CN104473781B - A kind of preparation containing powder cosmetic and preparation method thereof - Google Patents

A kind of preparation containing powder cosmetic and preparation method thereof Download PDF

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Publication number
CN104473781B
CN104473781B CN201410642825.3A CN201410642825A CN104473781B CN 104473781 B CN104473781 B CN 104473781B CN 201410642825 A CN201410642825 A CN 201410642825A CN 104473781 B CN104473781 B CN 104473781B
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parts
homogeneous
containing powder
preparation
powder cosmetic
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CN104473781A (en
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顾葵
周小桥
彭燕辉
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Abstract

The present invention provides a kind of preparation containing powder cosmetic and preparation method thereof.Described preparation containing powder cosmetic, it is composed of the following components in parts by weight, 0.2 2.0 parts of 20 ether of the double decyl tetradecyl alcohol polyethers of acrylic acid (ester) class/0.1 3.0 parts of acryloyl nitrogen copolymer sodium, 8 18 parts of NMF, PEG 240/HDI copolymers, 0.1 1.0 parts of sodium metasilicate magnesium lithium, 0.05 0.3 parts of xanthans, two (lauramide glutamy sodium) Sodium lysinates 0.01 0.15,5 15 parts of butanediol, 40 60 parts of water, 10 25 parts of oil phase, 1 10 parts of whitening agent, essence and preservative.

Description

A kind of preparation containing powder cosmetic and preparation method thereof
Technical field
The invention belongs to cosmetic field, and in particular to a kind of preparation containing powder cosmetic and preparation method thereof.
Background technology
In recent years, with cosmetics continue to develop and the women that likes to be beautiful demand increase, BB frost is increasingly pursued by people And as fashion trend.BB frosts are not only easy to use, and have foundation cream, sun-proof and isolated product effect concurrently.The female for liking to be beautiful Property only need to using BB frost can just possess flawless skin quality and skin sense.
BB frosts are the abbreviations of Blemish Balm, and effect mainly hides the flaw, the adjustment colour of skin, sun-proof, careful pore, can make Go out nude look effect.After BB frosts are originally peeling or whitening (brightening), protection and maintenance to skin that is impaired and damaging are used Regeneration frost.This regeneration frost can give to the problem of skin and rapidly improve in time, can improve and make up lacking for skin Point, thus BB frosts of gaining the name.
BB frosts are developed so far, and experienced first generation BB frosts (scar maintenance frost), and second generation BB frosts (have merged skin care products and powder The dual identity at bottom), third generation BB frosts have been proposed now.Scientific and technical constantly innovation, will initially after use on the face The BB frosts of airtight, dry skin even long-term use skin president's small pox are combined with maintenance frost, form third generation BB frosts.The Three generations BB frosts have advantages below:1st, make newborn skin permeability good;Because the third generation BB frosts decomposed with newest beauty science and technology Molecular weight is smaller, and pore will not be blocked later used on the face, and gas permeability is fine.2nd, deep layer is nourished:Because molecular weight is small, Ke Yizhi Up to the basalis of skin, cell is directly acted on, be conducive to the absorption of nutritional ingredient, uptake is three to the four of second generation BB frosts Times;On this basis, third generation BB frosts, also added the concept of deep moisturizing, and maintenance composition and moisturizing are added in BB frosts Optimal molecule, micromolecular water inside, moisture of skin can be preferably supplemented using newest sophisticated composition embedding techniques, make skin Moist state is chronically at, performance of keeping humidity is good, and long-term use skin will not be dried.3rd, easily makeup removing;Because nutritional ingredient is complete Hypersorption, so makeup removing is with general make up remover, or warm water adds the mildy wash just can be with.
BB frosts itself have maintenance and hide the dual identity of the flaw, the impression for ignoring skin to reach the effect for hiding the flaw, This belongs to a kind of phenomenon of contradiction in beauty treatment fields, so the BB frost technology innovation replacements are extremely urgent.
At present, the product containing powder of in the market:Foundation cream, BB frosts, CC frosts, sun screen etc. exist mostly in the form of Water-In-Oil. When this emulsifying manner consumer uses, compare greasy, airtight, easy blocked pore, cause skin to bear.Although, market On also have the product containing powder of oil-in-water form, but, this kind of product does not have the effect of the anti-sweat of water resistant, meets sweat and easily spends adornment.
The content of the invention
The present invention provides a kind of preparation containing powder cosmetic, it is characterised in that it is composed of the following components in parts by weight,
Oil phase is selected from Nexbase 2004, caprylic/capric triglyceride, Bai Chihua (LIMNANTHES ALBA) seed oil, fertility Phenol (vitamin E), pentaerythrite four (thylhexoic acid) ester, dimethyl silicone polymer, hydrogenation apricot kernel oil, mineral oil, smooth times of sorb Half oleate, ring five dimethyl silicone polymer, octyl dodecanol, Jojoba (SIMMONDSIA CHINENSIS) seed oil, fertility At least one in phenol (vitamin E), phenyl trimethicone;
Film forming agent includes two (lauramide glutamy sodium) Sodium lysinates, trimethyl silicane alkoxy esters of silicon acis, smooth times of sorb One or more combination in half oleate, cetyl dimethicone.
Preferably, described NMF is selected from glycerine, trimethylglycine, hyaluronic acid, trehalose, butanediol corn and carries Take at least one of thing and polyglutamic acid sodium.
Preferably, it is composed of the following components in parts by weight,
Wherein, whitening agent is titanium dioxide etc..
Preferably, it is composed of the following components in parts by weight,
Preferably, it is composed of the following components in parts by weight,
Preferably, it is composed of the following components in parts by weight,
Preferably, it is composed of the following components in parts by weight,
Preferably, it is composed of the following components in parts by weight,
The present invention also provides the described preparation method containing powder cosmetic preparation, and it comprises the following steps:
1) other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by.
2) B, C are poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns When pour into oil phase pot, it is stand-by.
3) emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B, C phase.
4) vacuum is put, homogeneous is beaten 3 minutes.
5) homogeneous is closed, 30 revs/min of stirring is opened.
6) filtering and discharging after continuing to stir 30 minutes.
Described formulation preparation method containing powder cosmetic, it comprises the following steps:
1) other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, and addition is warming up to 80 degree, It is stand-by.
2) B is poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns Oil phase pot is poured into, 80 degree are heated to, it is stand-by.
3) heating emulsification pot is vacuumized to 60 degree, opens stirring, first takes out A phases, then take out B phases.
4) vacuum is put, homogeneous is beaten 3 minutes.
5) homogeneous is closed, 30 revs/min of stirring is opened, while opening cooling water temperature, is lowered the temperature with speed once per minute.
6) C is added when temperature is down to 40 degree, is continued stirring and is cooled to 30 degree.
7) filtering and discharging.
Described formulation preparation method containing powder cosmetic, it comprises the following steps:
1) other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by.
2) B is poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns Oil phase pot is poured into, it is stand-by.
3) emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B phases.
4) vacuum is put, homogeneous is beaten 3 minutes.
5) homogeneous is closed, 30 revs/min of stirring is opened.
6) 80 degree are heated to, homogeneous is lowered the temperature after 3 minutes.
7) homogeneous is closed, 30 revs/min of stirring is opened, while opening cooling water temperature, is lowered the temperature with speed once per minute.
8) C is added when temperature is down to 40 degree, is continued stirring and is cooled to 30 degree.
9) filtering and discharging.
Oil phase:
The suitable ingredients that oil phase can be formed may be selected from polarity and nonpolar oils or its mixture.
The oil phase of preparation of the invention is advantageously selected from phosphatide such as lecithin and fatty acid triglycercide, selected from aliphatic acid third Diol ester or aliphatic acid butanediol ester, selected from the native paraffin in animal or plant source, selected from ester oil, selected from dialkyl ether and carbonic acid Dialkyl ester, selected from side chain and non-branched hydrocarbon and wax and selected from ring-type and linear silicone oils.
In one embodiment, oil phase includes at least one fatty acid alkyl esters such as decyl oleate, different n-nonanoic acid palm ester And/or at least one fatty alcohol such as 2- octyl dodecanols.Additionally, oil phase can contain aliphatic saturated hydrocarbon such as paraffin.
Decyl oleate for example can derive from Cognis companies with trade mark Cetiol V.Different n-nonanoic acid palm ester for example can be with the trade mark Cetiol SN derive from Cognis companies.2- octyl dodecanols for example can derive from Cognis companies with trade mark Eutanol G.
In preferred embodiments, oil phase includes at least one triglycerides.
Preferably, at least one triglycerides includes caprylic/capric triglyceride, and it can be with the trade mark Miglyol812 derives from Sasol companies, and itself and other oil and the mixture of wax composition.
Additionally, especially preferably triglycerides, especially Sasol companies/can be with can be derived from trade mark Miglyol 812 Trade mark Myritol 312 derives from the caprylic/capric triglyceride of Cognis companies.
Described NMF be selected from glycerine, trimethylglycine, hyaluronic acid, trehalose, butanediol corn extract and At least one of polyglutamic acid sodium.
Mineral oil refers to the base oil extracted from oil by physics distillating method, also referred to as White Mineral Oil or white Oil.
The present invention compared with prior art, with advantages below:
1) product prepared using the technology of the present invention, does not have the greasy of oil product, and Glycerin has oil-in-water again It is ventilative;And the present invention as a result of PEG-240/HDI copolymers it is double-ether of decyl tetradecyl alcohol polyethers -20, sodium metasilicate magnesium lithium and Acrylic acid (ester) class/acryloyl nitrogen copolymer, the water-resistance of formulation products containing powder cosmetic being prepared from is significantly improved, it is not easy to De- adornment.In addition, product appearance is novel, seem very thick, after swaggering, it is equally dilute to become like water, and mobility very well, can hear that water is rocked Sound;
2) special product appearance, because polymer is made up of many money raw materials, sodium lithium magnesium silicate has card in many money raw materials Room structure, the PEG-240/HDI copolymers pair-ether of decyl tetradecyl alcohol polyethers -20, acrylic acid (ester) class/acryloyl nitrogen copolymer sodium The thickener of formation has jelly sense, so that product has special outward appearance, the emulsion appearance made is similar to Yoghourt, and one runs into outward Power just can be with thinning.When consumer one shakes, the sound of the rapid thinning aquation of product can be heard at once, so that, product spread Well, product appearance is novel, and Consumer's Experience is good.
Specific embodiment
Embodiment 1
Operating procedure:
1st, other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, and addition is warming up to 80 degree, It is stand-by.
2nd, B is poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns Oil phase pot is poured into, 80 degree are heated to, it is stand-by.
3rd, heating emulsification pot is vacuumized to 60 degree, opens stirring, first takes out A phases, then take out B phases.
4th, vacuum is put, homogeneous is beaten 3 minutes.
5th, homogeneous is closed, 30 revs/min of stirring is opened, while opening cooling water temperature, is lowered the temperature with speed once per minute.
6th, C is added when temperature is down to 40 degree, is continued stirring and is cooled to 30 degree.
7th, filtering and discharging.
Embodiment 2
Operating procedure:
1st, other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by.
2nd, B, C are poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns When pour into oil phase pot, it is stand-by.
3rd, emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B, C phase.
4th, vacuum is put, homogeneous is beaten 3 minutes.
5th, homogeneous is closed, 30 revs/min of stirring is opened.
6th, filtering and discharging after continuing to stir 30 minutes.
Embodiment 3
Operating procedure:
1st, other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by.
2nd, B, C are poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns When pour into oil phase pot, it is stand-by.
3rd, emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B, C phase.
4th, vacuum is put, homogeneous is beaten 3 minutes.
5th, homogeneous is closed, 30 revs/min of stirring is opened.
6th, filtering and discharging after continuing to stir 30 minutes.
Embodiment 4
Operating procedure:
1st, other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by.
2nd, B is poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, when titanium white powder fineness reaches 40 microns Oil phase pot is poured into, it is stand-by.
3rd, emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B phases.
4th, vacuum is put, homogeneous is beaten 3 minutes.
5th, homogeneous is closed, 30 revs/min of stirring is opened.
6th, 80 degree are heated to, homogeneous is lowered the temperature after 3 minutes.
7th, homogeneous is closed, 30 revs/min of stirring is opened, while opening cooling water temperature, is lowered the temperature with speed once per minute.
8th, C is added when temperature is down to 40 degree, is continued stirring and is cooled to 30 degree.
9th, filtering and discharging.
Effect example water-resistance experiment
1. instrument and consumptive material
1.1PMMA plates, 5cIn × 5cm, French Europlast companies production;
The type electric heating constant temperature shaking water baths of 1.2DKZ 1, Shanghai Fuma Experiment Equipment Co., Ltd.'s production;
1.3 point samples l ml syringes, Becton Dickinson&Company productions;
1.4 latex finger cots, the state-run product of Shanghai Emulsion Factory's Long March subsidiary factory thirty;
1.5 liquid chromatographs
2. experimental condition selection
Existing some scholars of influence about tank water temperature and frequency of oscillation to test result carried out experiment, and conclusion is water Bath temperature degree is in 25-35 DEG C of scope.The measured result under conditions of 50-200 times/min of frequency of oscillation is very close.Therefore, I In this experiment using 25 DEG C water temperature and 100 times/min frequency of oscillation.
Take pressurization to pipette sample with point sample syringe, take the dosage of 4ul, with the dimension in hplc determination feed liquid The content of C ethylethers.
Pressurization is taken to pipette sample with point sample syringe, with 2ul/Cm2Dosage, uniform place is in the feather plucking of PMMA plates On face, spreading area 2cm2.Then sample is smeared with the forefinger with latex latex finger cot (to apply to enclose to be smeared with straight line and mutually tie Close), make uniform outer surface.The PMMA plates that will be prepared are placed under the conditions of (25 ± 2) DEG C, relative humidity 40% ± 5% 20min.Immediately sample panel is immersed on the electric heating constant temperature shaking water bath that water temperature is 25 DEG C and the shelf being fixed therein, with The frequency of oscillation of 100 times/min, vibrates 20min, takes out, and gets rid of the big drop of water on plate, then takes out, and is surveyed with liquid chromatograph Determine the content of the Vc ethylether of liquid in shaking water bath.
3. data processing
Enter the anti-water coefficient (Water Resistant Factor, WRF) after water immersion to be calculated with below equation:WRF In (%)=1- shaking water baths in the content/coating material liquid of the Vc ethylether of liquid Vc ethylether content.
In order to test sample spreadability is good and bad, its organoleptic attribute and rheological properties are tested, in sensory evaluation, Sense organ evaluation and test is carried out using scoring method of inspection, each organoleptic indicator carries out ten point system marking and evaluates, and sense organ group is small including 10 Group membership.
Sample Spreadability Salubrious degree Anti- water coefficient (%)
Embodiment 1 9.214 7.221 80
Embodiment 2 8.677 7.333 84
Embodiment 3 8.695 7.824 82
Embodiment 4 8.924 8.125 85
Commercially available BB frosts 7.413 5.513 62
Commercially available foundation emulsion 7.411 5.452 55
Above-mentioned detailed description is directed to illustrating for one of them possible embodiments of the present invention, and the embodiment is simultaneously not used to The scope of the claims of the invention is limited, all equivalence enforcements or change without departing from carried out by the present invention are intended to be limited solely by the technology of the present invention In the range of scheme.

Claims (8)

1. a kind of preparation containing powder cosmetic, it is characterised in that be composed of the following components in parts by weight,
Wherein, whitening agent is titanium dioxide;
Oil phase is selected from Nexbase 2004, caprylic/capric triglyceride, white pond flower seed oil, tocopherol Vitamin E, pentaerythrite four (thylhexoic acid) ester, dimethyl silicone polymer, hydrogenation apricot kernel oil, mineral oil, sorbitan sesquioleate, the poly dimethyl silicon of ring five At least one in oxygen alkane, octyl dodecanol, jojoba seed oil and phenyl trimethicone;
Described NMF is selected from glycerine, trimethylglycine, hyaluronic acid, trehalose, butanediol, corn extract and poly- paddy At least one in propylhomoserin sodium.
2. preparation containing powder cosmetic according to claim 1, it is characterised in that it is composed of the following components in parts by weight,
3. preparation containing powder cosmetic according to claim 1, it is characterised in that it is composed of the following components in parts by weight,
4. preparation containing powder cosmetic according to claim 1, it is characterised in that it is composed of the following components in parts by weight,
5. preparation containing powder cosmetic according to claim 1, it is characterised in that it is composed of the following components in parts by weight,
6. preparation containing powder cosmetic according to claim 1, it is characterised in that it is composed of the following components in parts by weight,
7. a kind of preparation method containing powder cosmetic preparation as claimed in claim 1, it is characterised in that it includes following step Suddenly:
1) other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, stand-by;
2) B, C are poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, fallen when titanium white powder fineness reaches 40 microns Enter oil phase pot, it is stand-by;
3) emulsification pot is vacuumized, opens stirring, first take out A phases, then take out B, C phase;
4) vacuum is put, homogeneous is beaten 3 minutes;
5) homogeneous is closed, 30 revs/min of stirring is opened;
6) filtering and discharging after continuing to stir 30 minutes.
8. a kind of preparation method containing powder cosmetic preparation as claimed in claim 1, it is characterised in that it includes following step Suddenly:
1) other raw materials by A in addition to water pour into dry water phase pot, stir, and add water, and 80 degree are warming up to after addition, treat With;
2) B is poured into stainless steel cask, homogeneous is beaten with mobile homogeneous head after stirring evenly, poured into when titanium white powder fineness reaches 40 microns Oil phase pot, is heated to 80 degree, stand-by;
3) heating emulsification pot is vacuumized to 60 degree, opens stirring, first takes out A phases, then take out B phases;
4) vacuum is put, homogeneous is beaten 3 minutes;
5) homogeneous is closed, 30 revs/min of stirring is opened, while opening cooling water temperature, is lowered the temperature with speed once per minute;
6) C is added when temperature is down to 40 degree, is continued stirring and is cooled to 30 degree;
7) filtering and discharging.
CN201410642825.3A 2014-11-14 2014-11-14 A kind of preparation containing powder cosmetic and preparation method thereof Expired - Fee Related CN104473781B (en)

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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107412115A (en) * 2017-02-09 2017-12-01 苏州安特化妆品股份有限公司 A kind of g., jelly-like foundation cream and preparation method thereof
CN107970138B (en) * 2017-12-06 2019-02-05 绿馨颜(惠州)生物科技有限公司 Not de- adornment BB frost of a kind of g., jelly-like and preparation method thereof
CN108785183A (en) * 2018-09-04 2018-11-13 苏州安特化妆品股份有限公司 Long-acting adornment of holding repairs pigment frost and preparation method thereof
CN110075007B (en) * 2019-06-06 2022-03-22 广州微肽生物科技有限公司 Oil-in-water sunscreen product with waterproof and skin elasticity improving functions and preparation method thereof
CN110664628B (en) * 2019-10-30 2020-10-02 绿馨颜(广东)生物科技有限公司 Oil-in-water solid cosmetic composition containing powder and preparation method and application thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1584321A1 (en) * 2004-04-06 2005-10-12 L'oreal Anhydrous cosmetic composition comprising an oil, a polymeric gelling agent and a polyurethane powder
CN103442702A (en) * 2011-01-07 2013-12-11 阿勒根公司 Melanin modification compositions and methods of use
CN103906550A (en) * 2011-11-03 2014-07-02 莱雅公司 Solid cosmetic composition in compact powder form

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1584321A1 (en) * 2004-04-06 2005-10-12 L'oreal Anhydrous cosmetic composition comprising an oil, a polymeric gelling agent and a polyurethane powder
CN103442702A (en) * 2011-01-07 2013-12-11 阿勒根公司 Melanin modification compositions and methods of use
CN103906550A (en) * 2011-11-03 2014-07-02 莱雅公司 Solid cosmetic composition in compact powder form

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