CN114224761A

CN114224761A - Color cosmetic composition, preparation method and application

Info

Publication number: CN114224761A
Application number: CN202111594895.2A
Authority: CN
Inventors: 姚增辉; 楼彪
Original assignee: Jiaoshi Daily Chemical Hangzhou Co ltd
Current assignee: Jiaoshi Daily Chemical Hangzhou Co ltd
Priority date: 2021-12-23
Filing date: 2021-12-23
Publication date: 2022-03-25
Anticipated expiration: 2041-12-23
Also published as: CN114224761B

Abstract

The application relates to the technical field of cosmetics, and particularly discloses a color cosmetic composition, a preparation method and application. The color cosmetic composition is prepared from the following raw materials in percentage by weight: 30-35% of pearling agent, 24-30% of octyldodecanol, 7-10% of diisostearyl malate, 7-10% of hydrogenated polyisobutene, 4-8% of caprylic/capric triglyceride, 4-7% of emollient I, 5-10% of emollient II, 2-5% of skin conditioner I, 1.2-2.5% of skin conditioner II and 0.1-0.2% of preservative. The makeup composition has the advantages of good moistening performance, no drying, difficult makeup removal after makeup, good ductility, no halation, easy makeup, good high brightness and good makeup effect.

Description

Color cosmetic composition, preparation method and application

Technical Field

The application relates to the technical field of cosmetics, in particular to a color cosmetic composition and a preparation method and application thereof.

Background

The cosmetic is a chemical industrial product or a fine chemical product which is applied, sprayed or the like to any part of the surface of a human body to achieve the purposes of cleaning, maintaining, beautifying, modifying and changing the appearance and keeping a good state. The cosmetics can be divided into skin care products and color cosmetics according to functions, the skin care products have the functions of beautifying and face, can enhance the elasticity and vitality of skin, and can make people young and beautiful after being frequently used; the color cosmetics are mainly applied to the face, nails and other parts, and utilize the change of color to give skin color, trim skin color or strengthen the shadow of eyes and nose parts to enhance the stereoscopic impression and make the product more attractive.

With the continuous progress of social economy and the abundance of material life, the existing color cosmetic products on the market are various in types, comprise foundation make-up, loose powder, face powder, blush, highlight, eye shadow and the like, and can meet different requirements of people. The makeup is a normal state, the cosmetics enhance the self-confidence of people, improve the beautiful image of people and promote the civilization of society.

However, the inventor finds that the existing makeup products on the market have poor moisture degree, make-up is easy to remove after 2 hours, and the skin becomes dry and rough after frequent use.

Disclosure of Invention

In order to improve the moistening degree and the brightness of a color cosmetic product, the application provides a color cosmetic composition, a preparation method and application.

In a first aspect, the present application provides a color cosmetic composition, using the following technical scheme:

the color cosmetic composition is prepared from the following raw materials in percentage by weight:

30-35% of pearling agent, 24-30% of octyldodecanol, 7-10% of diisostearyl malate, 7-10% of hydrogenated polyisobutene, 4-8% of caprylic/capric triglyceride, 4-7% of emollient I, 5-10% of emollient II, 2-5% of skin conditioner I, 1.2-2.5% of skin conditioner II and 0.1-0.2% of preservative.

Octyl dodecanol has high moistening effect and no irritation; the diisostearyl malate is mainly used as a softening agent and also has a good moistening effect; the hydrogenated polyisobutene has moistening and moisturizing effects; caprylic/capric triglyceride has lubricating and skin softening effects. According to the application, octyl dodecanol, diisostearyl malate, hydrogenated polyisobutene and caprylic/capric triglyceride are added into a system according to a formula ratio, on one hand, the four components are mutually matched, so that the four components are easily absorbed by skin, and the intangible water loss can be prevented, so that the skin can be well moistened, and the makeup removal is reduced; on the other hand, the mutual matching of octyl dodecanol, diisostearyl malate, hydrogenated polyisobutene, caprylic/capric triglyceride and the pearling agent has good dispersion effect on the pearling agent, and the product has high brightness when being used in a bright formula. In addition, the color cosmetic composition prepared according to the formula has good ductility, can reduce halation, and can beautify the makeup effect when being applied to color cosmetic products.

Preferably, the mass ratio of the octyldodecanol, diisostearyl malate, hydrogenated polyisobutene and caprylic/capric triglyceride is (25-27): (9-10): (9-10): (4-6). More preferably, the mass ratio of the octyldodecanol, diisostearyl malate, hydrogenated polyisobutene, and caprylic/capric triglyceride is 26.2:9.17:9.17: 5.67.

Octyl dodecanol, diisostearyl malate, hydrogenated polyisobutene, and caprylic/capric triglyceride are mixed in proportion, so that on one hand, the moisturizing effect and the ductility of the color cosmetic composition can be improved, and on the other hand, the pearlescent agent can be better dispersed, and the high brightness of the product is improved.

Preferably, the emollient I is selected from C12-15 alcohol benzoate, tridecyl alcohol trimellitate and polybutene, and the mass ratio of the C12-15 alcohol benzoate, the tridecyl alcohol trimellitate and the polybutene is (2-4): (1-3): (1-3). Further preferably, the mass ratio of the C12-15 alcohol benzoate, the tridecyl alcohol trimellitate and the polybutene is 4: 3: 3.

c12-15 alcohol benzoate is used as a softening agent in the system, so that the moistening effect of the composition can be improved; tridecyl alcohol trimellitate is used as emollient ester in the system, and can provide soft skin feel; the polybutene is used as a thickening agent in the system, and the viscosity of the system can be regulated and controlled. In the application, the C12-15 alcohol benzoate, the tridecyl alcohol trimellitate and the polybutene are mixed according to the formula proportion, so that on one hand, the skin can be moistened, and the moistening performance of the composition is improved, on the other hand, the product can be endowed with high refractive index, the brightness of the product is improved, and the composition is more suitable for bright products. When the mass ratio of C12-15 alcohol benzoate, tridecyl alcohol trimellitate and polybutene is 4: 3: 3, the viscosity of the composition can be adjusted, the refreshing feeling of the product can be improved, and the comfortable but not greasy skin feeling of the product can be given.

Preferably, the emollient ii is selected from ethylhexyl palmitate and isononyl isononanoate in amounts of 4% to 7.5% and 1% to 2.5% respectively of the total amount of the make-up composition. Further preferably, the ethylhexyl palmitate accounts for 5% of the total mass of the color cosmetic composition, and the isononyl isononanoate accounts for 2.5% of the total mass of the color cosmetic composition.

Ethylhexyl palmitate and isononyl isononanoate are used as the softening agent in the system, can penetrate into pores and have good moistening effect. In the application, the ethylhexyl palmitate and isononyl isononanoate are added into the system according to the formula proportion, so that the stability of the composition can be enhanced, and the composition is easy to apply and is not easy to be tinged.

Preferably, the pearling agent comprises CI 77019 and CI 77491, and the mass ratio of CI 77019 to CI 77491 is (5-7): (2-3.5). Further preferably, the mass ratio of CI 77019 to CI 77491 is 6.5: 3.5.

The main component of the CI 77019 colorant is mica which has good luster and brightness, and CI 77491, mineral pigments and red colorant belong to mineral pigments which do not cause any damage to skin and can be used with confidence. When CI 77019 and CI 77491 are added into the system according to the formula proportion, a unique brick red composition can be obtained, and the brick red composition has excellent gloss and brightness. The inventor has found through a great deal of experiments and investigations that when the mass ratio of CI 77019 to CI 77491 in the composition is 6.5:3.5, the color obtained by blending is most favored.

Preferably, the skin conditioner i comprises dibutyl ethylhexanoyl glutamide and dibutyl lauroyl glutamide; further preferably, the skin conditioning agent I is dibutyl ethylhexanoyl glutamine and dibutyl lauroyl glutamine, and the dibutyl ethylhexanoyl glutamine and dibutyl lauroyl glutamine account for 1.5% -3.5% and 0.5% -1.5% of the total amount of the color cosmetic composition respectively; most preferably, the dibutyl ethylhexanoyl glutamide and dibutyl lauroyl glutamide are used in an amount of 2.36% and 0.83% respectively based on the total amount of the make-up composition;

the skin conditioner II comprises lime peel oil, crambe abyssinica seed oil and crocus sativus flower extract; preferably, the skin conditioner II is lime peel oil, camelina sativa seed oil and crocus sativus flower extract, the lime peel oil accounts for 0.1-0.4% of the total amount of the color cosmetic composition, the camelina sativa seed oil accounts for 0.8-1.3% of the total amount of the color cosmetic composition, and the crocus sativus flower extract accounts for 0.4-0.8% of the total amount of the color cosmetic composition; preferably, the lime peel oil accounts for 0.2% of the total amount of the make-up composition, the crambe abyssinica seed oil accounts for 1% of the total amount of the make-up composition, and the crocus sativus flower extract accounts for 0.5% of the total amount of the make-up composition.

The dibutyl ethylhexanoyl glutamine and dibutyl lauroyl glutamine are added into the system according to the formula proportion, so that the moisture loss of the skin can be slowed down, and the skin-moistening cosmetic feeling of the composition is comfortable and the acne is not blocked. The Citrus aurantium pericarp extract contains multiple volatile oil components, and has effects of keeping moisture and water, sterilizing and removing toxic substance; the two sections of deep sea mustard oil are rich in oil nutrient components, and can enable the skin to be balanced and moisturized and keep healthy; the crocus sativus flower extract has effects of promoting blood circulation, resisting inflammation, resisting oxidation, etc., and contains natural pigments such as safflower yellow and safflower red, etc., and is safe and edible, and can modify dark skin. The sour orange peel extract, the deep sea two-section mustard seed oil and the crocus sativus flower extract are matched with each other according to the formula proportion, so that the deep moisture retention and water locking effects can be achieved, and the skin can be nourished.

In the application, the skin conditioner I and the skin conditioner II are matched with each other according to the formula proportion, so that on one hand, the moisture can be preserved, the water can be kept, the skin can be moistened, the makeup is natural and is not stuck, on the other hand, various nutrient components required by the skin can be deeply supplemented, the blood circulation of the skin is improved, the metabolism of the skin is promoted, the skin is prevented from being reddened, pruritus or seborrheic dermatitis and the like, and the skin is nourished.

Preferably, the color cosmetic composition further comprises disteardimonium hectorite and silica, which comprise from 0.2% to 0.5% and from 0.5% to 2%, respectively, of the color cosmetic composition.

The disteardimonium hectorite and the silica are used as an abrasive or a skin feel regulator of a system, can regulate the texture of the system, endow the product with good ductility and skin feel, make the cosmetic feel natural, conformable and durable, can better disperse CI 77019 and CI 77491, and make the composition more homogeneous and stable and have higher glossiness.

Preferably, the preservative is selected from phenoxyethanol and caprylyl glycol, and the weight ratio of the phenoxyethanol to the caprylyl glycol is (5-7): (2-4). More preferably, the weight ratio of the phenoxyethanol to the caprylyl glycol is 6.5: 3.5.

The phenoxyethanol can inhibit bacteria and fungi, when the phenoxyethanol and the caprylyl glycol are compounded for use, the system has a broad-spectrum antibacterial effect and can enhance the corrosion resistance of the system, and the caprylyl glycol can play a role in moisture retention and softness, so that the compound use of the phenoxyethanol and the caprylyl glycol can achieve the mild corrosion resistance effect, and the shelf life of the composition prepared by the application can reach 3-4 years. And the phenoxyethanol and the caprylyl glycol are used as the preservative and the antibacterial agent, are safe, generally have no influence on pregnant women and can be used safely.

The color cosmetic composition has the advantages of no stimulation to skin, high safety degree, no influence on pregnant women and safe use.

In a second aspect, the present application provides a method for preparing a color cosmetic composition, which adopts the following technical scheme:

a preparation method of a color cosmetic composition comprises the following steps:

according to the formula proportion, diisostearyl malate, hydrogenated polyisobutene, an emollient I, an emollient II, a skin conditioner II, a preservative and the skin conditioner I are mixed, dissolved and dispersed uniformly; adding pearling agent, stirring, adding octyl dodecanol and caprylic triglyceride, and making into fine particles with average particle diameter of 2-3 mm.

It is further preferred that when disteardimonium hectorite and silica are present in the system, the disteardimonium hectorite and silica are added after the addition of the preservative and then dissolved by heating.

By adopting the technical scheme, the prepared color cosmetic composition is homogeneous and stable, and has good texture.

In a third aspect, the present application provides a use of a color cosmetic composition selected from the above color cosmetic compositions or prepared by the above preparation method in highlight, eye cream or blush.

The color cosmetic composition prepared by the application is used in highlight, eye cream or blush, has good moistening performance, is not pulled dry, is not easy to remove after makeup, can endow a product with good ductility, is not tinged, is easy to make up, can endow the product with good brightness, and has a good makeup effect. In addition, the color cosmetic composition is also suitable for other bright formulas, and can enable the product to have high brightness.

In summary, the present application has the following beneficial effects:

1. the color cosmetic composition has good moisturizing property and long moisturizing effect;

2. the color cosmetic composition has good ductility, is easy to apply, is not easy to be tinged and is good in makeup;

3. the color cosmetic composition has good luster and high brightness, and is full in make-up effect.

Detailed Description

The present application will be described in further detail with reference to examples. Specifically, the following are described: the following examples, in which specific conditions are not specified, were conducted under conventional conditions or conditions recommended by the manufacturer; the starting materials used in the following examples are all those conventionally commercially available except where specifically noted.

Examples

Example 1

mixing 9.64g diisostearyl malate, 7g hydrogenated polyisobutene, 7g emollient I (7g C12-15 alcohol benzoate, 0g tridecyl trimellitate and 0g polybutene), 6g emollient II (6g ethylhexyl palmitate and 0g isononyl isononanoate), 3.19g skin conditioner II (2.36g dibutyl ethylhexanoyl glutamine and 0.83g dibutyl lauroyl glutamine), 0.17g preservative (0.11g phenoxyethanol and 0.06g caprylyl glycol) and 1.7g skin conditioner I (1.7g orange peel oil, 0g crambe oil and 0g saffron extract) to dissolve and disperse uniformly; then adding 33g of pearling agent (23g of CI 77019 and 10g of CI 77491) and stirring uniformly, adding 30g of octyl dodecanol and 4g of caprylic triglyceride, and preparing into particles with average particle size of 2-3mm to obtain the color cosmetic composition.

Examples 2 to 4

Examples 2-4 differ from example 1 only in that: in examples 2-4, octyldodecanol, diisostearyl malate, hydrogenated polyisobutene, and caprylic triglyceride were used in varying amounts, as shown in Table 1 below.

TABLE 1

Raw materials	Example 1	Example 2	Example 3	Example 4
					Octyl dodecanol/g	30	24	26.2	26.2
Diisostearyl malate/g	9.64	10	11.27	9.17
					Hydrogenated polyisobutene/g	7	8.64	7.27	9.17
Caprylic/capric triglyceride/g	4	8	5.9	5.67

Examples 5 to 8

Examples 5-8 differ from example 4 only in that: in examples 5-8, emollient I and emollient II were selected and used in varying amounts, as shown in Table 2 below.

TABLE 2

Examples 9 to 10

Examples 9-10 differ from example 8 only in that: in examples 9-10, the amounts of CI 77019 and CI 77491 used in the pearlescent agents were varied, as shown in Table 3 below.

TABLE 3

Examples 11 to 14

Examples 11-14 differ from example 10 only in that: examples 11-14, skin conditioner I and skin conditioner II were selected and used in varying amounts, as shown in Table 4 below.

TABLE 4

Examples 15 to 16

Examples 15-16 differ from example 14 only in that in examples 15-16, a disteardimonium hectorite and silica were added to the composition system as shown in Table 5 below.

TABLE 5

Comparative example

Comparative examples 1 to 4 differ from example 4 only in that: comparative examples 1-4 differ in the selection and/or amount of octyldodecanol, diisostearyl malate, hydrogenated polyisobutene, and caprylic triglyceride, as shown in table 6 below.

TABLE 6

Performance testing test 95 healthy women aged 18-40 were randomly selected and randomly divided into 19 groups, each group using one sample of the composition prepared in examples 1-15 or comparative examples 1-4. The test specimen was applied to the back of the hand, and the brightness immediately after application of the test specimen and the brightness after 4 hours were recorded, and the specific evaluation criteria of the brightness were as shown in Table 7 below. The specific statistics of the shine evaluation and the rate of change of moisture are shown in table 8 below.

Detecting the moisture change rate of the skin:

the moisture change rate is the moisture after 4h of application to the sample-moisture before application/moisture before application x 100%.

TABLE 7

TABLE 8

As can be seen by combining examples 1-4 and comparative examples 1-4 with tables 7-8, the addition of octyldodecanol, diisostearyl malate, hydrogenated polyisobutene, and caprylic/capric triglyceride in the present system at the formulation ratio improves the moisturizing and shine benefits of the color cosmetic composition, and lasts longer.

It can be seen from the combination of examples 4-8 and tables 7-8 that emollient I and emollient II, when added to the system in the formulation ratios of the present application, improve the moisturizing effect and enhance the shine benefit of the color cosmetic composition.

As can be seen by combining examples 9-10 with tables 7-8, the color cosmetic composition has the best brightening effect when CI 77019 and CI 77491 are compounded and used in a mass ratio of 6.5:3.5 in the pearlescent agent.

It can be seen from examples 10 to 14 and tables 7 to 8 that the skin conditioner I and the skin conditioner II are matched with each other according to the formula ratio, and can retain moisture and lock water, nourish the skin to make the makeup natural, improve the moisturizing effect and improve the brightening effect of the color cosmetic composition.

As can be seen by combining examples 14-16 with tables 7-8, the addition of specific levels of disteardimonium hectorite and silica to the system improves the shine benefits of the color cosmetic composition.

The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims

1. A color cosmetic composition characterized by: the composite material is prepared from the following raw materials in percentage by weight:

2. The color cosmetic composition according to claim 1, characterized in that: the mass ratio of the octyl dodecanol, the diisostearyl malate, the hydrogenated polyisobutene and the caprylic/capric triglyceride is (25-27): (9-10): (9-10): (4-6).

3. The color cosmetic composition according to claim 1, characterized in that: the emollient I is selected from C12-15 alcohol benzoate, tridecyl alcohol trimellitate and polybutene, and the mass ratio of the C12-15 alcohol benzoate, the tridecyl alcohol trimellitate and the polybutene is (2-4): (1-3): (1-3).

4. The color cosmetic composition according to claim 1, characterized in that: the emollient II is selected from ethylhexyl palmitate and isononyl isononanoate, and the dosage of the ethylhexyl palmitate and the dosage of the isononyl isononanoate respectively account for 4% -7.5% and 1% -2.5% of the total amount of the color cosmetic composition.

5. The color cosmetic composition according to claim 1, characterized in that: the pearling agent is selected from CI 77019 and CI 77491, and the mass ratio of the CI 77019 to the CI 77491 is (5-7): (2-3.5).

6. The color cosmetic composition according to any one of claims 1 to 5, wherein: the skin conditioning agent I comprises dibutyl ethylhexanoyl glutamine and dibutyl lauroyl glutamine;

the skin conditioner II comprises lime peel oil, crambe abyssinica seed oil and crocus sativus flower extract.

7. The color cosmetic composition according to claim 6, wherein: the skin conditioner I is dibutyl ethylhexanoyl glutamine and dibutyl lauroyl glutamine, and the dosage of the dibutyl ethylhexanoyl glutamine and the dosage of the dibutyl lauroyl glutamine respectively account for 1.5-3.5% and 0.5-1.5% of the total amount of the color cosmetic composition;

the skin conditioner II is orange peel oil, crambeabyssinica seed oil and crocus sativus flower extract; and the lime peel oil accounts for 0.1-0.4% of the total amount of the color cosmetic composition; the crambeabyssinica seed oil accounts for 0.8-1.3% of the total amount of the color cosmetic composition; the crocus sativus flower extract accounts for 0.4-0.8% of the total amount of the color cosmetic composition.

8. The color cosmetic composition according to claim 1, characterized in that: also comprises disteardimonium hectorite and silica, wherein the disteardimonium hectorite and the silica respectively account for 0.2% -0.5% and 0.5% -2% of the total weight of the color cosmetic composition.

9. A method of preparing a color cosmetic composition according to any one of claims 1 to 8, wherein: the method comprises the following steps:

10. Use of the color cosmetic composition according to any one of claims 1 to 8 or the preparation method according to claim 9 for highlighting, eye cream or blush.