CN116919867A - Whitening concealer uvioresistant composition and preparation method and application thereof - Google Patents
Whitening concealer uvioresistant composition and preparation method and application thereof Download PDFInfo
- Publication number
- CN116919867A CN116919867A CN202310895357.XA CN202310895357A CN116919867A CN 116919867 A CN116919867 A CN 116919867A CN 202310895357 A CN202310895357 A CN 202310895357A CN 116919867 A CN116919867 A CN 116919867A
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- 239000000203 mixture Substances 0.000 title claims abstract description 52
- 230000002087 whitening effect Effects 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000000284 extract Substances 0.000 claims abstract description 28
- -1 skin conditioners Substances 0.000 claims abstract description 19
- 239000003906 humectant Substances 0.000 claims abstract description 15
- 239000004909 Moisturizer Substances 0.000 claims abstract description 13
- 230000001333 moisturizer Effects 0.000 claims abstract description 13
- 241000196324 Embryophyta Species 0.000 claims abstract description 12
- 239000000419 plant extract Substances 0.000 claims abstract description 12
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 10
- 239000003974 emollient agent Substances 0.000 claims abstract description 9
- 239000000126 substance Substances 0.000 claims abstract description 9
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 8
- 239000003086 colorant Substances 0.000 claims abstract description 8
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- 239000000945 filler Substances 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 7
- 239000003381 stabilizer Substances 0.000 claims abstract description 7
- 241001520913 Phyllostachys edulis Species 0.000 claims abstract 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 12
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 11
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical group [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 7
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims description 6
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- GVJHHUAWPYXKBD-UHFFFAOYSA-N d-alpha-tocopherol Natural products OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 6
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- MSRJTTSHWYDFIU-UHFFFAOYSA-N octyltriethoxysilane Chemical compound CCCCCCCC[Si](OCC)(OCC)OCC MSRJTTSHWYDFIU-UHFFFAOYSA-N 0.000 claims description 5
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- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 4
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- DTPCFIHYWYONMD-UHFFFAOYSA-N decaethylene glycol Chemical compound OCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO DTPCFIHYWYONMD-UHFFFAOYSA-N 0.000 claims description 4
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
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- QELSKZZBTMNZEB-UHFFFAOYSA-N propylparaben Chemical compound CCCOC(=O)C1=CC=C(O)C=C1 QELSKZZBTMNZEB-UHFFFAOYSA-N 0.000 claims description 4
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- SZVJSHCCFOBDDC-UHFFFAOYSA-N ferrosoferric oxide Chemical compound O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 claims description 3
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims description 3
- 235000019341 magnesium sulphate Nutrition 0.000 claims description 3
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- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
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- MTZQAGJQAFMTAQ-UHFFFAOYSA-N benzoic acid ethyl ester Natural products CCOC(=O)C1=CC=CC=C1 MTZQAGJQAFMTAQ-UHFFFAOYSA-N 0.000 claims description 2
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- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 claims description 2
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- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 7
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- NIPNSKYNPDTRPC-UHFFFAOYSA-N N-[2-oxo-2-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C(CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F)N1CC2=C(CC1)NN=N2 NIPNSKYNPDTRPC-UHFFFAOYSA-N 0.000 description 2
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- GVJHHUAWPYXKBD-IEOSBIPESA-N α-tocopherol Chemical compound OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-IEOSBIPESA-N 0.000 description 2
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- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/361—Carboxylic acids having more than seven carbon atoms in an unbroken chain; Salts or anhydrides thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
- A61K8/894—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A—HUMAN NECESSITIES
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- A—HUMAN NECESSITIES
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- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
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- A61K2800/522—Antioxidants; Radical scavengers
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- A—HUMAN NECESSITIES
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- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The application relates to the field of cosmetics, and particularly discloses a whitening and concealing anti-ultraviolet composition, and a preparation method and application thereof. The composition comprises the following components: emollients, moisturizers, colorants, emulsifiers, antioxidants, emulsion stabilizers, fillers, skin conditioners, preservatives, and solvents; the moisturizer comprises a plant moisturizer and a chemical moisturizer. The composition provided by the application has a synergistic effect with a plant humectant through the skin conditioner, and the cyclopentamethylene dimethyl siloxane is added, so that the film forming capability of the product can be improved, and further the whitening and sun-screening effects and stability of the product are obviously improved. The composition disclosed by the application can promote the effective skin care ingredients to act on the skin through the film layer by the synergistic combination of the plant extract composition, the phyllostachys pubescens leaf extract and the crocus sativus extract, and has a good whitening and skin care effect.
Description
Technical Field
The application belongs to the field of cosmetics, and particularly relates to a whitening and concealing anti-ultraviolet composition, and a preparation method and application thereof.
Background
The skin is dull, uneven in complexion and dark yellow, most commonly, skin melanin is formed due to long-time exposure to ultraviolet rays in environmental factors, then pigment is deposited on the surface of the skin, and when the cutin cannot be normally updated for a long time, the skin darkness is further aggravated; secondly, the skin is dark and yellow due to long-time water shortage, and the skin is dry and wrinkled, and the skin appears grey and yellow at the moment; in addition, skin is also tarnished and dark yellow after aging; factors such as personal lifestyle can also cause dullness in the skin, such as: night stay, high pressure, alcoholism, smoking, insufficient sleep and the like can influence the health and normal metabolism of the skin; finally, scars left after mosquito bites or skin injuries in summer can affect the skin color uniformity of the whole skin. In order to cover various defects on the skin surface, the main aspects are moisture retention, concealer, wrinkle resistance and the like. As disclosed in chinese patent CN110314112a, a whitening composition and a preparation method thereof, the whitening composition comprises the following components: vitamin C, humectant, film forming agent, thickener, emulsifier, silica, and antioxidant. The vitamin C is wrapped by a silicon alcohol-coated system to isolate air, so that the property of the vitamin C is stable; the formula is anhydrous, and a bacteriostatic agent is not required to be added; meanwhile, the utilization rate of vitamin C can be improved by dissolving the vitamin C with the polyol humectant, so that the vitamin C better permeates into the deep layer of the skin to play a role, and the whitening and moisturizing effects are achieved. As further disclosed in chinese patent CN108888524a, a concealer composition and a method for preparing the same, the total mass of the concealer composition comprises the following components: the concealer comprises titanium dioxide and an HDI/trimethylol hexyl lactone cross-linked polymer, the concealer composition has high concealing force, excellent oil control effect, is suitable for people with oily skin, has whitening effect, can prevent melanin from deepening, and is not easy to cause acne.
However, various products such as foundation, moisturizing water, whitening cream and freckle-removing cream on the market at present have the defect of unobvious moisturizing effect and no lasting moisturizing effect; some have the defect of excessive whitening effect and unnatural whitening effect; some defects of insufficient spot shielding effect exist; there are some defects of excessive concealer marks and poor soft light. Therefore, there is a need for a highly stable product that combines multiple effects of whitening, concealing, uv protection and oxidation resistance.
Disclosure of Invention
As used herein, the singular forms "a," "an," and "the" include the singular and plural referents unless the context clearly dictates otherwise. The recitation of numerical ranges by endpoints includes all numbers and fractions subsumed within that corresponding range, and the endpoints recited.
Aiming at the problems existing in the prior art, the application provides a whitening concealer uvioresistant composition, a preparation method and application thereof.
In order to achieve the above purpose, the technical scheme adopted by the application is as follows:
in one aspect, the application provides a whitening concealer anti-ultraviolet composition comprising the following components: emollients, moisturizers, colorants, emulsifiers, antioxidants, emulsion stabilizers, fillers, skin conditioners, preservatives, and solvents; the moisturizer comprises a plant moisturizer and a chemical moisturizer.
Preferably, the whitening concealer-resistant composition comprises the following components in percentage by weight: 17.7 to 30.1 percent of emollient, 7.51 to 15.58 percent of humectant, 6.21 to 9.28 percent of colorant, 1.5 to 4.5 percent of emulsifier, 0.6 to 1.5 percent of antioxidant, 0.6 to 1.5 percent of emulsion stabilizer, 0.9 to 2.6 percent of filling agent, 0.1 to 0.8 percent of skin conditioning agent, 0.25 to 0.65 percent of preservative and 42 to 64 percent of solvent.
Preferably, the plant moisturizer comprises a plant extract composition, a phyllostachys pubescens leaf extract and a crocus sativus extract; the chemical humectant comprises at least one of propylene glycol, glycerin, polydimethylsiloxane alcohol and butylene glycol.
Preferably, the plant extract composition comprises cactus extract, radix Ophiopogonis root extract, oat bran extract, radix Paeoniae root extract and radix Scutellariae root extract.
Preferably, the mass ratio of the plant extract composition, the phyllostachys pubescens leaf extract and the crocus sativus extract is 0.02-0.10:1:1-3.
Preferably, the emollient comprises at least one of mineral oil, cyclopentadimethicone, cyclohexasilicone, C12-15 alcohol benzoate, beeswax, trimethylsiloxysilicate.
Preferably, the colorant includes at least one of titanium dioxide, aluminum oxide, iron oxide yellow, triethoxy octyl silane, iron oxide red, and iron oxide black.
Preferably, the emulsifier comprises cetyl PEG/PPG-10/1 polydimethylsiloxane and/or PEG-10 polydimethylsiloxane.
The polydimethylsiloxane is colorless and odorless, has better waterproof property and heat resistance, can form a waterproof protective film on the surface of skin, has stronger ultraviolet resistance, and can not be oxidized and deteriorated under ultraviolet rays. Wherein the PEG-10 polydimethylsiloxane has stable property, and plays a role in dispersion and emulsification, so that the composite material is more stable and uniform.
Preferably, the preservative comprises at least one of phenoxyethanol, ethylhexyl glycerol, methylparaben, and propylparaben; the filler comprises at least one of magnesium sulfate, mica, and triethoxy octyl silane; the solvent comprises water and/or ethanol.
Preferably, the antioxidant is tocopherol; the emulsion stabilizer is disteardimonium hectorite; the skin conditioner is magnesium stearate.
Tocopherol, namely vitamin E, is insoluble in water and soluble in organic solvents such as ethanol, has strong antioxidation, can remove free radicals in human bodies, protect cell membranes, and protect vitamin A, vitamin C and various amino acids in human bodies from being oxidized, thereby playing roles of whitening, concealing and resisting ultraviolet.
The application also provides a preparation method of the composition, which comprises the following steps: mixing the above materials.
The application also provides an application of the composition or the composition prepared by the preparation method in preparing cosmetics.
In another aspect, the present application provides a cosmetic comprising the composition described above.
Preferably, the cosmetic comprises BB cream.
Compared with the prior art, the application has the following beneficial effects:
(1) The composition provided by the application has a synergistic effect with a plant humectant through the skin conditioner, and the cyclopentamethylene dimethyl siloxane is added, so that the film forming capability of the product can be improved, the whitening and sun-screening effects are further remarkably improved, and the stability of the product is also remarkably influenced.
(2) The emulsifier provided by the application adopts cetyl PEG/PPG-10/1 polydimethylsiloxane and/or PEG-10 polydimethylsiloxane for synergistic cooperation, and can form a channel structure on a product film layer while playing a role of emulsifying and homogenizing, compensate the passing rate of hydrophilic substances of the film layer, promote the permeation of hydrophilic substances such as skin conditioning agents, emollients and the like to the skin surface, and ensure the whitening and concealing effects.
(3) The composition disclosed by the application can promote the effective skin care ingredients to act on the skin through the film layer by the synergistic combination of the plant extract composition, the phyllostachys pubescens leaf extract and the crocus sativus extract, so that the whitening, concealing and sun-screening capabilities of the product are obviously improved.
Detailed Description
The following description of the present application is provided by way of specific examples to facilitate understanding and grasping of the technical solution of the present application, but the present application is not limited thereto, and the described examples are only some, but not all, examples of the present application.
The endpoints and any values of the ranges disclosed herein are not limited to the precise range or value, and are understood to encompass values approaching those ranges or values. For numerical ranges, one or more new numerical ranges may be found between the endpoints of each range, between the endpoint of each range and the individual point value, and between the individual point value, in combination with each other, and are to be considered as specifically disclosed herein.
All other embodiments, which can be made by those skilled in the art based on the embodiments of the application without making any inventive effort, shall fall within the scope of the application. The experimental methods described in the following examples are all conventional methods unless otherwise specified; the reagents and materials, unless otherwise specified, are commercially available.
Note that, CI 77891 represents titanium dioxide, CI 77499 represents iron oxide black, CI 77492 represents iron oxide yellow, and CI 77491 represents iron oxide red.
Examples 1-3 and comparative examples 1-5 each provided a BB cream with whitening and concealer resistance to ultraviolet rays, the specific formulations are shown in Table 1.
Table 1 formulations of examples 1-3 and comparative examples 1-5
The formulation of each compound is shown in table 2.
Table 2 formulation of each compound
BB creams provided in examples 1-3 and comparative examples 1-5, were prepared by a process comprising the steps of:
s1, weighing all components according to the table 1 and the table 2, adding phase A raw materials comprising an emollient, an emulsifier, a compound of polydimethylsiloxane and dimethiconol, tocopherol, magnesium stearate and a preservative except a compound of phenoxyethanol and ethylhexyl glycerol into an oil phase pot, stirring at 600rpm, heating to 85 ℃, and stirring for 20min until the materials are uniformly mixed to obtain an oil phase 1;
s2, mixing and uniformly stirring the phase B raw materials including cyclopenta-dimethyl siloxane and disteardimethyl ammonium hectorite, homogenizing and emulsifying for 1 minute, and then adding the oil phase 1, stirring at 400rpm for 10 minutes until the mixture is uniformly mixed to obtain an oil phase 2;
s3, grinding the C-phase raw materials including the coloring agent, the compound of cyclopenta-dimethyl siloxane and cyclohexasiloxane and the compound raw materials of mica and triethoxy octyl silane by using a homogenizer, adding the oil phase 2, and stirring at 400rpm for 10min until the mixture is uniformly mixed to obtain an oil phase;
s4, adding a D-phase raw material comprising a chemical humectant, magnesium sulfate and water except a compound of polydimethylsiloxane and dimethiconol into a water phase pot, stirring at 400rpm, heating to 85 ℃, and stirring for 10min until the materials are uniformly mixed;
s5, pumping the oil phase material into a vacuum emulsifying pot, and homogenizing and emulsifying for 3 minutes; then preheating the reaction kettle, vacuumizing and pumping the water phase, stirring, slowly pumping the water phase into the oil phase, homogenizing and emulsifying for 3min; cooling to 45deg.C, adding phase E material including 95% ethanol, phenoxyethanol and ethylhexyl glycerol complex and plant humectant, stirring at 400rpm for 10min to mix well;
s6, filling a small sample comparison sample plate, sampling and detecting the qualified sample plate, and filtering and discharging the sample plate; sterilizing the packaging material for later use, filling, packaging, spraying codes after packaging, and boxing after the codes are sprayed; and warehousing after the sampling inspection is qualified.
The plant extract composition is prepared by mixing 50wt% butanediol, 7wt% Opuntia DILLENII (Opuntia DILLENII) extract, 3wt% radix Ophiopogonis (OPHIOPOGON JAPONICUS) extract, 3wt% oat (AVENA SATIVA) bran extract, 2wt% radix Paeoniae (PAEONIA ALBIFLORA) extract, 1wt% radix Scutellariae (SCUTELLARIA BAICALENSIS) extract, and 34wt% water.
Effect example 1 stability Effect study
1. Temperature influence
BB creams prepared in examples 1-3 and comparative examples 1-5 were sealed in clean PET bottles, circulated 4 times at (-18) deg.C and 45 deg.C, respectively, and stored 24 hours each time, namely, after storing 24 hours at (-18) deg.C, stored 24 hours at room temperature, and then placed in a 45 deg.C incubator for storing 24 hours, and circulated 4 times to observe the stability of the product.
2. Centrifugal influence
After BB creams prepared in examples 1-3 and comparative examples 1-5 were allowed to stand for one day, 10g of each paste was taken in a centrifuge tube, and centrifuged at 3000r/min for 30min in the centrifuge, and the stability of the product was observed.
3. Illumination influence
BB creams prepared in examples 1-3 and comparative examples 1-5 were sealed in clean transparent bottles and left under a fluorescent lamp for 1 month to observe the stability of the product.
The stability results are shown in Table 3.
TABLE 3 results of influence of temperature, centrifugation and light on stability of product
The results of the table show that the BB cream provided by the application has good stability under the conditions of cold and hot circulation, centrifugation and illumination, and meets the industrial production standard. In contrast, in comparative examples 1 and 2, the plant humectant and magnesium stearate cannot exert a synergistic effect due to the absence of magnesium stearate or plant humectant, so that the adhesiveness of BB cream is reduced, the extensibility is reduced, and the stability is reduced; comparative example 3, comparative example 4 and comparative example 5 were unable to exert the synergistic effect between the plant extract composition, phyllostachys pubescens and crocus sativus extracts, resulting in reduced stability of BB cream in the cold and hot cycle and light influence experiments. The BB cream prepared from the specific components can enhance the stability in the environment and prolong the storage time.
Effect example 2 study of whitening Effect
Healthy female subjects of 20-50 years old were selected, standardized facial cleansing and quantitative skin care were first performed, and after maintaining a fixed position in a constant temperature and humidity environment ((20±2) °c, 50% ±10%) for 20min, they were randomly divided into 8 groups of example 1-3 and comparative example 1-5, respectively, 10 persons each, and BB cream prepared in example 1-3 and comparative example 1-5 was smeared on the cheeks, and clinical tests and evaluations were performed before use, 15min after use, and 12h after use. During the test, the skin brightness L x value before and after makeup was analyzed by sensing skin light through RGB and calculating color space coordinates using Delfin skincolorcatch skin color test probes without using other cosmetics. The specific results are shown in the following table:
table 4 comparison of whitening effect
Note that: in comparison to pre-makeup, # represents P <0.05, # represents P <0.01.
As can be seen from the results of the table, the BB cream prepared in the present application has a remarkable whitening effect and a more excellent make-up effect than the BB creams prepared in comparative examples 1 to 5, indicating that the effect of lightening skin color can be achieved by using the BB cream of the present application.
Effect example 3 anti-ultraviolet Effect study
The experimental samples were BB creams prepared in examples 1-3 and comparative examples 1-5. Before the sample test, the filter disc and the standard substance attached to the instrument are used for spot detection test, and after all the sample tests are normal, the sample test is carried out. Measuring background curve of blank film, uniformly spot-applying sample on 3M adhesive tape with spotter, and applying with finger with latex finger stall to make sample on film surface be 2 μL/cm 2 Distribution. And then the smeared sample plate is placed in a constant temperature drying oven at 37 ℃ for drying, 6 points are randomly selected on the transparent film for testing by using an SPF-290AS analyzer, and finally, data are processed by using a workstation, so that corresponding SPF values are obtained. The specific results are shown in the following table.
TABLE 5 SPF value test results
| Grouping | SPF value |
| Example 1 | 41.5 |
| Example 2 | 41.3 |
| Example 3 | 40.8 |
| Comparative example 1 | 34.2 |
| Comparative example 2 | 30.5 |
| Comparative example 3 | 28.3 |
| Comparative example 4 | 27.9 |
| Comparative example 5 | 27.0 |
The data show that the BB cream has excellent sun-screening effect, SPF value can meet daily sun-screening requirement, and comparative examples 1-5 lack one or more components in the skin conditioner or plant extract of the application and cannot exert good sun-screening effect, which indicates that the skin conditioner of the application needs to be used cooperatively with a plant humectant, and the ultraviolet-screening effect of the BB cream can be improved by exerting synergistic effect among specific plant extracts in the plant humectant.
Finally, it should be noted that the above description is only for illustrating the technical solution of the present application, and not for limiting the scope of the present application, and that the simple modification and equivalent substitution of the technical solution of the present application can be made by those skilled in the art without departing from the spirit and scope of the technical solution of the present application.
Claims (13)
1. A whitening concealer anti-uv composition, characterized in that: the composition comprises the following components: emollients, moisturizers, colorants, emulsifiers, antioxidants, emulsion stabilizers, fillers, skin conditioners, preservatives, and solvents; the moisturizer comprises a plant moisturizer and a chemical moisturizer.
2. The composition of claim 1, wherein: the composite material comprises the following components in percentage by weight: 17.7 to 30.1 percent of emollient, 7.51 to 15.58 percent of humectant, 6.21 to 9.28 percent of colorant, 1.5 to 4.5 percent of emulsifier, 0.6 to 1.5 percent of antioxidant, 0.6 to 1.5 percent of emulsion stabilizer, 0.9 to 2.6 percent of filling agent, 0.1 to 0.8 percent of skin conditioning agent, 0.25 to 0.65 percent of preservative and 42 to 64 percent of solvent.
3. The composition of claim 1, wherein: the plant humectant comprises a plant extract composition, a phyllostachys pubescens leaf extract and a crocus sativus extract; the chemical humectant comprises at least one of propylene glycol, glycerin, polydimethylsiloxane alcohol and butylene glycol.
4. A composition according to claim 3, characterized in that: the plant extract composition comprises cactus extract, radix Ophiopogonis root extract, oat bran extract, radix Paeoniae root extract and radix Scutellariae root extract.
5. A composition according to claim 3, characterized in that: the mass ratio of the plant extract composition, the phyllostachys pubescens leaf extract and the crocus sativus extract is 0.02-0.10:1:1-3.
6. The composition of claim 1, wherein: the emollient comprises at least one of mineral oil, cyclopentadimethicone, cyclohexasilicone, C12-15 alcohol benzoate, beeswax, and trimethylsiloxysilicate.
7. The composition of claim 1, wherein: the colorant includes at least one of titanium dioxide, aluminum oxide, iron oxide yellow, triethoxyoctylsilane, iron oxide red, and iron oxide black.
8. The composition of claim 1, wherein: the emulsifier comprises cetyl PEG/PPG-10/1 polydimethylsiloxane and/or PEG-10 polydimethylsiloxane.
9. The composition of claim 1, wherein: the preservative comprises at least one of phenoxyethanol, ethylhexyl glycerol, methylparaben and propylparaben; the filler comprises at least one of magnesium sulfate, mica, and triethoxy octyl silane; the solvent comprises water and/or ethanol.
10. The composition of claim 1, wherein: the antioxidant is tocopherol; the emulsion stabilizer is disteardimonium hectorite; the skin conditioner is magnesium stearate.
11. A process for the preparation of a composition as claimed in any one of claims 1 to 10, characterized in that: the method comprises the following steps: mixing the above materials.
12. Use of a composition according to any one of claims 1 to 10 or a composition prepared by a method of preparation according to claim 11 for the preparation of a cosmetic.
13. A cosmetic product characterized by: comprising a composition according to any one of claims 1-10.
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