CN110960449B - Smooth lipstick and its production process - Google Patents
Smooth lipstick and its production process Download PDFInfo
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- CN110960449B CN110960449B CN201911423429.0A CN201911423429A CN110960449B CN 110960449 B CN110960449 B CN 110960449B CN 201911423429 A CN201911423429 A CN 201911423429A CN 110960449 B CN110960449 B CN 110960449B
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
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- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
- A61Q1/06—Lipsticks
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Abstract
The invention discloses a moistening and smoothing lipstick and a production process thereof, belonging to the technical field of lipstick, and the lipstick comprises: 1-5% of ethylene/propylene copolymer; 5-10% of polyethylene; 2-8% of ozokerite; silica dimethyl silylate 0.1-4%; 6-15% of starch aluminum octenyl succinate; 5-10% of polyisobutylene; 3-9% of a first emollient; 0.1-2% of a second emollient; 10-20% of tri (octyldodecanol) citrate; 1-10% of phenyl isopropyl polydimethylsiloxane; 16-36% of a dispersant; 1-5% of trimethylsiloxy silicate; 2-6% of deionized water; 0.03-3% of humectant; 10-19% of hexyl laurate; 7-13% of a colorant; 0.5 to 1.0 percent of preservative; the first emollient comprises at least two of avocado oil, phytosterols, and olive oil; the second emollient comprises at least three of ethylhexyl palmitate, behenyl, sorbitan isostearate, palmitoyl tripeptide-1. The moistening smooth lipstick has the advantages of moistening, no fading and high temperature resistance, can bear the high temperature of 50 ℃, keeps good integrity, does not have the deflection phenomenon, and is favorable for long-distance transportation.
Description
Technical Field
The invention relates to the technical field of lipstick, in particular to a Yingrun smooth lipstick and a production process thereof.
Background
Lipstick is a kind of cosmetic for lip, and after it is used, it can show better smell, vitality and quality.
At present, the lipstick on the market has various types, and can meet the requirements of different consumers, such as moistening, no color loss, color change and the like.
Chinese patents with application publication numbers of CN110292545A and application publication dates of 2019, 07 months and 19 days disclose a pure plant lipstick, which comprises 10-16% of candelilla wax, 50-80% of vegetable oil and 10-25% of radish root extract; the vegetable oil comprises rosewood seed oil, shea butter, jojoba seed oil and grape seed oil.
Although the prior art is prepared from pure plant extracts, the contained plant oil contains the rosewood seed oil, the shea butter, the jojoba seed oil and the grape seed oil, which have the effects of safety and moistening, the color fading of the prior art is easily caused because the rosewood seed oil, the shea butter, the jojoba seed oil and the grape seed oil are contained. Meanwhile, in the process of exporting the lipstick to abroad, the lipstick is generally centralized in an integrated cabinet which is closed and has the temperature as high as 50 ℃, and because vegetable oil is used in the prior art, the lipstick is easy to melt or skew, so that trade disputes are easy to occur, the lipstick is not beneficial to sale and use, and the experience feeling of users is reduced.
Therefore, the lipstick which is moist, does not fade and has high temperature resistance has great market demand.
Disclosure of Invention
Aiming at the defects in the prior art, the first object of the invention is to provide a moist smooth lipstick which has the advantages of moistening, no fading and high temperature resistance.
The second purpose of the invention is to provide a production process of the moistening smooth lipstick, so that the prepared lipstick has the advantages of uniform texture and smooth surface.
In order to achieve the first object, the invention provides the following technical scheme:
the Yingrun smooth lipstick comprises the following components in percentage by weight:
1-5% of ethylene/propylene copolymer;
5-10% of polyethylene;
2-8% of ozokerite;
silica dimethyl silylate 0.1-4%;
6-15% of starch aluminum octenyl succinate;
5-10% of polyisobutylene;
3-9% of a first emollient;
0.1-2% of a second emollient;
10-20% of tri (octyldodecanol) citrate;
1-10% of phenyl isopropyl polydimethylsiloxane;
16-36% of a dispersant;
1-5% of trimethylsiloxy silicate;
2-6% of deionized water;
0.03-3% of humectant;
10-19% of hexyl laurate;
7-13% of a colorant;
0.5 to 1.0 percent of preservative;
the first emollient comprises at least two of avocado oil, phytosterols, and olive oil;
the second emollient comprises at least three of ethylhexyl palmitate, tribehenate, sorbitan isostearate and palmitoyl tripeptide-1.
By adopting the technical scheme, the ethylene/propylene copolymer has higher gloss than polyethylene wax, and is high-temperature resistant and low-temperature resistant. The polyethylene and the ozokerite can enable the lipstick to have better toughness and not to be easily broken.
The lipstick has the advantages that the ethylene/propylene copolymer, the polyethylene, the ozokerite, the silica dimethyl silylate and the aluminum starch octenyl succinate are matched with one another, so that the lipstick has a good high-temperature resistance function, can keep the integral feeling of the lipstick even at a high temperature in the transportation process, and is not easy to incline and adhere in the shell.
The polyisobutylene can improve the caking property of the lipstick, and the trimethylsiloxy silicate ester can ensure that the lipstick has a better film-forming effect, so that the lips of the lipstick coated with the polyisobutylene are full. The silica dimethyl silylate has better anti-caking effect, and the aluminum starch octenyl succinate has better adsorption and anti-caking capabilities. The polyisobutylene, the trimethylsiloxysilicate, the dimethyl silica silylate and the aluminum starch octenyl succinate are matched with each other, so that the obtained components added in the invention have better mixing uniformity, the viscosity is well adjusted, and the phenomena of caking and the like are not easy to occur.
Meanwhile, polyisobutylene and trimethylsiloxy silicate are matched with each other, so that the lipstick has the function of being difficult to remove makeup.
Tri (octyldodecanol) citrate has good skin moisturizing effect, and can protect delicate lip skin. The addition of the phenyl isopropyl polydimethylsiloxane can enable the lipstick to have smooth feeling, so that the smooth degree of smearing is improved, and the experience feeling of a user is improved.
Cetyl polydimethylsiloxane and triisostearin have good skin moistening and dispersing effects; in the first emollient, avocado oil, phytosterol and olive oil all have skin-friendly and moisturizing effects; in the second emollient, ethylhexyl palmitate, behenyl alcohol, sorbitan isostearate and palmitoyl tripeptide-1 can provide better moistening feeling.
Tests show that the mutual cooperation of the first emollient, the second emollient, the tri (octyl dodecanol) citrate, the phenyl isopropyl polydimethylsiloxane, the cetyl polydimethylsiloxane, the triisostearin, the trimethylsiloxysilicate, the ethylhexyl stearate, the betaine, the sodium hyaluronate and the ceramide 2 can help to improve the moistening degree and the skin painting feeling of the lipstick in the application.
More preferably: the first emollient is composed of avocado oil, phytosterols and olive fruit oil, and the ratio of the avocado oil to the phytosterols to the olive fruit oil is 51: 31: 18.
by adopting the technical scheme, researches show that when the avocado oil, the phytosterols and the olive fruit oil are composed, and the mass ratio of the avocado oil, the phytosterols and the olive fruit oil is as shown in the specification, the lipstick moistening feeling is further promoted.
More preferably: in the second emollient, the ratio of ethylhexyl palmitate, behenyl, sorbitan isostearate to palmitoyl tripeptide-1 is 74.9: 20: 5: 0.1.
by adopting the technical scheme, researches show that when the mass ratio of the ethylhexyl palmitate, the behenyl sanmate, the sorbitan isostearate and the palmitoyl tripeptide-1 is as shown above, the ethylhexyl palmitate, the behenyl sanmate, the sorbitan isostearate and the palmitoyl tripeptide-1 can form better matching with the first emollient, so that the lipstick can achieve better moistening feeling and has better smearing smoothness.
More preferably: the humectant consists of the following components in percentage by weight:
0.01-1% of betaine;
0.01-1% of sodium hyaluronate;
ceramide 2 is 0.01-1%.
By adopting the technical scheme, the betaine, the sodium hyaluronate and the ceramide 2 are added according to the weight percentage content range, so that components for nourishing lips in the obtained lipstick can be absorbed by the skin of the lips quickly, and the moistening effect is achieved.
More preferably: the dispersing agent comprises the following components in percentage by weight:
2-6% of cetyl polydimethylsiloxane;
8-15% of triisostearin;
6-15% of ethylhexyl stearate.
By adopting the technical scheme, when the dispersing agent adopts the components and is matched with the application amount, the components in the obtained lipstick are favorably and fully mixed, and the integral high-temperature resistance is good.
In order to achieve the second object, the invention provides the following technical scheme:
a production process of the Yingrun smooth lipstick comprises the following steps:
step one, fully mixing tri (octyldodecanol) citrate, phenyl isopropyl polydimethylsiloxane, a dispersing agent, trimethylsiloxysilicate and dimethyl silica silylate to obtain a first mixture;
step two, fully mixing aluminum starch octenyl succinate, hexyl laurate and a coloring agent to obtain a second mixture;
step three, fully mixing water and a humectant to obtain a third mixture;
fully mixing the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the phenoxyethanol, the first mixture and the second mixture to obtain a fourth mixture;
and step five, fully mixing the third mixture and the fourth mixture, and filling to obtain the thin and smooth lipstick.
By adopting the technical scheme, the first mixture, the second mixture and the third mixture are respectively mixed and then sequentially mixed, so that the obtained lipstick has more uniform texture and better overall moistening performance.
More preferably: in the first step, the tri (octyldodecanol) citrate, the phenylisopropyl polydimethylsiloxane, the dispersing agent and the trimethylsiloxysilicate are heated to 75-80 ℃, and then the silica dimethyl silylate is added, and the mixture is homogenized for 5-10min at the speed of 3000-3500 rpm.
By adopting the technical scheme, the tri (octyldodecanol) citrate, the phenylisopropyl polydimethylsiloxane, the dispersing agent and the trimethylsiloxy silicate are heated to 75-80 ℃, and the process can also be carried out by heating and stirring, and then the dimethyl silica silylate is added, so that the uniform dispersion is facilitated.
The temperature, homogenizing speed and homogenizing time all have great influence on the mixing uniformity of the components.
More preferably: in the second step, the starch aluminum octenyl succinate, the hexyl laurate and the colorant are fully mixed and then ground to a particle size of 0.7-2.5 μm to obtain a second mixture.
Through adopting above-mentioned technical scheme, grind to the particle diameter comparatively unified to help making the texture of the second mixture that obtains comparatively exquisite, in subsequent step, the too big phenomenon of particle diameter is difficult for appearing, still is favorable to making to mix more abundant and even.
More preferably: in the fourth step, the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the phenoxyethanol, the first mixture and the second mixture are completely dissolved at the temperature of 75-80 ℃ to obtain a fourth mixture.
By adopting the technical scheme, in the temperature range, the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient and the phenoxyethanol can be fully dissolved and can be fully mixed with the first mixture and the second mixture.
More preferably: in the fifth step, the third mixture and the fourth mixture are fully mixed at the temperature of 75-80 ℃; the temperature during filling is 75-80 ℃.
By adopting the technical scheme, when the temperature difference between the third mixture and the fourth mixture is not large, better mixing can be realized, and the uniformity degree of the obtained lipstick is higher. In addition, the filling is carried out within the temperature range, which is beneficial to ensuring that the obtained lipstick still can keep better fluidity and uniformity degree during filling.
In conclusion, the invention has the following beneficial effects:
firstly, the lipstick has a good high-temperature resistance function by mutually matching the ethylene/propylene copolymer, the polyethylene, the ozokerite, the silica dimethyl silylate and the aluminum starch octenyl succinate.
Secondly, the polyisobutylene and the trimethylsiloxy silicate are matched with each other, so that the lipstick has the function of difficult makeup removal.
Thirdly, the first emollient, the second emollient, the tri (octyldodecanol) citrate, the phenylisopropyl polydimethylsiloxane, the cetyl polydimethylsiloxane, the triisostearin, the trimethylsiloxysilicate, the ethylhexyl stearate, the betaine, the sodium hyaluronate and the ceramide 2 are matched with one another, so that the moisturizing degree and the skin painting feeling in the application are improved.
Detailed Description
The present invention will be described in further detail with reference to examples.
Example 1: the Yingrun smooth lipstick comprises the components and corresponding mass percentage contents shown in the table 1, and is prepared by the following steps:
firstly, heating tri (octyldodecanol) citrate, phenylisopropyl polydimethylsiloxane, a dispersing agent and trimethylsiloxysilicate to 80 ℃, adding dimethyl silica silylate, and homogenizing at 3000rpm for 5mi to obtain a first mixture;
step two, fully mixing aluminum starch octenyl succinate, hexyl laurate and a coloring agent, and grinding to obtain a second mixture, wherein the particle size of the second mixture is 0.7-2.5 microns;
step three, fully mixing water and a humectant to obtain a third mixture;
completely dissolving the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the phenoxyethanol, the first mixture and the second mixture at the temperature of 80 ℃ to obtain a fourth mixture;
step five, fully mixing the third mixture and the fourth mixture at the temperature of 80 ℃; filling at 80 deg.C to obtain the final product.
Wherein, the first emollient is composed of avocado oil, phytosterols, and olive fruit oil, and the ratio of avocado oil, phytosterols, and olive fruit oil is 51: 31: 18. in the second emollient, the ratio of ethylhexyl palmitate, behenyl, sorbitan isostearate and palmitoyl tripeptide-1 is 74.9: 20: 5: 0.1.
examples 2 to 5: the lubricous lipstick is different from the lipstick prepared in example 1 in that the components and the corresponding mass percentages are shown in table 1.
Table 1 components included in examples 1-5 and their corresponding mass percents
Example 6: the difference between the Yingrunshui lipstick and the Yingrunui lipstick in example 1 is that the first emollient is composed of avocado oil, phytosterols and olive oil in a ratio of 3:2: 1. The second emollient is prepared from 70.6: 25: 3.8: 0.1 of ethylhexyl palmitate, behenyl trimaran, sorbitan isostearate and palmitoyl tripeptide-1.
Example 7: the moisturizing and silky lipstick is different from the lipstick prepared in example 1 in that the first emollient is a mixture of 1: 1 avocado oil, phytosterols. The second emollient is prepared from the following components in a ratio of 11: 1: 1 of ethylhexyl palmitate, sorbitan isostearate and palmitoyl tripeptide-1.
Example 8: the moisturizing and silky lipstick is different from the lipstick prepared in example 1 in that the first emollient is a mixture of 3: 1 avocado oil, olive oil. The second emollient is composed of the following components in a ratio of 10: 6: 1 of ethylhexyl palmitate, behenyl trisilicate and palmitoyl tripeptide-1.
Example 9: the moisturizing smooth lipstick is different from the lipstick prepared in example 1 in that the steps in the production process are as follows:
step one, heating tri (octyldodecanol) citrate, phenylisopropyl polydimethylsiloxane, a dispersing agent and trimethylsiloxysilicate to 75 ℃, adding dimethyl silica silylate, and homogenizing at 3500rpm for 10mi to obtain a first mixture;
step two, fully mixing aluminum starch octenyl succinate, hexyl laurate and a coloring agent, and grinding to obtain a second mixture, wherein the particle size of the second mixture is 0.7-2.5 microns;
step three, fully mixing water and a humectant to obtain a third mixture;
completely dissolving the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the phenoxyethanol, the first mixture and the second mixture at the temperature of 75 ℃ to obtain a fourth mixture;
step five, fully mixing the third mixture and the fourth mixture at the temperature of 75 ℃; filling at 75 deg.C to obtain the final product.
Comparative example
Comparative example 1: a pure plant lipstick, which is different from example 1 in that it comprises candelilla wax 13% and rosewood seed oil 11%, shea butter 6%, jojoba seed oil 27%, grape seed oil 24.4%, radish root extract 18.5%, and magnolia bark extract 0.1%, as disclosed in example 1 of chinese patent publication No. CN110292545A, having publication date number 2019, 07/19.
The preparation method comprises the following steps:
(1) heating candelilla wax to 80-85 ℃, and stirring until the candelilla wax is dissolved uniformly;
(2) adding vegetable oil, stirring, and keeping the temperature;
(3) adding radix Raphani extract, stirring and dispersing;
(4) cooling to 65-70 ℃, adding the magnolia bark extract, uniformly stirring, filling and forming to obtain the pure plant lipstick.
Comparative examples 2 to 4: the lipstick differs from example 1 in that the components included and their respective mass percentages are shown in table 2.
TABLE 2 Components included in comparative examples 1 to 4 and their corresponding mass percents
Comparative examples 5 to 7: the lipstick differs from example 1 in that the components included and their respective mass percentages are shown in table 3.
TABLE 3 Components included in comparative examples 5 to 7 and their respective mass percentages
Comparative examples 8 to 10: the lipstick differs from example 1 in that the components included and their respective mass percentages are shown in table 4.
TABLE 4 Components and their respective percentages by mass included in comparative examples 8 to 10
Comparative example 11: lipstick, different from example 1, was obtained by adding all the components simultaneously and heating to 80 ℃ during the production process, stirring for 30min, and filling.
Test one: high temperature test
Test samples: examples 1 to 9 and comparative examples 1 to 4 (after filling) were used as test samples.
The test method comprises the following steps:
1. 3 samples are selected from each test sample respectively for parallel test. The lipstick sections in examples 1 to 9 and comparative examples 1 to 4 were each completely unscrewed under a constant temperature of 55 ℃ and placed and held horizontally without touching the plane, left to stand for 1 hour, and the condition of 3 parallel samples of each test sample was observed, recorded and analyzed.
2. 3 samples of each test are respectively selected for parallel test. The lipstick sections in examples 1 to 9 and comparative examples 1 to 4 were each completely unscrewed at a constant temperature of 70 ℃ and horizontally placed and kept out of contact with the flat surface, left to stand for 10min, and the condition of 3 parallel samples of each test sample was observed, recorded and analyzed.
And (3) test results: the high temperature resistance of examples 1 to 9 and comparative examples 1 to 4 is shown in Table 5.
TABLE 5 high temperature resistance of examples 1 to 9 and comparative examples 1 to 4
Test sample | 55℃,1h | 70℃,10min |
Example 1 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 2 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 3 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 4 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 5 | Three replicates were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 6 | Three replicates were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 7 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three replicates |
Example 8 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three parallel samples |
Example 9 | All three parallel samples were kept horizontal and not askew | No melting occurred in all three replicates |
Comparative example 1 | All three parallel samples are inclined | Three parallel samples all appeared melting |
Comparative example 2 | All three parallel samples are inclined | Three parallel samples all appeared melting |
Comparative example 3 | All three parallel samples are inclined | Melting occurred in two parallel samples |
Comparative example 4 | Three parallel samples all have skew | Three parallel samples all appeared melting |
As can be seen from Table 5, examples 1 to 9 were kept at 55 ℃ for 1 hour without skewing; the melting phenomenon did not occur when the alloy was left to stand at 70 ℃ for 10min, indicating that the high temperature resistance of examples 1 to 9 was excellent.
In comparative examples 1 to 4, the skew phenomenon occurred in the horizontal standing for 1 hour at 55 ℃; the melting phenomenon was observed even when the mixture was left standing at 70 ℃ for 10min, indicating that the comparative examples 1 to 4 had poor high temperature resistance.
The main reasons for the above differences are: the vegetable oil and fat used in comparative example 1 was not resistant to high temperature, and thus comparative example 1 could not withstand high temperatures of 55 c and 70 c, and the phenomena of skewing and melting occurred, respectively.
In comparative examples 2 to 4, the ethylene/propylene copolymer, polyethylene, ozokerite, silica dimethyl silylate, aluminum starch octenyl succinate were deleted to various degrees in the use of the components, and finally the high temperature resistance of comparative examples 2 to 4 was affected.
In summary, the comparative examples 1 to 4 require extra attention during transportation and need to place cooling supplies in the integrated cabinet, thereby easily causing the increase of transportation cost.
And (2) test II: test for observing color loss
Test samples: examples 1 to 9 and comparative examples 5 to 7 (after filling) were used as test samples.
The test method comprises the following steps: selecting 120 white-collar female subjects with similar lip skin moistening degree and age range of 25-30 years in the same region, averagely dividing into 12 groups, and respectively applying 10 subjects in each group to the subjects of examples 1-9 and comparative examples 5-7 in an application amount of 0.005g/cm2And after smearing, drawing paper with the same style by a mouth, observing the condition of the red mark on the paper towel, recording and analyzing.
And (3) test results: the discoloration of examples 1 to 9 and comparative examples 5 to 7 is shown in Table 6.
TABLE 6 discoloration of examples 1 to 9 and comparative examples 5 to 7
As can be seen from Table 6, the subjects using examples 1 to 9 did not show any discoloration, while the subjects using comparative examples 5 to 7 showed various degrees of discoloration. This indicates that: the polyisobutylene and the trimethylsiloxy silicate are compounded, and then are matched with other components in the lipstick, so that the lipstick has remarkable effect of preventing the lipstick from fading.
And (3) testing three: moisture test
Test samples: examples 1 to 9 and comparative examples 8 to 11 (after filling) were used as test samples.
The test method comprises the following steps: 39 white-collar female subjects with similar lip skin moistening degree and age range of 25-30 years in the same area are selected and averagely divided into 13 groups of 3 subjects. Examples 1-9 and comparative examples 8-11 were used in 13 groups of subjects, respectively. Before use, the average roughness of lips and the average depth of lip wrinkles were measured and recorded for 3 subjects in each group. The application amount of each subject is 0.005g/cm2The test period lasts 30 days, and the average roughness of lips and the average depth of cheilogramma of each subject are detected on 31 th day without using a test sample, and the change condition is recorded and analyzed.
And (3) test results: the degrees of moistening of examples 1 to 9 and comparative examples 8 to 11 are shown in Table 7.
TABLE 7 degree of moisturizing for examples 1 to 9 and comparative examples 8 to 11
As can be seen from Table 7, after the test period of one month, the lip roughness and the average depth of cheilogramma of each group of the subjects using the test subjects of examples 1 to 9 are improved significantly, which indicates that the test subjects of examples 1 to 9 have better moisturizing degree. In addition, the testee feels that the smearing process is smooth and the phenomenon of uneven smearing is not easy to occur in the using process.
And the subjects using the comparative examples 8-10 have no obvious change in lip roughness and average depth of cheilogramma after one month of test period, which indicates that the comparative examples 8-10 have poor moistening degree and are easy to have uneven smearing in the smearing use process.
The main reason for the above difference was that in comparative examples 8 to 10, the first emollient, the second emollient, tri (octyldodecanol) citrate, phenylisopropyl dimethicone, cetyl dimethicone, triisostearin, trimethylsiloxysilicate, ethylhexyl stearate, betaine, sodium hyaluronate, ceramide 2 were deleted to various degrees. The mutual matching of the first emollient, the second emollient, the tri (octyldodecanol) citrate, the phenylisopropyl polydimethylsiloxane, the cetyl polydimethylsiloxane, the triisostearin, the trimethylsiloxysilicate, the ethylhexyl stearate, the betaine, the sodium hyaluronate and the ceramide 2 is also proved to be beneficial to ensuring better moistening effect and smearing uniformity of the lipstick and improving the experience of users.
The subject using comparative example 11 showed more remarkable changes in lip roughness and average depth of chevrons over a one-month test period than those using comparative examples 8 to 10, but inferior to those of the subjects using examples 1 to 9, mainly because the mixing process of comparative example 11 did not allow sufficient mixing of all the added components during the production process, resulting in insufficient moisturizing of lipstick and insufficient uniformity of application.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.
Claims (9)
1. The moisturizing smooth lipstick is characterized by comprising the following components in percentage by weight:
1-5% of ethylene/propylene copolymer;
5-10% of polyethylene;
2-8% of ozokerite;
silica dimethyl silylate 0.1-4%;
6-15% of starch aluminum octenyl succinate;
5-10% of polyisobutylene;
3-9% of a first emollient;
0.1-2% of a second emollient;
10-20% of tri (octyldodecanol) citrate;
1-10% of phenyl isopropyl polydimethylsiloxane;
16-36% of a dispersant;
1-5% of trimethylsiloxy silicate;
2-6% of deionized water;
0.03-3% of humectant;
10-19% of hexyl laurate;
7-13% of a colorant;
0.5 to 1.0 percent of preservative;
the first emollient comprises at least two of avocado oil, phytosterols, and olive oil;
the second emollient comprises at least three of ethylhexyl palmitate, tribehenate, sorbitan isostearate and palmitoyl tripeptide-1;
the dispersing agent comprises the following components in percentage by weight:
2-6% of cetyl polydimethylsiloxane;
8-15% of triisostearin;
6-15% of ethylhexyl stearate.
2. The moisturizing lipstick according to claim 1, wherein said first emollient consists of avocado oil, phytosterols, olive oil, and the ratio of avocado oil, phytosterols, olive oil is 51: 31: 18.
3. the moisturizing lipstick according to claim 1, wherein the ratio of ethylhexyl palmitate, behenyl alcohol, sorbitan isostearate to palmitoyl tripeptide-1 in the second emollient is 74.9: 20: 5: 0.1.
4. the lip balm according to claim 1, wherein the moisturizer comprises the following components in percentage by weight:
0.01-1% of betaine;
0.01-1% of sodium hyaluronate;
ceramide 2 is 0.01-1%.
5. A process for the production of a lip balm according to any one of claims 1 to 4, comprising the steps of:
step one, fully mixing tri (octyldodecanol) citrate, phenyl isopropyl polydimethylsiloxane, a dispersing agent, trimethylsiloxysilicate and dimethyl silica silylate to obtain a first mixture;
step two, fully mixing the starch octenyl aluminum succinate, the hexyl laurate and the coloring agent to obtain a second mixture;
step three, fully mixing water and a humectant to obtain a third mixture;
fully mixing the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the preservative, the first mixture and the second mixture to obtain a fourth mixture;
and step five, fully mixing the third mixture and the fourth mixture, and filling to obtain the thin and smooth lipstick.
6. The process for producing the Yinhui lipstick as claimed in claim 5, wherein in the first step, the tri (octyldodecanol) citrate, the phenylisopropylpolydimethylsiloxane, the dispersant and the trimethylsiloxysilicate are heated to 75-80 ℃, and then the dimethylsilylated silica is added and homogenized at 3000-3500rpm for 5-10 min.
7. The process for producing an emollient lipstick according to claim 5, wherein in step two, aluminum starch octenylsuccinate, hexyl laurate and the coloring agent are mixed together and then ground to a particle size of 0.7-2.5 μm to obtain the second mixture.
8. The process for producing the Yinhuang smooth lipstick according to claim 5, wherein in the fourth step, the ethylene/propylene copolymer, the polyethylene, the ozokerite, the polyisobutylene, the first emollient, the second emollient, the preservative, the first mixture and the second mixture are completely dissolved at a temperature of 75-80 ℃ to obtain a fourth mixture.
9. The process for producing the englen smooth lipstick according to claim 5, wherein in the fifth step, the third mixture and the fourth mixture are fully mixed at a temperature of 75-80 ℃; the temperature during filling is 75-80 ℃.
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CN113181083B (en) * | 2021-04-02 | 2023-03-21 | 科丝美诗(中国)化妆品有限公司 | Matte mud lip, cheek and eye three-purpose composition and preparation method thereof |
CN113332178A (en) * | 2021-05-12 | 2021-09-03 | 广州笔匠化妆品有限公司 | Lip balm with silky and smooth fog feeling |
CN114191346B (en) * | 2021-12-23 | 2023-03-31 | 娇时日化(杭州)股份有限公司 | Lip balm and preparation method thereof |
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