CN109044889B - Glossy and smooth matte lipstick and production process thereof - Google Patents

Glossy and smooth matte lipstick and production process thereof Download PDF

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CN109044889B
CN109044889B CN201811247431.2A CN201811247431A CN109044889B CN 109044889 B CN109044889 B CN 109044889B CN 201811247431 A CN201811247431 A CN 201811247431A CN 109044889 B CN109044889 B CN 109044889B
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parts
lipstick
mixture
oil
emollient
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CN109044889A (en
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楼彪
陈榕洪
石蓓君
从云玲
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Hangzhou Weikela Investment Co., Ltd.
Yu Qiongfei
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Hangzhou Weikela Investment Co ltd
Yu Qiongfei
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/89Polysiloxanes
    • A61K8/891Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
    • A61K8/894Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone modified by a polyoxyalkylene group, e.g. cetyl dimethicone copolyol
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/001Preparations for care of the lips

Abstract

The invention discloses a sparkling and lubricous matte lipstick and a production process thereof. The sparkling, smooth and lubricous matte lipstick comprises the following components in parts by weight: 3-8 parts of butyl octanol salicylate; 10-20 parts of isohexadecane; 5-9 parts of diisostearyl malate; 0.1-1.2 parts of dimethyl silica silylate; 8-15 parts of polydimethylsiloxane; 2-8 parts of a first emollient; 10-15 parts of a second emollient; 3-7 parts of trimethylsiloxy silicate; 0.8-1.9 parts of sorbitan sesquiisostearate; 10-15 parts of a plastic forming agent; 3.5-5 parts of a thickening agent; 0.01-0.05 part of skin conditioner; 0.1-0.55 part of tocopherol acetate; 3.25 to 16.50 portions of colorant. The sparkling and smooth matte lipstick provided by the invention has the advantages of moistening, smoothness, refreshing and matte.

Description

Glossy and smooth matte lipstick and production process thereof
Technical Field
The invention relates to the technical field of lip cosmetics, in particular to a sparkling and smooth matte lipstick and a production process thereof.
Background
Lipstick is a common lip makeup product, can provide beautiful color for lips, and improves the quality of a user.
Chinese patents with application publication numbers of CN107519096A and application publication dates of 2017, 12 and 29 disclose a lubricating lipstick which mainly comprises the following components in parts by weight: 4-8 parts of natural pigment, 13-20 parts of natural wax, 45-75 parts of natural grease, 3-6 parts of natural perfume and 2-5 parts of other natural functional additives; wherein the natural wax comprises candelilla wax, olive wax and beeswax; the natural oil is composed of Aloe oil, jojoba oil, shea butter, oleum Armeniacae amarum, oleum ricini, and oleum Lavandula Angustifolia.
Although the prior art uses a few components, the main components are natural and nontoxic, the natural wax is composed of candelilla wax, olive wax and beeswax, the natural oil is composed of aloe oil, jojoba oil, shea butter, almond oil, castor oil and lavender oil, and although the components can show a moistening effect, the permeability is poor, the possibility of the components being absorbed by lip skin is low, the lips are easily sticky and not smooth enough, and meanwhile, the mirror surface gloss of the lips is too strong, so that the experience of a user is reduced.
Disclosure of Invention
In view of the defects in the prior art, the first object of the present invention is to provide a glossy and smooth matte lipstick, which has the advantages of moistening, smoothness, refreshing and matte.
The second purpose of the invention is to provide a production process of the sparkling and lubricous matte lipstick, which has the advantages of fast production of the lipstick and no influence on the appearance of the lipstick obtained by production.
In order to achieve the first object, the invention provides the following technical scheme:
a sparkling and smooth matte lipstick comprises the following components in parts by weight:
3-8 parts of butyl octanol salicylate;
10-20 parts of isohexadecane;
5-9 parts of diisostearyl malate;
0.1-1.2 parts of dimethyl silica silylate;
8-15 parts of polydimethylsiloxane;
2-8 parts of a first emollient;
10-15 parts of a second emollient;
3-7 parts of trimethylsiloxy silicate;
0.8-1.9 parts of sorbitan sesquiisostearate;
10-15 parts of a plastic forming agent;
3.5-5 parts of a thickening agent;
0.01-0.05 part of skin conditioner;
0.1-0.55 part of tocopherol acetate;
3.25-16.50 parts of a coloring agent;
the first moistening agent comprises at least one of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane;
the second moistening agent is a mixture of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polydimethylsiloxane;
the plasticizer comprises at least one of polyethylene and synthetic wax;
the thickener comprises at least two of hydrogenated olive oil, olive fruit oil and olive oil unsaponifiable matter;
the skin conditioner comprises at least two of sunflower seed oil, shea butter, olive oil and rose oil.
By adopting the technical scheme, in the application, adopted isohexadecane not only has the effect of dissolving other components, but also can increase the effect of softening and moistening, and is favorable for improving the texture of the matte lipstick in the application. The diisostearyl malate has skin softening effect. The polydimethylsiloxane has waterproof performance, and in addition, the foaming condition among components can be reduced on one hand, and the polydimethylsiloxane can also play a role in softening and moistening the skin on the other hand; and the high-purity polydimethylsiloxane is non-toxic and harmless, has a silky feeling, is beneficial to enabling the lipstick in the application to form a fresh, non-sticky and waterproof film when in use, has light and non-heavy texture, and can also achieve the purpose of moistening the skin of lips. Trimethylsiloxy silicate and diisostearyl malate form a mutual coordination effect, so that the effects of inhibiting bubbles, removing bubbles and refreshing and not being sticky are further improved, and the lipstick obtained in the application is not easy to have the phenomenon of being stained with a cup and the like.
The sorbitan sesquiisostearate is a water-in-oil emulsifier, so that the components of the water phase and the oil phase adopted in the application can be fully mixed, and the phenomenon of layering is not easy to occur; furthermore, sorbitan sesquiisostearate also has skin moisturizing effect.
The butyl octanol salicylate has the functions of softening skin and stabilizing the system; the silica dimethyl silylate has the functions of moistening skin, controlling viscosity and stabilizing liquid phase system. The butyl octanol salicylate can be matched with the dimethyl silica silylate to achieve better color fixing effect, so that the lipstick obtained in the application can keep gorgeous color for a long time.
In the first emollient, the C26-28 alkyl polydimethylsiloxane has good emollient, dispersing and film forming effects; polymethylsilsesquioxane has good smoothness and helps to maintain good color for the lipstick herein. The C26-28 alkyl polydimethylsiloxane and the polymethylsilsesquioxane can be used independently or together to form a synergistic effect, so that the moistening, refreshing and non-sticky effects of the formed lipstick are improved. In the second emollient, the dimethicone/vinyl dimethicone crosspolymer and dimethicone form a mutual cooperation, help improving the moist, fresh and non-sticky feel of lipstick in this application. And the first emollient and the second emollient are mutually matched, so that the matte effect of the lipstick can be improved, the phenomenon that the mirror surface is too bright when the grease is too much is avoided, namely the matte effect is achieved, the requirements of consumers who like the matte effect are met, and meanwhile, the lipstick can have a better moisturizing effect and keep good refreshing feeling, and the phenomenon of greasiness is not easy to occur.
In the plastic forming agent, polyethylene and synthetic wax both have a relatively balanced dispersion effect and a relatively balanced adhesion effect, so that the purpose of controlling the viscosity of a liquid phase system is achieved, the components adopted in the application can be fully dispersed, and the lipstick can be formed.
In the thickening agent, hydrogenated olive oil, olive fruit oil and olive oil unsaponifiable matters have certain sticky feeling, and the sticky feeling of a liquid phase system is improved. In addition, the hydrogenated olive oil has emulsifying and skin softening effects, the olive fruit oil is helpful for grinding, and the olive oil unsaponifiable matter has skin moistening effects. In the three components, the three components can be mutually matched, so that the lipstick is beneficial to improving the sticky feeling, is not easy to generate fluid feeling and is beneficial to promoting the forming.
In the skin conditioner, sunflower seed oil, shea butter, olive oil and rose oil all have the effect of softening the skin. The sunflower seed oil contains abundant vitamin E and linoleic acid, has good oxidation resistance and capability of promoting epidermal defense, and is helpful for keeping skin moist. The shea butter is rich in unsaturated fatty acid, triterpene alcohol, vitamin E, vitamin A and allantoin, is easy to be absorbed by skin, and has outstanding effects of enhancing skin moisturizing ability, preventing skin moisture loss, helping wound healing, increasing skin defense ability and the like. The olive fruit oil has the functions of moistening skin, keeping moisture and locking water. The rose oil has pleasant fragrance, is easily absorbed by skin, and is not easy to make skin greasy.
The tocopherol acetate has excellent effects of resisting grease oxidation and preserving moisture, can maintain connective tissues from being influenced by external environment, keeps the skin soft, relieves inflammation and the like.
In addition, the colorants used in the present application are environmentally friendly and harmless to the human body.
More preferably: the first moistening agent consists of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane in the weight ratio of (1-3.5) to 1.
By adopting the technical scheme, researches (experiment I) show that the cooperation of the C26-28 alkyl polydimethylsiloxane and the polymethylsilsesquioxane in the proportion range is beneficial to further improving the moistening but non-sticky effect of the obtained first moistening agent.
More preferably: the second moistening agent consists of polydimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer in the weight portion ratio of 3: 1.
By adopting the technical scheme, researches (experiment I) show that the mutual matching of the polydimethylsiloxane and the polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer in the proportion is beneficial to further improving the moistening but non-sticky effect of the obtained second moistening agent, so that the second moistening agent and the first moistening agent can achieve a better matching effect.
More preferably: the plasticizer consists of polyethylene and synthetic wax in the weight ratio of 1 to (1-1.5).
By adopting the technical scheme, the polyethylene and the synthetic wax in the proportion range are matched with each other, so that the plastic forming agent is favorable for achieving a better forming effect, and the lipstick is easy to process and produce.
More preferably: the thickener comprises the following components in percentage by weight:
60-70% of hydrogenated olive oil;
20-35% of olive fruit oil;
5-10% of olive oil unsaponifiable matter.
By adopting the technical scheme, researches (experiment I) find that the thickener is prepared by mutually matching hydrogenated olive oil, olive fruit oil and olive oil unsaponifiable matters in the weight percentage content range, so that the lipstick in the application can be more favorably matched with each component to achieve proper viscosity, and can keep the effects of moistening and silky lipstick.
More preferably: the skin conditioner comprises sunflower seed oil, shea butter, olive fruit oil and rose oil.
By adopting the technical scheme, the sunflower seed oil, the shea butter, the olive oil and the rose oil can be matched with each other, so that the lipstick can achieve a better effect of moistening the skin of the lips.
More preferably: also comprises 0.1 to 0.5 weight portion of preservative.
Through adopting above-mentioned technical scheme, the shelf life that adds of antiseptic helps making the lipstick in this application is longer, can maintain stable state of moistening, not sticky greasy and having the matte effect for a long time.
More preferably: the preservative consists of phenoxyethanol and caprylyl glycol in a weight part ratio of 1.86: 1.
By adopting the technical scheme, the phenoxyethanol and the caprylyl glycol in parts by weight are matched with each other, so that the antiseptic effect is achieved, and the lip skin is not easily damaged.
In order to achieve the second object, the invention provides the following technical scheme:
a production process of sparkling, moist and smooth matte lipstick comprises the following steps:
step one, according to parts by weight, sufficiently mixing butyl octanol salicylate, isohexadecane, diisostearyl malate, dimethyl silylated silica, polydimethylsiloxane, a first emollient, a second emollient, trimethylsiloxy silicate, sorbitan sesquiisostearate, a plastic forming agent and a thickening agent to obtain a first mixture;
step two, fully mixing the skin conditioner, the tocopherol acetate and the preservative according to the parts by weight to obtain a second mixture;
step three, fully mixing the second mixture obtained in the step two with the first mixture obtained in the step one to obtain a third mixture;
step four, adding a colorant into the third mixture obtained in the step three according to the weight parts, and fully mixing to obtain a fourth mixture;
and step five, grinding and filling the fourth mixture obtained in the step four to obtain the glittering and lubricous matte lipstick.
Through adopting above-mentioned technical scheme, mix first mixture, second mixture respectively, help improving the mixing homogeneity of the first mixture that obtains, second mixture, and then when first mixture, second mixture mix in step three, more laborsaving and more be favorable to making the third mixture that obtains have better homogeneity. The colorant is added to the third mixture in step four to facilitate uniform dispersion of the colorant. After the finally obtained fluid fourth mixture is ground, the granular substances possibly existing in the fluid fourth mixture can be finely ground, and the obtained lipstick has fine, uniform and glossy texture.
More preferably: in the first step, the mixture is heated to 90-100 ℃ during mixing; in the second step, the first mixture obtained in the first step is cooled to 70-80 ℃, and then is fully mixed with a skin conditioner, tocopherol acetate and a preservative; in the fourth step, the third mixture in the third step is kept at the temperature of 70-80 ℃ and mixed with the colorant.
By adopting the technical scheme, in the step one, the temperature range is favorable for realizing melting and mixing of the components, and is favorable for enabling the mixing to be more uniform and sufficient. And in the second step, the temperature of the first mixture is reduced to the temperature range, so that the effective components in the added skin conditioner, the tocopherol acetate and the preservative can be effectively reserved, and the skin conditioner, the tocopherol acetate and the preservative are not easy to damage to cause the reduction of the effect. In step four, the colorant is better mixed with the third mixture in this temperature range.
In conclusion, the invention has the following beneficial effects:
first, first emollient and second emollient mutually support, help improving the matte sense of lipstick, and do not have the too strong phenomenon of mirror surface light sense that appears when grease is too much, reach the effect of matte promptly to satisfy the consumer's that likes the matte sense demand, still can make the lipstick have better moist effect and make it keep good fresh and cool feeling simultaneously, the greasy phenomenon is difficult for appearing.
Secondly, through mutually supporting of thickener, skin conditioner, tocopherol acetate, help improving the effect that various nutrient composition in the lipstick in this application permeate lip skin to make lip skin reach and moisturize, smooth, fresh and cool effect, be difficult for appearing the sense of viscosity, be favorable to improving user's experience sense.
Thirdly, through the mutual matching of the butyl octanol salicylate and the dimethyl silyl silica, the lipstick can be applied to achieve a better color fixing effect, so that the gorgeous color can be maintained for a long time.
Detailed Description
The present invention will be described in further detail with reference to examples.
Example 1: the sparkling and smooth matte lipstick comprises the components and corresponding parts by weight shown in Table 1, and is prepared by the following steps:
heating butyl octanol salicylate, isohexadecane, diisostearyl malate, dimethyl silylated silica, polydimethylsiloxane, a first emollient, a second emollient, trimethylsiloxy silicate, sorbitan sesquiisostearate, a plasticizer and a thickening agent to 95 ℃, and fully mixing to obtain a first mixture;
step two, cooling the first mixture obtained in the step one to 75 ℃, and fully mixing the skin conditioner, the tocopherol acetate and the preservative to obtain a second mixture;
step three, fully mixing the second mixture obtained in the step two with the first mixture obtained in the step one to obtain a third mixture;
step four, adding a colorant to the third mixture obtained in step three, at which point the process is carried out at a temperature of 75 ℃, and thoroughly mixing to obtain a fourth mixture;
and step five, grinding and filling the fourth mixture obtained in the step four to obtain the glittering and lubricous matte lipstick.
Wherein the first moistening agent consists of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane in a weight part ratio of 1: 1;
the second moistening agent consists of polydimethylsiloxane and polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer in the weight portion ratio of 3: 1;
the plastic forming agent consists of polyethylene and synthetic wax with the weight portion ratio of 1: 1.2;
the thickener comprises 60 wt% of hydrogenated olive oil, 35 wt% of olive fruit oil and 5 wt% of olive oil unsaponifiable matter; the skin conditioner consists of sunflower seed oil, shea butter, olive oil and rose oil in the weight ratio of 1: 1;
the preservative consists of phenoxyethanol and caprylyl glycol in a weight portion ratio of 1.86: 1.
Examples 2 to 5: a clear and smooth matte lipstick is different from the lipstick in example 1 in that the components and the corresponding parts by weight are shown in Table 1.
TABLE 1 Components and their respective parts by weight (parts) included in examples 1-5
Figure BDA0001840097810000071
Example 6: a glittering and translucent matte lipstick is different from the lipstick prepared in example 2 in that the first moistening agent consists of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane in a weight portion ratio of 1.9: 1.
Example 7: a glittering and translucent matte lipstick is different from the lipstick prepared in example 2 in that the first moistening agent consists of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane in a weight portion ratio of 3.5: 1.
Example 8: a glittering and translucent matte lipstick, differing from example 2 in that the second humectant is C26-28 alkyl dimethicone.
Example 9: a clear and smooth matte lipstick, differing from example 2 in that the second humectant was polymethylsilsesquioxane.
Example 10: a clear and smooth matte lipstick is different from the lipstick prepared in example 2 in that a plasticizer consists of polyethylene and synthetic wax in a weight ratio of 1: 1.
Example 11: a clear and smooth matte lipstick is different from the lipstick prepared in example 2 in that a plasticizer consists of polyethylene and synthetic wax in a weight ratio of 1: 1.5.
Example 12: a clear and smooth matte lipstick differed from example 2 in that the plasticizer was polyethylene.
Example 13: a clear and smooth matte lipstick differed from example 2 in that the plasticizer was a synthetic wax.
Example 14: a sparkling and smooth matte lipstick is different from the lipstick prepared in the embodiment 2 in that the skin conditioner consists of sunflower seed oil, shea butter, olive oil and rose oil in a weight ratio of 1: 1.1: 1.2: 1.5.
Example 15: a sparkling and smooth matte lipstick is different from the lipstick prepared in the embodiment 2 in that the skin conditioner consists of shea butter and rose oil in a weight ratio of 1: 1.
Example 16: a clear and smooth matte lipstick is different from example 2 in that the skin conditioner consists of sunflower seed oil and olive fruit oil in a weight ratio of 1.8: 1.
Example 17: a clear and smooth matte lipstick is different from the lipstick prepared in example 2 in that the thickening agent consists of 68 weight percent of hydrogenated olive oil, 25 weight percent of olive oil and 7 weight percent of olive oil unsaponifiable matter.
Example 18: a sparkling and smooth matte lipstick is different from the lipstick prepared in example 2 in that a thickening agent consists of 70 wt% of hydrogenated olive oil, 20 wt% of olive fruit oil and 10 wt% of olive oil unsaponifiable matter.
Example 19: a sparkling and smooth matte lipstick is different from the lipstick prepared in example 2 in that a thickening agent consists of hydrogenated olive oil and olive fruit oil in a weight ratio of 1: 2.5.
Example 20: a clear and smooth matte lipstick is different from the lipstick prepared in example 2 in that the thickening agent consists of hydrogenated olive oil and olive oil unsaponifiable matter in the weight ratio of 1: 1.
Example 21: a clear and smooth matte lipstick is different from the lipstick prepared in example 2 in that the thickening agent consists of olive oil and olive oil unsaponifiable matter in the weight ratio of 1.3: 1.
Example 22: a sparkling and smooth matte lipstick is different from the lipstick prepared in the example 2 in that in the step one, the mixture is heated to 90 ℃; in the second step, the first mixture obtained in the first step is cooled to 70 ℃, and then is fully mixed with a skin conditioner, tocopherol acetate and a preservative; in step four, the third mixture of step three is kept at a temperature of 70 ℃ and mixed with the colorant.
Example 23: a sparkling and smooth matte lipstick is different from the lipstick prepared in the example 2 in that in the step one, the mixture is heated to 100 ℃; in the second step, the first mixture obtained in the first step is cooled to 80 ℃, and then is fully mixed with a skin conditioner, tocopherol acetate and a preservative; in step four, the third mixture of step three is kept at a temperature of 80 ℃ and mixed with the colorant.
Comparative example 1: the lubricating lipstick is different from the lubricating lipstick in example 2 in that the scheme in example 1 disclosed in patent documents with application publication number of CN107519096A and application publication date of 2017, 12 and 29 is as follows: 4 parts of cranberry juice, 4 parts of candelilla wax, 6 parts of olive wax, 8 parts of beeswax, 5 parts of aloe oil, 9 parts of jojoba oil, 6 parts of shea butter, 10 parts of almond oil, 20 parts of castor oil, 3 parts of lavender oil, 0.5 part of vitamin E, 1.2 parts of vitamin B and 120.3 parts of vitamin B.
Comparative examples 2 to 5: a lipstick differing from example 2 in that the components included and their respective parts by weight are shown in table 2.
TABLE 2 Included ingredients and their respective parts by weight (parts) in comparative examples 2-5
Figure BDA0001840097810000091
Comparative examples 6 to 9: a lipstick differing from example 2 in that the components included and their respective parts by weight are shown in table 3.
TABLE 3 Components and their respective parts by weight (parts) encompassed by comparative examples 6-9
Figure BDA0001840097810000092
Comparative examples 10 to 13: a lipstick differing from example 2 in that the components included and their respective parts by weight are shown in table 4.
TABLE 4 Components included in comparative examples 10-13 and their corresponding parts by weight (parts)
Figure BDA0001840097810000101
Comparative example 14: a lipstick differing from example 2 in that in the production process, butyl octanol salicylate, isohexadecane, diisostearyl malate, dimethylsilylated silica, polydimethylsiloxane, first emollient, second emollient, trimethylsiloxysilicate, sorbitan sesquiisostearate, a plasticizer, a thickener, a skin conditioner, tocopherol acetate, a preservative, and a coloring agent were mixed together, and stirred at 95 ℃ for 0.5h to obtain lipstick.
Test one: experience test
Test samples: examples 1 to 23 and comparative examples 1 to 9 were selected as test samples to carry out the test.
Test subjects: 320 female white collars (hereinafter, referred to as subjects) in the same area, with age range of 25-30 years, healthy body, no inflammation on lips and similar moistening degree are selected and marked as 1-32 groups, and each group contains 10 persons.
The test method comprises the following steps: the subjects in groups 1-23 correspond to the use of examples 1-23, respectively, and the subjects in groups 24-32 correspond to the use of comparative examples 1-9, respectively.
The subjects of groups 1 to 28 applied the corresponding examples 1 to 23 and comparative examples 1 to 5 to the lips, observed the gloss sensation of the test samples on the lips of the subjects, recorded and analyzed;
subjects of groups 1-24, 29-32 applied the corresponding examples 1-23, comparative examples 1, comparative examples 6-9 to the lips, and the test samples were observed for sliminess on the lips of the subjects, recorded and analyzed;
using examples 1-23 and comparative examples 1-9, respectively, in groups 1-32, the corresponding subjects applied the corresponding test samples to the lips once a day for 1 month, and collected experience feedback information as follows: evenness of smearing, lip moistening degree and lip line coverage degree. The sensory evaluation was performed on each item in five grades of 1-5, 1-5 being represented as: 1-very poor; 2-poor; 3-general; 4-good; 5-better. After each group of subjects was scored according to the above evaluation criteria, each group was scored and averaged with one decimal place kept, recorded and analyzed.
And (3) test results: the glossy feeling of examples 1 to 23 and comparative examples 1 to 5 is shown in Table 5; the sticky feel of examples 1-23, comparative example 1, and comparative examples 6-9 is shown in Table 6; the evenness of application, the degree of lip moistness and the degree of lip coverage of the subjects after using examples 1 to 23 and comparative examples 1 to 9 are shown in Table 7.
TABLE 5 gloss impression of examples 1-23, comparative examples 1-5
Test sample Sense of luster Test sample Sense of luster
Example 1 Fog face Example 15 Fog face
Example 2 Fog face Practice ofExample 16 Fog face
Example 3 Fog face Example 17 Fog face
Example 4 Fog face Example 18 Fog face
Example 5 Fog face Example 19 Fog face
Example 6 Fog face Example 20 Fog face
Example 7 Fog face Example 21 Fog face
Example 8 Fog face Example 22 Fog face
Example 9 Fog face Example 23 Fog face
Example 10 Fog face Comparative example 1 Mirror surface and brightness
Example 11 Fog face Comparative example 2 Strong mirror sense
Example 12 Fog face Comparative example 3 Strong mirror sense
Example 13 Fog face Comparative example 4 Strong mirror sense
Example 14 Fog face Comparative example 5 Strong mirror sense
As is clear from Table 5, the effect of the matte surface was achieved after the coating of examples 1 to 23, while the gloss of the mirror surface was clearly exhibited on the lips and the gloss was strong after the coating of comparative examples 1 to 5.
The main reasons for this are: the grease contained in comparative example 1 was mainly absorbed by the skin of lips, which is less delicate, and although evaporation of water inside the skin of lips was prevented after application, the grease enhanced the sense of brilliance.
In comparative examples 2 to 5, the amounts of the first emollient and the second emollient were not within the reasonable ranges of protection, and it was difficult to sufficiently mix with other components added, resulting in a strong mirror-like feel.
TABLE 6 slimy feel of examples 1-23, comparative example 1, comparative examples 6-9
Test sample Sticky feeling Test sample Sticky feeling
Example 1 Good absorption, no stickiness and refreshing Example 15 Good absorption, no stickiness and refreshing
Example 2 Good absorption, no stickiness and refreshing Example 16 Good absorption, no stickiness and refreshing
Example 3 Good absorption, no stickiness and refreshing Example 17 Good absorption, no stickiness and refreshing
Example 4 Good absorption, no stickiness and refreshing Example 18 Good absorption, no stickiness and refreshing
Example 5 Good absorption, no stickiness and refreshing Example 19 Good absorption, no stickiness and refreshing
Example 6 Good absorption, no stickiness and refreshing Example 20 Good absorption, no stickiness and refreshing
Example 7 Good absorption, no stickiness and refreshing Example 21 Good absorption, no stickiness and refreshing
Example 8 Good absorption, no stickiness and refreshing Example 22 Good absorption, no stickiness and refreshing
Example 9 Good absorption, no stickiness and refreshing Example 23 Good absorption, no stickiness and refreshing
Example 10 Good absorption, no stickiness and refreshing Comparative example 1 Poor absorption, stickiness and heaviness
Example 11 Good absorption, no stickiness and refreshing Comparative example 6 Poor absorption, sticky and heavy
Example 12 Good absorption, no stickiness and refreshing Comparative example 7 Poor absorption, sticky and heavy
Example 13 Good absorption, no stickiness and refreshing Comparative example 8 Poor absorption, sticky and heavy
Example 14 Good absorption, no stickiness and refreshing Comparative example 9 Poor absorption, sticky and heavy
As can be seen from Table 6, examples 1-23 absorbed the skin of the lips well and helped to help other components to be absorbed by the skin of the lips, so that after the application of examples 1-23, the lips were kept fresh and non-sticky, and the components absorbed by the skin of the lips were sufficient to nourish the skin, thereby nourishing the skin of the lips; in comparative example 1, however, the main component was oil and fat, and the oil and fat content was high, so that it was difficult to be absorbed into the skin of the lips, resulting in a heavy and sticky feeling after application.
In comparative examples 6-9, the thickening agent, the skin conditioner and the tocopherol acetate are not used in reasonable ranges, so that other components are difficult to be sufficiently absorbed by the skin of lips, and the phenomena of sliminess and heaviness are caused.
TABLE 7 evenness of spread, lip moistness, lip coverage of subjects using examples 1-23 and comparative examples 1-9
Figure BDA0001840097810000131
As is clear from Table 7, the average scores of the coating uniformity, lip gloss and lip coverage of examples 1 to 23 were higher than the average scores of the coating uniformity, lip gloss and lip coverage of comparative examples 1 to 9, respectively.
The main reasons for the above differences are: in comparative example 1, the content of the main component, namely oil is high, and although the dispersibility is good, the added components can be fully dispersed, but the oil is difficult to be absorbed by the skin of the lips, so that other components are difficult to be fully permeated into the skin of the lips, the skin of the lips cannot be nourished, the skin moistening degree is poor, and the lip wrinkle coverage is serious, namely the numerical value is low;
in comparative examples 2 to 5, the first emollient and the second emollient are not used in reasonable protection ranges and are difficult to form sufficient coordination with other added components, so that the nourishing effect on the skin of lips is poor, but compared with comparative example 1, the moisturizing effect on the lips is better, the coverage of the cheilogramma is slightly better, namely the numerical value is slightly higher;
in comparative examples 6 to 9, since the thickening agent, the skin conditioner, and the tocopherol acetate were not used in a reasonable range, other components thereof were not sufficiently absorbed by the skin of lips, resulting in severe insufficiency of moisturizing and nourishing of the skin of lips, and finally resulted in more lip coverage, i.e., lower values, than those of comparative examples 1 to 5.
And (2) test II: fixation test
Test samples: examples 1 to 23 and comparative examples 10 to 14 were selected as test samples to carry out the test.
Test subjects: 280 female white collars (hereinafter referred to as subjects) in the same area, with age range of 25-30 years, healthy body, no inflammation on lips and similar moistening degree are selected and marked as 1-28 groups of 10 persons.
The test method comprises the following steps: the subjects in groups 1-23 correspond to the use of examples 1-23, respectively, and the subjects in groups 24-28 correspond to the use of comparative examples 10-14, respectively. The test subjects smeared the corresponding test samples on the lips, lightly pressed the lips with the mind-print facial tissue, observed whether the test samples were wiped by the facial tissue, recorded and analyzed.
And (3) test results: the fixation of examples 1 to 23 and comparative examples 10 to 14 is shown in Table 8.
TABLE 8 fixation of examples 1-23, comparative examples 10-14
Test sample Color fixing effect Test sample Color fixing effect
Example 1 Good fixation, no lipstick on the paper towel Example 15 Good fixation, no lipstick on the paper towel
Example 2 Good fixation, no lipstick on the paper towel Example 16 Good fixation, no lipstick on the paper towel
Example 3 Good fixation, no lipstick on the paper towel Example 17 Good fixation, no lipstick on the paper towel
Example 4 Good fixation, no lipstick on the paper towel Example 18 Good fixation, no lipstick on the paper towel
Example 5 Good fixation, no lipstick on the paper towel Example 19 Good fixation, no lipstick on the paper towel
Example 6 Good fixation, no lipstick on the paper towel Example 20 Good fixation, no lipstick on the paper towel
Example 7 Good fixation, no lipstick on the paper towel Example 21 Good fixation, no lipstick on the paper towelStamp
Example 8 Good fixation, no lipstick on the paper towel Example 22 Good fixation, no lipstick on the paper towel
Example 9 Good fixation, no lipstick on the paper towel Example 23 Good fixation, no lipstick on the paper towel
Example 10 Good fixation, no lipstick on the paper towel Comparative example 10 The lipstick on the paper towel is very dense
Example 11 Good fixation, no lipstick on the paper towel Comparative example 11 The lipstick on the paper towel is thicker
Example 12 Good fixation, no lipstick on the paper towel Comparative example 12 The lipstick on the paper towel is thicker
Example 13 Good fixation, no lipstick on the paper towel Comparative example 13 The lipstick on the paper towel is thicker
Example 14 Good fixation, no lipstick on the paper towel Comparative example 14 The paper towel has lipstick printed thereon and is not uniform
As can be seen from Table 8, the color of the paper towel of examples 1-23 was maintained after the paper towel was wiped, and the paper towel was not easily stuck, so the color fixing effect was good; while comparative examples 10-14 were able to be wiped off with paper towels to different degrees of lipstick and, therefore, were less effective in fixing.
The main reasons for this are: in comparative examples 10 to 13, the amounts of butyloctanol salicylate and dimethylsilylated silica were out of the reasonable range, and even the same parts by weight of the colorant were used, resulting in poor fixation of comparative examples 10 to 13; in the comparative example 14, the preparation process is simple and single, and the difference of the adopted components is not considered in a centralized manner, so that the effects of the components cannot be fully exerted, and the result of poor color fixing effect is finally caused.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.

Claims (10)

1. The glittering and lubricous matte lipstick is characterized by comprising the following components in parts by weight:
3-8 parts of butyl octanol salicylate;
10-20 parts of isohexadecane;
5-9 parts of diisostearyl malate;
0.1-1.2 parts of dimethyl silica silylate;
8-15 parts of polydimethylsiloxane;
2-8 parts of a first emollient;
10-15 parts of a second emollient;
3-7 parts of trimethylsiloxy silicate;
0.8-1.9 parts of sorbitan sesquiisostearate;
10-15 parts of a plastic forming agent;
3.5-5 parts of a thickening agent;
0.01-0.05 part of skin conditioner;
0.1-0.55 part of tocopherol acetate;
3.25-16.50 parts of a coloring agent;
the first emollient comprises at least one of C26-28 alkyl polydimethylsiloxane and polymethylsilsesquioxane;
the second emollient is a mixture of polydimethylsiloxane/vinyl polydimethylsiloxane cross-linked polymer and polydimethylsiloxane;
the plasticizer comprises at least one of polyethylene and synthetic wax;
the thickener comprises at least two of hydrogenated olive oil, olive fruit oil and olive oil unsaponifiable matter;
the skin conditioner comprises at least two of sunflower seed oil, shea butter, olive oil and rose oil.
2. A glittering and translucent matte lipstick as claimed in claim 1, wherein the first emollient is composed of C26-28 alkyl dimethicone and polymethylsilsesquioxane in the weight ratio of (1-3.5): 1.
3. A glittering and translucent matte lipstick according to claim 1, wherein the second emollient is comprised of dimethicone, dimethicone/vinyl dimethicone crosspolymer in a weight ratio of 3: 1.
4. A glittering and translucent matte lipstick as claimed in claim 1, wherein the plasticizer comprises polyethylene and synthetic wax in the weight ratio of 1 (1-1.5).
5. A glittering and translucent matte lipstick according to claim 1, which is characterized in that the thickener comprises the following components in percentage by weight:
60-70% of hydrogenated olive oil;
20-35% of olive fruit oil;
5-10% of olive oil unsaponifiable matter.
6. A glossy and clear matte lipstick as claimed in claim 1, wherein said skin conditioner is composed of sunflower seed oil, shea butter, olive oil, rose oil.
7. A sparkling and smooth matte lipstick according to claim 1, further comprising 0.1 to 0.5 parts by weight of a preservative.
8. A sparkling and smooth matte lipstick as claimed in claim 7, wherein the preservative comprises phenoxyethanol and caprylyl glycol in a weight ratio of 1.86: 1.
9. A process for producing a sparkling and smooth matte lipstick according to any one of claims 1 to 8, comprising the steps of:
step one, according to parts by weight, sufficiently mixing butyl octanol salicylate, isohexadecane, diisostearyl malate, dimethyl silylated silica, polydimethylsiloxane, a first emollient, a second emollient, trimethylsiloxy silicate, sorbitan sesquiisostearate, a plastic forming agent and a thickening agent to obtain a first mixture;
step two, fully mixing the skin conditioner, the tocopherol acetate and the preservative according to the parts by weight to obtain a second mixture;
step three, fully mixing the second mixture obtained in the step two with the first mixture obtained in the step one to obtain a third mixture;
step four, adding a colorant into the third mixture obtained in the step three according to the weight parts, and fully mixing to obtain a fourth mixture;
and step five, grinding and filling the fourth mixture obtained in the step four to obtain the glittering and lubricous matte lipstick.
10. A process for producing a glittering and translucent matte lipstick according to claim 9, wherein in the first step, the mixture is heated to 90-100 ℃; in the third step, the first mixture obtained in the first step is cooled to 70-80 ℃, and then is fully mixed with a second mixture formed by mixing the skin conditioner, the tocopherol acetate and the preservative in the second step; in the fourth step, the third mixture in the third step is kept at the temperature of 70-80 ℃ and mixed with the colorant.
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