CN107496201A - One kind emulsification lipstick and preparation method thereof - Google Patents
One kind emulsification lipstick and preparation method thereof Download PDFInfo
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- CN107496201A CN107496201A CN201710809836.XA CN201710809836A CN107496201A CN 107496201 A CN107496201 A CN 107496201A CN 201710809836 A CN201710809836 A CN 201710809836A CN 107496201 A CN107496201 A CN 107496201A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses one kind emulsification lipstick and preparation method thereof, belong to cosmetic technical field.Wherein emulsification lipstick includes the component of following percentage by weight：Emollient 51 71%；Curing agent 13 17%；Brightener 4 10%；The isostearate 2 3% of polyglycereol 2 three；Dipentaerythritol trimerization hydroxy stearic acid ester 0.5 1%；Phytosterol/octyl dodecanol lauroyl glutamate ester 2 5%；Water 2 5%；Water soluble humectants 2.01 4.02%；Water soluble plant extract 0.5 2.5%.The present invention uses two kinds of emulsifying agents, coordinates ultrasonic emulsification technique, avoids aqueous phase evaporation from producing bubble, improves yield rate；Make that NMF, cyani flos extract, ginkgo biloba p.e, golden yellow camomile extract can be added in lipstick, desalinate cheilogramma, increase elasticity of skin, effectively exclude toxin, stimulate microcirculation, nutrition skin, widened the function of lipstick；Glycerine, hyaluronic acid, the three's Synergistic of polyquaternium 51, the bionical moisture film of natural skin is formed, make lip skin water profit smooth.
Description
Technical field
The present invention relates to cosmetic technical field, more specifically, it relates to a kind of emulsification lipstick and preparation method thereof.
Background technology
Lipstick is lipstick, one kind of lip rod, is to make lip ruddy glossy, reaches moist, protection lip, it is beautiful to increase face
Sense and amendment lip outline have the product for the effect of setting off.Lipstick or lipstick typically use pure oiliness formula, and common lipstick is typically not
Add moisture.But it is water solubility largely to have the composition of protectiveness to skin or lip, therefore it is difficult to be added to tradition
Lipstick in.Occur the lip gloss or lipstick with certain water content at present, but its water content is general still very low.
A kind of edible natural lipstick of preparing is disclosed in Publication No. CN107049858A Chinese invention patent
Method, comprise the following steps：By two isooctadecanol malates, ethylhexyl palmitate, pentaerythritol tetraoctyl stearate, hydrogen
Change polyisobutene, polyisobutene, ceresin, microwax, avocado oil, macadimia nut oil, lanolin oil, which is put into, to be emulsified in pot, heating
Stir and be warming up to 80~85 DEG C, stir to material and be completely dissolved；Then tocopherol acetate, natural perfume material, natural colour are added
Element, allantoin and preservative, it is 75~80 DEG C to control temperature, stirs to being completely dissolved, obtains mixed material；Material to be mixed
Temperature is reduced to 65-75 DEG C, and mixed material is injected in mould, is cooled to 4-10 DEG C, the demoulding, produces edible natural lipstick.
In above-mentioned lipstick preparation method, because production technology be at 65-75 DEG C it is filling, aqueous phase can largely evaporate, during production
A large amount of steam bubbles can be produced, therefore can not be produced or yield rate is low, cause the function of presently commercially available lipstick to be subject to certain restrictions.
It is, therefore, desirable to provide a kind of new scheme solves the above problems.
The content of the invention
In view of the deficienciess of the prior art, the purpose of the present invention one is to provide a kind of emulsification lipstick, by using poly- sweet
Oily -2 three isostearates and dipentaerythritol three-two kinds of poly- hydroxy stearic acid ester emulsifying agent, coordinate ultrasound at a high temperature of 90 DEG C
Ripple emulsifying process, solves the above problems, and it, which has, eliminates bubble, improves yields, can largely add the advantages of water soluble ingredient.
To achieve the above object one, the invention provides following technical scheme：
One kind emulsification lipstick, include the component of following percentage by weight：
Emollient 51-71%；
Curing agent 13-17%；
Brightener 4-10%；
The isostearate 2-3% of polyglycereol -2 three；
Dipentaerythritol three-poly- hydroxy stearic acid ester 0.5-1%；
Phytosterol/octyl dodecanol lauroyl glutamate ester 2-5%；
Water 2-5%；
Water soluble humectants 2.01-4.02%；
Water soluble plant extract 0.5-2.5%.
Further, the water soluble humectants include glycerine, Sodium Hyaluronate, polyquaternium -51, according to emulsification lipstick
Total amount meter, the glycerine, Sodium Hyaluronate, the percentage by weight of polyquaternium -51 are respectively：1-2%, 0.01-0.02%, 1-2%.
Further, the emollient includes tridecanol trimellitate, Parleam, two isooctadecanol apples
Acid esters, caprylic/capric triglyceride, the more acyl group adipate esters -2 of double-two glycerine, Jojoba (SIMMONDSIA CHINENSIS)
Seed oil, according to the total amount meter of emulsification lipstick, the tridecanol trimellitate, Parleam, two isooctadecanol apples
Acid esters, caprylic/capric triglyceride, the more acyl group adipate esters -2 of double-two glycerine, Jojoba (SIMMONDSIA CHINENSIS)
Seed oil percentage by weight be respectively：18-25%, 15-18%, 8-10%, 6-8%, 2-5%, 2-5%.
Further, the curing agent includes polyethylene, beeswax, according to the total amount meter of emulsification lipstick, the polyethylene, honeybee
The percentage by weight of wax is respectively：10-12%, 3-5%.
Further, the brightener includes VP/ hexadecene copolymers, the poly- trimethyl of diphenyl silicon phenyl
Siloxanes, according to the total amount meter of emulsification lipstick, the VP/ hexadecene copolymers, the poly- front three of diphenyl silicon phenyl
The percentage by weight of radical siloxane is respectively：2-5%, 2-5%.
Further, the emulsification lipstick also includes preservative, colouring agent, described anti-according to the total amount meter of emulsification lipstick
Rotten agent, the percentage by weight of colouring agent are respectively：0.1-1%, 1-10%.
Further, the water soluble plant extract includes corn flower (CENTAUREA CYANUS) flower extract, silver
Any one in apricot (GINKGO BILOBA) leaf extract, golden yellow chamomile (CHRYSANTHELLUM INDICUM) extract.
Corn flower (CENTAUREA CYANUS) flower extract has antiphlogistic antibacterial, calm, releives, instantaneously keeps the skin wet,
Wake up skin vigor, quality is gentle and other effects.Cheilogramma can be desalinated, increase elasticity of skin, effectively exclude toxin, stimulate capilary
Circulation, meets the needs of skin is to nutrient.
Ginkgo (GINKGO BILOBA) flavones contained by leaf extract has strong oxygen radical removing effect, can protect
Shield Skin Cell is not influenceed by oxygen radical over oxidation, so as to extend the life-span of Skin Cell, strengthens the energy of its anti-aging
Power.Lactone in ginkgo biloba p.e can also accelerate metabolism, improve blood circulation, strengthen cell viability, moisturizing, also have
High-efficiency broad spectrum bactericidal action.
Golden yellow chamomile (CHRYSANTHELLUM INDICUM) extract have good Shu Min, maintenance sensitivity skin,
Reduce thin red blood silk, reduce rubescent, the adjustment unequal effect of the colour of skin, chamomile is rich in flavones active component, and the composition has
Anti-oxidant, antiangiogenic, anti-inflammatory, anti-allergy and it is antiviral the effect of.With moisturizing, convergence pore, refrigerant, help skin
The effect of skin tissue regeneration.
The purpose of the present invention two is to provide a kind of preparation method for emulsifying lipstick, this method have eliminate lipstick bubble,
Improve yields, can largely add the advantages of water soluble ingredient.
To achieve the above object two, the invention provides following technical scheme：
A kind of preparation method for emulsifying lipstick, comprises the following steps：
Step 1, by tridecanol trimellitate, Parleam, two isooctadecanol malates, caprylic/capric glycerine
Three esters, the more acyl group adipate esters -2 of double-two glycerine, Jojoba (SIMMONDSIA CHINENSIS) seed oil, polyethylene, beeswax,
VP/ hexadecene copolymers, the poly- trimethicone of diphenyl silicon phenyl, the isostearate of polyglycereol -2 three, two
Polypentaerythritol three-poly- hydroxy stearic acid ester, phytosterol/octyl dodecanol lauroyl glutamate ester, preservative, colouring agent add
Heat to 90 DEG C, heat while stirring, to expect body and pigment dispersion it is uniform, without after obvious granule foreign through examine it is qualified be transferred to it is filling
Machine melt bucket, insulation, form A phases；
Step 2, by water, glycerine, Sodium Hyaluronate, polyquaternium -51, water soluble plant extract, homogeneous mixes at normal temperatures
Uniformly, B phases are formed；
Step 3, well mixed B phases are slowly added into 90 DEG C of A phases, added while stirring, open ultrasound after the entry to be completely
Ripple homogenizer, continuous homogenizing to material body aqueous phase is completely dispersed uniformly, and bubble-free, filling into Rouge mold, cooling and demolding, is obtained
To emulsification lipstick.
Further, it is homogeneous that ultrasonic wave of per half an hour unlatching is also included when filling in the step 3, disperse water
Phase simultaneously eliminates bubble.
Tridecanol trimellitate is a kind of thick and heavy but not sticky liquid, is provided for during low content extraordinary soft
Pad sense, the colorant of up to 60% mass percent can be carried as outstanding colorant dispersant.
Parleam also known as synthesizes saualane, can strengthen maintenance epidermis, is effectively formed natural diaphragm, helps flesh
Balance between skin and sebum.Affinity is strong, can be combined together with the sebum film of mankind itself, and one layer of day is formed in skin surface
Right barrier.The peroxidating of skin lipid can also be suppressed, can effectively infiltrate through skin, and promote the propagation of skin base cell,
Delay skin aging.Blood microcirculation is may additionally facilitate, promotes the metabolism of cell, damaged cell is repaired in help.
Caprylic/capric triglyceride can will not block pore as the base-material of moisturizing factor, and it has non-greasy texture,
There is lubrication and make the soft effect of skin, and had the function of filtering ultraviolet.
Jojoba (SIMMONDSIA CHINENSIS) seed oil is vegetalitas liquid wax, has moisture-keeping efficacy, and can moisten
And soft skin, protective layer can be formed in skin after smearing, and stable skin surface grease, its contained vitamin E can protect flesh
Skin connective tissue, reduce cheilogramma and produce.
Beeswax has very strong tolerance to temperature, is not easy to be influenceed by natural temperature, make the change of preparation as curing agent
Cosmetic keeps application state, the nutrition of beeswax energy and improvement hypodermis situation, activates its elastic fibers, prevents its hardening, promotes
Skin is soft and moist, reduces cheilogramma.
VP/ hexadecene copolymers are dispersed superior to inorganic particle and colouring agent, with mixing for other oil components
Property is good, and oxidation stability is good.
Phytosterol/octyl dodecanol lauroyl glutamate ester forms stratiform liquid crystal structure in skin surface, maintains skin
Barrier function, reach high-quality moistening effect.
Sodium Hyaluronate is the sodium salt of hyaluronic acid, and its theoretical water retention value is up to more than 500ml/g, in connective tissue
Actual water retention value is about 80ml/g.Therefore its distinctive water retention makes that skin is flexible, high resilience；Sufficient moisture makes skin
Smooth delicacy.It can play a part of supplementing and storing moisture of skin using the cosmetics containing hyaluronic acid, recover and keep skin
Youth gloss.Sodium Hyaluronate can be removed in epidermis in sunlight ultraviolet irradiation caused by active oxygen radical, keep
Skin does harm to from it, is referred to as efficient free radical " street cleaner ".Skin is regenerated, repaired simultaneously.
Sodium Hyaluronate belongs to high molecular polymer, has very strong lubrication sense and film forming sense.Skin care containing Sodium Hyaluronate
Lubrication sense is obvious when product are smeared, and feel is good.After being applied to skin, one layer of ventilative hydrated films can be formed in skin surface, made
Skin produces good smooth feeling and moist feeling, and skin is played a protective role, and has repair to damage skin.
Polyquaternium -51 is the artificial cell membrane for imitating cell membrane to design, and is protected than hyaluronic acid with more preferably moisture absorption
It is moist, the moisture of skin can be more pinned, more permanent moist and smooth sense is given, it is good to suppress chapped skin effect.
In summary, the invention has the advantages that：
(1) by adding aqueous phase in being formulated in lipstick, and using the isostearate of polyglycereol -2 three and dipentaerythritol three-poly-
Two kinds of emulsifying agents of hydroxy stearic acid ester, ultrasonic emulsification technique is coordinated at a high temperature of 90 DEG C, can be very good scattered aqueous phase extremely
In oil phase, and stable system is formed, avoid aqueous phase evaporation from producing bubble, improve yield rate；
(2) by ultrasonic technique, can make can to add in lipstick substantial amounts of water soluble humectants, cyani flos extract,
Ginkgo biloba p.e, golden yellow camomile extract, cheilogramma can be desalinated, increase elasticity of skin, effectively exclude toxin, stimulate micro- blood
Pipe circulates, and nutrition skin, has widened the function of lipstick；
(3) glycerine, hyaluronic acid, the three's Synergistic of polyquaternium -51, and the bionical moisture film of natural skin is formed, carry significantly
The high moisture retention of product, makes lip skin water profit smooth.
Brief description of the drawings
Fig. 1 is the process chart of the present invention.
Embodiment
With reference to the accompanying drawings and examples, the present invention will be described in detail.
Embodiment 1：As shown in figure 1, a kind of emulsification lipstick, each component and its corresponding percentage by weight are as shown in table 1,
And acquisition is made by the steps：
Step 1, by tridecanol trimellitate, Parleam, two isooctadecanol malates, caprylic/capric glycerine
Three esters, the more acyl group adipate esters -2 of double-two glycerine, Jojoba (SIMMONDSIA CHINENSIS) seed oil, polyethylene, beeswax,
VP/ hexadecene copolymers, the poly- trimethicone of diphenyl silicon phenyl, the isostearate of polyglycereol -2 three, two
Polypentaerythritol three-poly- hydroxy stearic acid ester, phytosterol/octyl dodecanol lauroyl glutamate ester, preservative, colouring agent add
Heat heats while stirring to 90 DEG C, and mixing speed is 30 revs/min, disperses 4 hours, uniform to material body and pigment dispersion, nothing
Bottle placer melt bucket is transferred to through inspection is qualified after obvious granule foreign, insulation, forms A phases；
Step 2, by water, glycerine, Sodium Hyaluronate, polyquaternium -51, water soluble plant extract, homogeneous mixes at normal temperatures
Uniformly, B phases are formed；
Step 3, well mixed B phases are slowly added into 90 DEG C of A phases, added while stirring, open ultrasound after the entry to be completely
Ripple homogenizer, 30 minutes extremely material body aqueous phases of continuous homogenizing are completely dispersed uniformly, and bubble-free, because aqueous phase volatilization can coagulate during heating
Become the globule, ultrasonic wave of unlatching is homogeneous per half an hour, and scattered aqueous phase simultaneously eliminates bubble, filling into Rouge mold, cold
But it is stripped, obtains emulsifying lipstick.
Wherein preservative is Phenoxyethanol, and colouring agent is CI 15850, and water-soluble extractive is corn flower (CENTAUREA
CYANUS) flower extract.
Embodiment 2-10：One kind emulsification lipstick, is, each component and its corresponding weight with the difference of embodiment 1
Percentage is as shown in table 1.
Each component and its percentage by weight in the embodiment 1-10 of table 1
Embodiment 11-21：One kind emulsification lipstick, is, each component and its corresponding weight percent with the difference of embodiment 3
Than as shown in table 2.
Each component and its percentage by weight in the embodiment 11-21 of table 2
Embodiment 22：One kind emulsification lipstick, is that water soluble plant extract replaces with ginkgo with the difference of embodiment 20
(GINKGO BILOBA) leaf extract.
Embodiment 23：One kind emulsification lipstick, is that water soluble plant extract replaces with the difference of embodiment 20
Golden yellow chamomile (CHRYSANTHELLUM INDICUM) extract.
Comparative example 1：One kind emulsification lipstick, is with the difference of embodiment 3, acquisition is made by the steps：
Step 1, by tridecanol trimellitate, Parleam, two isooctadecanol malates, caprylic/capric glycerine
Three esters, the more acyl group adipate esters -2 of double-two glycerine, Jojoba (SIMMONDSIA CHINENSIS) seed oil, polyethylene, beeswax,
VP/ hexadecene copolymers, the poly- trimethicone of diphenyl silicon phenyl, the isostearate of polyglycereol -2 three, two
Polypentaerythritol three-poly- hydroxy stearic acid ester, phytosterol/octyl dodecanol lauroyl glutamate ester, preservative, colouring agent add
Heat heats while stirring to 90 DEG C, and mixing speed is 30 revs/min, disperses 4 hours, uniform to material body and pigment dispersion, nothing
Bottle placer melt bucket is transferred to through inspection is qualified after obvious granule foreign, insulation, forms A phases；
Step 2, by water, glycerine, Sodium Hyaluronate, polyquaternium -51, water soluble plant extract, homogeneous mixes at normal temperatures
Uniformly, B phases are formed；
Step 3, well mixed B phases are slowly added into 90 DEG C of A phases, added while stirring, it is filling to lipstick after stirring
In mould, cooling and demolding, obtain emulsifying lipstick.
Comparative example 2：One kind emulsification lipstick, is with the difference of embodiment 3, does not add the isostearic acid of polyglycereol -2 three
Ester.
Comparative example 3：One kind emulsification lipstick, is with the difference of embodiment 3, does not add dipentaerythritol three-poly-
Hydroxy stearic acid ester.
Comparative example 4：One kind emulsification lipstick, is with the difference of comparative example 1, does not add the isostearic acid of polyglycereol -2 three
Ester.
Comparative example 5：One kind emulsification lipstick, is with the difference of comparative example 1, does not add dipentaerythritol three-poly-
Hydroxy stearic acid ester.
Comparative example 6：One kind emulsification lipstick, is with the difference of embodiment 3, by the isostearate of polyglycereol -2 three and
Dipentaerythritol three-poly- hydroxy stearic acid ester such as replaces with the cholesterol isostearate of percentage by weight.
Comparative example 7：One kind emulsification lipstick, is, NMF only adds 1% glycerine with the difference of comparative example 3.
Comparative example 8：One kind emulsification lipstick, is, NMF only adds 1% hyaluronic acid with the difference of comparative example 3
Sodium.
Comparative example 9：One kind emulsification lipstick, be with the difference of comparative example 3, NMF only add 1% polyquaternium-
51。
Test a hardness test
Test specimen：Using the emulsification lipstick obtained in embodiment 1-23 as test specimen 1-23, using being obtained in comparative example 1-9
For the emulsification lipstick obtained as control sample 1-9, number consecutively is 1-32 groups.
Test method：Breaking force test is carried out to 1-32 groups sample using ZDY-01 ampoule bottle breakings force tester, often
Three times, lotion hardness takes the average value measured three times to the measurement of group sample.
Result of the test：Test specimen 1-23 and control sample 1-9 lotion hardness test data are as shown in table 3.
The test specimen 1-23 of table 3 and control sample 1-9 lotion hardness test data
Test two outward appearances and yield rate detection
Test specimen：Using the emulsification lipstick obtained in embodiment 1-23 as test specimen 1-23, using being obtained in comparative example 1-9
For the emulsification lipstick obtained as control sample 1-9, number consecutively is 1-32 groups.
Test method：Each 100 of 1-32 group samples are taken successively, detect its blibbing situation, record yield rate.
Result of the test：Test specimen 1-23 and control sample 1-9 testing result are as shown in table 4.With reference to table 3 and table 4, say
The bright present invention uses the isostearate of polyglycereol -2 three and dipentaerythritol three-two kinds of poly- hydroxy stearic acid ester emulsifying agent,
Coordinate ultrasonic emulsification technique at a high temperature of 90 DEG C, can be very good scattered aqueous phase into oil phase, and form stable system, keep away
Exempt from aqueous phase evaporation and produce bubble, strengthen lotion hardness, improve yield rate.
The test specimen 1-23 of table 4 and control sample 1-9 testing result
Test the test of three moistening effects
Test specimen：Using the emulsification lipstick obtained in embodiment 3-8 as test specimen 1-6, using being obtained in comparative example 7-9
Emulsification lipstick as control sample 1-3, using commercially available common lipstick as control sample 4, and number consecutively is 1-10 groups.
Test method：The healthy women crowd case 1000 for randomly selecting 18-35 year of areal is used as subject,
There is the symptoms such as slight drying, furfur, cheilogramma in subject's skin of lip, be randomly divided into 10 groups, every group without allergies
100 people.1-10 groups subject uses test specimen 1-6 and control sample 1-4, application method respectively：After cleaning lip, uniformly
Lips are applied to, twice a day.Record use feeling and effect after subject uses one month.
Result of the test：Use feeling and effect such as table 5 of the 1-10 groups subject to test specimen 1-6 and control sample 1-4
It is shown.As shown in Table 5, glycerine, hyaluronic acid, the three's Synergistic of polyquaternium -51, and form the bionical moisturizing of natural skin
Film, the moisture retention of product is substantially increased, make lip skin water profit smooth.
The test specimen 1-6 of table 5 and control sample 1-4 use feeling and effect
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-described embodiment,
All technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
For those of ordinary skill, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications also should
It is considered as protection scope of the present invention.
Claims (9)
1. one kind emulsification lipstick, it is characterised in that include the component of following percentage by weight：
Emollient 51-71%；
Curing agent 13-17%；
Brightener 4-10%；
The isostearate 2-3% of polyglycereol -2 three；
Dipentaerythritol three-poly- hydroxy stearic acid ester 0.5-1%；
Phytosterol/octyl dodecanol lauroyl glutamate ester 2-5%；
Water 2-5%；
Water soluble humectants 2.01-4.02%；
Water soluble plant extract 0.5-2.5%.
2. emulsification lipstick according to claim 1, it is characterised in that the water soluble humectants include glycerine, hyalomitome
Sour sodium, polyquaternium -51, according to the total amount meter of emulsification lipstick, the glycerine, Sodium Hyaluronate, the weight hundred of polyquaternium -51
Point ratio is respectively：1-2%、0.01-0.02%、1-2%.
3. emulsification lipstick according to claim 2, it is characterised in that the emollient includes tridecanol trimellitic acid
Ester, Parleam, two isooctadecanol malates, caprylic/capric triglyceride, the more acyl group adipate esters of double-two glycerine-
2nd, Jojoba（SIMMONDSIA CHINENSIS）Seed oil, according to the total amount meter of emulsification lipstick, the tridecanol trimellitic acid
Ester, Parleam, two isooctadecanol malates, caprylic/capric triglyceride, the more acyl group adipate esters of double-two glycerine-
2nd, Jojoba（SIMMONDSIA CHINENSIS）Seed oil percentage by weight be respectively：18-25%、15-18%、8-10%、6-
8%、2-5%、2-5%。
4. emulsification lipstick according to claim 3, it is characterised in that the curing agent includes polyethylene, beeswax, according to breast
Change the total amount meter of lipstick, the polyethylene, the percentage by weight of beeswax are respectively：10-12%、3-5%.
5. emulsification lipstick according to claim 4, it is characterised in that the brightener include VP/ hexadecene copolymers,
The poly- trimethicone of diphenyl silicon phenyl, according to the total amount meter of emulsification lipstick, the VP/ hexadecenes copolymerization
Thing, the percentage by weight of the poly- trimethicone of diphenyl silicon phenyl are respectively：2-5%、2-5%.
6. emulsification lipstick according to claim 5, it is characterised in that the emulsification lipstick also includes preservative, colouring agent,
According to the total amount meter of emulsification lipstick, the preservative, the percentage by weight of colouring agent are respectively：0.1-1%、1-10%.
7. emulsification lipstick according to claim 6, it is characterised in that the water soluble plant extract includes corn flower
（CENTAUREA CYANUS）Flower extract, ginkgo（GINKGO BILOBA）Leaf extract, golden yellow chamomile
（CHRYSANTHELLUM INDICUM）Any one in extract.
8. a kind of preparation method for emulsifying lipstick, it is characterised in that comprise the following steps：
Step 1, by tridecanol trimellitate, Parleam, two isooctadecanol malates, caprylic/capric glycerine
Three esters, the more acyl group adipate esters -2 of double-two glycerine, Jojoba（SIMMONDSIA CHINENSIS）Seed oil, polyethylene, beeswax,
VP/ hexadecene copolymers, the poly- trimethicone of diphenyl silicon phenyl, the isostearate of polyglycereol -2 three, two
Polypentaerythritol three-poly- hydroxy stearic acid ester, phytosterol/octyl dodecanol lauroyl glutamate ester, preservative, colouring agent add
Heat to 90 DEG C, heat while stirring, to expect body and pigment dispersion it is uniform, without after obvious granule foreign through examine it is qualified be transferred to it is filling
Machine melt bucket, insulation, form A phases；
Step 2, by water, glycerine, Sodium Hyaluronate, polyquaternium -51, water soluble plant extract, homogeneous mixes at normal temperatures
Uniformly, B phases are formed；
Step 3, well mixed B phases are slowly added into 90 DEG C of A phases, added while stirring, open ultrasound after the entry to be completely
Ripple homogenizer, continuous homogenizing to material body aqueous phase is completely dispersed uniformly, and bubble-free, filling into Rouge mold, cooling and demolding, is obtained
To emulsification lipstick.
9. the preparation method of emulsification lipstick according to claim 8, it is characterised in that also wrapped when filling in the step 3
It is homogeneous to include ultrasonic wave of per half an hour unlatching, disperses aqueous phase and simultaneously eliminates bubble.
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| CN201710809836.XA CN107496201A (en) | 2017-09-09 | 2017-09-09 | One kind emulsification lipstick and preparation method thereof |
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| CN201710809836.XA CN107496201A (en) | 2017-09-09 | 2017-09-09 | One kind emulsification lipstick and preparation method thereof |
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| CN107997992A (en) * | 2017-12-29 | 2018-05-08 | 广州慈康生物科技有限公司 | A kind of velvet lipstick of plentiful lip and preparation method thereof |
| CN108578262A (en) * | 2018-03-30 | 2018-09-28 | 浙江工业大学 | A kind of production method of the moisturizing lipstick containing alkannin liposome |
| CN108578274A (en) * | 2018-08-02 | 2018-09-28 | 高宝化妆品（中国）有限公司 | A kind of aqueous lipstick and preparation method thereof |
| CN109044893A (en) * | 2018-11-02 | 2018-12-21 | 花安堂生物科技集团有限公司 | A kind of solid water-in-oil composition and preparation method thereof |
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| CN109125188B (en) * | 2018-10-30 | 2021-05-25 | 广州艾蓓生物科技有限公司 | Lipstick with lip plumping effect and preparation method thereof |
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Application publication date: 20171222 |