group used the hair wax of comparative example two, the sixth group used the hair wax of comparative example three, the seventh group used a commercially available common hair wax, the seven groups of volunteers washed their hair every morning and then evenly applied the hair wax, and each group of volunteers used the corresponding hair wax for 30 days, and the effect of using the hair wax was counted. The average of the statistical results is shown in the table below. Wherein the score of 0 is the worst and the score of 5 is the best effect. The sensory effect refers to the whole sensory effect of whether the product is wet or percolated, whether the product is greasy or not, whether the product is unevenly smeared or not and the like.
As can be seen from the above table, the hair waxes prepared in examples one to three of the present invention have excellent setting effects, hair care effects and pleasant sensory effects, compared to the hair waxes in comparative examples one to three and a commercially available common hair wax. It can be seen that there is a synergistic effect between the acrylic/steareth-20 methacrylate copolymer, isododecane and polyvinylpyrrolidone, and that absent any of these components, the styling, hair and sensory effects are poor.
In addition, the hair wax can close the opened hair scales due to interaction of various components in the hair wax, so that the problem that the hair quality is damaged by the coloring agent in the hair wax and alkaline conditions is solved, the hair wax has good shaping effect, has clear stereoscopic impression of a hair layer, is natural and not greasy, has matte texture and fragrant and natural smell, and can play a role in moistening and improving the hair quality.
Various other changes and modifications to the above embodiments and concepts will become apparent to those skilled in the art, and all such changes and modifications are intended to be included within the scope of the present invention as defined in the appended claims.
Claims (9)
1. A water-soluble coloring modeling hair wax with matte texture is characterized in that: the hair wax comprises the following components in percentage by mass: emulsifier: 3.5% -15%; auxiliary emulsifier: 1% -5%; and (3) an emollient: 2% -16%; glycerol: 0.5% -5%; colorant: 5.51% -18.1%; suspending agent: 0.5% -3%; film-forming agent: 0.1% -0.3%; pH regulators: 0.05% -0.4%; preservative: 0.5% -2.2%; water: and (4) the balance.
2. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the emulsifier comprises the following components in percentage by mass: glycerol stearate: 2% -8%; PEG-100 stearate: 1% -5%; laureth-25: 0.5 to 2 percent.
3. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the auxiliary emulsifier is cetearyl alcohol.
4. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the emollient comprises the following components in percentage by mass: beeswax: 1% -10%; isododecane: 1 to 6 percent.
5. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the colorant comprises the following components in percentage by mass: CI 77019: 5% -15%; CI 77891: 0.5% -2.6%; CI 77266: 0.01 to 0.5 percent.
6. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the suspending agent is acrylic acid (ester)/stearyl alcohol polyether-20 methacrylate copolymer; the film forming agent is polyvinylpyrrolidone.
7. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the preservative comprises the following components in percentage by mass: phenoxyethanol: 0.2% -1%; methyl hydroxybenzoate: 0.1% -0.5%; propyl hydroxybenzoate: 0.1% -0.4%; chlorphenesin: 0.1 to 0.3 percent.
8. A matte-feel, water-soluble color-styling wax according to claim 1, characterized in that: the hair wax also contains 0% -2.5% of aromatic.
9. A preparation method of water-soluble coloring modeling hair wax with matte texture is characterized in that: the method comprises the following steps:
the method comprises the following steps: adding the emulsifier, the co-emulsifier, the emollient and the preservative with the formula amount of 0.2-0.9% by mass into an emulsifying pot, stirring and mixing, heating to 80-85 ℃, and keeping the temperature for 20-60 min; adding water, film forming agent, glycerol, suspending agent and preservative with the mass percent of 0.1-0.3% into a stirring pot, stirring and mixing, heating to the temperature of 80-85 ℃, and preserving heat for 20-60 min;
step two: pumping the mixture in the stirring pot into an emulsifying pot, homogenizing for 3-5min, adding a pH regulator into the emulsifying pot, continuously homogenizing and stirring uniformly, adding a formula amount of colorant into the emulsifying pot, stirring uniformly, and degassing in vacuum;
step three: cooling the temperature in an emulsifying pot to 48-50 ℃, adding 0.2-1% by mass of preservative and daily essence according to the formula amount into the emulsifying pot, uniformly stirring, taking out the mixture from the emulsifying pot, and screening the mixture by a 80-mesh filter screen after the mixture is detected to be qualified;
step four: and after the detection is qualified, filling and packaging.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911035741.2A CN110664634A (en) | 2019-10-29 | 2019-10-29 | Matte water-soluble coloring modeling hair wax and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911035741.2A CN110664634A (en) | 2019-10-29 | 2019-10-29 | Matte water-soluble coloring modeling hair wax and preparation method thereof |
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| CN110664634A true CN110664634A (en) | 2020-01-10 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115317388A (en) * | 2022-09-14 | 2022-11-11 | 广州市柏凡生物科技有限公司 | High-gloss hair styling wax and preparation method thereof |
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2019
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| CN107072897A (en) * | 2015-03-27 | 2017-08-18 | 株式会社漫丹 | Hair grooming Unctuous compositions |
| CN105997555A (en) * | 2016-05-13 | 2016-10-12 | 山西大学 | Dyeing pomade which can be washed out with warm water and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115317388A (en) * | 2022-09-14 | 2022-11-11 | 广州市柏凡生物科技有限公司 | High-gloss hair styling wax and preparation method thereof |
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