CN107970138A - Not de- adornment BB frosts of a kind of g., jelly-like and preparation method thereof - Google Patents
Not de- adornment BB frosts of a kind of g., jelly-like and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/733—Alginic acid; Salts thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/08—Preparations containing skin colorants, e.g. pigments for cheeks, e.g. rouge
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The present invention provides a kind of not de- adornment BB frosts of g., jelly-like, it contains following each component：Sodium metasilicate magnesium lithium, polymeric rheology conditioning agent, emulsifying agent, pretreatment colorant slurry, macromolecule film former, polyalcohol moisturizer, moisturizing grease, deionized purified water, wherein, the polymeric rheology conditioning agent is at least two in following polymer：(A) 30 alkylol acrylamide acid esters cross-linked polymers of acrylic acid (ester) class/C10；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen copolymer sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum.BB frosts provided by the invention are easy to apply, and it is good to hide lump in the abdomen effect, dressing naturally, endurance is strong, it is sustainable 8 it is small when more than do not spend adornment, and long-time service is not in the skin problems such as the obscure, comedo and acne of skin, and user's evaluation is good.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to not de- adornment BB frosts of a kind of g., jelly-like and preparation method thereof.
Background technology
BB frosts, the effect of having foundation cream, sun-proof and isolated product concurrently due to it, are increasingly pursued and are become by the women that likes to be beautiful
Fashion trend.
BB frosts (Blemish Blam) originate from Germany, are initially the German artificial patients designs for receiving laser surgery,
Quality is more thick and heavy, containing skin care and sun-prevention component, impaired skin can be made to obtain repairing and regeneration, after drawn by South Korea's cosmetics circle
Into, after improveing and developing, just become daily use chemicals cosmetics from medicine cosmetics, and be evolved into collection hide the flaw, isolation, prevent
Shine, repair single product of the functions such as face, bottom adornment.
Existing BB frosts are all the emulsification systems of Water-In-Oil on the market, are to communicate Over emulsfication dosage form into stabilization by oil phase and water
System.But emulsification system is had a great influence by external environment such as temperature and air pressure, larger temperature Change may be destroyed
, there is the phenomenon being demulsified in the stabilization of emulsification system, and shows as emulsification system and obvious layering occurs, and then influences the extension of BB frosts
Property and stability.Although the water-tolerant of water-in-oil type BB frosts, because people knows from experience secretion sweat, dressing is easily broken
Badly, it is necessary to repeat to refine the make-up, inconvenience is produced；Skin sense at the same time is more thick and heavy, and poor air permeability, easily causes the skins such as comedo and acne
Problem.
In order to improve the thick and heavy skin sense of water-in-oil system in itself, makeup formulators have done various trials to improve BB frosts
Usage experience sense.Part commercial product ensures the salubrious skin sense of BB frosts by adding a large amount of volatility greases, but this kind of production
Product can allow a very big consumer to feel too dry and astringent, and moisture feeling is inadequate, and dressing persistence is poor.Also some products are in order to chase after
Ask it is superpower it is permanent hold adornment effect, with the addition of substantial amounts of macromolecule film former in formula, but this kind of product must coordinate and make
With the extremely strong makeup remover or make-up remover of makeup removing power, this kind of product easilys lead to that the comedo and acne colour of skin is dark yellow or even the skin such as allergy
Problem.People need a salubrious and lasting BB frost products, but this is a huge technological challenge for formulator.
Through retrieval, with patent document record solve the above problems have following several method：Such as Chinese patent application
201410425432.7《A kind of BB frosts with long-lasting moisturization and preparation method thereof》One kind is disclosed by organic matter such as ring
Five dimethyl silicone polymers, different tridecanol isononoate etc., and inorganic matter stearoyl-glutamic acid disodium/aluminium hydroxide/iron oxide
A kind of BB frosts with long-lasting moisturization made of black grade.The BB frost skin senses exquisiteness, frivolous ventilative, moistening effect are small up to eight
When, skin water content of stratum corneum can be dramatically increased, realizes that adornment is not floated in long-time moisturizing.But since product made from the patent adds
Substantial amounts of macromolecule organic is entered, makeup removing power extremely strong makeup remover or make-up remover, this kind of production must be used cooperatively in cleaning
Product easily lead to that comedo and acne, the colour of skin be dark yellow or even the skin problem such as allergy.
And for example, Chinese patent application 201110127193.3《A kind of BB frosts and preparation method thereof》One kind is disclosed with gel
For substrate, BB frosts made of dispersant and BB frost particles are added.Wherein, BB frosts particle is by BB frosts embedding capsule and titanium white whitening
Two kinds of BB frost particles of capsule, and then the technical problem that the BB frosts for solving emulsification formulation now are unstable, oil-containing is excessive.But the BB
BB frost particles in frost be by the extruding of pump head, it is scattered after with powdered be applied to skin surface, it is poor to still suffer from skin sense
Problem.
For to sum up, disclosed BB frosts can not meet that moisturizing, the lasting, easy cleaning of dressing etc. will at the same time in the prior art
Ask, and then various skin problems can be caused to user.
The content of the invention
One of goal of the invention of the application is that BB frosts moisture feeling in the prior art is poor, dressing persistence in order to solve
Difference, requires cleaning supplies high, easily causes comedo and acne, the colour of skin dark yellow or even the skin problem such as allergy, there is provided a kind of g., jelly-like
The BB frosts of not de- adornment.
Another goal of the invention of the application is to provide the preparation method of above-mentioned BB frosts.
In order to realize foregoing invention purpose, the technical solution of the application provides a kind of BB of the not de- adornment of g., jelly-like
Frost, it contains following each component：
Sodium metasilicate magnesium lithium,
Polymeric rheology conditioning agent,
Emulsifying agent,
Colorant slurry is pre-processed,
Macromolecule film former,
Polyalcohol moisturizer,
Moisturizing grease,
Deionized purified water,
Wherein, the polymeric rheology conditioning agent is at least two in following polymer：(A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymers, such as commercial goods PemulenTMTR-2 polymer and PemulenTMTR-1 polymerize
Thing；(B) carbomer sodium；(C) agarose gel, if commercial product is the SeapureAgarose that Lonza companies produce；(D) propylene
Sour (ester) class/acryloyl nitrogen copolymer sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum, such as city
Sell commodity PC806.
Preferably, the ratio of the sodium metasilicate magnesium lithium and polymeric rheology conditioning agent is 1 weight % to 30 weight %；
It is further preferred that the ratio of the sodium metasilicate magnesium lithium and polymeric rheology conditioning agent is 1 weight % to 20 weights
Measure %；
It is further preferred that the ratio is 5 weight % to 20 weight %；More preferably 12 weight % to 20 weight %,
Such as 12 weight %, 15 weight %, 18 weight %, 20 weight %.
Wherein, sodium metasilicate magnesium lithium often claims lithium magnesium silicate, is called hectorite, has nano microcrystalline structure, disperses shape in water
Into nanometer water white transparency thixotropy gel；Commercially available typical products have Laponite series of products, and Laponite can contain with most of
The thickener compatibility that aqueous systems use.
Preferably, the additive amount of the sodium metasilicate magnesium lithium is 0.05-1.0 parts by weight.
Preferably, the polymeric rheology conditioning agent is at least two in following polymer：(A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymers；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen
Copolymer sodium；
Preferably, the additive amount of described (A) acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymers is 0.1-
0.8 parts by weight；More preferably 0.1-0.7 parts by weight；Further it is preferably 0.1-0.6 parts by weight, such as 0.1 part, 0.15
Part, 0.2 part, 0.3 part, 0.5 part, 0.6 part；
Preferably, the additive amount of described (B) carbomer sodium is 0.01-0.5 parts by weight；More preferably 0.05-0.5 weights
Measure part；Further it is preferably 0.1-0.5 parts by weight, such as 0.1 part, 0.2 part, 0.3 part, 0.4 part, 0.5 part；
Preferably, the additive amount of described (C) agarose gel is 0.01-0.2 parts by weight；More preferably 0.05-0.2
Part；Further it is preferably 0.05-0.18 parts, such as 0.05 part, 0.08 part, 0.1 part, 0.15 part, 0.18 part；
Preferably, the additive amount of described (D) acrylic acid (ester) class/acryloyl nitrogen copolymer sodium is 0.01-0.5 parts by weight；
More preferably 0.05-0.5 parts by weight；Further it is preferably 0.1-0.5 parts by weight, such as 0.1 part, 0.2 part, 0.3 part,
0.4 part, 0.5 part；
It is further preferred that the polymeric rheology conditioning agent is the combination of following polymer:(A) acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymers；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen
Copolymer sodium；
It is further preferred that the additive amount of the polymeric rheology conditioning agent is 0.5-2.0 parts by weight.
By the combination of above-mentioned polymer A, B, C, D as the formula system that polymeric rheology conditioning agent provides with stronger
Pseudoplastic behavior, i.e. water moisten jelly sense appearance, by effective compounding of above-mentioned each polymer and sodium metasilicate magnesium lithium, can overcome inorganic matter
Caused partially dry and astringent skin sense in formula, while the sticky sense of discomfort for avoiding excessive high molecular polymer from bringing.
Preferably, the polymeric rheology conditioning agent is following polymer：(E) Scleroglucan；(F) mosanom, cellulose,
The compound of cellulose gum；The combination can provide stronger suspendability, prevent the aggregation of powder class raw material from sinking；
Preferably, the additive amount of described (E) Scleroglucan is 0.01-1.00 parts by weight；
Preferably, described (F) mosanom, cellulose, the additive amount of compound of cellulose gum are 0.1-0.8 parts by weight；
More preferably 0.1-0.7 parts by weight；Further it is preferably 0.15-0.6 parts by weight, such as 0.2 part, 0.3 part, 0.5 part,
0.6 part.
Preferably, the polymeric rheology conditioning agent is at least one of (A), (B), (C) and (D), with (F) alginic acid
Sodium, cellulose, cellulose gum compound combination, formula system and the sodium metasilicate magnesium lithium which provides compound, not only may be used
To overcome inorganic matter caused partially dry and astringent skin sense in formula, the sticky discomfort for avoiding excessive high molecular polymer from bringing
Sense, is also prevented from the aggregation of powder class raw material and sinks, improve the stability of product, and can strengthen the ductility of product and easily apply
Smearing property, user experience are good.
Preferably, the HLB value of the emulsifying agent is 1-10, more preferably 2-7, is still more preferably 3-6, optimal
Elect 4-6 as.
Preferably, the emulsifying agent is sorbitan sesquioleate (HLB value 3.7), anhydrous sorbitol isostearate
At least one of (HLB value 4.7) and sorbitan monooleate (HLB value 4.0)；More preferably anhydrous sorbitol
Isostearate.
Preferably, the additive amount of the emulsifying agent is 2-12 parts by weight, more preferably 2-10 parts by weight, further
Preferably 2-8 parts by weight, as 2-6 parts by weight, 3-6 parts by weight, 2-6 parts by weight, 4-6 parts by weight, 5-6 parts by weight are specific such as breast
The additive amount of agent is 2 parts, 3 parts, 4 parts, 5.5 parts, 6 parts.
As a kind of optimum embodiment, selected emulsifying agent is anhydrous sorbitol isostearate, its additive amount is 2-6 weight
Part, which is not easy corruption during using and storing, and stability is high, improves the homogeneity, stability and peace of product
Quan Xing.
The pretreatment colorant slurry, is the slurry of the inorganic toner and titanium dioxide by pretreatment.The pretreatment
Inorganic toner refer to using silicon processing iron oxides toner, the iron oxides toner for iron oxide yellow, iron oxide red and
One kind in iron oxide black；The main component of the titanium dioxide slurry is titanium dioxide, its content is more than 60%.
It is strong that the product that slurry by pretreatment makes uses docile property, and it is strong to hide flaw ability, is not easy de- adornment, with without
The formula of processing is compared, it is easier to is cleaned up by common facial cleanser, without using the extremely strong makeup remover of makeup removing power or makeup removing
Cream.
Preferably, the additive amount of the pretreatment colorant slurry is 5-20 parts by weight, more preferably 5-18 parts by weight,
And preferably 5-16 parts by weight, more preferably 5-15 parts by weight, such as 5-10 parts by weight.
Preferably, the additive amount of titanium dioxide slurry is 60-75 parts by weight in the pretreatment colorant slurry.
Preferably, the macromolecule film former is acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer and/or trimethyl
Siloxy esters of silicon acis.The macromolecule film former can improve the hydrophobicity, anti-sebum and wearability of product so that product
Dressing it is more lasting.
It is further preferred that the macromolecule film former is the mixture of high molecular polymer and volatility finish, make
During, with volatilization one layer of softness of formation of volatilization finish, uniform film, representative products have Japanese SHIN-ETSU HANTOTAI's organosilicon public affairs
KP-545, KP-549, KP-7312J, KF-7312L of department and the DC749 of Dow corning company Dow Corning.
Preferably, the additive amount of the macromolecule film former is no more than 5 parts by weight, it is further preferred that content does not surpass
Cross 3 parts by weight；Obtained product frost has preferable dressing endurance and easy cleaning degree concurrently at the same time in the content range.
Preferably, the polyalcohol moisturizer is glycerine, propane diols, 1,3 propane diols, butanediol, dipropylene glycol, sorbose
At least one of alcohol, Natrulon H-10 and polyglycereol -6；More preferably propane diols and polyglycereol -6.
Preferably, the additive amount of the polyalcohol moisturizer is 10-30 parts by weight；More preferably 12-30 parts by weight；
Further it is preferably 13-30 parts by weight；Such as 14-30 parts by weight, 15-30 parts by weight, 16-30 parts by weight, 18-30 parts by weight；
Still more preferably it is 18-29 parts by weight, such as 18 parts by weight, 18.5 parts by weight, 19 parts by weight, 21 parts by weight, 25 parts by weight, 26
Parts by weight, 27 parts by weight, 28 parts by weight.
It is further preferred that the polyalcohol moisturizer is propane diols and polyglycereol -6, its additive amount is 10-30 weight
Part.
Preferably, the moisturizing grease is in vegetable oil, silicone oil, Synthetic Oil, silicone oil quasi-grease and induction biosynthesis wax
It is at least one；
It is further preferred that the silicone oil quasi-grease is selected from dimethyl silicone polymer, cyclomethicone, poly- diformazan
Radical siloxane alcohol, alkyl dimethicone, phenyl dimethicones, silicone elastomer and cetearyl poly dimethyl
At least one of siloxanes/vinyl dimethicone cross polymer；
It is further preferred that the silicone oil quasi-grease is phenyl dimethicones, phenyl trimethicone
At least one of with cyclomethicone；Such as ring five dimethyl silicone polymer, six dimethyl silicone polymer of ring, ring six
The compound of dimethyl silicone polymer and dimethiconol；Such as commercially available compound LOF 81；
Further preferably, the silicone oil quasi-grease is six dimethyl silicone polymer of silicone oil grease collar and poly dimethyl
The compound of silica alkanol, its additive amount are 0.1-5.0 parts by weight.
It is further preferred that the Synthetic Oil is selected from C12-15 alcohol benzoic ethers, myristyl alcohol myristinate, three hydroxyls
Three isostearate of methylpropane, pentaerythritol tetraoctyl stearate, caprylic/capric triglyceride, Parleam, hydrogenation
Poly decene, ethylhexyl palmitate, two octanoic acids of butanediol/dicaprate, lauric alcohol-caprylate/decylate, the octanoic acid of propane diols two
Ester/dicaprate, cetanol ethylhexoate, neopentyl glycol dicaprylate/dicaprate, isononyl isononanoate and palmitic acid are different
Propyl ester；
It is further preferred that the Synthetic Oil for Nexbase 2004, two octanoic acids of butanediol/dicaprate, lauric alcohol-
At least one of caprylate/decylate, cetanol ethylhexoate and propylene/dicaprate；
Further preferably, the additive amount of the Synthetic Oil is 0.0001-3 parts by weight.When grease is the formula
Obtained BB frosts stimulation is small, is not easy to cause acne.
Preferably, the pH of the deionized purified water is controlled in 5.5-7.0, its additive amount is 20-100 parts by weight.
Preferably, the not de- adornment BB frosts of the g., jelly-like include each component of following parts by weight：
Sodium metasilicate magnesium lithium, 0.05-1.0 parts by weight；
Polymeric rheology conditioning agent
Emulsifying agent, 2-12 parts by weight；
Pre-process colorant slurry, 5-20 parts by weight；
Macromolecule film former, no more than 5 parts by weight；
Polyalcohol moisturizer, 10-30 parts by weight；
Moisturizing grease, 5-15 parts by weight；
Deionized purified water 20-100 parts by weight,
Wherein, the ratio of sodium metasilicate magnesium lithium and polymeric rheology conditioning agent is 1 weight % to 30 weight %；
The polymeric rheology conditioning agent is at least two in following polymer：(A) acrylic acid (ester) class/C10-30 alkane
Alcohol acrylate crosspolymers；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen copolymer
Sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum.
It is further preferred that also containing at least one of preservative, essence in the BB frosts.
It is further preferred that also contain powerful moisturizer in the BB frosts, as beta glucan, Sodium Hyaluronate, ursin,
In polyglutamic acid, glycine betaine, trehalose, biological polyoses glue, purslane extract, Narcissus Tazetta L. Var extract and erythrite at least
It is a kind of.
Preferably, another technical solution of the application provides a kind of preparation method of above-mentioned BB frosts, it includes as follows
Step：
1) by polymeric rheology conditioning agent and the mixed liquor of water, it is added in the mixed liquor of sodium metasilicate magnesium lithium and water, with equal
Then matter machine homogeneous uniform adds polyalcohol moisturizer, is warming up to 80-90 DEG C to no particle colloid；
2) step 1) is added after mixing emulsifying agent, pretreatment colorant slurry and moisturizing grease homogeneous to fine and smooth uniform sizing material
Gained mixture, homogeneous to uniform lotion, adds film forming agent, is cooled to 35 DEG C after mixing, takes part lotion censorship qualified
Discharging.
It is further preferred that when in BB frosts also containing at least one of preservative, essence, the preparation method step
2 operation is as follows：Step is added after emulsifying agent, pretreatment colorant slurry and moisturizing grease homogeneous are mixed to fine and smooth uniform sizing material
1) gained mixture, homogeneous to uniform lotion, adds film forming agent, is cooled to 45 DEG C after mixing, adds essence and preservative；
35 DEG C are finally cooled to, takes the qualified discharging of part lotion censorship.
Compared with prior art, the BB frosts that the application provides have following beneficial effect：
(1) the BB frosts that the application provides are easy to apply due to its special g., jelly-like appearance, and it is good to hide lump in the abdomen effect, dressing naturally,
Endurance is strong, it is sustainable 8 it is small when more than not spend adornment.
(2) the BB frosts that the application provides have excellent stability, easily stored, safe, water resistant good film-forming property, clearly
Refreshing degree is high, easy to clean, and user experience is high.
(3) BB frosts provided by the invention are safe, and long-time service is not in that the skins such as the obscure, comedo and acne of skin are asked
Topic.
Embodiment
The present invention is further elaborated with reference to embodiment.These embodiments are only in order at purpose of explanation,
And do not limit the scope of the invention and essence.Unless otherwise instructed, the unit of weight of each component is g in the embodiment of the present invention.
Embodiment 1-4
It is as shown in table 1 below, for the formula of the embodiment 1-4 not de- adornment BB frosts of g., jelly-like provided：
The preparation process of BB frosts described in above-described embodiment is as follows：
1) A1, A2 phase are uniformly dispersed respectively with homogenizer, then A phases 1 are added to A2 after mixing and continue homogeneous extremely
Without particle colloid A phases, A3 phases are then added, are warming up to 85 DEG C；
2) B1, B2 phase homogeneous mix to fine and smooth uniform sizing material and obtain B phases；
3) B is added to A phases, homogeneous to uniform lotion, adds C phases, start to cool down；
4) 35 DEG C are cooled to, takes the qualified discharging of part lotion censorship.
Embodiment 5-8
Such as table 2 below, the formula of adornment BB frosts is not taken off for the g., jelly-like of embodiment 5-8 offers：
The preparation process of each embodiment BB frosts is substantially the same as embodiment 1-4.
Performance test
1st, high temperature low tempertaure storage stability test
BB frosts prepared by each embodiment are fitted into the PET bottle of 30mL, circulation storage 3 times at -10 DEG C and 40 DEG C, respectively
Storage 24h every time, i.e., after -10 DEG C are stored 24h, store 24h, place into 40 DEG C of insulating boxs and store 24h, successively at room temperature
Circulation 3 times, observes the stability of product, and judged according to following 3 grade determinating references.Test result is shown in Table 3.Its
In,
A represents that compared with before experiment appearance is without obvious permeability, bleed, coarse grain or demulsifying phenomenon；
B is represented compared with before experiment, there is slight permeability, bleed, coarse grain or demulsifying phenomenon；
C is represented compared with before experiment, there is obvious permeability, bleed, coarse grain or demulsifying phenomenon.
2nd, centrifugal stability is tested
One day is stood after the completion of the product that Example provides, takes 8-10g lotions in centrifuge tube, the 3000r/ in centrifuge
Min, centrifuges 30min, observes the stability of product, and judged according to above-mentioned 3 grade determinating references.Test result is shown in Table
3。
3rd, water resistant film forming is tested
Specific test method is as follows：
A. 80 female subjects are chosen, the range of age 20-45 Sui, is randomly divided into 8 groups, every group of 10 people first will with ink
The left face of subject and the dyeing of right face；
B. sample to be tested is coated in dyeing part；
C. the ink of SLES solution washes away subject's test positions is used, and observes the shade of test position, color is deep
It is shallow to be given a mark by 8 skilled researchers, be 0 point without color, color it is the same with before not rinsing for 10 points, calculate and put down
Equal score.Test result is shown in Table 3.
4th, salubrious property test
Choosing 80 has the female subjects being accustomed to using color make-up product, and the range of age 20-45 Sui, is randomly divided into 8 groups, often
10 people of group.Subject passes through face cleaning successively, toner, and the product that 1-8 of the embodiment of the present invention is provided is smeared after skin care milk, and sense organ is commented
Valency product is clearly spent, and scoring criterion is as follows：
Without greasy feeling, clearly spend it is very satisfied for 9-10 points,
There is dividing for 7-8 for slight greasy feeling,
There is dividing for 4-6 for greasy feeling,
There is dividing for 1-3 for obvious greasy feeling,
Stronger soapy feeling is 0 point,
Calculate average.Test result is shown in Table 3.
The performance measurement result for the BB frosts that 3 each embodiment of table provides
4th, clean-up performance is tested
Choosing 90 has the female subjects being accustomed to using color make-up product, and the range of age 20-45 Sui, is randomly divided into 9 groups, often
10 people of group.Subject smear according to a conventional method 1-8 of the embodiment of the present invention offer product and commercially available BB frost (hundred sparrow antelope water tenderizers are pure
Star repaiies Yan Shuan), 8 it is small when after using hundred sparrow antelope water tender net extract cleanser (being suitable for all skin quality), warm water face cleaning thoroughly.Sense
Official evaluates the easy removing performance of product, and gives a mark by following standard：
9-10 very easy to clean points,
6-8 more easy to clean points,
3-5 easy to clean points,
0-2 not easy to clean points,
Calculate average.Test result is shown in Table 4.
Research staff, will be pre- in embodiment 1 in order to further inquire into influence of the pretreatment colorant slurry for spatter property
Colorant slurry is handled to replace using undressed colorant slurry, other constant, obtained BB frosts carry out as above identical test,
As a result score value is 7.9, and with the increase (increasing to original 2 times) of colouring matter slurry dosage, too big influence is had no on score value.
In addition, research staff allows tested also using the method that subject is tested is randomly selected in as above performance test
Person uses product provided in an embodiment of the present invention, persistently using after 30 days, observing subjects skin's situation and being counted, as a result
It was found that the problems such as BB frosts that subject is provided using 1-8 of the embodiment of the present invention shade after 30 days without comedo and acne, skin.
Subject's reflection more than 90%, BB frosts are easy to apply, hide that lump in the abdomen effect is good, and dressing is naturally, endurance is strong, and sustainable 8
Adornment is not spent more than hour.
Only illustratively, the scope of the present invention is not limited thereto for above-mentioned example.To those skilled in the art
For modify be it will be apparent that the present invention only limited by scope.
Claims (10)
1. a kind of BB frosts of the not de- adornment of g., jelly-like, it contains following each component：
Sodium metasilicate magnesium lithium,
Polymeric rheology conditioning agent,
Emulsifying agent,
Colorant slurry is pre-processed,
Macromolecule film former,
Polyalcohol moisturizer,
Moisturizing grease,
Deionized purified water,
Wherein, the polymeric rheology conditioning agent is at least two in following polymer：(A) acrylic acid (ester) class/C10-30
Alkylol acrylamide acid esters cross-linked polymer；(B) carbomer sodium；(C) agarose gel；(D) acrylic acid (ester) class/acryloyl nitrogen copolymer
Sodium；(E) Scleroglucan；(F) compound of mosanom, cellulose, cellulose gum.
2. BB frosts according to claim 1, the ratio of the sodium metasilicate magnesium lithium and polymeric rheology conditioning agent is 1 weight %
To 30 weight %.
3. BB frosts according to claim 1, the additive amount of the sodium metasilicate magnesium lithium is 0.05-1.0 parts by weight.
4. BB according to any one of claim 1-3 frost, the polymeric rheology conditioning agent is (A), (B), (C) and
At least one of (D), with (F) mosanom, cellulose, cellulose gum compound combination.
5. BB frosts according to any one of claim 1-3, the HLB value of the emulsifying agent is 1-10.
6. BB frosts according to any one of claim 1-3, the additive amount of the emulsifying agent is 2-12 parts by weight.
7. BB frosts according to any one of claim 1-3, the additive amount of the pretreatment colorant slurry is 5-20 weight
Part.
8. BB frosts according to any one of claim 1-3, the additive amount of the macromolecule film former is no more than 5 weight
Part.
9. BB according to any one of claim 1-3 frost, the polyalcohol moisturizer is glycerine, propane diols, 1,3 the third two
At least one of alcohol, butanediol, dipropylene glycol, D-sorbite, Natrulon H-10 and polyglycereol -6.
10. BB according to any one of claim 1-3 frost, the moisturizing grease is vegetable oil, silicone oil, Synthetic Oil,
At least one of silicone oil quasi-grease and induction biosynthesis wax.
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| CN111529431A (en) * | 2020-05-12 | 2020-08-14 | 广东芭薇生物科技股份有限公司 | Composition with make-up maintaining and oil controlling effects and cosmetic |
| CN112932994A (en) * | 2021-02-26 | 2021-06-11 | 上海家化联合股份有限公司 | Sunscreen composition for reducing transdermal penetration of sunscreen |
| CN113440436A (en) * | 2020-03-26 | 2021-09-28 | 万华化学集团股份有限公司 | BB cream containing nonionic silicon-containing modified aqueous polyurethane dispersion |
| CN113440433A (en) * | 2021-06-28 | 2021-09-28 | 上海丽知品牌管理有限公司 | Smoothie-like makeup remover composition and preparation method thereof |
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| CN112932994A (en) * | 2021-02-26 | 2021-06-11 | 上海家化联合股份有限公司 | Sunscreen composition for reducing transdermal penetration of sunscreen |
| CN113440433A (en) * | 2021-06-28 | 2021-09-28 | 上海丽知品牌管理有限公司 | Smoothie-like makeup remover composition and preparation method thereof |
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