CN109288723A - A kind of cosmetic composition and preparation method thereof containing nano-cellulose - Google Patents

A kind of cosmetic composition and preparation method thereof containing nano-cellulose Download PDF

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Publication number
CN109288723A
CN109288723A CN201811440214.5A CN201811440214A CN109288723A CN 109288723 A CN109288723 A CN 109288723A CN 201811440214 A CN201811440214 A CN 201811440214A CN 109288723 A CN109288723 A CN 109288723A
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Prior art keywords
cosmetic composition
cellulose
total weight
nano
content
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王习文
李仁坤
董凯辉
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South China University of Technology SCUT
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South China University of Technology SCUT
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/731—Cellulose; Quaternized cellulose derivatives
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/413—Nanosized, i.e. having sizes below 100 nm

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to the preparation technical fields of cosmetics, and in particular to a kind of cosmetic composition and preparation method thereof containing nano-cellulose.The cosmetic composition takes full advantage of the pure plant attribute of nano-cellulose, and cost of material is low, resourceful, and a large amount of hydroxyl is contained on surface, and water suction performance of keeping humidity is excellent.Simultaneously, nano-cellulose has high length-diameter ratio and high-specific surface area, diameter is less than 100nm, the far smaller than wavelength of ultraviolet light, can ultraviolet light in reflecting sunlight, further addition skin-moisturizing, skin ingredient, whitening spot-removing ingredient or the crease-resistant ingredient of smoothing wrinkle, make cosmetics have both excellent whitening effect on this basis, to no skin irritation, the comfortableness and security of product are improved.

Description

A kind of cosmetic composition and preparation method thereof containing nano-cellulose
Technical field
The invention belongs to the preparation technical fields of cosmetics, and in particular to a kind of cosmetic combinations containing nano-cellulose Object and preparation method thereof.
Background technique
Cosmetics are one of main skin care modes, and effect depends primarily on the effective component contained by itself.At present Cosmetics huge number on the market, effect are not quite similar.Wherein, the principle active component of Moisturizer is sodium hyaluronate or water The biomolecule such as collagen are solved, still not using natural plant fibre as the Moisturizer of principle active component.
Summary of the invention
The primary purpose of the present invention is that providing a kind of cosmetic composition containing nano-cellulose.
Another object of the present invention is to provide the preparation methods of the above-mentioned cosmetic composition containing nano-cellulose.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of cosmetic composition containing nano-cellulose, with the total weight of cosmetic composition, containing 20%~ The partial size of 50% nano-cellulose, nano-cellulose is less than 100nm.
Preferably, the partial size of the nano-cellulose is less than 80nm.
It is furthermore preferred that the partial size of the nano-cellulose is less than 60nm.
Preferably, the cosmetic composition containing nano-cellulose is lotion or cream.
Preferably, the cosmetic composition containing nano-cellulose also include thickener, emulsifier, antibacterial agent, Finish, essence and deionized water, and include that moisturizer, emollient, sun-screening agent, antioxidant, whitening spot-removing ingredient and smoothing wrinkle are crease-resistant One or more of ingredient.
It is furthermore preferred that the moisturizer be one or both of glycerol, propylene glycol, sorbierite and polyethylene glycol with On.
It is further preferred that the content of the moisturizer is the 1%~5% of cosmetic composition total weight, more into one Step preferably 2%~3%.
It is furthermore preferred that the emollient be ethylhexyl palmitate, decyl oleate, saualane, phenethyl benzoate, One or more of cetanol lactate and maleic acid ricinolein.
It is further preferred that the content of the emollient is the 1%~5% of cosmetic composition total weight, more into one Step preferably 2%~4%.
It is furthermore preferred that the sun-screening agent is zinc oxide, titanium dioxide, dimethyl PABA ethylhexyl, butylmethoxy One or more of dibenzoyl methane and bis-ethylhexoxyphenol methoxyphenyl triazine.
It is further preferred that the content of the sun-screening agent be cosmetic composition total weight 0.5%~3%, more into One step is preferably 1.7%~2.3%.
It is furthermore preferred that the antioxidant is tert-butyl hydroquinone, glutamic acid, tocopherol, propylgallate, positive dihydro are cured Create one or more of sour (NDGA).
It is further preferred that the content of the antioxidant is the 0.01%~0.1% of cosmetic composition total weight, more Further preferably 0.05%~0.08%.
It is furthermore preferred that the whitening spot-removing ingredient is one or both of quinhydrones, arbutin, kojic acid and vitamin C More than.
It is further preferred that the content of the whitening spot-removing ingredient is the 2%~6% of cosmetic composition total weight, It is still more preferably 3%~5%.
It is furthermore preferred that the crease-resistant ingredient of the smoothing wrinkle is Sodium Hyaluronate, collagen, mate leaf extract and rose One of rare gadol extract is a variety of.
It is further preferred that the content of the crease-resistant ingredient of the smoothing wrinkle is the 2~6% of cosmetic composition total weight, more Further preferably 3~5%.
It is furthermore preferred that the emulsifier is glycerin monostearate, hydrolecithin, lanolin and the smooth olive oil of sorb One or more of acid esters.
It is further preferred that the content of the emulsifier is the 3%~6% of cosmetic composition total weight, more into one Step preferably 4%~5%.
It is furthermore preferred that the antibacterial agent is Buddhist nun's platinum rouge, p-hydroxybenzoate, benzyl alcohol, one in dehydroacetic acid Kind is two or more.
It is further preferred that the content of the antibacterial agent be cosmetic composition total weight 0.1%~2%, more into One step is preferably 0.5%~0.8%.
It is furthermore preferred that the thickener is hydroxyethyl cellulose, carboxymethyl cellulose, sodium alginate, PEG-80 glycerol One or more of base butter ester and sodium acrylate/ethylene isodecyl acid esters cross-linked polymer.
It is further preferred that the content of the thickener is the 2%~5% of cosmetic composition total weight, more into one Step preferably 3%~4%.
It is furthermore preferred that the finish is one or both of olive oil, stearate, beeswax, silicone oil and vaseline More than.
It is further preferred that the content of the finish is the 2%~5% of cosmetic composition total weight, further Preferably 3%~4%.
It is furthermore preferred that the content of the essence is the 0.5%~1% of cosmetic composition total weight, it is further excellent It is selected as 0.6%~0.8%.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with moisture-keeping functions.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with whitening spot-removing function.
It is furthermore preferred that the cosmetic composition containing nano-cellulose is by following raw material by weight percentage Composition:
Above-mentioned raw materials weight adds up to 100%.The formula is the cosmetic composition with crease-resistant smoothing wrinkle function.
Invention further provides the preparation method of the above-mentioned cosmetic composition containing nano-cellulose, including it is as follows Step:
(1) preparation of nano-cellulose
Microcrystalline cellulose is soluble in water, it is high-pressure homogeneous, cellulose solution is obtained, metal salt solution bridge joint is added, from Heart concentration, obtains nano-cellulose gel；
(2) preparation of water phase
By nano-cellulose gel, moisturizer, emollient, whitening spot-removing ingredient, the crease-resistant ingredient of smoothing wrinkle, sun-screening agent, emulsification Agent, essence, antioxidant and deionized water mixing, dissolve by heating, stir evenly, obtain mixture A；
(3) preparation of oily phase
Thickener, vitamin derivative, antibacterial agent and finish are mixed, is dissolved by heating, is stirred evenly, obtain mixture B；
(4) preparation of cosmetic composition
Mixture A and mixture B is mixed, is stirred evenly, is dissolved by heating, heat preservation, then high pressure or emulsifying homogeneous, it is cooled to Room temperature to get arrive the cosmetic composition containing nano-cellulose.
Preferably, when described in step (1) that microcrystalline cellulose is soluble in water, the mass ratio of microcrystalline cellulose and water is 1:20。
Preferably, pressure high-pressure homogeneous described in step (1) be 20000~30000psi, circular treatment 3~6 times.
Preferably, metal salt solution described in step (1) is in calcium chloride solution, magnesium chloride solution and sodium chloride solution One or more.
Preferably, the quality that metal salt solution is added described in step (1) is the 3~6% of cellulose solution quality.
Preferably, the temperature of heating for dissolving described in step (2) is 60~90 DEG C.
Preferably, the temperature of heating for dissolving described in step (3) is 50~80 DEG C.
Preferably, the temperature of heating for dissolving described in step (4) is 60~80 DEG C, when a length of 30~60min of heat preservation.
Preferably, high-pressure homogeneous described in step (4) to be carried out using high pressure homogenizer, pressure is 10~30MPa, circulation 1~3 time.
Preferably, emulsifying homogeneous described in step (4) is carried out using emulsifying homogeneous machine, and temperature is 60 DEG C, circulation 30min。
Compared with the prior art, the invention has the following advantages and beneficial effects:
Nano-cellulose is added in cosmetics by the present invention, take full advantage of the pure plant of nano-cellulose at Point, cost of material is low, and it is resourceful, and a large amount of hydroxyl is contained on surface, water suction performance of keeping humidity is excellent.Meanwhile nanofiber Element has high length-diameter ratio and a high-specific surface area, and diameter is less than 100nm, the far smaller than wavelength of ultraviolet light, can be in reflecting sunlight Ultraviolet light, further addition skin-moisturizing, skin ingredient, whitening spot-removing ingredient or the crease-resistant ingredient of smoothing wrinkle, make cosmetics on this basis Excellent whitening effect is had both, to no skin irritation, improves the comfortableness and security of product.
Specific embodiment
Below with reference to embodiment, invention is further described in detail, and embodiments of the present invention are not limited thereto.It is right In not specifically specified technological parameter, routine techniques progress can refer to.
The purchase of the microcrystalline cellulose used in the following example is in Wei Feng Biotechnology Co., Ltd of Zhengzhou City, food Grade, partial size are 20~80 μm.
Embodiment 1
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, sorbierite 2%, polyethylene glycol 1.5%, ethylhexyl palmitate 2%, saualane 2.5%, Glycerin monostearate 2.5%, hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, and sodium acrylate/ethylene isodecyl acid esters crosslinking gathers Close object 3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 56.05%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from Sub- water mixing, dissolves by heating at 60 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, 30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived Cosmetic compositions.
Embodiment 2
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, sorbierite 2.5%, polyethylene glycol 1%, ethylhexyl palmitate 2.5%, saualane 2%, Glycerin monostearate 2% hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymeric Object 3%, olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, positive dihydro are cured Create acid (NDGA) 0.07%, essence 0.8% and water 47.43%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from Sub- water mixing, dissolves by heating at 90 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, 30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived Cosmetic compositions.
Embodiment 3
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with skin-moisturizing, skin function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, sorbierite 1.5%, polyethylene glycol 2%, ethylhexyl palmitate 2%, saualane 3% are single Tristerin 3% hydrogenates lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, positive dihydro is cured Create acid (NDGA) 0.08%, essence 0.8% and water 24.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with skin-moisturizing, skin function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) nano-cellulose gel, sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, monostearate is sweet Grease, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and go from Sub- water mixing, dissolves by heating at 75 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, 30min is recycled in emulsifying homogeneous machine, temperature is cooled to room temperature at 60 DEG C to get the change containing nano-cellulose is arrived Cosmetic compositions.
Reference examples 1
Reference examples of the present embodiment as embodiment 1, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 2%, polyethylene glycol 1.5%, ethylhexyl palmitate 2%, saualane 2.5%, glycerin monostearate 2.5%, hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive Oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 76.05%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 60 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, 30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 2
Reference examples of the present embodiment as embodiment 2, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 2.5%, polyethylene glycol 1%, ethylhexyl palmitate 2.5%, saualane 2%, glycerin monostearate 2%, hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, essence 0.8% and water 77.43%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 90 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, 30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 3
Reference examples of the present embodiment as embodiment 3, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sorbierite 1.5%, polyethylene glycol 2%, ethylhexyl palmitate 2%, saualane 3%, glycerin monostearate 3%, hydrogenation lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, Beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence 0.8% and water 74.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by sorbierite, polyethylene glycol, ethylhexyl palmitate, saualane, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 75 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, 30min is recycled in emulsifying homogeneous machine, temperature at 60 DEG C, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
The cosmetic composition of Examples 1 to 3 and reference examples 1~3 is used one week to 30 volunteers, with 0~10 point Scoring mechanism give the marking of following indices, the sum of overall assessment result=indices score/index quantity, evaluation index has Appearance, smear, moistening effect, toughness.
The measuring method of moisturizing rate: each three parts of cosmetic composition of 2g are accurately weighed, are moved in culture dish, on balance Culture dish, is then put into drier, weighs again after 8 hours by weighing, calculates moisturizing rate.
Moisturizing rate=M2/M1× 100%
M in formula1It is the example weight before placing, M2It is the example weight after placing.
The evaluation result of 1 skin-moisturizing, skin effect of table
Sample Skin sense top SCORES Moisturizing rate
Embodiment 1 7 64%
Embodiment 2 8 72%
Embodiment 3 9 78%
Reference examples 1 6 54%
Reference examples 2 7 50%
Reference examples 3 6 56%
The experimental results showed that, in embodiments of the present invention, the cosmetic composition skin sense of nano-cellulose is added in table 1 Scoring is high, and improves the moisturizing rate of cosmetic composition, and moisture preserving time is long, and soothing effect is significant.
Embodiment 4
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, quinhydrones 2%, arbutin 1.5%, vitamin C 1.5%, glycerin monostearate 2.5%, Hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 59.05%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice) Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 60 DEG C Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, It recycles 3 times, processing pressure 10MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Embodiment 5
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, quinhydrones 2.5%, arbutin 1%, vitamin C 1%, glycerin monostearate 3%, hydrogenation Lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%, Bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence 0.8% and water 48.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice) Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 90 DEG C Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, It recycles 1 time, processing pressure 30MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Embodiment 6
The present embodiment provides a kind of cosmetic composition and its system containing nano-cellulose with whitening spot-removing function Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, quinhydrones 2%, arbutin 1.5%, vitamin C 1.3%, glycerin monostearate 2%, hydrogen Change lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, perfume Essence 0.8% and water 30.63%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with whitening spot-removing function, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, perfume (or spice) Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, add at 75 DEG C Heat of solution stirs evenly, and obtains mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, It recycles 2 times, processing pressure 20MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Reference examples 4
Reference examples of the present embodiment as embodiment 4, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2%, arbutin 1.5%, vitamin C 1.5%, glycerin monostearate 2.5% hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil 1.5%, beeswax 2.5%, double- Ethyl hexyl oxy phenol anisyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 79.05%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid, Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 60 DEG C, stir evenly, Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, Recycled 3 times, processing pressure 10MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 5
Reference examples of the present embodiment as embodiment 5, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2.5%, arbutin 1%, vitamin C 1%, glycerin monostearate 3% hydrogenate lecithin 2%, Buddhist nun's platinum Rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%, double-ethyl hexyl oxy phenol Anisyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence 0.8% and water 78.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid, Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 90 DEG C, stir evenly, Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, Recycled 1 time, processing pressure 30MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 6
Reference examples of the present embodiment as embodiment 6, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Quinhydrones 2%, arbutin 1.5%, vitamin C 1.3%, glycerin monostearate 2% hydrogenate lecithin 2.5%, Buddhist nun Platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax 2%, double-ethyl hexyl oxygen Phenol anisyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, essence 0.8% and water 80.63%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by quinhydrones, arbutin, vitamin C, glycerin monostearate, hydrogenation lecithin, essence, nordihydroguaiaretic acid, Bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, dissolve by heating at 75 DEG C, stir evenly, Obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, Recycled 2 times, processing pressure 20MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
The detection method of whitening spot-removing effect: selection volunteer 40 uses embodiment 4~6 and reference examples 4~6 respectively In cosmetics, using at face's color spot as trial zone, every morning to face's color spot smear, persistently use one month, observe face Portion's Colour patterns situation.
The evaluation result of 2 whitening spot-removing effect of table
The experimental results showed that, in embodiments of the present invention, the cosmetic composition whitening of nano-cellulose is added in table 2 Freckle effect is better than being not added with the cosmetic composition of nano-cellulose, and it is obvious to promote effect to the cosmetics of whitening spot-removing.
Embodiment 7
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 20%, Sodium Hyaluronate 2%, collagen 1.5%, mate leaf extract 2% are single stearic Acid glyceride 2.5% hydrogenates lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, just Dihydro traumatic acid (NDGA) 0.05%, essence 0.6% and water 58.55%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 20000psi, circular treatment 6 times, (quality that metal salt solution is added is cellulose solution quality to addition calcium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization Water mixing, dissolves by heating at 60 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, It recycles 3 times, processing pressure 10MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Embodiment 8
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 30%, Sodium Hyaluronate 1%, collagen 2%, mate leaf extract 2.5% are single stearic Acid glyceride 2%, hydrogenation lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, Olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, essence 0.8% and water 49.93%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 30000psi, circular treatment 3 times, (quality that metal salt solution is added is cellulose solution quality to addition magnesium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization Water mixing, dissolves by heating at 90 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, It recycles 1 time, processing pressure 30MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Embodiment 9
The present embodiment provides a kind of cosmetic compositions and its system containing nano-cellulose with the crease-resistant function of smoothing wrinkle Preparation Method.
The cosmetic composition is made of following raw material by weight percentage:
Nano-cellulose 50%, Sodium Hyaluronate 2%, collagen 2.5%, mate leaf extract 3% are single stearic Acid glyceride 3% hydrogenates lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive Olive oil 1%, beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, essence 0.8% and water 28.52%.
The preparation method of the above-mentioned cosmetic composition containing nano-cellulose with the crease-resistant function of smoothing wrinkle, including it is following Step:
(1) microcrystalline cellulose 1:20 in mass ratio is soluble in water, the homogeneous in high pressure homogenizer, homogenization pressure 25000psi, circular treatment 4 times, (quality that metal salt solution is added is cellulose solution quality to addition sodium chloride solution bridge joint 5%), obtain nano-cellulose gel after centrifugal concentrating.
(2) by nano-cellulose gel, Sodium Hyaluronate, collagen, mate leaf extract, glycerol monostearate Ester, hydrogenation lecithin, essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionization Water mixing, dissolves by heating at 75 DEG C, stirs evenly, obtain mixture A.
(3) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(4) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, It recycles 2 times, processing pressure 20MPa, is cooled to room temperature to get the change containing nano-cellulose is arrived in high pressure homogenizer Cosmetic compositions.
Reference examples 7
Reference examples of the present embodiment as embodiment 7, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 2%, collagen 1.5%, mate leaf extract 2%, glycerin monostearate 2.5%, Hydrogenate lecithin 2.5%, Buddhist nun's platinum rouge 0.7%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3.5%, olive oil 1.5%, beeswax 2.5%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.6%, nordihydroguaiaretic acid (NDGA) 0.05%, essence 0.6% and water 78.55%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 60 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 50 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 60 DEG C, keep the temperature 60min, Recycled 3 times, processing pressure 10MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 8
Reference examples of the present embodiment as embodiment 8, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 1%, collagen 2%, mate leaf extract 2.5%, glycerin monostearate 2%, hydrogen Change lecithin 2.5%, Buddhist nun's platinum rouge 0.5%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 3%, olive oil 2%, beeswax 2%, bis-ethylhexoxyphenol methoxyphenyl triazine 1%, titanium dioxide 0.7%, nordihydroguaiaretic acid (NDGA) 0.07%, perfume Essence 0.8% and water 79.93%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 90 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 80 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 80 DEG C, keep the temperature 30min, Recycled 1 time, processing pressure 30MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
Reference examples 9
Reference examples of the present embodiment as embodiment 9, provide a kind of cosmetic composition without containing nano-cellulose and Preparation method.
The cosmetic composition is made of following raw material by weight percentage:
Sodium Hyaluronate 2%, collagen 2.5%, mate leaf extract 3%, glycerin monostearate 3%, hydrogen Change lecithin 2%, Buddhist nun's platinum rouge 0.8%, sodium acrylate/ethylene isodecyl acid esters cross-linked polymer 4%, olive oil 1%, beeswax 3%, bis-ethylhexoxyphenol methoxyphenyl triazine 1.5%, titanium dioxide 0.8%, nordihydroguaiaretic acid (NDGA) 0.08%, Essence 0.8% and water 75.52%.
The preparation method of the above-mentioned cosmetic composition without containing nano-cellulose, comprising the following steps:
(1) by Sodium Hyaluronate, collagen, mate leaf extract, glycerin monostearate, hydrogenation lecithin, Essence, nordihydroguaiaretic acid, bis-ethylhexoxyphenol methoxyphenyl triazine, titanium dioxide and deionized water mixing, at 75 DEG C It dissolves by heating, stirs evenly, obtain mixture A.
(2) sodium acrylate/ethylene isodecyl acid esters cross-linked polymer, Buddhist nun's platinum rouge, olive oil and beeswax are mixed, at 65 DEG C Lower heating for dissolving, stirs evenly, and obtains mixture B.
(3) it is stirred after mixing mixture A and mixture B, dissolves by heating, stir evenly at 70 DEG C, keep the temperature 45min, Recycled 2 times, processing pressure 20MPa in high pressure homogenizer, be cooled to room temperature to get to described without containing nano-cellulose Cosmetic composition.
The detection method of smoothing wrinkle anti-wrinkle effect: selection volunteer 40 uses embodiment 7~9 and reference examples 7~9 respectively In cosmetics, using at face wrinkles as trial zone, every morning to face wrinkles smear, persistently use one month, observe face Portion's wrinkle situation of change.
The crease-resistant evaluation result of 3 smoothing wrinkle of table
The experimental results showed that, each product is to the improvement degree of facial wrinkles than respectively producing in reference examples in embodiment in table 3 The improvement degree of product will be high, illustrates that the cosmetic composition for being added to nano-cellulose is able to ascend smoothing wrinkle anti-wrinkle effect, right The improvement of wrinkle is significant.
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention, It should be equivalent substitute mode, be included within the scope of the present invention.

Claims (10)

1. a kind of cosmetic composition containing nano-cellulose, it is characterised in that: with the total weight of cosmetic composition, contain There is 20%~50% nano-cellulose, the partial size of nano-cellulose is less than 100nm.
2. the cosmetic composition according to claim 1 containing nano-cellulose, it is characterised in that: the Nanowire The partial size of dimension element is less than 60nm.
3. the cosmetic composition according to claim 1 or 2 containing nano-cellulose, it is characterised in that: described contains The cosmetic composition for having nano-cellulose also includes thickener, emulsifier, antibacterial agent, finish, essence and deionized water, and is wrapped Containing one or more of moisturizer, emollient, sun-screening agent, antioxidant, whitening spot-removing ingredient and the crease-resistant ingredient of smoothing wrinkle.
4. the cosmetic composition according to claim 3 containing nano-cellulose, it is characterised in that:
The moisturizer is one or more of glycerol, propylene glycol, sorbierite and polyethylene glycol；
The emollient is ethylhexyl palmitate, decyl oleate, saualane, phenethyl benzoate, cetanol lactate One or more of with maleic acid ricinolein；
The sun-screening agent is zinc oxide, titanium dioxide, dimethyl PABA ethylhexyl, butylmethoxydibenzoylmethane One or more of with bis-ethylhexoxyphenol methoxyphenyl triazine；
The antioxidant is tert-butyl hydroquinone, in glutamic acid, tocopherol, propylgallate, nordihydroguaiaretic acid (NDGA) One or more；
The whitening spot-removing ingredient is one or more of quinhydrones, arbutin, kojic acid and vitamin C；
The crease-resistant ingredient of the smoothing wrinkle is that Sodium Hyaluronate, collagen, mate leaf extract and rose root of kirilow rhodiola extract One of object is a variety of；
The emulsifier is one of glycerin monostearate, hydrolecithin, lanolin and the smooth olive oleate of sorb Or it is two or more；
The antibacterial agent is one or more of Buddhist nun's platinum rouge, p-hydroxybenzoate, benzyl alcohol, dehydroacetic acid；
The thickener is hydroxyethyl cellulose, carboxymethyl cellulose, sodium alginate, PEG-80 glyceryl butter ester and propylene One or more of sour sodium/ethylene isodecyl acid esters cross-linked polymer；
The finish is one or more of olive oil, stearate, beeswax, silicone oil and vaseline.
5. the cosmetic composition according to claim 4 containing nano-cellulose, it is characterised in that:
The content of the moisturizer is the 1%~5% of cosmetic composition total weight；
The content of the emollient is the 1%~5% of cosmetic composition total weight；
The content of the sun-screening agent is the 0.5%~3% of cosmetic composition total weight；
The content of the antioxidant is the 0.01%~0.1% of cosmetic composition total weight；
The content of the whitening spot-removing ingredient is the 2%~6% of cosmetic composition total weight；
The content of the crease-resistant ingredient of the smoothing wrinkle is the 2~6% of cosmetic composition total weight；
The content of the emulsifier is the 3%~6% of cosmetic composition total weight；
The content of the antibacterial agent is the 0.1%~2% of cosmetic composition total weight；
The content of the thickener is the 2%~5% of cosmetic composition total weight；
The content of the finish is the 2%~5% of cosmetic composition total weight；
The content of the essence is the 0.5%~1% of cosmetic composition total weight.
6. the cosmetic composition according to claim 5 containing nano-cellulose, it is characterised in that:
The content of the emollient is the 2%~4% of cosmetic composition total weight；
The content of the sun-screening agent is the 1.7%~2.3% of cosmetic composition total weight；
The content of the antioxidant is the 0.05%~0.08% of cosmetic composition total weight；
The content of the whitening spot-removing ingredient is the 3%~5% of cosmetic composition total weight；
The content of the crease-resistant ingredient of the smoothing wrinkle is the 3~5% of cosmetic composition total weight；
The content of the emulsifier is the 4%~5% of cosmetic composition total weight；
The content of the antibacterial agent is the 0.5%~0.8% of cosmetic composition total weight；
The content of the thickener is the 3%~4% of cosmetic composition total weight；
The content of the finish is the 3%~4% of cosmetic composition total weight；
The content of the essence is the 0.6%~0.8% of cosmetic composition total weight.
7. the cosmetic composition according to claim 4 containing nano-cellulose, it is characterised in that；By it is following by weight The raw material of percentages forms:
Above-mentioned raw materials weight adds up to 100%；
Or it is made of following raw material by weight percentage:
Above-mentioned raw materials weight adds up to 100%；
Or it is made of following raw material by weight percentage:
Above-mentioned raw materials weight adds up to 100%.
8. the preparation method of the cosmetic composition described in claim 3~7 Arbitrary Term containing nano-cellulose, feature exist In including the following steps:
(1) preparation of nano-cellulose
Microcrystalline cellulose is soluble in water, it is high-pressure homogeneous, cellulose solution is obtained, metal salt solution bridge joint is added, is centrifuged dense Contracting, obtains nano-cellulose gel；
(2) preparation of water phase
By nano-cellulose gel, moisturizer, emollient, whitening spot-removing ingredient, the crease-resistant ingredient of smoothing wrinkle, sun-screening agent, emulsifier, perfume (or spice) Essence, antioxidant and deionized water mixing, dissolve by heating, stir evenly, obtain mixture A；
(3) preparation of oily phase
Thickener, vitamin derivative, antibacterial agent and finish are mixed, is dissolved by heating, is stirred evenly, obtain mixture B；
(4) preparation of cosmetic composition
Mixture A and mixture B is mixed, is stirred evenly, is dissolved by heating, heat preservation, then high pressure or emulsifying homogeneous, it is cooled to room Temperature to get arrive the cosmetic composition containing nano-cellulose.
9. the preparation method of the cosmetic composition according to claim 8 containing nano-cellulose, it is characterised in that:
When described in step (1) that microcrystalline cellulose is soluble in water, the mass ratio of microcrystalline cellulose and water is 1:20；
High-pressure homogeneous pressure described in step (1) be 20000~30000psi, circular treatment 3~6 times；
Metal salt solution described in step (1) is one of calcium chloride solution, magnesium chloride solution and sodium chloride solution or two Kind or more；
The quality that metal salt solution is added described in step (1) is the 3~6% of cellulose solution quality.
10. the preparation method of the cosmetic composition according to claim 8 containing nano-cellulose, it is characterised in that:
The temperature of heating for dissolving described in step (2) is 60~90 DEG C；
The temperature of heating for dissolving described in step (3) is 50~80 DEG C；
The temperature of heating for dissolving described in step (4) is 60~80 DEG C, when a length of 30~60min of heat preservation；
High-pressure homogeneous described in step (4) to be carried out using high pressure homogenizer, pressure is 10~30MPa, is recycled 1~3 time；
Emulsifying homogeneous described in step (4) is carried out using emulsifying homogeneous machine, and temperature is 60 DEG C, recycles 30min.
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