CN112168732A - Matte velvet lipstick and preparation method thereof - Google Patents

Matte velvet lipstick and preparation method thereof Download PDF

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Publication number
CN112168732A
CN112168732A CN202011207999.9A CN202011207999A CN112168732A CN 112168732 A CN112168732 A CN 112168732A CN 202011207999 A CN202011207999 A CN 202011207999A CN 112168732 A CN112168732 A CN 112168732A
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percent
matte
velvet
lipstick
agent
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CN202011207999.9A
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Inventor
田贵丰
王光灿
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Guangzhou Baoyan Biotech Co ltd
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Guangzhou Baoyan Biotech Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The invention relates to a matte velvet lipstick which comprises the following components in percentage by mass: adhesive: 12% -18%; film-forming agent: 3% -5%; and (3) an emollient: 50% -60%; skin feel modifier: 5% -8%; colorant: 8% -13%; filling agent: 4% -10%; aromatic agent: 0.02% -0.1%; skin conditioner: 0.05-0.1 percent. When the matte velvet lipstick is used, the film forming agent and the skin feel regulator can quickly form a protective film on the surface of lips, so that the matte velvet lipstick has a protective effect, has the advantages of difficult makeup removal and excellent color fixing effect, and has the effects of moisturizing, moistening skin, resisting aging and the like.

Description

Matte velvet lipstick and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, in particular to matte velvet lipstick and a preparation method thereof.
Background
The lipstick is a common lip makeup product, can provide beautiful color for lips, makes the lips beautiful and attractive, and plays a role in drawing dragon and striking eyes for facial makeup.
At present, the lipstick on the market is various, wherein the matte lipstick is widely used; however, the existing matte lipstick has a plurality of problems in the using process; for example, currently, matte lipstick on the market generally only focuses on beauty, but neglects health care and maintenance of lips of users, so that the matte lipstick not only has beautifying function, but also has health effects of moisturizing, moistening skin, resisting aging and the like, and lips are easy to crack, peel and be sensitive after long-term use. In addition, the current matte lipstick has too long film forming time when in use and is easy to decolorize and remove makeup in the use process.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the matte velvet lipstick and the preparation method thereof, when in use, the film forming agent and the skin feeling modifier can quickly form a protective film on the surface of lips, so that the matte velvet lipstick has a protective effect, has the advantages of difficult make-up removal and excellent color fixing effect, and simultaneously has the effects of moisturizing, moistening skin, resisting aging and the like.
The technical purpose of the invention is realized by the following technical scheme: the matte velvet lipstick comprises the following components in percentage by mass: adhesive: 12% -18%; film-forming agent: 3% -5%; and (3) an emollient: 50% -60%; skin feel modifier: 5% -8%; colorant: 8% -13%; filling agent: 4% -10%; aromatic agent: 0.02% -0.1%; skin conditioner: 0.05-0.1 percent.
Further, the paint comprises the following components in percentage by mass: adhesive: 16 percent; film-forming agent: 4 percent; and (3) an emollient: 51.8 percent; skin feel modifier: 7 percent; colorant: 11 percent; filling agent: 10 percent; aromatic agent: 0.1 percent; skin conditioner: 0.1 percent; the film forming agent is trimethylsiloxy silicate.
Further, the skin feel modifier is a composition of polydimethylsiloxane and a polydimethylsiloxane cross-linked polymer; the content of the polydimethylsiloxane and the polydimethylsiloxane cross-linked polymer is 2% and 5%, respectively.
Further, the skin conditioner is at least one of fullerene, phytosterol and olive oil ceramide.
Further, the emollient is at least one of isopropyl palmitate, isooctyl palmitate, isopropyl myristate, polybutene, sorbitan oleate, caprylic/capric triglyceride, neopentyl glycol diheptanoate, hydrogenated polyisobutene, pentaerythritol tetraisostearate, octyldodecanol, isononyl isononanoate, tridecanol trimellitate, isohexadecane, and di-diglycerol polyacyladipic acid.
Further, the adhesive is at least one of ceresin wax, polyethylene and microcrystalline wax.
Further, the colorant is at least one of iron oxide, yellow No. 6 and red No. 7.
Further, the filler is at least one of HDI/trihydroxymethyl hexyl lactone cross-linked polymer, MICA and boron nitride.
Further, the aromatic is at least one of edible raspberry flavor and vanilla essence.
The application also provides a preparation method of the matte velvet lipstick, which comprises the following steps:
(1) mixing the adhesive and the emollient, heating to 90-100 ℃ until the adhesive and the emollient are completely dissolved, sequentially adding the skin feel modifier, the film-forming agent and the filler, heating and stirring until the mixture is uniformly mixed to obtain a mixture A;
(2) adding a coloring agent into the mixture A, and uniformly grinding to obtain a mixture B;
(3) adding a fragrance and a skin conditioner to the mixture B to obtain the matte velvet lipstick.
In conclusion, the invention has the following beneficial effects:
1. when the matte velvet lipstick is used, the film forming agent and the skin feel regulator can quickly form a protective film on the surface of lips, so that the matte velvet lipstick has a protective effect, has the advantages of difficult makeup removal and excellent color fixing effect, and has the effects of moisturizing, moistening skin, resisting aging and the like.
2. The polydimethylsiloxane and the polydimethylsiloxane cross-linked polymer adopted by the lipstick color fixing agent can further accelerate the time of forming a protective film on lips by trimethylsiloxysilicate when being used as a skin regulator, and can also keep the stability of the trimethylsiloxysilicate on the lips, so that the color fixing effect of the lipstick color fixing agent is more durable.
3. The emollient that this application adopted can thin the lip line, restores the impaired cortex of lip skin, makes lip skin keep moist smooth elasticity, and anti-aging effect is showing.
Detailed Description
In order to make the objects, technical solutions and advantages of the present application more apparent, the present application is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the present application and are not intended to limit the present application.
Example 1:
a matte velvet lipstick comprises the following components (in percentage by weight):
adhesive: and (3) ceresin wax: 5 percent; polyethylene: 5 percent; microcrystalline wax: 6 percent;
film-forming agent: trimethylsiloxy silicate: 4 percent;
and (3) an emollient: isopropyl palmitate: 15 percent; isopropyl myristate: 10 percent; polybutylene: 5 percent; pentaerythritol tetraisostearate: 6 percent; sorbitan oleate: 2 percent; neopentyl glycol diheptanoate: 9 percent; octyl dodecanol: 2.9; isohexadecane: 2 percent;
skin feel modifier: polydimethylsiloxane: 2 percent; polydimethylsiloxane crosslinked polymer: 5 percent;
colorant: iron oxide: 3 percent; yellow No. 6: 2 percent; red No. 7: 6 percent;
filling agent: HDI/trimethylolhexyllactone crosspolymer: 2.95 percent; MICA: 3 percent; boron nitride: 4 percent;
aromatic agent: edible raspberry flavor: 0.05 percent;
skin conditioner: fullerene: 0.1 percent.
The preparation method of the matte velvet lipstick comprises the following steps:
(1) adding ceresin, polyethylene, microcrystalline wax, isopropyl palmitate, isopropyl myristate, polybutene, pentaerythritol tetraisostearate, sorbitan oleate, neopentyl glycol diheptanoate and octyl dodecanol into a stirring pot, heating to 100 ℃ until the materials are completely dissolved, independently dissolving polydimethylsiloxane, polydimethylsiloxane cross-linked polymer and isohexadecane, adding the mixture into the stirring pot, sequentially adding trimethylsiloxy silicate, HDI/trimethylol hexyl lactone cross-linked polymer, MICA and boron nitride, and uniformly mixing to obtain a mixture A;
(2) adding iron oxide, yellow No. 6 and red No. 7 into the mixture A, and uniformly grinding to obtain a mixture B;
(3) adding edible raspberry flavor and fullerene peel into mixture B, and stirring uniformly to obtain the matte velvet lipstick of example 1.
Example 2:
a matte velvet lipstick comprises the following components (in percentage by weight):
adhesive: and (3) ceresin wax: 4 percent; polyethylene: 6 percent; microcrystalline wax: 6 percent;
film-forming agent: trimethylsiloxy silicate: 5 percent;
and (3) an emollient: isopropyl palmitate: 14 percent; isopropyl myristate: 8 percent; polybutylene: 7 percent; pentaerythritol tetraisostearate: 6.5 percent; sorbitan oleate: 1.5 percent; neopentyl glycol diheptanoate: 6 percent; octyl dodecanol: 5.9; isohexadecane: 2 percent;
skin feel modifier: polydimethylsiloxane: 2 percent; polydimethylsiloxane crosslinked polymer: 5 percent;
colorant: iron oxide: 2.5 percent; yellow No. 6: 2.5 percent; red No. 7: 6 percent;
filling agent: HDI/trimethylolhexyllactone crosspolymer: 2.95 percent; MICA: 2.5 percent; boron nitride: 4.5 percent;
aromatic agent: vanilla flavor: 0.05 percent;
skin conditioner: phytosterol: 0.1 percent.
The preparation method of the matte velvet lipstick comprises the following steps:
(1) adding ceresin, polyethylene, microcrystalline wax, isopropyl palmitate, isopropyl myristate, polybutene, pentaerythritol tetraisostearate, sorbitan oleate, neopentyl glycol diheptanoate and octyldodecanol into a stirring pot, heating to 100 ℃ until the materials are completely dissolved, separately dissolving polydimethylsiloxane, polydimethylsiloxane cross-linked polymer and isohexadecane, adding the mixture into the stirring pot, sequentially adding trimethylsiloxy silicate, HDI/trimethylol hexyl lactone cross-linked polymer, MICA and boron nitride, and uniformly mixing to obtain a mixture A;
(2) adding iron oxide, yellow No. 6 and red No. 7 into the mixture A, and uniformly grinding to obtain a mixture B;
(3) then, the vanilla flavor and the phytosterol were added to the mixture B and stirred uniformly to obtain the matte velvet lipstick of example 2.
Example 3:
a matte velvet lipstick comprises the following components (in percentage by weight):
adhesive: and (3) ceresin wax: 5.5 percent; polyethylene: 4.5 percent; microcrystalline wax: 6 percent;
film-forming agent: trimethylsiloxy silicate: 4 percent;
and (3) an emollient: isopropyl palmitate: 12 percent; isopropyl myristate: 13 percent; polybutylene: 8 percent; pentaerythritol tetraisostearate: 3 percent; sorbitan oleate: 2.5 percent; neopentyl glycol diheptanoate: 8.5 percent; octyl dodecanol: 2.9; isohexadecane: 2 percent;
skin feel modifier: polydimethylsiloxane: 2 percent; polydimethylsiloxane crosslinked polymer: 4.8 percent;
colorant: iron oxide: 3 percent; yellow No. 6: 2 percent; red No. 7: 6 percent;
filling agent: HDI/trimethylolhexyllactone crosslinked polymer: 2.95 percent; MICA: 3.7 percent; boron nitride: 3.5 percent;
aromatic agent: vanilla flavor: 0.05 percent;
skin conditioner: olive oil ceramide: 0.1 percent.
The preparation method of the matte velvet lipstick comprises the following steps:
(1) adding ceresin, polyethylene, microcrystalline wax, isopropyl palmitate, isopropyl myristate, polybutene, pentaerythritol tetraisostearate, sorbitan oleate, neopentyl glycol diheptanoate and octyldodecanol into a stirring pot, heating to 100 ℃ until the materials are completely dissolved, separately dissolving polydimethylsiloxane, polydimethylsiloxane cross-linked polymer and isohexadecane, adding the mixture into the stirring pot, sequentially adding trimethylsiloxy silicate, HDI/trimethylol hexyl lactone cross-linked polymer, MICA and boron nitride, and uniformly mixing to obtain a mixture A;
(2) adding iron oxide, yellow No. 6 and red No. 7 into the mixture A, and uniformly grinding to obtain a mixture B;
(3) then, vanilla flavor and olive oil ceramide were added to the mixture B and stirred uniformly to obtain the matte velvet lipstick of example 3.
The matte velvet lipstick prepared in the examples 1 to 3 is subjected to performance test, and the specific test results are shown in the following table 1:
table 1:
Figure BDA0002757667260000061
Figure BDA0002757667260000071
as can be seen from the test results in Table 1, the matte velvet lipstick has the advantages of no abnormal appearance, cold resistance and heat resistance, good stability under high-temperature and low-temperature conditions, and no makeup removal phenomenon at higher temperature.
Comparative examples 1 to 4:
comparative example 1 trimethylsiloxysilicate was not added, and other ingredients and preparation methods were the same as in example 1.
Comparative example 2 no polydimethylsiloxane was added and the other ingredients and preparation method were the same as in example 1.
Comparative example 3 no polydimethylsiloxane crosspolymer was added, and the other ingredients and preparation method were the same as in example 1.
Comparative example 4 is a commercial matte velvet lipstick.
To better illustrate the beneficial effects of the present invention, efficacy evaluation tests were performed on the silky moist matte lipstick prepared in the above examples and comparative examples:
since the majority of users of lipstick are women, 140 female volunteers were selected, the age was between 20 and 50 years, and all volunteers had no history of skin allergy. All volunteers can use the product according to the standard, only use the appointed lipstick in the test process, and cooperate with the staff to finish the evaluation work according to the requirement, have certain expression ability, can really reflect the feeling after using.
The test method comprises the following steps: 20 volunteers were randomly drawn for each example and comparative example and blinded. The corresponding lipstick is selected and evenly smeared on the lips, and the lip color matte degree, the moistening degree and the color fixing effect are observed and scored after 5min, 1 hour and 5 hours of volunteers of each group.
The comprehensive evaluation standard is 5 points, the worst is 1 point, and the best is 5 points, the evaluation result is the average point of all the volunteers, and the higher the average point is, the better the effect is.
The test results are specifically shown in the following tables 3-1, 3-2, 3-3 and 4.
TABLE 3-1 test results after 5 min:
numbering Matte finish Moistening degree Color fixing effect
Example 1 4.8 3.8 5.0
Example 2 4.3 3.4 4.5
Example 3 4.5 3.5 4.3
Comparative example 1 2.8 2.8 2.9
Comparative example 2 3.2 3.0 3.2
Comparative example 3 3.5 3.2 3.4
Comparative example 4 3.0 2.5 3.0
Table 3-2 test results after 1 hour:
Figure BDA0002757667260000081
Figure BDA0002757667260000091
tables 3-3 test results after 5 hours:
numbering Matte finish Moistening degree Color fixing effect
Example 1 4.1 4.8 4.3
Example 2 3.7 4.3 4.0
Example 3 3.8 4.4 3.9
Comparative example 1 1.8 3.5 2.0
Comparative example 2 2.4 3.8 2.3
Comparative example 3 2.2 4.0 2.2
Comparative example 4 2.0 3.5 2.0
Analysis of tables 3-1 shows that the lipsticks prepared in examples 1-3 of the present application have a significant color fixing effect within 5min compared to the lipsticks prepared in comparative examples 1-4, and thus, the scheme of the present application, in which trimethylsiloxysilicate, polydimethylsiloxane, and polydimethylsiloxane cross-linked polymer are added, enables the lipsticks of the present application to rapidly form a protective film on the surface of lips during use, thereby playing a role in protection, and enabling the lipsticks of the present application to have a significant color fixing effect during use.
In contrast, in comparative examples 1 to 3, when only one of trimethylsiloxysilicate, polydimethylsiloxane, and polydimethylsiloxane crosslinked polymer was added, both matte degree and color fixing effect were significantly reduced in use; it can be seen that the trimethylsiloxysilicate, polydimethylsiloxane, and polydimethylsiloxane crosslinked polymers used in the embodiments of the present application have a synergistic effect. The solution of the present application does not belong to a simple substitution between the components.
The polydimethylsiloxane and the polydimethylsiloxane cross-linked polymer adopted by the lipstick can be used as a skin regulator, and meanwhile, the time of forming a protective film on lips by trimethylsiloxysilicate can be further shortened, the protective film can be formed within 5min, and the color fixing effect of lipstick is further improved.
As can be seen from the analysis of tables 3-2 and 3-3, the lipsticks of examples 1-3 still had excellent fixation effects after 5 hours of use; therefore, when the lipstick is used, the polydimethylsiloxane and the polydimethylsiloxane cross-linked polymer can accelerate the time of forming the protective film on the lips by the trimethylsiloxysilicate, and can also maintain the stability of the trimethylsiloxysilicate on the lips, so that the color fixing effect of the lipstick is more durable.
The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims (10)

1. The matte velvet lipstick is characterized by comprising the following components in percentage by mass: adhesive: 12% -18%; film-forming agent: 3% -5%; and (3) an emollient: 50% -60%; skin feel modifier: 5% -8%; colorant: 8% -13%; filling agent: 4% -10%; aromatic agent: 0.02% -0.1%; skin conditioner: 0.05-0.1 percent.
2. The matte velvet lipstick according to claim 1, which is characterized by comprising the following components in percentage by mass: adhesive: 16 percent; film-forming agent: 4 percent; and (3) an emollient: 51.8 percent; skin feel modifier: 7 percent; colorant: 11 percent; filling agent: 10 percent; aromatic agent: 0.1 percent; skin conditioner: 0.1 percent; the film forming agent is trimethylsiloxy silicate.
3. Matte-velvet lipstick according to claim 1 or 2, characterized in that said skin feel modifier is a combination of polydimethylsiloxane and polydimethylsiloxane crosspolymer; the content of the polydimethylsiloxane and the polydimethylsiloxane cross-linked polymer is 2% and 5%, respectively.
4. The matte-velvet lipstick according to claim 1 or 2, characterized in that the skin conditioning agent is at least one of fullerene, phytosterol, olive oil ceramide.
5. The matte-velvet lipstick according to claim 1 or 2, characterized in that the emollient is at least one of isopropyl palmitate, isooctyl palmitate, isopropyl myristate, polybutene, sorbitan oleate, caprylic/capric triglyceride, neopentyl glycol diheptanoate, hydrogenated polyisobutene, pentaerythritol tetraisostearate, octyldodecanol, isononyl isononanoate, tridecyl alcohol trimellitate, isohexadecane, bis-diglycerol polyacyladipic acid.
6. The matte velvet lipstick according to claim 1 or 2, characterized in that the binder is at least one of ozokerite, polyethylene, microcrystalline wax.
7. Matte-velvet lipstick according to claim 1 or 2, characterized in that the colorant is at least one of iron oxide, yellow No. 6, Red No. 7.
8. The matte velvet lipstick according to claim 1 or 2, characterized in that the filler is at least one of HDI/trimethylol hexyl lactone crosspolymer, MICA, boron nitride.
9. The matte velvet lipstick according to claim 1 or 2, wherein the aromatic is at least one of edible raspberry flavor and vanilla extract.
10. A process for the preparation of a matte-velvet lipstick according to any one of claims 1 to 9, comprising the following steps:
(1) mixing the adhesive and the emollient, heating to 90-100 ℃ until the adhesive and the emollient are completely dissolved, sequentially adding the skin feel modifier, the film-forming agent and the filler, heating and stirring until the mixture is uniformly mixed to obtain a mixture A;
(2) adding a coloring agent into the mixture A, and uniformly grinding to obtain a mixture B;
(3) adding a fragrance and a skin conditioner to the mixture B to obtain the matte velvet lipstick.
CN202011207999.9A 2020-11-03 2020-11-03 Matte velvet lipstick and preparation method thereof Pending CN112168732A (en)

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Application publication date: 20210105