CN107970138B - Not de- adornment BB frost of a kind of g., jelly-like and preparation method thereof - Google Patents
Not de- adornment BB frost of a kind of g., jelly-like and preparation method thereof Download PDFInfo
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- CN107970138B CN107970138B CN201711276637.3A CN201711276637A CN107970138B CN 107970138 B CN107970138 B CN 107970138B CN 201711276637 A CN201711276637 A CN 201711276637A CN 107970138 B CN107970138 B CN 107970138B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
Abstract
The present invention provides a kind of not de- adornment BB frosts of g., jelly-like, it contains following each component: sodium metasilicate magnesium lithium, polymeric rheology regulator, emulsifier pre-process colorant slurry, macromolecule film former, polyol humectant, moisturizing grease, deionized purified water, wherein, the polymeric rheology regulator is at least two in following polymer: (A) acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen copolymer sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum.BB frost provided by the invention is easy to apply, hides that lump in the abdomen effect is good, and dressing does not spend adornment for sustainable 8 hours or more naturally, endurance is strong, and long-time service is not in the skin problems such as the obscure, comedo and acne of skin, and user's evaluation is good.
Description
Technical field
The invention belongs to cosmetic technical fields, and in particular to not de- adornment BB frost of a kind of g., jelly-like and preparation method thereof.
Background technique
The effect of BB is white, has both foundation cream, sun-proof and isolated product due to it, is increasingly pursued and is become by the women that likes to be beautiful
Fashion trend.
BB frost (Blemish Blam) is initially the German patients design for artificially receiving laser surgery originating from Germany,
Quality is more thick and heavy, contains skin care and sun-prevention component, and impaired skin can be made to obtain repairing and regeneration, after drawn by South Korea's cosmetics circle
Into after improveing and developing, just becoming daily use chemicals cosmetics from medicine cosmetics, and be evolved into collection concealing, isolation, anti-
Shine, repair the single-item of the functions such as face, bottom adornment.
Existing BB frost is all the emulsification system of Water-In-Oil on the market, is mutually to form stabilization by emulsifier with water phase by oily
System.But emulsification system is affected by external environment such as temperature and air pressure, biggish temperature change may be destroyed
The stabilization of emulsification system the phenomenon that demulsification, shows as emulsification system and apparent layering occurs, and then influence the extension of BB frost
Property and stability.Although the water-tolerant of water-in-oil type BB frost, because human body can secrete sweat, dressing is easily broken
It is bad, it needs to repeat to refine the make-up, generates inconvenience；Skin sense simultaneously is more thick and heavy, and poor air permeability easily causes the skins such as comedo and acne
Problem.
In order to improve the thick and heavy skin sense of water-in-oil system itself, makeup formulators have done various trials to improve BB frost
Usage experience sense.Part commercial product guarantees the salubrious skin sense of BB frost by adding a large amount of volatility greases, but this kind of production
Product can allow a very big consumer to feel too dry and astringent, and moisture feeling is inadequate, and dressing persistence is poor.There are also some products in order to chase after
Ask it is superpower it is permanent hold adornment effect, be added to a large amount of macromolecule film former in formula, but this kind of product must cooperate and make
With the extremely strong makeup remover of makeup removing power or make-up remover, this kind of product easilys lead to that the comedo and acne colour of skin is dark yellow or even the skins such as allergy
Problem.People need a salubrious and lasting BB frost product, but this is a huge technological challenge for formulator.
Through retrieving, with patent document record solve the above problems have following several method: such as Chinese patent application
201410425432.7 " a kind of BB frosts and preparation method thereof with long-lasting moisturization " disclose one kind by organic matter such as ring
Five dimethyl silicone polymers, different tridecanol isononoate etc. and inorganic matter stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide
A kind of black equal manufactured BB frost with long-lasting moisturization.The BB frost skin sense is fine and smooth, frivolous and ventilative, moistening effect is small up to eight
When, skin water content of stratum corneum can be dramatically increased, realizes that adornment is not floated in long-time moisturizing.But the product as made from the patent adds
Enter a large amount of macromolecule organic, it must be with the use of the extremely strong makeup remover of makeup removing power or make-up remover, this kind of production in cleaning
Product easily lead to that comedo and acne, the colour of skin be dark yellow or even the skin problems such as allergy.
For another example, Chinese patent application 201110127193.3 " a kind of BB frost and preparation method thereof " discloses one kind with gel
For substrate, the frost of BB made of dispersing agent and BB frost particle is added.Wherein, BB frost particle is to embed capsule and titanium white whitening by BB frost
Two kinds of BB frost particles of capsule, and then the technical problem that the BB frost for solving emulsification dosage form now is unstable, oil-containing is excessive.But the BB
BB frost particle in frost is by being applied to skin surface after the extruding of pump head, dispersion with powdered, and there are still skin sense is poor
Problem.
For to sum up, BB frost disclosed in the prior art can not meet moisturizing, the lasting, easy cleaning of dressing etc. simultaneously to be wanted
It asks, and then various skin problems can be caused to user.
Summary of the invention
One of goal of the invention of the application is that BB frost moisture feeling in the prior art is poor, dressing persistence in order to solve
Difference, requires cleaning supplies high, easily causes comedo and acne, the colour of skin dark yellow or even the skin problems such as allergy, provides a kind of g., jelly-like
The BB frost of not de- adornment.
Another goal of the invention of the application is to provide the preparation method of above-mentioned BB frost.
In order to achieve the above-mentioned object of the invention, the technical solution of the application provides a kind of BB of not de- adornment of g., jelly-like
Frost contains following each component:
Sodium metasilicate magnesium lithium,
Polymeric rheology regulator,
Emulsifier,
Colorant slurry is pre-processed,
Macromolecule film former,
Polyol humectant,
Moisturizing grease,
Deionized purified water,
Wherein, the polymeric rheology regulator is at least two in following polymer: (A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer, such as commercial goods PemulenTMTR-2 polymer and PemulenTMTR-1 polymerization
Object；(B) carbomer sodium；(C) agarose gel, if commercial product is the SeapureAgarose that Lonza company produces；(D) propylene
Sour (ester) class/acryloyl nitrogen copolymer sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum, such as city
Sell commodity PC806.
Preferably, the ratio of the sodium metasilicate magnesium lithium and polymeric rheology regulator is 1 weight % to 30 weight %；
It is further preferred that the ratio of the sodium metasilicate magnesium lithium and polymeric rheology regulator is 1 weight % to 20 weights
Measure %；
It is further preferred that the ratio is 5 weight % to 20 weight %；More preferably 12 weight % to 20 weight %,
Such as 12 weight %, 15 weight %, 18 weight %, 20 weight %.
Wherein, sodium metasilicate magnesium lithium often claims lithium magnesium silicate, is called hectorite, has nano microcrystalline structure, disperses shape in water
At the colorless and transparent thixotropy gel of nanometer；Commercially available typical products have Laponite series of products, and Laponite can contain with most of
The thickener compatibility that aqueous systems use.
Preferably, the additive amount of the sodium metasilicate magnesium lithium is 0.05-1.0 parts by weight.
Preferably, the polymeric rheology regulator is at least two in following polymer: (A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen
Copolymer sodium；
Preferably, described (A) acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer additive amount is 0.1-
0.8 parts by weight；Further preferably 0.1-0.7 parts by weight；It is further preferably 0.1-0.6 parts by weight, such as 0.1 part, 0.15
Part, 0.2 part, 0.3 part, 0.5 part, 0.6 part；
Preferably, the additive amount of described (B) the carbomer sodium is 0.01-0.5 parts by weight；Further preferably 0.05-0.5 weight
Measure part；It is further preferably 0.1-0.5 parts by weight, such as 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part；
Preferably, the additive amount of described (C) agarose gel is 0.01-0.2 parts by weight；Further preferably 0.05-0.2
Part；It is further preferably 0.05-0.18 parts, such as 0.05 part, 0.08 part, 0.1 part, 0.15 part, 0.18 part；
Preferably, described (D) acrylic acid (ester) class/acryloyl nitrogen copolymer sodium additive amount is 0.01-0.5 parts by weight；
Further preferably 0.05-0.5 parts by weight；It is further preferably 0.1-0.5 parts by weight, such as 0.1 part, 0.2 part, 0.3 part,
0.4 part, 0.5 part；
It is further preferred that the polymeric rheology regulator is the combination of following polymer: (A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen
Copolymer sodium；
It is further preferred that the additive amount of the polymeric rheology regulator is 0.5-2.0 parts by weight.
The formula system provided as polymeric rheology regulator is combined with stronger by above-mentioned polymer A, B, C, D
Pseudoplastic behavior, i.e. water moisten jelly sense appearance, are compounded by above-mentioned each polymer with the effective of sodium metasilicate magnesium lithium, can overcome inorganic matter
Partially dry and astringent skin sense caused by formula, while avoiding the excessive sticky sense of discomfort of high molecular polymer bring.
Preferably, the polymeric rheology regulator is following polymer: (E) Scleroglucan；(F) mosanom, cellulose,
The compound of cellulose gum；The combination can provide stronger suspendability, prevent the aggregation of powder class raw material from sinking；
Preferably, the additive amount of described (E) Scleroglucan is 0.01-1.00 parts by weight；
Preferably, described (F) mosanom, cellulose, cellulose gum compound additive amount be 0.1-0.8 parts by weight；
Further preferably 0.1-0.7 parts by weight；It is further preferably 0.15-0.6 parts by weight, such as 0.2 part, 0.3 part, 0.5 part,
0.6 part.
Preferably, the polymeric rheology regulator is at least one of (A), (B), (C) and (D), with (F) alginic acid
Sodium, cellulose, cellulose gum compound combination, the combination provide formula system compounded with sodium metasilicate magnesium lithium, not only may be used
To overcome inorganic matter caused partially dry and astringent skin sense in formula, the excessive sticky discomfort of high molecular polymer bring is avoided
Sense can also prevent the aggregation of powder class raw material from sinking, improve the stability of product, and the ductility of product can be enhanced and easily apply
Smearing property, user experience are good.
Preferably, the HLB value of the emulsifier is 1-10, further preferably 2-7, is still more preferably 3-6, optimal
It is selected as 4-6.
Preferably, the emulsifier is sorbitan sesquioleate (HLB value 3.7), anhydrous sorbitol isostearate
At least one of (HLB value 4.7) and sorbitan monooleate (HLB value 4.0)；Further preferably anhydrous sorbitol
Isostearate.
Preferably, the additive amount of the emulsifier is 2-12 parts by weight, further preferably 2-10 parts by weight, further
Preferably 2-8 parts by weight, such as 2-6 parts by weight, 3-6 parts by weight, 2-6 parts by weight, 4-6 parts by weight, 5-6 parts by weight, specific such as cream
The additive amount of agent is 2 parts, 3 parts, 4 parts, 5.5 parts, 6 parts.
As a kind of optimum embodiment, selected emulsifier is anhydrous sorbitol isostearate, and additive amount is 2-6 weight
Part, which is not easy corruption during using and storing, and stability is high, improves the homogeneity, stability and peace of product
Quan Xing.
The pretreatment colorant slurry is the slurry by pretreated inorganic toner and titanium dioxide.The pretreatment
Inorganic toner refer to using silicon handle iron oxides toner, the iron oxides toner be iron oxide yellow, iron oxide red and
One of iron oxide black；The main component of the titanium dioxide slurry is titanium dioxide, and content is 60% or more.
Use that docile property is strong, and concealing ability is strong by the product that pretreated slurry makes, be not easy de- adornment, with without
The formula of processing is compared, it is easier to be cleaned up by common facial cleanser, without using the extremely strong makeup remover of makeup removing power or makeup removing
Cream.
Preferably, the additive amount of the pretreatment colorant slurry is 5-20 parts by weight, further preferably 5-18 parts by weight,
And preferably 5-16 parts by weight, more preferably 5-15 parts by weight, such as 5-10 parts by weight.
Preferably, the additive amount of titanium dioxide slurry is 60-75 parts by weight in the pretreatment colorant slurry.
Preferably, the macromolecule film former is acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer and/or trimethyl
Siloxy esters of silicon acis.The hydrophobicity, anti-sebum and wearability of product can be improved in the macromolecule film former, so that product
Dressing it is more lasting.
It is further preferred that the macromolecule film former is the mixture of high molecular polymer Yu volatility finish, make
With in the process, with volatilization one layer of softness of formation of volatilization finish, uniform film, representative products have Japanese SHIN-ETSU HANTOTAI's organosilicon public
KP-545, KP-549, KP-7312J, KF-7312L of department and the DC749 of Dow corning company Dow Corning.
Preferably, the additive amount of the macromolecule film former is no more than 5 parts by weight, it is further preferred that content does not surpass
Cross 3 parts by weight；Product obtained is white in the content range has both preferable dressing endurance and easy cleaning degree simultaneously.
Preferably, the polyol humectant is glycerol, propylene glycol, 1,3 propylene glycol, butanediol, dipropylene glycol, sorbose
At least one of alcohol, Natrulon H-10 and polyglycereol -6；Further preferably propylene glycol and polyglycereol -6.
Preferably, the additive amount of the polyol humectant is 10-30 parts by weight；Further preferably 12-30 parts by weight；
It is further preferably 13-30 parts by weight；Such as 14-30 parts by weight, 15-30 parts by weight, 16-30 parts by weight, 18-30 parts by weight；
It is still more preferably 18-29 parts by weight, such as 18 parts by weight, 18.5 parts by weight, 19 parts by weight, 21 parts by weight, 25 parts by weight, 26
Parts by weight, 27 parts by weight, 28 parts by weight.
It is further preferred that the polyol humectant is propylene glycol and polyglycereol -6, additive amount is 10-30 weight
Part.
Preferably, the moisturizing grease is in vegetable oil, silicone oil, Synthetic Oil, silicone oil quasi-grease and induction biosynthesis wax
It is at least one；
It is further preferred that the silicone oil quasi-grease is selected from dimethyl silicone polymer, cyclomethicone, poly- diformazan
Radical siloxane alcohol, alkyl dimethicone, phenyl dimethicones, silicone elastomer and cetearyl poly dimethyl
At least one of siloxanes/vinyl dimethicone cross polymer；
It is further preferred that the silicone oil quasi-grease is phenyl dimethicones, phenyl trimethicone
At least one of with cyclomethicone；Such as ring five dimethyl silicone polymer, six dimethyl silicone polymer of ring, ring six
The compound of dimethyl silicone polymer and dimethiconol；Such as commercially available compound LOF 81；
Further preferably, the silicone oil quasi-grease is six dimethyl silicone polymer of silicone oil grease collar and poly dimethyl
The compound of siloxanes alcohol, additive amount are 0.1-5.0 parts by weight.
It is further preferred that the Synthetic Oil is selected from C12-15 alcohol benzoic ether, myristyl alcohol myristinate, three hydroxyls
Three isostearate of methylpropane, pentaerythritol tetraoctyl stearate, caprylic/capric triglyceride, Parleam, hydrogenation
Poly decene, ethylhexyl palmitate, two octanoic acids of butanediol/dicaprate, lauric alcohol-caprylate/decylate, two octanoic acid of propylene glycol
Ester/dicaprate, cetanol ethylhexoate, neopentyl glycol dicaprylate/dicaprate, isononyl isononanoate and palmitinic acid are different
Propyl ester；
It is further preferred that the Synthetic Oil is Nexbase 2004, two octanoic acids of butanediol/dicaprate, lauric alcohol-
At least one of caprylate/decylate, cetanol ethylhexoate and propylene/dicaprate；
Further preferably, the additive amount of the Synthetic Oil is 0.0001-3 parts by weight.When grease is the formula
BB frost stimulation obtained is small, is not easy to cause acne.
Preferably, in 5.5-7.0, additive amount is 20-100 parts by weight for the pH control of the deionized purified water.
Preferably, the not de- adornment BB frost of the g., jelly-like includes each component of following parts by weight:
Sodium metasilicate magnesium lithium, 0.05-1.0 parts by weight；
Polymeric rheology regulator
Emulsifier, 2-12 parts by weight；
Pre-process colorant slurry, 5-20 parts by weight；
Macromolecule film former is no more than 5 parts by weight；
Polyol humectant, 10-30 parts by weight；
Moisturizing grease, 5-15 parts by weight；
Deionized purified water 20-100 parts by weight,
Wherein, the ratio of sodium metasilicate magnesium lithium and polymeric rheology regulator is 1 weight % to 30 weight %；
The polymeric rheology regulator is at least two in following polymer: (A) acrylic acid (ester) class/C10-30 alkane
Alcohol acrylate crosspolymers；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen copolymer
Sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum.
It is further preferred that also containing at least one of preservative, essence in the BB frost.
It is further preferred that also contain powerful moisturizer in BB frost, as beta glucan, Sodium Hyaluronate, arbutin,
In polyglutamic acid, glycine betaine, trehalose, biological polyoses glue, purslane extract, Narcissus Tazetta L. Var extract and erythrite at least
It is a kind of.
Preferably, another technical solution of the application provides a kind of preparation method of above-mentioned BB frost comprising as follows
Step:
1) it by the mixed liquor of polymeric rheology regulator and water, is added in the mixed liquor of sodium metasilicate magnesium lithium and water, with equal
Then matter machine homogeneous uniform is added polyol humectant, is warming up to 80-90 DEG C to no particle colloid；
2) step 1) is added after mixing emulsifier, pretreatment colorant slurry and moisturizing grease homogeneous to fine and smooth uniform sizing material
Gained mixture, homogeneous to uniform lotion are added film forming agent, are cooled to 35 DEG C after mixing, take part lotion inspection qualified
Discharging.
It is further preferred that when also containing at least one of preservative, essence in BB frost, the preparation method step
2 operation is as follows: step is added after emulsifier, pretreatment colorant slurry and moisturizing grease homogeneous are mixed to fine and smooth uniform sizing material
1) film forming agent is added in gained mixture, homogeneous to uniform lotion, is cooled to 45 DEG C after mixing, and essence and preservative is added；
35 DEG C are finally cooled to, part lotion inspection qualification is taken to discharge.
Compared with prior art, BB frost provided by the present application have it is below the utility model has the advantages that
(1) BB frost provided by the present application is easy to apply due to its special g., jelly-like appearance, and it is good to hide lump in the abdomen effect, dressing naturally,
Endurance is strong, does not spend adornment within sustainable 8 hours or more.
(2) BB frost provided by the present application has excellent stability, easily stored, highly-safe, water resistant good film-forming property, clearly
Refreshing degree is high, easy to clean, and user experience is high.
(3) BB frost provided by the invention is highly-safe, and long-time service is not in that the skins such as the obscure, comedo and acne of skin are asked
Topic.
Specific embodiment
The present invention is further elaborated below with reference to embodiment.These embodiments be only for illustrative purposes,
And do not limit the scope of the invention and essence.Unless otherwise instructed, the unit of weight of each component is g in the embodiment of the present invention.
Embodiment 1-4
As shown in table 1 below, it is the formula of the embodiment 1-4 not de- adornment BB frost of g., jelly-like provided:
The preparation process of the frost of BB described in above-described embodiment is as follows:
1) A1, A2 phase are uniformly dispersed respectively with homogenizer, continue homogeneous extremely after then mixing the addition of A phase 1 to A2
Without particle colloid A phase, A3 phase is then added, is warming up to 85 DEG C；
2) B1, B2 phase homogeneous mix to fine and smooth uniform sizing material and obtain B phase；
3) B is added to A phase, homogeneous to uniform lotion is added C phase, starts to cool down；
4) 35 DEG C are cooled to, part lotion inspection qualification is taken to discharge.
Embodiment 5-8
Such as the following table 2, the formula of adornment BB frost is not taken off for the g., jelly-like that embodiment 5-8 is provided:
The preparation process of each embodiment BB frost is substantially the same as embodiment 1-4.
Performance test
1, high temperature low tempertaure storage stability test
BB frost prepared by each embodiment is fitted into the PET bottle of 30mL, circulation storage 3 times at -10 DEG C and 40 DEG C, respectively
Storage for 24 hours, i.e., after -10 DEG C of storages for 24 hours, stores for 24 hours at room temperature, places into 40 DEG C of insulating boxs and store for 24 hours, successively every time
Circulation 3 times, observes the stability of product, and determined according to following 3 grade determinating references.Test result is shown in Table 3.Its
In,
A indicates that compared with before test, appearance is without obvious permeability, bleed, coarse grain or demulsifying phenomenon；
B is indicated compared with before test, there is slight permeability, bleed, coarse grain or demulsifying phenomenon；
C is indicated compared with before test, there is apparent permeability, bleed, coarse grain or demulsifying phenomenon.
2, centrifugal stability is tested
One day is stood after the completion of the product that Example provides, takes 8-10g lotion in centrifuge tube, the 3000r/ in centrifuge
Min is centrifuged 30min, observes the stability of product, and determined according to above-mentioned 3 grade determinating references.Test result is shown in Table
3。
3, water resistant film forming is tested
The specific test method is as follows:
A. 80 female subjects are chosen, the range of age 20-45 years old, are randomly divided into 8 groups, every group of 10 people first will with ink
The left face of subject and the dyeing of right face；
B. sample to be tested is coated in dyeing part；
C. the ink of SLES solution washes away subject's test position is used, and observes the shade of test position, color is deep
It is shallowly given a mark by 8 skilled researchers, is 0 point without color, color is 10 points with before not rinsing, is calculated flat
Equal score.Test result is shown in Table 3.
4, salubrious property test
Choosing 80 has the female subjects being accustomed to using color make-up product, the range of age 20-45 years old, is randomly divided into 8 groups, often
10 people of group.Subject successively passes through face cleaning, toner, and the product that 1-8 of the embodiment of the present invention is provided is smeared after skin care milk, and sense organ is commented
Valence product is clearly spent, and scoring criterion is as follows:
Without greasy feeling, clearly spending very satisfied is 9-10 points,
Having slight greasy feeling is 7-8 points,
Having greasy feeling is 4-6 points,
Having obvious greasy feeling is 1-3 points,
Stronger soapy feeling is 0 point,
Calculate average.Test result is shown in Table 3.
The performance measurement result for the BB frost that each embodiment of table 3 provides
4, clean-up performance is tested
Choosing 90 has the female subjects being accustomed to using color make-up product, the range of age 20-45 years old, is randomly divided into 9 groups, often
10 people of group.(hundred sparrow antelope water tenderizers are pure for the product and commercially available BB frost that subject smears 1-8 of embodiment of the present invention offer according to a conventional method
Star repairs Yan Shuan), the tender net extract cleanser thoroughly (being suitable for all skin quality) of hundred sparrow antelope water, warm water face cleaning are all made of after 8 hours.Sense
Official evaluates the easy removing performance of product, and gives a mark by following standard:
9-10 very easy to clean points,
6-8 more easy to clean points,
3-5 easy to clean points,
0-2 not easy to clean points,
Calculate average.Test result is shown in Table 4.
Research staff, will be pre- in embodiment 1 in order to further inquire into influence of the pretreatment colorant slurry for spatter property
Colorant slurry is handled to replace using untreated colorant slurry, other constant, obtained BB frost carries out as above identical test,
As a result score value is 7.9, and with the increase of colouring matter slurry dosage (increasing to original 2 times), has no too big influence to score value.
In addition, research staff allows tested also using the method that subject is tested is randomly selected in performance test as above
Person uses product provided in an embodiment of the present invention, persistently using after 30 days, observing subjects skin's situation and counting, as a result
It was found that the problems such as BB frost that subject is provided using 1-8 of the embodiment of the present invention shades without comedo and acne, skin after 30 days.
Subject's reflection more than 90%, BB frost is easy to apply, hides that lump in the abdomen effect is good, and dressing is naturally, endurance is strong, and sustainable 8
Hour or more not spend adornment.
Only illustratively, the scope of the present invention is not limited thereto for above-mentioned example.To those skilled in the art
For to modify be it will be apparent that the present invention is only limited by attached rights require scope.
Claims (4)
1. a kind of BB frost of the not de- adornment of g., jelly-like, is made of following each component:
2. a kind of BB frost of the not de- adornment of g., jelly-like, is made of following each component:
3. a kind of BB frost of the not de- adornment of g., jelly-like, is made of following each component:
4. a kind of BB frost of the not de- adornment of g., jelly-like, is made of following each component:
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| CN111529431B (en) * | 2020-05-12 | 2022-06-07 | 广东芭薇生物科技股份有限公司 | Composition with make-up maintaining and oil controlling effects and cosmetic |
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